CN107034019A - A kind of cigarette quick-fried pearl red-jujube flavor essence and its application in cigarette - Google Patents
A kind of cigarette quick-fried pearl red-jujube flavor essence and its application in cigarette Download PDFInfo
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- CN107034019A CN107034019A CN201710287357.6A CN201710287357A CN107034019A CN 107034019 A CN107034019 A CN 107034019A CN 201710287357 A CN201710287357 A CN 201710287357A CN 107034019 A CN107034019 A CN 107034019A
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- cigarette
- quick
- fried pearl
- red
- jujube
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
- C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of cigarette quick-fried pearl red-jujube flavor essence and its patent application of the application in cigarette.The red-jujube flavor essence is made up of the butanone of 3 hydroxyl 2, faenum graecum absolute oil, ethyl laurate, ethylmaltol, jujube absolute oil, Glycerin, mixed triester with caprylic acid capric acid.The quick-fried pearl of red-jujube flavor cigarette can be prepared using the essence, the quick-fried pearl can be added in filter stick and the quick-fried pearl cigarette application of cigarette is prepared.The application is by providing a kind of red-jujube flavor essence for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl production technology, Forming Quality stabilization, the uniform quick-fried pearl product of cigarette can be prepared, the quick-fried pearl is inserted after cigarette filter, the excitant of cigarette can preferably be weakened, improve and abundant cigarette flavor, the fragrance that is obviously improved cigarette is rich, the interest of aesthetic quality and suction, thus has preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.
Description
Technical field
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of quick-fried pearl of cigarette with red-jujube flavor essence and its
The patent application of application in cigarette.
Background technology
In traditional cigarette perfuming technology, spice liquid is mainly added in pipe tobacco by it, and the feed liquid that this mode is added is past
Toward meeting, partition losses fall during cigarette burning, simultaneously because the reaction of complex material system is difficult to be expected under high temperature, part
Feed liquid can also produce some bad organoleptic effects.Quick-fried pearl perfuming, being capable of necessarily journey as a kind of emerging perfuming cigarette mode
The defect in existing perfuming mode is overcome on degree, its main cause is：Include spices in quick-fried pearl, suck before cigarette, consumer
The first choice quick-fried pearl being contained in filter stick of crumbing burns and sucks cigarette again, and now flue gas is through together acting on and disappearing with quick-fried pearl feed liquid during filter tip
Fei Zhe, so that completing perfuming mends fragrant process；On the one hand this mode can be prevented effectively from feed liquid of the spices during result of combustion of tobacco
Loss, on the other hand, because spices is placed in sealed quick-fried pearl, thus will not be lost, so that really during cigarette is stored
The stabilization of cigarette quality is protected.
" quick-fried pearl ", due to the special delivery mode of its inclusion, is being supplemented, changed as a kind of emerging material in cigarette
Function in terms of kind, coordination smoking property of cigarette quality and lifting, change, cigarette product style is increasingly protruded, and improves cigarette
The interest of suction and aesthetic quality, thus " quick-fried pearl " cigarette is obtaining increasing in Chinese-style cigarette production in recent years
Using also obtaining liking for consumers in general.
In the prior art, although there is the fragrance in a number of quick-fried pearl cigarette, this quick-fried pearl in the market
Because lack of targeted is designed, thus it is relatively poor with flue gas harmony, and the odor characteristic influence on cigarette in itself is larger, because
And have impact on quick-fried pearl cigarette suck impression.
" quick-fried pearl ", although cigarette occurs like the mushrooms after rain, is due to its product relative new, current production standard and
Specification is relative to be lacked, so that the addition of " quick-fried pearl " and use also occur in that many new problems.Especially for cigarette
For the particularity of product, the design of composition formula is included " quick-fried pearl ", inclusion stability discharges, and " quick-fried pearl " filter stick is for cigarette
Rare report in terms of physical index, chemical index, the influence of harm sex index.Therefore " the quick-fried pearl " of different constituents is designed
Inclusion, systematization research " quick-fried pearl " Special inclusion release rule, " quick-fried pearl " inclusion refers to cigarette physical index, flue gas
There is important theory and application value in terms of mark, the influence of harm sex index.
The content of the invention
Present invention aims at a kind of red-jujube flavor essence being targetedly used in cigarette filter rod is provided, so that abundant volume
Smoke product type, to provide the cigarette product of different-style feature.
Details are as follows for the technical scheme that the application is taken.
