CN114410376A - Cigarette bead-blasting essential oil with pepper flavor and preparation method thereof - Google Patents
Cigarette bead-blasting essential oil with pepper flavor and preparation method thereof Download PDFInfo
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- CN114410376A CN114410376A CN202111631383.9A CN202111631383A CN114410376A CN 114410376 A CN114410376 A CN 114410376A CN 202111631383 A CN202111631383 A CN 202111631383A CN 114410376 A CN114410376 A CN 114410376A
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- pepper
- parts
- essential oil
- refined
- tobacco
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- 235000002566 Capsicum Nutrition 0.000 title claims abstract description 88
- 239000006002 Pepper Substances 0.000 title claims abstract description 88
- 235000016761 Piper aduncum Nutrition 0.000 title claims abstract description 88
- 235000017804 Piper guineense Nutrition 0.000 title claims abstract description 88
- 235000008184 Piper nigrum Nutrition 0.000 title claims abstract description 88
- 239000000341 volatile oil Substances 0.000 title claims abstract description 54
- 238000005422 blasting Methods 0.000 title claims abstract description 53
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 51
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 28
- 235000019634 flavors Nutrition 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 244000203593 Piper nigrum Species 0.000 title 1
- 241000722363 Piper Species 0.000 claims abstract description 87
- 239000011324 bead Substances 0.000 claims abstract description 38
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims abstract description 23
- 235000019477 peppermint oil Nutrition 0.000 claims abstract description 23
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 12
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 12
- 239000002826 coolant Substances 0.000 claims abstract description 12
- 229930007744 linalool Natural products 0.000 claims abstract description 12
- 235000019505 tobacco product Nutrition 0.000 claims abstract description 12
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 11
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 11
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 11
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 claims abstract description 11
- 229940041616 menthol Drugs 0.000 claims abstract description 11
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 9
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 7
- 241000208125 Nicotiana Species 0.000 claims description 26
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 26
- 238000000605 extraction Methods 0.000 claims description 23
- 239000000126 substance Substances 0.000 claims description 21
- 239000002904 solvent Substances 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 16
- 238000001035 drying Methods 0.000 claims description 14
- 241000949456 Zanthoxylum Species 0.000 claims description 12
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 10
- 235000007650 Aralia spinosa Nutrition 0.000 claims description 8
- 239000012634 fragment Substances 0.000 claims description 8
- 150000001408 amides Chemical class 0.000 claims description 7
- 239000011347 resin Substances 0.000 claims description 7
- 229920005989 resin Polymers 0.000 claims description 7
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 238000000199 molecular distillation Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 4
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 3
- 239000001273 butane Substances 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 claims description 3
- QEGNUYASOUJEHD-UHFFFAOYSA-N gem-dimethylcyclohexane Natural products CC1(C)CCCCC1 QEGNUYASOUJEHD-UHFFFAOYSA-N 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 3
- 239000003208 petroleum Substances 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 238000007670 refining Methods 0.000 claims description 3
- 210000000582 semen Anatomy 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 235000019506 cigar Nutrition 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000007790 scraping Methods 0.000 claims description 2
- 238000002791 soaking Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 20
- 235000009508 confectionery Nutrition 0.000 abstract description 5
- 230000000052 comparative effect Effects 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
- 239000011162 core material Substances 0.000 description 5
- 238000005096 rolling process Methods 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 4
- 235000006679 Mentha X verticillata Nutrition 0.000 description 3
- 235000002899 Mentha suaveolens Nutrition 0.000 description 3
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 3
- 206010013911 Dysgeusia Diseases 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000008534 Capsicum annuum var annuum Nutrition 0.000 description 1
- 240000008384 Capsicum annuum var. annuum Species 0.000 description 1
- 239000004593 Epoxy Chemical class 0.000 description 1
- 238000012356 Product development Methods 0.000 description 1
- 241001093501 Rutaceae Species 0.000 description 1
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- 244000089698 Zanthoxylum simulans Species 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000112 cooling gas Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003571 electronic cigarette Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 239000012156 elution solvent Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000011325 microbead Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
The invention provides cigarette bead blasting essential oil with pepper flavor and a preparation method thereof, wherein the cigarette bead blasting essential oil with pepper flavor is prepared from the following raw materials in parts by weight: 1-10 parts of refined pepper product, 1-10 parts of peppermint oil, 1-5 parts of bergamot oil, 1-5 parts of peppermint oil, 1-5 parts of menthol, 1-5 parts of linalool, 0.1-2 parts of menthyl acetate, 1-10 parts of refined tobacco product, 30.1-1 parts of cooling agent WS and 47-92.8 parts of caprylic/capric glyceride. The cigarette bead-blasting essential oil has the special fragrance of the pepper, has a certain cool feeling, has comfortable, coordinated and natural overall fragrance style, shows the style characteristics of freshness, refreshing, sweet and smooth throat, and has a good application prospect.
