CN107022415B - Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette - Google Patents
Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette Download PDFInfo
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- CN107022415B CN107022415B CN201710288574.7A CN201710288574A CN107022415B CN 107022415 B CN107022415 B CN 107022415B CN 201710288574 A CN201710288574 A CN 201710288574A CN 107022415 B CN107022415 B CN 107022415B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
- C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- General Health & Medical Sciences (AREA)
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- Agronomy & Crop Science (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention belongs to the technical field of cigarette filter stick production, and particularly relates to a sterculia scaphigera essence for cigarette blasting beads and application thereof in cigarettes. The boat-fruited sterculia essence consists of boat-fruited sterculia extract, ethyl isovalerate, cassia oil, eugenol, myrcene, linalool and caprylic capric glyceride. The essence can be used for preparing the scaphium scaphigerum poppy cigarette pops, and the pops can be added into a filter stick and used for preparing cigarette pops. The application can prepare and obtain cigarette bead blasting products with stable and uniform forming quality by providing the boat-fruited sterculia seed essence specially used for cigarette bead blasting and combining a relatively perfect bead blasting production process, and after the bead blasting is placed into a cigarette filter, the irritation of cigarettes can be better weakened, the fragrance of the cigarettes can be improved and enriched, the fragrance richness, the sensory quality and the suction interest of the cigarettes can be obviously improved, so that the boat-fruited sterculia seed essence has relatively good application value and popularization and application significance in design, development, production and sale of the bead blasting cigarettes.
Description
Technical Field
The invention belongs to the technical field of cigarette filter stick production, and particularly relates to a sterculia scaphigera essence for cigarette blasting beads and application thereof in cigarettes.
Background
In the traditional cigarette flavoring technology, the flavoring liquid is mainly added into tobacco shreds, the added flavoring liquid is partially lost in the cigarette combustion process, and meanwhile, as the reaction of a complex material system at high temperature is difficult to expect, part of the flavoring liquid can generate some undesirable sensory effects. As a novel cigarette flavoring mode, the bead blasting flavoring can overcome the defects of the existing flavoring mode to a certain extent, and the main reasons are as follows: the exploded beads contain spices, before smoking cigarettes, consumers preferably crush the exploded beads contained in the filter rods and then smoke the cigarettes, and smoke gas passes through the filter tips and acts on the consumers together with the exploded bead feed liquid, so that the flavoring and fragrance supplementing process is completed; the mode can effectively avoid the loss of the spice liquid in the combustion process of the tobacco on one hand, and on the other hand, the spice is arranged in the sealed exploding bead, so that the loss can not occur during the storage of the cigarette, and the stability of the quality of the cigarette is ensured.
The bead blasting cigarette is used as a new material in cigarettes, and due to the special release mode of the content of the bead blasting cigarette, the bead blasting cigarette has more and more outstanding functions in the aspects of supplementing, improving and coordinating the smoking quality of the cigarettes, improving, changing, cigarette product style and the like, and improves the interestingness and sensory quality of cigarette smoking, so that the bead blasting cigarette is increasingly applied to Chinese cigarette production in recent years and is also popular with consumers.
In the prior art, although a certain number of bead-exploded cigarettes exist in the market at present, the fragrance in the bead-exploded cigarettes is poor in coordination with smoke due to lack of targeted design, and the smoking feeling of the bead-exploded cigarettes is influenced due to large influence on the fragrance characteristics of the cigarettes.
Although the 'bead-popping' cigarette appears like a bamboo shoot in spring after rain, the 'bead-popping' cigarette has a plurality of new problems in the aspects of addition and use due to the fact that the product is relatively novel and the current production standard and specification are relatively lacked. Particularly, for the particularity of cigarette products, the influence of the 'bead blasting' filter stick on physical indexes, chemical indexes, hazard indexes and the like of cigarettes is rarely reported in the aspects of the design of a 'bead blasting' inclusion formula, the stable release of the inclusion and the like. Therefore, the 'bead blasting' inclusion with different components is designed, the special inclusion release rule of the 'bead blasting' is systematically researched, and the 'bead blasting' inclusion has important theoretical and application significance on the aspects of the influence of physical indexes, smoke indexes, hazard indexes and the like of cigarettes.
Disclosure of Invention
The invention aims to provide a boat-fruited sterculia essence which is used in a cigarette filter stick in a targeted manner, so that the types of cigarette products are enriched, and the cigarette products with different style characteristics are provided.
The technical solution adopted in the present application is detailed as follows.
