CN106947598A - A kind of cigarette quick-fried pearl agate card essence and its application in cigarette - Google Patents

A kind of cigarette quick-fried pearl agate card essence and its application in cigarette Download PDF

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Publication number
CN106947598A
CN106947598A CN201710287641.3A CN201710287641A CN106947598A CN 106947598 A CN106947598 A CN 106947598A CN 201710287641 A CN201710287641 A CN 201710287641A CN 106947598 A CN106947598 A CN 106947598A
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China
Prior art keywords
cigarette
quick
fried pearl
agate card
essence
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201710287641.3A
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Chinese (zh)
Inventor
高明奇
顾亮
李明哲
冯晓民
纪朋
孟洋
张展
杨金初
董艳娟
田海英
刘文博
杨帆
李禄成
鲁平
李耀光
罗灿选
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China Tobacco Henan Industrial Co Ltd
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China Tobacco Henan Industrial Co Ltd
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Application filed by China Tobacco Henan Industrial Co Ltd filed Critical China Tobacco Henan Industrial Co Ltd
Priority to CN201710287641.3A priority Critical patent/CN106947598A/en
Publication of CN106947598A publication Critical patent/CN106947598A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention belongs to cigarette filter rod production technical field, and in particular to a kind of cigarette quick-fried pearl agate card essence and its patent application of the application in cigarette.The agate card essence is made up of agate card extract, methyl linoleate, 3,4 xylenols, D limonenes, indoles, davana oil, Glycerin, mixed triester with caprylic acid capric acid.The quick-fried pearl of agate card cigarette can be prepared using the essence, the quick-fried pearl can be added in filter stick and the quick-fried pearl cigarette application of cigarette is prepared.The application is by providing a kind of agate card essence for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl production technology, Forming Quality stabilization, the uniform quick-fried pearl product of cigarette can be prepared, the quick-fried pearl is inserted after cigarette filter, the excitant of cigarette can preferably be weakened, improve and abundant cigarette flavor, the fragrance that is obviously improved cigarette is rich, the interest of aesthetic quality and suction, thus has preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.