Description
Technical Field
The invention relates to the technical field of tobacco, in particular to cigarette bead-blasting essential oil with pepper flavor and a preparation method thereof.
Background
The cigarette blasting bead is a micro bead hidden in a filter tip and burst when certain pressure is applied, essence with different fragrance styles is contained in the cigarette blasting bead, various different experiences are brought to smokers after the cigarette blasting bead is broken, artificial controllable characteristic fragrance release in the cigarette smoking process is realized, and the influence of the external environment on the smoking taste and the loss of the essence caused by the external environment are reduced. In recent years, the market development of foreign bead-blasting cigarettes is vigorous, a plurality of bead-blasting essence products represented by mint essence are formed, domestic bead-blasting cigarettes are developed later, at present, the bead-blasting essence is in a product development stage, the style of bead-blasting essence has the problems of insufficient varieties and insufficient obvious characteristics, and the market of bead-blasting cigarettes is greatly limited.
The fructus Zanthoxyli is dry mature pericarp of green pepper or fructus Zanthoxyli of Rutaceae, is pungent and warm in flavor, and has effects of warming lung, dispelling fluid, warming channel, dispelling cold, relieving ascarid, and relieving pain. The chemical components of the pepper mainly comprise volatile oil, alkaloid, amide, flavonoid, triterpene, sterol, fatty acid and the like, the volatile oil of the pepper is also called pepper essential oil, determines the fragrance of the pepper and is one of the active components of the pepper, and the chemical components mainly comprise terpenes, alcohols, ketones, aldehydes, olefins, esters, epoxy compounds and the like, but the chemical components contain amide substances and have certain irritation when being added into cigarette products. According to the existing research reports, the pricklyash peel can bring prickling and numb feelings to people, mainly because the pricklyash peel contains amide substances, particularly a series of unsaturated fatty acid amides which are insoluble in cold petroleum ether, so that the numb substances and the fragrant substances can be separated in a targeted way by technologies such as an extraction method, a chromatography method, an adsorption method and the like, the pricklyash peel essential oil is refined, a large amount of irritant amide substances are removed, the fragrance of the pricklyash peel is reserved, the pricklyash peel essential oil can bring distinctive and novel experiences to consumers when added into cigarette products, and the pricklyash peel essential oil has a good market application prospect.
Disclosure of Invention
In order to overcome the technical defects, the invention provides the cigarette bead-blasting essential oil with the pepper flavor and the preparation method thereof, which are used for solving the problems of insufficient varieties and insufficient obvious characteristics existing in the style of bead-blasting essence, adding the pepper flavor, bringing distinctive and novel experience to consumers when being added into cigarette products, and having excellent market application prospect.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides cigarette bead blasting essential oil with pepper flavor and a preparation method thereof, wherein the bead blasting essential oil is prepared from the following components in parts by weight: 1-10 parts of refined pepper product, 1-10 parts of peppermint oil, 1-5 parts of bergamot oil, 1-5 parts of peppermint oil, 1-5 parts of menthol, 1-5 parts of linalool, 0.1-2 parts of menthyl acetate, 1-10 parts of refined tobacco product, 30.1-1 parts of cooling agent WS and 47-92.8 parts of caprylic/capric glyceride.