A kind of cigarette quick-fried pearl red-jujube flavor essence, is calculated in mass percent, composed of the following components：
0.5 ~ 2.0% 3- hydroxy-2-butanones,
1.0 ~ 3.0% faenum graecum absolute oil,
2.0 ~ 5.0% ethyl laurate,
5.0 ~ 10.0% ethylmaltol,
5.0 ~ 10.0% jujube absolute oil,
70.0 ~ 86.5% Glycerin, mixed triester with caprylic acid capric acid；
The Glycerin, mixed triester with caprylic acid capric acid is medium chain triglyceride (MCT), for the aliphatic acid containing 8-12 carbochain and glycerine esterification
Product.
The cigarette quick-fried pearl red-jujube flavor essence, specific formula is, for example,：1.5% 3- hydroxy-2-butanones, 2.0% calabash
Reed bar absolute oil, 3.5% ethyl laurate, 7.0% ethylmaltol, 7.0% jujube absolute oil, 79% Glycerin, mixed triester with caprylic acid capric acid.
It is to be understood that in industry, as the top grade variety in natural perfume material, the essential oil extracted by solvent extraction
It is called absolute oil；Absolute oil described herein is to refer to plant extract（Or balm, botany bar gum, essential oil）Alcohol extractive, be one
Plant purer essential oil.
Also need to explain, different essence are different according to purposes, it, which is formulated, is generally particular design, described herein red
The savory essence of jujube be with reference to the quick-fried pearl of cigarette production technology characteristic, while according in final cigarette purposes carry out particular design, from
And regulation flue gas mass can be preferably realized on quick-fried pearl quality base is ensured, improves the result of cigarette sucking quality.
Using the quick-fried pearl of the cigarette with the quick-fried pearl of red-jujube flavor cigarette prepared by red-jujube flavor essence, the quick-fried pearl of cigarette refers to use
Natural macromolecular material or synthesis high polymer material, essence and flavoring agent is wrapped among a closed quick-fried pearl, formed it is a kind of with
Essence content is 20 ~ 25 μ L/ in the quick-fried pearl of sealing of circular different colours in the majority, a diameter of 2.0 ~ 4.0mm of quick-fried pearl, quick-fried pearl
Grain；Specifically for example：The quick-fried a diameter of 3.65mm of pearl, weight are 23mg/；Essence content is 23 μ L/ in quick-fried pearl, in a word, and it has
Body specification can be adjusted according to machinery equipment difference and institute using filter stick specification difference.
Application of the quick-fried pearl of red-jujube flavor cigarette in cigarette, the quick-fried pearl of cigarette is made an addition to commonly（Circumference 24.3mm）Cigarette filter rod
In, quick-fried pearl position is that, apart from lip end 12.5mm, every cigarette adds a quick-fried pearl.
Cigarette quick-fried pearl red-jujube flavor essence has obvious burnt fragrant and sweet and fresh and sweet perfume (or spice) etc. provided in the application, and these are fragrant
Gas is most important note feature in cigarette smoke；It is prepared into " quick-fried pearl " product form and applied to after cigarette, product inhale knot
Fruit shows：Compared to control sample, after the quick-fried pearl cigarette smoking of red-jujube flavor cigarette, cigarette smoke fragrance can not only not changed
On the premise of style, and can significantly improve that flue gas fragrance is rich, strengthen the satiety of flue gas by with rich, Jin Erti
The harmony of fragrance and product sensory quality has been risen, the interest of cigarette smoking is added.
In general, the red-jujube flavor essence employed in the application, by being obtained to be extracted from natural jujube, therefore
These aroma substances can reduce the excitant of flue gas, more highlight " roasting sweet tea " note of cigarette, carry after cigarette smoke is entered
Soft roundness degree, fragrance richness and the plumpness of cigarette smoke are risen, and then improves its sucking quality and sense organ comfort level.
In a word, the application is by providing a kind of red-jujube flavor essence for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried
Pearl production technology, can prepare Forming Quality stabilization, the uniform quick-fried pearl product of cigarette, the quick-fried pearl is inserted into cigarette filter
Afterwards, it can preferably weaken the excitant of cigarette, improve and abundant cigarette flavor, the fragrance for being obviously improved cigarette is rich, sense organ
Quality and the interest of suction, thus for quick-fried pearl cigarette design, exploitation and production and sales have preferable application value and
Popularization and application meaning.