Description

A kind of cigarette quick-fried pearl agate card essence and its application in cigarette
Technical field
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of quick-fried pearl of cigarette is with agate card essence and its in volume The patent application of application in cigarette.
Background technology
In traditional cigarette perfuming technology, spice liquid is mainly added in pipe tobacco by it, and the feed liquid that this mode is added is past Toward meeting, partition losses fall during cigarette burning, simultaneously because the reaction of complex material system is difficult to be expected under high temperature, part Feed liquid can also produce some bad organoleptic effects.Quick-fried pearl perfuming, being capable of necessarily journey as a kind of emerging perfuming cigarette mode The defect in existing perfuming mode is overcome on degree, its main cause is:Include spices in quick-fried pearl, suck before cigarette, consumer The first choice quick-fried pearl being contained in filter stick of crumbing burns and sucks cigarette again, and now flue gas is through together acting on and disappearing with quick-fried pearl feed liquid during filter tip Fei Zhe, so that completing perfuming mends fragrant process;On the one hand this mode can be prevented effectively from feed liquid of the spices during result of combustion of tobacco Loss, on the other hand, will not be lost, so that really because spices is placed in the quick-fried pearl of sealing, thus during cigarette is stored The stabilization of cigarette quality is protected.
" quick-fried pearl ", due to the special delivery mode of its inclusion, is being supplemented, changed as a kind of emerging material in cigarette Function in terms of kind, coordination smoking property of cigarette quality and lifting, change, cigarette product style is increasingly protruded, and improves cigarette The interest of suction and aesthetic quality, thus " quick-fried pearl " cigarette is obtaining increasing in Chinese-style cigarette production in recent years Using also obtaining liking for consumers in general.
In the prior art, although there is the fragrance in a number of quick-fried pearl cigarette, this quick-fried pearl in the market Because lack of targeted is designed, thus it is relatively poor with flue gas harmony, and the odor characteristic influence on cigarette in itself is larger, because And have impact on quick-fried pearl cigarette suck impression.
" quick-fried pearl ", although cigarette occurs like the mushrooms after rain, is due to its product relative new, current production standard and Specification is relative to be lacked, so that the addition of " quick-fried pearl " and use also occur in that many new problems.Especially for cigarette For the particularity of product, the design of composition formula is included " quick-fried pearl ", inclusion stability discharges, and " quick-fried pearl " filter stick is for cigarette Rare report in terms of physical index, chemical index, the influence of harm sex index.Therefore " the quick-fried pearl " of different constituents is designed Inclusion, systematization research " quick-fried pearl " Special inclusion release rule, " quick-fried pearl " inclusion refers to cigarette physical index, flue gas There is important theory and application value in terms of mark, the influence of harm sex index.
The content of the invention
Present invention aims at a kind of agate card essence being targetedly used in cigarette filter rod is provided, so that abundant cigarette Product type, to provide the cigarette product of different-style feature.
Details are as follows for the technical scheme that the application is taken.
A kind of cigarette quick-fried pearl agate card essence, is calculated in mass percent, composed of the following components:
10.0 ~ 15.0% agate card extract,
3.0 ~ 5.0% methyl linoleate,
0.5 ~ 1.0% 3,4- xylenols,
1.0 ~ 3.0% D- limonenes,
0.3 ~ 0.5% indoles,
0.5 ~ 1.0% davana oil,
74.5 ~ 84.7% Glycerin, mixed triester with caprylic acid capric acid.
The agate card extract is the ethanol extract of agate card;
The Glycerin, mixed triester with caprylic acid capric acid is medium chain triglyceride (MCT), for the aliphatic acid containing 8-12 carbochain and glycerine esterification Product.
The agate card extract, specifically refers to following steps and prepares:
(1)By dried maca powder it is broken after, cross 40 ~ 60 mesh sieves, prepare maca powder;
(2)To step(1)Maca powder in add the ethanol solution of volume fraction 60 ~ 90%, water-bath heat backflow 3 at 60 ~ 80 DEG C ~ 5h;The solid-liquid ratio of maca powder and ethanol solution is, maca powder:Ethanol=1g:4~6mL;
(3)By step(2)Middle hot phegma is concentrated under reduced pressure into that volume is unchanged under the conditions of 55 ~ 65 DEG C, 60 ~ 80Kpa, and gained is carried It is agate card extract to take thing.
The cigarette quick-fried pearl agate card essence, Ju Ti Pei Fang is, for example,:12% agate card extract, 4% methyl linoleate, 0.7% 3,4- xylenols, 1.5% D- limonenes, 0.4% indoles, 0.7% davana oil and 80.7% pungent capric acid are sweet Grease.
It is to be understood that different essence are different according to purposes, it, which is formulated, is generally particular design, agate described herein Card essence be with reference to the quick-fried pearl of cigarette production technology characteristic, while according in final cigarette purposes carry out particular design so that Regulation flue gas mass can be preferably realized on quick-fried pearl quality base is ensured, improves the result of cigarette sucking quality.
Using the quick-fried pearl of the cigarette with the quick-fried pearl of agate card cigarette prepared by agate card essence, the quick-fried pearl of cigarette refers to natural Macromolecular material or synthesis macromolecular material, essence and flavoring agent is wrapped among a closed quick-fried pearl, forms one kind with circle Essence content is 20 ~ 25 μ L/ in the quick-fried pearl of sealing of different colours in the majority, a diameter of 2.0 ~ 4.0mm of quick-fried pearl, quick-fried pearl;Tool Body is for example:The quick-fried a diameter of 3.65mm of pearl, weight are 23mg/;Essence content is 23 μ L/, in a word, its The concrete specification in quick-fried pearl It can be adjusted according to machinery equipment difference and institute using filter stick specification difference.