The boat-fruited sterculia essence for the cigarette bead blasting comprises the following components in percentage by mass:
10.0-15.0% of boat-fruited sterculia seed extract,
1.0 to 2.5% of ethyl isovalerate,
1.0-1.5% of cassia oil,
0.5 to 1.5 percent of eugenol,
0.6 to 1.8% of myrcene,
1.0 to 3.0% of linalool,
74.7-85.9% of caprylic/capric glyceride.
The boat-fruited sterculia seed extract is an ethanol extract of boat-fruited sterculia seeds;
the caprylic capric glyceride (MCT) is the product of esterification of fatty acid containing 8-12 carbon chains with glycerol.
The boat-fruited sterculia seed extract can be prepared by the following steps:
(1) crushing the dried boat-fruited sterculia seed, and sieving with a 55-65-mesh sieve to prepare boat-fruited sterculia seed powder;
(2) adding 60-90% by volume of ethanol solution into the boat-fruited sterculia seed powder in the step (1), and carrying out hot reflux for 3-5 h in water bath at 65-85 ℃; the material-liquid ratio of the boat-fruited sterculia seed powder to the ethanol solution is as follows: ethanol =1 g: 4-6 mL;
(3) and (3) concentrating the hot reflux liquid in the step (2) under reduced pressure at 55-65 ℃ and 60-80 Kpa until no volume change exists, and obtaining the extract, namely the boat-fruited sterculia seed extract.
The boat-fruited sterculia essence for cigarette bead blasting comprises the following specific formula: 12.5 percent of boat-fruited sterculia seed extract, 1.8 percent of ethyl isovalerate, 1.3 percent of cassia oil, 0.8 percent of eugenol, 1.2 percent of myrcene, 1.5 percent of linalool and 80.9 percent of caprylic capric glyceride.
It should be explained that different essences are different according to purposes, and the formula is generally designed specially, in the application, the sterculia scaphigera essence is specially designed according to the purposes in the final cigarette by combining the characteristics of the production process of the bead blasting of the cigarette, so that the results of adjusting the smoke quality and improving the smoking quality of the cigarette can be better realized on the basis of ensuring the bead blasting quality.
The sterculia scaphigera seed cigarette bead is prepared by using the sterculia scaphigera seed essence for the cigarette bead, the cigarette bead is made of natural polymer materials or synthetic polymer materials, essence and spice are wrapped in a closed bead to form a sealed bead with more circles and different colors, the diameter of the bead is 2.0-4.0 mm, and the essence content in the bead is 20-25 mu L per bead; specific examples thereof include: the diameter of the blasting beads is 3.65mm, and the weight is 23 mg/granule; the content of essence in the exploded bead is 23 muL/granule, in a word, the specific specification can be adjusted according to different machine equipment and different specifications of used filter sticks.
The application of the sterculia scaphigera cigarette bead blasting in cigarettes is characterized in that the cigarette bead blasting is added into a common (circumference is 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, and one bead blasting is added to each cigarette.
The boat-fruited sterculia seed essence for the bead blasting of the cigarettes has obvious fresh and sweet fragrance and herbal fragrance, and the fragrance is the most important aroma characteristic in the smoke of the cigarettes; after the cigarette is prepared into a product form of 'bead blasting' and applied to cigarettes, the result of cigarette smoking shows that: compared with a comparison sample, after the scaphium scaphigerum cigarette is smoked by using the bead-exploded cigarette, the smoke aroma richness can be obviously improved on the premise of not changing the smoke aroma style of the cigarette, the full feeling and richness of smoke are enhanced, the coordination of aroma and the sensory quality of products is further improved, and the interestingness of cigarette smoking is increased; meanwhile, the sterculia lychnophora has the effects of clearing heat, moistening lung, relieving sore throat, detoxifying, relaxing bowel and the like, so that the cigarette smoking harm is relieved to a certain extent.
In general, the boat-fruited sterculia essence adopted in the application is obtained by extracting from natural boat-fruited sterculia, so that after the fragrant substances enter cigarette smoke, the irritation of the smoke can be reduced, the soft fullness, aroma fullness and plumpness of the cigarette smoke are improved, and the smoking quality and the sensory comfort of the cigarette smoke are further improved.
In a word, the sterculia scaphigera essence specially used for cigarette bead blasting and the relatively perfect bead blasting production process are provided, so that a cigarette bead blasting product with stable and uniform forming quality can be prepared, after the beads are placed into a cigarette filter, the irritation of the cigarette can be weakened well, the aroma of the cigarette can be improved and enriched, the aroma richness, the sensory quality and the smoking interestingness of the cigarette can be remarkably improved, and the effects of clearing heat, moistening lung, relieving sore throat, detoxifying, relaxing bowel, reducing the harm of the cigarette and the like are achieved, so that the sterculia scaphigera essence has relatively good application value and popularization and application significance for design, development, production and sale of the bead blasting cigarette.