The further technical scheme is that the refined product of the pepper is one or more refined products of pepper substances in Chinese tribute pepper, Wudu dahongpao and Hancheng dahongpao;
the further technical scheme is that the pepper used in the refined pepper product is fresh pepper;
the further technical scheme is that the preparation method of the refined zanthoxylum bungeanum product comprises the following steps: selecting mildew-free and full pepper, removing impurities, cleaning, and drying in a hot air in a rotary cage dryer at the drying temperature of 30-40 ℃ for 1-2 h; immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling, and standing for 20-30 min; after standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper cooled and kept stand for the third time into a freeze dryer, and drying for 12-24 hours; separating the dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing, and sieving with 50 mesh sieve; collecting pericarpium Zanthoxyli powder, and extracting with solvent to obtain pericarpium Zanthoxyli essential oil; removing amide substances in the zanthoxylum essential oil by using a macroporous resin method to obtain a refined zanthoxylum product;
the further technical scheme includes that the solvent extraction method is a Soxhlet extraction method, the ratio of pepper powder to a solvent is 1: 5-1: 15, the solvent is one of ethanol, ether and petroleum ether, the soaking time is 30-50 min, the water bath temperature is 50-80 ℃, the extraction time is 3-4 h, the distillate obtained after the extraction is finished is dried by anhydrous sodium sulfate for 12-24h, and the anhydrous sodium sulfate is removed by filtration after the drying;
the further technical proposal is that the macroporous resin is AB8 macroporous resin, the elution solvent is one or more of methanol, ethyl acetate and ethanol, and the elution flow rate is 0.5 mL/min-2.5 mL/min;
the further technical proposal is that the tobacco refined substance is one or more of burley tobacco, flue-cured tobacco or cigar tobacco fragment refined substances;
the further technical proposal is that the preparation method of the refined tobacco product comprises the following steps: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume of the tobacco fragments and the extraction solvent is 1: 5-1: 7, the extraction temperature is 30-50 ℃, the extraction time is 3-5 hours, and the obtained sample is a tobacco extract; refining the tobacco extract by molecular distillation, collecting light components under different conditions, and mixing the light components according to a certain proportion to obtain a tobacco refined substance;
the molecular distillation method has the further technical scheme that the molecular distillation conditions comprise that the feeding speed is 6.0-8.0 mL/min, the vacuum degree is 10-20 Pa, the heating temperature is 40, 60, 80 and 100 ℃, the cooling temperature is 25-35 ℃, and the film scraping rotation speed is 140-150 r/min;
in the invention, the raw materials for providing the fragrance of the pepper mainly comprise refined pepper products, and the refined pepper products have special fragrance of the pepper, but have single fragrance, lack sweet fragrance and cool feeling, and cannot make people smell the pepper products with the feeling of promoting the secretion of saliva or body fluid. The peppermint oil, the bergamot oil, the dementholized peppermint oil, the menthol, the linalool and the cooling agent WS-3 are used as a blending agent, wherein the dementholized peppermint oil has fresh and strong mint fragrance with little green grass smell, the cooling gas can be kept through all the time, the bergamot oil has fresh and sweet lemon-like fruit fragrance and fresh fruit sweet fragrance, the dementholized peppermint oil has special cooling fragrance, the menthol has cool mint feeling, the linalool has weak citrus fruit fragrance, the fragrance is soft and transparent, the aftertaste is obvious, and the cooling agent WS-3 can increase the cooling feeling and is refreshing to the heart and the spleen. The invention combines the substances with the refined substances of the pepper, increases cool feeling and fresh feeling, and enriches the fragrance of the pepper; the menthyl acetate adds light fragrance to the electronic cigarette oil with the pepper flavor; the refined tobacco product can increase the original fragrance of tobacco. Through the matching use of the raw materials, the prepared pepper popping essential oil has rich fragrance, and consumers feel like pictures when smelling the pepper popping essential oil.