Application of the quick-fried pearl of agate card cigarette in cigarette, the quick-fried pearl of cigarette is made an addition to commonly(Circumference 24.3mm)Cigarette is filtered In rod, quick-fried pearl position is that, apart from lip end 12.5mm, every cigarette adds a quick-fried pearl.
Cigarette quick-fried pearl agate card essence has obvious fresh and sweet fragrant and draft fragrant provided in the application, and these fragrance are Most important note feature in cigarette smoke;It is prepared into " quick-fried pearl " product form and applied to after cigarette, product inhale result table It is bright:Compared to control sample, after the quick-fried pearl cigarette smoking of agate card cigarette, cigarette smoke aromatic style can not only not changed Under the premise of, and can significantly improve that flue gas fragrance is rich, strengthen the satiety of flue gas by with it is rich, and then improve perfume (or spice) Gas and the harmony of product sensory quality, add the interest of cigarette smoking;Simultaneously because agate card has antifatigue, added body Power, improves the effects such as sleep, anti-climacteric, active fertility, enhancing memory, so that the application has mitigates volume to a certain degree Cigarette sucks the effect of harm.
In general, the agate card essence employed in the application, by being obtained to be extracted from natural agate card, therefore this A little aroma substances can reduce the excitant of flue gas after cigarette smoke is entered, and lift soft roundness degree, the fragrance of cigarette smoke Richness and plumpness, and then improve its sucking quality and sense organ comfort level.
In a word, the application is by providing a kind of agate card essence for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl Production technology, can prepare Forming Quality stabilization, the uniform quick-fried pearl product of cigarette, the quick-fried pearl is inserted after cigarette filter, It can preferably weaken the excitant of cigarette, improve and abundant cigarette flavor, the fragrance for being obviously improved cigarette is rich, aesthetic quality And the interest of suction, and due to it is certain it is antifatigue, regain one's strength of body, improve sleep, anti-climacteric, actively give birth to, strengthen Memory, reduction cigarette be the effects such as endanger, thus have for design, exploitation and the production and sales of quick-fried pearl cigarette and preferably apply valency Value and popularization and application meaning.
Embodiment
Explanation is further explained to the present invention with reference to embodiment.Before specific embodiment is introduced, first to following The preparation process of the quick-fried pearl of cigarette described in embodiment is briefly discussed below.
The main preparation process of the quick-fried pearl of cigarette of prior art is as described below:
The mainstream technology of quick-fried pearl production mainly prepares technique using drop method in shunting-liquid and produced, that is, utilizes cooling oil The shearing force cut-out glue post liquidated, completes quick-fried droplet system;Specifically:Exist first with two different cooling oils of incident angle Shearing force is formed in solenoid, the wall material during lower drop and core liquid are cut off, finally by surface tension in cooling oil Effect condenses balling-up, then the quick-fried pearl of final finished product is made after the program such as deoiling, drying, sieve;It is prepared in following embodiments Quick-fried pearl entrusts company of Shanghai Huabao Biotechnology Co., Ltd. to machine using the method;
It should be noted that, material employed in following embodiments:Methyl linoleate, 3,4- xylenols, D- limonenes, Yin Diindyl, davana oil and Glycerin, mixed triester with caprylic acid capric acid etc. are also Shanghai Huabao Biotechnology Co., Ltd.'s Products;
Agate card extract, is prepared as follows employed in following embodiments:
(1)By dried maca powder it is broken after, cross 50 mesh sieves, prepare maca powder;
(2)To step(1)Maca powder in add the ethanol solution of volume fraction 75%, water-bath heat backflow 4h at 70 DEG C;Maca powder Solid-liquid ratio with ethanol solution is, maca powder:Ethanol=1g:5mL;
(3)By step(2)It is unchanged that middle hot phegma is concentrated under reduced pressure into volume under the conditions of 60 DEG C, 70Kpa, it is extract obtained i.e. For agate card extract.
Embodiment 1
Cigarette quick-fried pearl agate card essence in the present embodiment, is calculated in mass percent, composed of the following components:
10% agate card extract, 3% methyl linoleate, 0.5% 3,4- xylenols, 1.0% D- limonenes, 0.3% Indoles, 0.5% davana oil and 84.7% Glycerin, mixed triester with caprylic acid capric acid.
This agate card essence is prepared into essence content in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl For 23 μ L/, the as quick-fried pearl of agate card cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common(Circumference 24.3mm)In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick, And be the quick-fried pearl cigarette of agate card after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette of agate card, by 7 professional sensory evaluation personnel to the sample and reference examples blank cigarette Sample(Same position adds the quick-fried pearl of blank)Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that the personnel that smoke panel test unanimously think 7 cigarette, after it with the addition of the quick-fried pearl of agate card cigarette, cigarette Substantially, the fragrance of flue gas is rich certain lifting to " agate card is fragrant " fragrance of sample, and fresh and sweet fragrant and burnt fragrant and sweet impression enhancing has back Sweet sense, excitant reduction, miscellaneous gas is reduced, and flue gas sophistication is improved, and pleasant impression makes moderate progress.