Detailed Description
The present invention is further illustrated by the following examples. Before describing the specific embodiments, the process for preparing the cigarette blasting beads described in the following embodiments will be briefly described as follows.
The main preparation process of the cigarette blasting bead in the prior art is as follows:
the mainstream technology of the bead blasting production mainly adopts a split-flow method-liquid mid-point drop method preparation process to carry out production, namely, a rubber column is cut off by utilizing the shearing force of the counter punching of cooling oil, and the bead blasting and drop preparation is finished; specifically, the method comprises the following steps: firstly, utilizing two cooling oils with different incident angles to form shearing force in a solenoid, cutting off wall materials and core liquid in the dripping process, finally condensing the wall materials and the core liquid into balls in the cooling oil under the action of surface tension, and then preparing the final finished product blasting balls after procedures of deoiling, drying, screening and the like; the method is adopted to finish the processing of the populous in the following examples by Shanghai Huabao Biotech Co., Ltd;
it should also be noted that the materials used in the following examples: ethyl isovalerate, cassia oil, eugenol, myrcene, linalool, caprylic capric acid glyceride and the like are also products of Shanghai Huabao Biotech Co., Ltd;
the boat-fruited sterculia seed extract adopted in the following examples is prepared by the following steps:
(1) pulverizing dried semen Scaphii Lychnophori, and sieving with 60 mesh sieve to obtain semen Scaphii Lychnophori powder;
(2) adding 75% ethanol solution by volume into the boat-fruited sterculia seed powder in the step (1), and carrying out hot reflux for 4h in water bath at 70 ℃; the material-liquid ratio of the boat-fruited sterculia seed powder to the ethanol solution is as follows: ethanol =1 g: 5 mL;
(3) and (3) concentrating the hot reflux liquid in the step (2) under reduced pressure at 60 ℃ and 70Kpa until the volume is unchanged, and obtaining the extract, namely the boat-fruited sterculia seed extract.
Example 1
The boat-fruited sterculia essence for cigarette bead blasting in the embodiment comprises the following components in percentage by mass:
10 percent of boat-fruited sterculia seed extract, 1.0 percent of ethyl isovalerate, 1.0 percent of cassia oil, 0.5 percent of eugenol, 0.6 percent of myrcene, 1.0 percent of linalool and 85.9 percent of caprylic capric glyceride.
The boat-fruited sterculia essence is prepared into cigarette blasting beads with the diameter of 3.65mm and the weight of 23 mg/bead, and the content of the essence in the blasting beads is 23 mu L/bead, namely the boat-fruited sterculia essence for cigarette blasting beads.
According to the existing filter stick production process, the bead blasting machine is used for placing the bead blasting machine in the center of a filter stick and adding the bead blasting machine into a common (circumference 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, one bead blasting machine is added into each cigarette to obtain a bead blasting filter stick, and the bead blasting filter stick is obtained after cigarette samples are rolled and connected.
For the prepared sterculia scaphigera popshot cigarettes, 7 professional sensory evaluators perform detection and comparative smoking evaluation on the samples and blank cigarette samples (blank popshots are added at the same positions) of a control example.
Smoke detection and specific puff score see subsequent tables.
The smoking evaluation results show that 7 cigarette evaluation staff consistently think that after the sterculia scaphigera popsicle is added, the sterculia scaphigera fragrance of the cigarette sample is obvious, the fragrance richness of the smoke is improved to a certain extent, the feeling of fresh sweet fragrance and burnt sweet fragrance is enhanced, the sweet feeling is realized, the irritation is reduced, the offensive odor is reduced, the smoke fineness is improved, and the aftertaste is improved.
Example 2
The boat-fruited sterculia essence for cigarette bead blasting in the embodiment comprises the following components in percentage by mass:
12.5 percent of boat-fruited sterculia seed extract, 1.8 percent of ethyl isovalerate, 1.3 percent of cassia oil, 0.8 percent of eugenol, 1.2 percent of myrcene, 1.5 percent of linalool and 80.9 percent of caprylic capric glyceride.
The boat-fruited sterculia essence is prepared into cigarette blasting beads with the diameter of 3.65mm and the weight of 23 mg/bead, and the content of the essence in the blasting beads is 23 mu L/bead, namely the boat-fruited sterculia essence for cigarette blasting beads.