Embodiment
Explanation is further explained to the present invention with reference to embodiment.Before specific embodiment is introduced, first to following
The preparation process of the quick-fried pearl of cigarette described in embodiment is briefly discussed below.
The main preparation process of the quick-fried pearl of cigarette of prior art is as described below：
The mainstream technology of quick-fried pearl production mainly prepares technique using drop method in shunting-liquid and produced, that is, utilizes cooling oil
The shearing force cut-out glue post liquidated, completes quick-fried droplet system；Specifically：Exist first with two different cooling oils of incident angle
Shearing force is formed in solenoid, the wall material during lower drop and core liquid are cut off, finally by surface tension in cooling oil
Effect condenses balling-up, then the quick-fried pearl of final finished product is made after the program such as deoiling, drying, sieve；It is prepared in following embodiments
Quick-fried pearl entrusts company of Shanghai Huabao Biotechnology Co., Ltd. to machine using the method；
It should be noted that, material employed in following embodiments：3- hydroxy-2-butanones, faenum graecum absolute oil, ethyl laurate,
Ethylmaltol, jujube absolute oil, Glycerin, mixed triester with caprylic acid capric acid etc. are also Shanghai Huabao Biotechnology Co., Ltd.'s Products.
Embodiment 1
Cigarette quick-fried pearl red-jujube flavor essence in the present embodiment, is calculated in mass percent, composed of the following components：
0.5% 3- hydroxy-2-butanones, 1.0% faenum graecum absolute oil, 2.0% ethyl laurate, 5.0% ethylmaltol,
5.0% jujube absolute oil, 86.5% Glycerin, mixed triester with caprylic acid capric acid.
This red-jujube flavor essence is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl to contain
Measure as 23 μ L/, the as quick-fried pearl of red-jujube flavor cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And be the quick-fried pearl cigarette of red-jujube flavor after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette of red-jujube flavor, by 7 professional sensory evaluation personnel to the sample and reference examples blank coil
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the quick-fried pearl of red-jujube flavor cigarette, volume
Substantially, the fragrance of flue gas is rich certain lifting to " jujube is fragrant " fragrance of cigarette sample, and fresh and sweet fragrant and burnt fragrant and sweet impression enhancing has
Sweet tea sense is returned, excitant reduction, miscellaneous gas is reduced, and flue gas sophistication is improved, and pleasant impression improves obvious.
Embodiment 2
Cigarette quick-fried pearl red-jujube flavor essence in the present embodiment, is calculated in mass percent, composed of the following components：
1.5% 3- hydroxy-2-butanones, 2.0% faenum graecum absolute oil, 3.5% ethyl laurate, 7.0% ethylmaltol,
7.0% jujube absolute oil, 79% Glycerin, mixed triester with caprylic acid capric acid.
This red-jujube flavor essence is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl to contain
Measure as 23 μ L/, the as quick-fried pearl of red-jujube flavor cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And be the quick-fried pearl cigarette of red-jujube flavor after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette of red-jujube flavor, by 7 professional sensory evaluation personnel to the sample and reference examples blank coil
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the quick-fried pearl of red-jujube flavor cigarette, volume
" jujube is fragrant " of cigarette sample is obvious, and flue gas fragrance is rich to be dramatically increased, and fresh and sweet fragrant and burnt fragrant and sweet impression is remarkably reinforced, and is had
Sweet tea sense is significantly returned, excitant is significantly reduced, miscellaneous gas is reduced, flue gas sophistication is significantly improved, and pleasant impression is obviously improved.
Embodiment 3
Cigarette quick-fried pearl red-jujube flavor essence in the present embodiment, is calculated in mass percent, composed of the following components：
2.0% 3- hydroxy-2-butanones, 3.0% faenum graecum absolute oil, 5.0% ethyl laurate, 10.0% ethylmaltol, 10.0%
Jujube absolute oil, 70.0% Glycerin, mixed triester with caprylic acid capric acid.
This red-jujube flavor essence is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl to contain
Measure as 23 μ L/, the as quick-fried pearl of red-jujube flavor cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And be the quick-fried pearl cigarette of red-jujube flavor after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette of red-jujube flavor, by 7 professional sensory evaluation personnel to the sample and reference examples blank coil
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the quick-fried pearl of red-jujube flavor cigarette, volume
" jujube is fragrant " of cigarette sample is fairly obvious, and flue gas fragrance harmony reduction, excitant increase, miscellaneous gas is reduced, flue gas inaccurate coordination
And having uncomfortable sweet sense, pleasant impression is not so good as normal cigarette（Control sample cigarette）.