Embodiment 2
Cigarette quick-fried pearl agate card essence in the present embodiment, is calculated in mass percent, composed of the following components:
12% agate card extract, 4% methyl linoleate, 0.7% 3,4- xylenols, 1.5% D- limonenes, 0.4% Indoles, 0.7% davana oil and 80.7% Glycerin, mixed triester with caprylic acid capric acid.
This agate card essence is prepared into essence content in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl For 23 μ L/, the as quick-fried pearl of agate card cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common(Circumference 24.3mm)In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick, And be the quick-fried pearl cigarette of agate card after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette of agate card, by 7 professional sensory evaluation personnel to the sample and reference examples blank cigarette Sample(Same position adds the quick-fried pearl of blank)Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that the personnel that smoke panel test unanimously think 7 cigarette, after it with the addition of the quick-fried pearl of agate card cigarette, cigarette " agate card is fragrant " of sample is obvious, and flue gas fragrance is rich to be dramatically increased, and fresh and sweet fragrant and burnt fragrant and sweet impression is remarkably reinforced, and has bright Aobvious returns sweet sense, and excitant is significantly reduced, and miscellaneous gas is reduced, and flue gas sophistication is significantly improved, and pleasant impression is obviously improved.
Embodiment 3
Cigarette quick-fried pearl agate card essence in the present embodiment, is calculated in mass percent, composed of the following components:
15% agate card extract, 5% methyl linoleate, 1.0% 3,4- xylenols, 3.0% D- limonenes, 0.5% Indoles, 1.0% davana oil and 74.5% Glycerin, mixed triester with caprylic acid capric acid.
This agate card essence is prepared into essence content in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl For 23 μ L/, the as quick-fried pearl of agate card cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common(Circumference 24.3mm)In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick, And be the quick-fried pearl cigarette of agate card after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette of agate card, by 7 professional sensory evaluation personnel to the sample and reference examples blank cigarette Sample(Same position adds the quick-fried pearl of blank)Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that the personnel that smoke panel test unanimously think 7 cigarette, after it with the addition of the quick-fried pearl of agate card cigarette, cigarette " the agate card fragrant " of sample is fairly obvious, and flue gas fragrance harmony reduction, excitant increase, miscellaneous gas is reduced, flue gas inaccurate coordination and There is uncomfortable sweet sense, pleasant impression is not so good as normal cigarette(Control sample cigarette).
Quick-fried pearl product prepared by not be the same as Example is detected, while being carried out to prepared cigarette in above-described embodiment Conventional detection, with to the physical and chemical index of diacetate fiber sample, the physical index of filter stick sample, the reason of cigarette sample in cigarette sample Change index to be measured, further according to《The conventional analysis of the cigarette of GB/T 19609-2004 determines TPM with smoking machine And tar》Method determine the index such as TPM, tar, nicotine and moisture in cigarette mainstream flue gas and detected, specifically As a result it is as shown in the table.
Table 1, not in be the same as Example prepared quick-fried pearl testing result:
The testing result of table 2, the not prepared filter stick containing quick-fried pearl of be the same as Example:
Table 3, the physical index and main flume testing result of kinds of cigarettes sample:
It is can be seen that from the above-mentioned data of table 2 compared with normal diacetate fiber filter stick, the filter stick physics for placing the quick-fried pearl of agate card refers to Mark is without significant difference, and mainly filter stick pressure drop there occurs significant changes.As can be seen from Table 3, with the normal cigarette of reference examples Compare, the main flume of the quick-fried pearl cigarette of agate card is varied from, but after quick-fried pearl pinches brokenly, influence the key index tar of cigarette sense organ And nicotine does not have significant changes.
Table 4, kinds of cigarettes sample sensory quality assessment result:
As can be seen from Table 4, by using the quick-fried pearl of agate card cigarette sensory quality can be made to significantly improve, its sense organ Scoring highest can improve 0.92 point, and fragrance is significantly improved, and pleasant impression improves, and excitant and miscellaneous gas also have larger reduction.
To sum up, it is formulated by targetedly designing the quick-fried pearl of specific fragrance, is applied to after cigarette, can be obviously improved Impression is sucked in odor characteristic during smoking property of cigarette, abundant and raising, simultaneously because the standby special efficacy of agate fixture can also reduce volume Cigarette endangers.Therefore the application highlights the new agate that cigarette " agate card " note, improvement sucking quality, reduction cigarette endanger as one kind Block quick-fried pearl, in industry with definitely application value.
It is emphasized that above-mentioned quick-fried pearl formula is directed to conventional formulation cigarette improvement design, when applied to ramuscule cigarette, Equally there is preferable application effect, but need to be added according to specific tobacco blend and design requirement to quick-fried pearl specification and in filter stick Amount is suitably adjusted, and will not be described in detail herein.