According to the existing filter stick production process, the bead blasting machine is used for placing the bead blasting machine in the center of a filter stick and adding the bead blasting machine into a common (circumference 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, one bead blasting machine is added into each cigarette to obtain a bead blasting filter stick, and the bead blasting filter stick is obtained after cigarette samples are rolled and connected.
For the prepared sterculia scaphigera popshot cigarettes, 7 professional sensory evaluators perform detection and comparative smoking evaluation on the samples and blank cigarette samples (blank popshots are added at the same positions) of a control example.
Smoke detection and specific puff score see subsequent tables.
The smoking evaluation results show that 7 cigarette evaluation staff agree that after the sterculia scaphigera poplars are added, the sterculia scaphigera flavor of the cigarette sample is obvious, the richness of the smoke flavor is obviously increased, the feeling of fresh sweet flavor and burnt sweet flavor is obviously enhanced, the obvious sweet taste is achieved, the irritation is obviously reduced, the offensive odor is reduced, the fineness of the smoke is obviously improved, and the aftertaste is obviously improved.
Example 3
The boat-fruited sterculia essence for cigarette bead blasting in the embodiment comprises the following components in percentage by mass:
15 percent of boat-fruited sterculia seed extract, 2.5 percent of ethyl isovalerate, 1.5 percent of cassia oil, 1.5 percent of eugenol, 1.8 percent of myrcene, 3.0 percent of linalool and 74.7 percent of caprylic capric glyceride.
The boat-fruited sterculia essence is prepared into cigarette blasting beads with the diameter of 3.65mm and the weight of 23 mg/bead, and the content of the essence in the blasting beads is 23 mu L/bead, namely the boat-fruited sterculia essence for cigarette blasting beads.
According to the existing filter stick production process, the bead blasting machine is used for placing the bead blasting machine in the center of a filter stick and adding the bead blasting machine into a common (circumference 24.3 mm) cigarette filter stick, the bead blasting position is 12.5mm away from the lip end, one bead blasting machine is added into each cigarette to obtain a bead blasting filter stick, and the bead blasting filter stick is obtained after cigarette samples are rolled and connected.
For the prepared sterculia scaphigera popshot cigarettes, 7 professional sensory evaluators perform detection and comparative smoking evaluation on the samples and blank cigarette samples (blank popshots are added at the same positions) of a control example.
Smoke detection and specific puff score see subsequent tables.
The smoking evaluation results show that 7 cigarette evaluation workers consistently think that after the puffed sterculia scaphigera cigarettes are added, the sterculia scaphigera flavor of the cigarette samples is very obvious, the coordination of the smoke flavor is reduced, the irritation is increased, the offensive odor is reduced, the smoke compatibility is poor, the cigarette has uncomfortable sweet and greasy feeling, and the aftertaste is inferior to that of normal cigarettes (control cigarettes).
The bead blasting products prepared in different embodiments are detected, meanwhile, the cigarettes prepared in the embodiments are subjected to conventional detection, so that the physicochemical indexes of an acetate fiber tow sample, the physical indexes of a filter stick sample and the physicochemical indexes of the cigarette sample in the cigarette sample are measured, in addition, the indexes of total particulate matter, tar, nicotine, moisture and the like in the main stream smoke of the cigarettes are measured according to the method of measuring the total particulate matter and the tar by a smoking machine for conventional analysis of GB/T19609-2004 cigarettes, and the specific results are shown in the following table.
Table 1, test results of the exploded beads prepared in the different examples:
table 2, test results of filter rods containing exploded beads prepared in different examples:
table 3, physical indexes and mainstream smoke detection results for different cigarette samples:
as can be seen from the data in the table 2, compared with the normal acetate fiber tow filter stick, the physical indexes of the filter stick for placing the scaphium scaphigerum populus balls have no obvious difference, and the pressure drop of the filter stick is obviously changed. As can be seen from the data in Table 3, compared with the normal cigarette of the control example, the mainstream smoke of the scaphium scaphigerum populus popped bead cigarette is changed, but after the poplites are pinched and broken, the key indexes of tar and nicotine which influence the cigarette sense are not obviously changed.
Table 4, sensory quality evaluation results for different cigarette samples:
as can be seen from the results in Table 4, the sensory quality of the cigarettes can be remarkably improved by using the sterculia lychnophora blasting beads, the sensory score can be improved by 0.61 min to the maximum, the aroma is remarkably improved, the aftertaste is improved, and the irritation and the offensive odor are also greatly reduced.