The cigarette blasting bead essential oil with pepper flavor and the preparation method thereof disclosed by the application can bring beneficial effects including but not limited to:
the bead blasting essential oil prepared by the invention has obvious pepper characteristic flavor, shows the style characteristics of freshness, dainty taste, sweet aftertaste and smooth throat, enriches the style of the bead blasting essential oil, and can meet the requirements of different consumer groups.
Detailed Description
In order to make the objects, technical solutions and advantages of the present application more apparent, the present application is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the present application and are not intended to limit the present application.
On the contrary, this application is intended to cover any alternatives, modifications, equivalents, and alternatives that may be included within the spirit and scope of the application as defined by the appended claims. Furthermore, in the following detailed description of the present application, certain specific details are set forth in order to provide a better understanding of the present application. It will be apparent to one skilled in the art that the present application may be practiced without these specific details.
The cigarette blasting bead essential oil with pepper flavor and the preparation method thereof according to the embodiment of the application are explained in detail below. It is to be noted that the following examples are only for explaining the present application and do not constitute a limitation to the present application.
Example 1
The cigarette bead-blasting essential oil with pepper flavor comprises the following raw materials in parts by weight:
1 part of refined pepper product, 10 parts of peppermint oil, 1 part of bergamot oil, 5 parts of peppermint oil, 1 part of menthol, 5 parts of linalool, 2 parts of menthyl acetate, 1 part of refined tobacco product, 30.1 parts of cooling agent WS and 73.9 parts of caprylic/capric glyceride.
The preparation method comprises the following steps:
dripping the prepared pepper bead blasting essential oil as a core material to prepare bead blasting for cigarettes, adding the bead blasting essential oil into a filter rod in the process of forming filter tow, and then rolling the filter rod to prepare the cigarettes.
Comparative example 1
The preparation method of the raw materials is the same as that of example 1 except that the raw materials do not contain pepper refined powder.
Example 2
The cigarette bead-blasting essential oil with pepper flavor comprises the following raw materials in parts by weight:
3 parts of refined pepper product, 7 parts of peppermint oil, 2 parts of bergamot oil, 4 parts of dementholized peppermint oil, 2 parts of menthol, 4 parts of linalool, 1.5 parts of menthyl acetate, 5 parts of refined tobacco product, 30.3 parts of cooling agent WS and 69.2 parts of caprylic/capric triglyceride.
The preparation method comprises the following steps:
dripping the prepared pepper bead blasting essential oil as a core material to prepare bead blasting for cigarettes, adding the bead blasting essential oil into a filter rod in the process of forming filter tow, and then rolling the filter rod to prepare the cigarettes.
Comparative example 2
The preparation method of the raw materials is the same as that of example 2 except that the raw materials do not contain peppermint oil.
Example 3
The cigarette bead-blasting essential oil with pepper flavor comprises the following raw materials in parts by weight:
5 parts of refined pepper product, 5 parts of peppermint oil, 3 parts of bergamot oil, 3 parts of peppermint oil, 3 parts of menthol, 3 parts of linalool, 1 part of menthyl acetate, 7 parts of refined tobacco product, 30.5 parts of cooling agent WS and 69.5 parts of caprylic/capric glyceride.
The preparation method comprises the following steps:
dripping the prepared pepper bead blasting essential oil as a core material to prepare bead blasting for cigarettes, adding the bead blasting essential oil into a filter rod in the process of forming filter tow, and then rolling the filter rod to prepare the cigarettes.
Comparative example 3
The preparation method of the raw materials is the same as that of example 3 except that the raw materials do not contain linalool.