Claims (6)

1. a kind of cigarette quick-fried pearl agate card essence, it is characterised in that be calculated in mass percent, composed of the following components:
10.0 ~ 15.0% agate card extract,
3.0 ~ 5.0% methyl linoleate,
0.5 ~ 1.0% 3,4- xylenols,
1.0 ~ 3.0% D- limonenes,
0.3 ~ 0.5% indoles,
0.5 ~ 1.0% davana oil,
74.5 ~ 84.7% Glycerin, mixed triester with caprylic acid capric acid;
The agate card extract is the ethanol extract of agate card.
2. cigarette quick-fried pearl agate card essence as claimed in claim 1, it is characterised in that 12% agate card extract, 4% linoleic acid Methyl esters, 0.7% 3,4- xylenols, 1.5% D- limonenes, 0.4% indoles, 0.7% davana oil and the 80.7% pungent last of the ten Heavenly stems Acid glyceride.
3. the quick-fried pearl of cigarette described in claim 1 is utilized with the quick-fried pearl of agate card cigarette prepared by agate card essence, it is characterised in that quick-fried pearl A diameter of 2.0 ~ 4.0mm, essence content is 20 ~ 25 μ L/ in quick-fried pearl.
4. the quick-fried pearl of agate card cigarette as claimed in claim 3, it is characterised in that the quick-fried a diameter of 3.65mm of pearl, weight are 23mg/, Essence content is 23 μ L/ in quick-fried pearl.
5. application of the quick-fried pearl of agate card cigarette in cigarette described in claim 3, it is characterised in that the quick-fried pearl of cigarette is made an addition into filter stick In.
6. application of the quick-fried pearl of agate card cigarette as claimed in claim 5 in cigarette, it is characterised in that the quick-fried pearl of cigarette is located in filter stick A quick-fried pearl is added in portion, every cigarette filter rod.
CN201710287641.3A 2017-04-27 2017-04-27 A kind of cigarette quick-fried pearl agate card essence and its application in cigarette Pending CN106947598A (en)

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Publication number Priority date Publication date Assignee Title
CN109156870A (en) * 2018-10-23 2019-01-08 云南中烟工业有限责任公司 A kind of additive with tongue fur note style and features and include the cigarette of the additive
CN109156868A (en) * 2018-10-23 2019-01-08 云南中烟工业有限责任公司 A kind of essence with tongue fur note style and features and include the cigarette of the essence
CN111040876A (en) * 2019-12-19 2020-04-21 云南瑞升烟草技术(集团)有限公司 Preparation method of natural spice suitable for cigarette bead blasting
CN113325128A (en) * 2021-05-28 2021-08-31 四川中烟工业有限责任公司 Method for detecting moisture of surface skin of blasting bead

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109156870A (en) * 2018-10-23 2019-01-08 云南中烟工业有限责任公司 A kind of additive with tongue fur note style and features and include the cigarette of the additive
CN109156868A (en) * 2018-10-23 2019-01-08 云南中烟工业有限责任公司 A kind of essence with tongue fur note style and features and include the cigarette of the essence
CN111040876A (en) * 2019-12-19 2020-04-21 云南瑞升烟草技术(集团)有限公司 Preparation method of natural spice suitable for cigarette bead blasting
CN113325128A (en) * 2021-05-28 2021-08-31 四川中烟工业有限责任公司 Method for detecting moisture of surface skin of blasting bead

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Application publication date: 20170714