To when prepared cigarette carries out conventional detection in above-described embodiment, to the physics and chemistry of diacetate fiber sample in cigarette sample
Index, the physical index of filter stick sample, the physical and chemical index of cigarette sample are determined, while according to《GB/T 19609—
2004 cigarette conventional analyses determine TPM and tar with smoking machine》Method determine total grain phase in cigarette mainstream flue gas
The indexs such as thing, tar, nicotine and moisture are detected that concrete outcome is as shown in the table.
Table 1, the physical index and main flume testing result of cigarette sample：
As can be seen from Table 1, compared with normal diacetate fiber filter stick cigarette, the diacetate fiber filter stick cigarette of quick-fried pearl is added
Physical and chemical index is without significant difference, and showing to add the quick-fried pearl of specific fragrance in diacetate fiber will not be to the filter efficiency of be molded filter stick
Adversely affect.
Table 2, cigarette sample sensory quality assessment result：
As can be seen from Table 2, by using the quick-fried pearl of specific fragrance, the organoleptic quality of cigarette can be made to significantly improve,
Its sensory evaluation scores highest can improve 1.33 points, and cigarette flavor is significantly improved, and pleasant impression improves, and excitant and miscellaneous gas also have larger drop
It is low.
To sum up, it is formulated by targetedly designing the quick-fried pearl of specific fragrance, is applied to after cigarette, can be obviously improved
Impression is sucked in odor characteristic during smoking property of cigarette, abundant and raising, with preferably application value.
It is emphasized that above-mentioned quick-fried pearl formula is directed to conventional cigarette improvement design, when applied to ramuscule cigarette, equally
With preferable application effect, but need to quick-fried pearl specification and in filter stick, addition enters according to specific tobacco blend and design requirement
The appropriate adjustment of row, will not be described in detail herein.
Claims (6)
1. a kind of cigarette quick-fried pearl red-jujube flavor essence, it is characterised in that be calculated in mass percent, composed of the following components：
0.5 ~ 2.0% 3- hydroxy-2-butanones,
1.0 ~ 3.0% faenum graecum absolute oil,
2.0 ~ 5.0% ethyl laurate,
5.0 ~ 10.0% ethylmaltol,
5.0 ~ 10.0% jujube absolute oil,
70.0 ~ 86.5% Glycerin, mixed triester with caprylic acid capric acid.
2. cigarette quick-fried pearl red-jujube flavor essence as claimed in claim 1, it is characterised in that be calculated in mass percent, 1.5% 3-
Hydroxy-2-butanone, 2.0% faenum graecum absolute oil, 3.5% ethyl laurate, 7.0% ethylmaltol, 7.0% jujube are net
Oil, 79% Glycerin, mixed triester with caprylic acid capric acid.
3. the quick-fried pearl of cigarette described in claim 1 is utilized with the quick-fried pearl of red-jujube flavor cigarette prepared by red-jujube flavor essence, it is characterised in that
Essence content is 20 ~ 25 μ L/ in a diameter of 2.0 ~ 4.0mm of quick-fried pearl, quick-fried pearl.
4. the quick-fried pearl of red-jujube flavor cigarette as claimed in claim 3, it is characterised in that the quick-fried a diameter of 3.65mm of pearl, weight are 23mg/
Essence content is 23 μ L/ in grain, quick-fried pearl.
5. application of the quick-fried pearl of red-jujube flavor cigarette in cigarette described in claim 3, it is characterised in that the quick-fried pearl of cigarette is made an addition into filter
In rod.
6. application of the quick-fried pearl of red-jujube flavor cigarette as claimed in claim 5 in cigarette, it is characterised in that the quick-fried pearl of cigarette is located at filter stick
A quick-fried pearl is added in middle part, every cigarette filter rod.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710287357.6A CN107034019A (en) | 2017-04-27 | 2017-04-27 | A kind of cigarette quick-fried pearl red-jujube flavor essence and its application in cigarette |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710287357.6A CN107034019A (en) | 2017-04-27 | 2017-04-27 | A kind of cigarette quick-fried pearl red-jujube flavor essence and its application in cigarette |
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| CN109868185A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of faenum graecum cigarette quick-fried pearl essence and its application in cigarette |
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Application publication date: 20170811 |
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