Example 4
The cigarette bead-blasting essential oil with pepper flavor comprises the following raw materials in parts by weight:
7 parts of refined pepper product, 3 parts of peppermint oil, 4 parts of bergamot oil, 2 parts of dementholized peppermint oil, 4 parts of menthol, 2 parts of linalool, 1.5 parts of menthyl acetate, 10 parts of refined tobacco product, 30.7 parts of cooling agent WS and 65.8 parts of caprylic/capric triglyceride.
The preparation method comprises the following steps:
dripping the prepared pepper bead blasting essential oil as a core material to prepare bead blasting for cigarettes, adding the bead blasting essential oil into a filter rod in the process of forming filter tow, and then rolling the filter rod to prepare the cigarettes.
Comparative example 4
The procedure of example 4 was repeated except that the starting materials contained no menthyl acetate.
Example 5
The cigarette bead-blasting essential oil with pepper flavor comprises the following raw materials in parts by weight:
10 parts of refined pepper product, 1 part of peppermint oil, 5 parts of bergamot oil, 1 part of dementholized peppermint oil, 5 parts of menthol, 1 part of linalool, 0.1 part of menthyl acetate, 10 parts of refined tobacco product, 31 parts of cooling agent WS and 65.9 parts of caprylic/capric glyceride.
The preparation method comprises the following steps:
dripping the prepared pepper bead blasting essential oil as a core material to prepare bead blasting for cigarettes, adding the bead blasting essential oil into a filter rod in the process of forming filter tow, and then rolling the filter rod to prepare the cigarettes.
Comparative example 5
The procedure of preparation of the same materials and preparation method as example 5 was repeated except that the materials contained no cooling agent WS-3.
The popped-bead cigarettes of examples 1 to 5 and comparative examples 1 to 5 were evaluated with reference to the national bureau of smoking standards. The 13 cigarette sensory evaluation experts form a smoking panel, sensory evaluation is carried out in a dark evaluation mode, and the sensory evaluation results are shown in table 1.
TABLE 1 evaluation results of sensory Effect of exploded cigarette
As can be seen from table 1, sensory evaluation of the popped bead cigarettes of examples 1 to 5 and comparative examples 1 to 5 clearly shows that the sensory quality evaluation indexes of examples 1 to 5 are superior to those of comparative examples 1 to 5.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.
Claims (10)
1. The cigarette bead-blasting essential oil with pepper flavor is characterized by being prepared from the following raw materials in parts by weight: 1-10 parts of refined pepper product, 1-10 parts of peppermint oil, 1-5 parts of bergamot oil, 1-5 parts of peppermint oil, 1-5 parts of menthol, 1-5 parts of linalool, 0.1-2 parts of menthyl acetate, 1-10 parts of refined tobacco product, 30.1-1 parts of cooling agent WS and 47-92.8 parts of caprylic/capric glyceride.
2. The essential oil for cigarette blasting beads with pepper flavor according to claim 1, wherein the refined product of pepper is one or more refined products of pepper substances from Chinese tribute pepper, Wudu dahongpao and Hancheng dahongpao.
3. The essential oil for cigarette blasting beads with pepper flavor according to claim 1, wherein the pepper used in the refined pepper product is fresh pepper.
4. The essential oil for cigarette blasting beads with pepper flavor according to claim 1, wherein the preparation method of the refined pepper product comprises the following steps: selecting mildew-free and full pepper, removing impurities, cleaning, and drying in a hot air in a rotary cage dryer at the drying temperature of 30-40 ℃ for 1-2 h; immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling, and standing for 20-30 min; after standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper cooled and kept stand for the third time into a freeze dryer, and drying for 12-24 hours; separating the dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing, and sieving with 50 mesh sieve; collecting pericarpium Zanthoxyli powder, and extracting with solvent to obtain pericarpium Zanthoxyli essential oil; removing amide substances in the pricklyash peel essential oil by using a macroporous resin method to obtain a refined pricklyash peel product.