In conclusion, after the formula of the blasting beads with specific fragrance is designed in a targeted manner and applied to cigarettes, the fragrance characteristics of the cigarettes during smoking can be obviously improved, the smoking feeling is enriched and improved, and meanwhile, the harm of the cigarettes can be reduced due to the special effect of the sterculia lychnophora. Therefore, the novel scaphium scaphigerum popping bead capable of highlighting the fragrance of the scaphium scaphigerum, improving the smoking quality and reducing the harm of cigarettes has certain popularization and application values in the industry.
It should be emphasized that the above formula of popping beads is designed for improving cigarettes with conventional formula, and has good application effect when applied to fine cigarettes, but the specification of popping beads and the addition amount in the filter stick need to be properly adjusted according to the specific tobacco formula and design requirements, and will not be described in detail herein.
Claims (6)
1. The boat-fruited sterculia essence for cigarette bead blasting is characterized by comprising the following components in percentage by mass:
10.0-15.0% of boat-fruited sterculia seed extract,
1.0 to 2.5% of ethyl isovalerate,
1.0-1.5% of cassia oil,
0.5 to 1.5 percent of eugenol,
0.6 to 1.8% of myrcene,
1.0 to 3.0% of linalool,
74.7-85.9% of caprylic/capric glyceride;
the boat-fruited sterculia seed extract is an ethanol extract of boat-fruited sterculia seeds; the preparation method comprises the following steps:
(1) pulverizing dried semen Scaphii Lychnophori, and sieving with 60 mesh sieve to obtain semen Scaphii Lychnophori powder;
(2) adding 75% ethanol solution by volume into the boat-fruited sterculia seed powder in the step (1), and carrying out hot reflux for 4h in water bath at 70 ℃; the material-liquid ratio of the boat-fruited sterculia seed powder to the ethanol solution is as follows: ethanol =1 g: 5 mL;
(3) and (3) concentrating the hot reflux liquid in the step (2) under reduced pressure at 60 ℃ and 70Kpa until the volume is unchanged, and obtaining the extract, namely the boat-fruited sterculia seed extract.
2. The essence of boat-fruited sterculia seed for cigarette blasting according to claim 1,
12.5 percent of boat-fruited sterculia seed extract, 1.8 percent of ethyl isovalerate, 1.3 percent of cassia oil, 0.8 percent of eugenol, 1.2 percent of myrcene, 1.5 percent of linalool and 80.9 percent of caprylic capric glyceride;
or the following steps:
10% of boat-fruited sterculia seed extract, 1.0% of ethyl isovalerate, 1.0% of cassia oil, 0.5% of eugenol, 0.6% of myrcene, 1.0% of linalool and 85.9% of caprylic capric glyceride;
or the following steps:
15 percent of boat-fruited sterculia seed extract, 2.5 percent of ethyl isovalerate, 1.5 percent of cassia oil, 1.5 percent of eugenol, 1.8 percent of myrcene, 3.0 percent of linalool and 74.7 percent of caprylic capric glyceride.
3. The sterculia scaphigera essence for cigarette bead blasting according to claim 2, wherein the diameter of the bead blasting is 2.0-4.0 mm, and the essence content in the bead blasting is 20-25 μ L/bead.
4. The scaphium scaphigerum cigarette blasting bead as claimed in claim 3, wherein the diameter of the blasting bead is 3.65mm, the weight is 23 mg/bead, and the content of essence in the blasting bead is 23 μ L/bead.
5. The use of the scaphium scaphigerum cigarette blasting beads in cigarettes as claimed in claim 3, wherein the cigarette blasting beads are added into the filter stick.
6. The use of a scaphium scaphigerum cigarette blasting bead in a cigarette as claimed in claim 5, wherein the cigarette blasting bead is positioned in the middle of a filter stick, and one blasting bead is added in each cigarette filter stick.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710288574.7A CN107022415B (en) | 2017-04-27 | 2017-04-27 | Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette |
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| CN201710288574.7A CN107022415B (en) | 2017-04-27 | 2017-04-27 | Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette |
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| CN107022415A CN107022415A (en) | 2017-08-08 |
| CN107022415B true CN107022415B (en) | 2020-09-29 |
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| CN109234013A (en) * | 2018-09-05 | 2019-01-18 | 河南中烟工业有限责任公司 | A kind of tobacco aromaticss with throat soothing characteristic and preparation method thereof and the application in cigarette |
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| CN201234543Y (en) * | 2008-03-28 | 2009-05-13 | 张小团 | Multi-layer bombax malabaricum cigarette holder with smoke filter |
| RU2010151986A (en) * | 2008-05-19 | 2012-06-27 | Джапан Тобакко Инк. (Jp) | COVERING FRAGRANCE MATERIAL FOR A CIGARETTE, METHOD FOR PRODUCING IT AND A CIGARETTE |
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