5. The essential oil for cigarette blasting beads with pepper flavor according to claim 4, wherein the ratio of the pepper powder to the solvent is 1: 5-1: 15, the solvent is one of ethanol, diethyl ether and petroleum ether, the soaking time is 30-50 min, the water bath temperature is 50-80 ℃, the extraction time is 3-4 h, the distillate obtained after the extraction is dried by anhydrous sodium sulfate for 12-24h, and the anhydrous sodium sulfate is removed by filtering after the drying.
6. The essential oil for cigarette blasting beads with pepper flavor according to claim 4, wherein the macroporous resin is AB8 macroporous resin, the eluting solvent is one or more of methanol, ethyl acetate and ethanol, and the eluting flow rate is 0.5 mL/min-2.5 mL/min.
7. The essential oil for cigarette blasting beads with pepper flavor according to claim 1, wherein the tobacco refined substance is one or more of burley tobacco, flue-cured tobacco or cigar tobacco fragment refined substances.
8. The essential oil for cigarette blasting beads with pepper flavor according to claim 1, wherein the preparation method of the tobacco refined product comprises the following steps: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume of the tobacco fragments and the extraction solvent is 1: 5-1: 7, the extraction temperature is 30-50 ℃, the extraction time is 3-5 hours, and the obtained sample is a tobacco extract; refining the tobacco extract by molecular distillation, collecting light components under different conditions, and mixing the light components according to a certain proportion to obtain the refined tobacco product.
9. The essential oil for cigarette blasting beads with pepper flavor and the preparation method thereof according to claim 8, wherein the molecular distillation conditions are that the feeding speed is 6.0-8.0 mL/min, the vacuum degree is 10-20 Pa, the heating temperature is 40, 60, 80, 100 ℃, the cooling temperature is 25-35 ℃, and the film scraping rotation speed is 140-150 r/min.
10. The preparation method of the cigarette bead-blasting essential oil with the pepper flavor is characterized by comprising the following steps of:
(1) preparing a pepper refined product: selecting mildew-free and full pepper, removing impurities, cleaning, and drying in a hot air in a rotary cage dryer at the drying temperature of 30-40 ℃ for 1-2 h; immediately placing the dried pepper in a refrigerator at the temperature of-5 ℃ for cooling, and standing for 20-30 min; after standing, taking out the pepper, placing the pepper in a rotary cage dryer, and repeating the steps of heating and drying, cooling and standing for three times; putting the pepper cooled and kept stand for the third time into a freeze dryer, and drying for 12-24 hours; separating the dried pericarpium Zanthoxyli from semen Zanthoxyli, pulverizing, and sieving with 50 mesh sieve; collecting pericarpium Zanthoxyli powder, and extracting with solvent to obtain pericarpium Zanthoxyli essential oil; removing amide substances in the zanthoxylum essential oil by using a macroporous resin method to obtain a refined zanthoxylum product;
(2) preparing a tobacco refined product: placing tobacco fragments into a closed extraction tank, vacuumizing, and injecting an extraction solvent into the tank, wherein the extraction solvent is one or more of dimethyl ether, butane and cyclohexane, the volume of the tobacco fragments and the extraction solvent is 1: 5-1: 7, the extraction temperature is 30-50 ℃, the extraction time is 3-5 hours, and the obtained sample is a tobacco extract; refining the tobacco extract by molecular distillation, collecting light components under different conditions, and mixing the light components according to a certain proportion to obtain a tobacco refined substance;
(3) preparing the essential oil for popping the beads of the cigarettes: the essential oil for the popping beads of the cigarettes is obtained by fully and uniformly mixing the following raw materials in parts by weight: 1-10 parts of refined pepper product, 1-10 parts of peppermint oil, 1-5 parts of bergamot oil, 1-5 parts of peppermint oil, 1-5 parts of menthol, 1-5 parts of linalool, 0.1-2 parts of menthyl acetate, 1-10 parts of refined tobacco product, 30.1-1 parts of cooling agent WS and 47-92.8 parts of caprylic/capric glyceride.
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| CN115226926A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Mint essence, mint essence oil for cigarettes and cigarettes |
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