CN106987314A - A kind of quick-fried pearl of the cigarette small blue or green savory essence of mandarin orange and its application in cigarette - Google Patents
A kind of quick-fried pearl of the cigarette small blue or green savory essence of mandarin orange and its application in cigarette Download PDFInfo
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- CN106987314A CN106987314A CN201710288573.2A CN201710288573A CN106987314A CN 106987314 A CN106987314 A CN 106987314A CN 201710288573 A CN201710288573 A CN 201710288573A CN 106987314 A CN106987314 A CN 106987314A
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- cigarette
- quick
- fried pearl
- green
- mandarin orange
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Abstract
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of quick-fried pearl of the cigarette small blue or green savory essence of mandarin orange and its patent application of the application in cigarette.The small blue or green savory essence of mandarin orange is made up of small blue or green mandarin orange extract, diacetyl, Ethyl vanillin, methyl cinnamate, geraniol, orange oil, Glycerin, mixed triester with caprylic acid capric acid.The small blue or green quick-fried pearl of mandarin orange taste cigarette can be prepared using the essence, the quick-fried pearl can be added in filter stick and the quick-fried pearl cigarette application of cigarette is prepared.The application is by providing a kind of small blue or green savory essence of mandarin orange for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl production technology, Forming Quality stabilization, the uniform quick-fried pearl product of cigarette can be prepared, the quick-fried pearl is inserted after cigarette filter, the excitant of cigarette can preferably be weakened, improve and abundant cigarette flavor, the fragrance that is obviously improved cigarette is rich, the interest of aesthetic quality and suction, thus has preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.
Description
Technical field
The invention belongs to cigarette filter rod production technical field, and in particular to a kind of quick-fried pearl of cigarette with the savory essence of small blue or green mandarin orange and its
The patent application of application in cigarette.
Background technology
In traditional cigarette perfuming technology, spice liquid is mainly added in pipe tobacco by it, and the feed liquid that this mode is added is past
Toward meeting, partition losses fall during cigarette burning, simultaneously because the reaction of complex material system is difficult to be expected under high temperature, part
Feed liquid can also produce some bad organoleptic effects.Quick-fried pearl perfuming, being capable of necessarily journey as a kind of emerging perfuming cigarette mode
The defect in existing perfuming mode is overcome on degree, its main cause is：Include spices in quick-fried pearl, suck before cigarette, consumer
The first choice quick-fried pearl being contained in filter stick of crumbing burns and sucks cigarette again, and now flue gas is through together acting on and disappearing with quick-fried pearl feed liquid during filter tip
Fei Zhe, so that completing perfuming mends fragrant process；On the one hand this mode can be prevented effectively from feed liquid of the spices during result of combustion of tobacco
Loss, on the other hand, because spices is placed in sealed quick-fried pearl, thus will not be lost, so that really during cigarette is stored
The stabilization of cigarette quality is protected.
" quick-fried pearl ", due to the special delivery mode of its inclusion, is being supplemented, changed as a kind of emerging material in cigarette
Function in terms of kind, coordination smoking property of cigarette quality and lifting, change, cigarette product style is increasingly protruded, and improves cigarette
The interest of suction and aesthetic quality, thus " quick-fried pearl " cigarette is obtaining increasing in Chinese-style cigarette production in recent years
Using also obtaining liking for consumers in general.
In the prior art, although there is the fragrance in a number of quick-fried pearl cigarette, this quick-fried pearl in the market
Because lack of targeted is designed, thus it is relatively poor with flue gas harmony, and the odor characteristic influence on cigarette in itself is larger, because
And have impact on quick-fried pearl cigarette suck impression.
" quick-fried pearl ", although cigarette occurs like the mushrooms after rain, is due to its product relative new, current production standard and
Specification is relative to be lacked, so that the addition of " quick-fried pearl " and use also occur in that many new problems.Especially for cigarette
For the particularity of product, the design of composition formula is included " quick-fried pearl ", inclusion stability discharges, and " quick-fried pearl " filter stick is for cigarette
Rare report in terms of physical index, chemical index, the influence of harm sex index.Therefore " the quick-fried pearl " of different constituents is designed
Inclusion, systematization research " quick-fried pearl " Special inclusion release rule, " quick-fried pearl " inclusion refers to cigarette physical index, flue gas
There is important theory and application value in terms of mark, the influence of harm sex index.
The content of the invention
Present invention aims at a kind of small blue or green savory essence of mandarin orange being targetedly used in cigarette filter rod is provided, so that abundant
Cigarette product type, to provide the cigarette product of different-style feature.
Details are as follows for the technical scheme that the application is taken.
A kind of quick-fried pearl of cigarette is calculated in mass percent with the small blue or green savory essence of mandarin orange, composed of the following components：
10.0 ~ 15.0% small blue or green mandarin orange extract,
1.0 ~ 2.0% diacetyl,
0.3 ~ 0.6% Ethyl vanillin,
0.5 ~ 1.0% methyl cinnamate,
0.2 ~ 0.5% geraniol,
1.0 ~ 2.0% orange oil,
78.9 ~ 87.0% Glycerin, mixed triester with caprylic acid capric acid.
The small blue or green mandarin orange extract is the ethanol extract of small blue or green mandarin orange；
The Glycerin, mixed triester with caprylic acid capric acid is medium chain triglyceride (MCT), for the aliphatic acid containing 8-12 carbochain and glycerine esterification
Product.
The small blue or green mandarin orange extract, specifically refers to following steps and prepares：
（1）After dried small blue or green mandarin orange is crushed, 40 ~ 60 mesh sieves are crossed, small blue or green mandarin orange powder is prepared；
（2）To step（1）Small blue or green mandarin orange powder in add the ethanol solution of volume fraction 60 ~ 90%, water-bath heat backflow 3 at 60 ~ 80 DEG C
~5h；The solid-liquid ratio of small blue or green mandarin orange powder and ethanol solution is, small blue or green mandarin orange powder：Ethanol=1g：4~6mL；
（3）By step（2）Middle hot phegma is concentrated under reduced pressure into that volume is unchanged under the conditions of 55 ~ 65 DEG C, 60 ~ 80Kpa, and gained is carried
It is small blue or green mandarin orange extract to take thing.
The quick-fried pearl of cigarette is, for example, with the small blue or green savory essence of mandarin orange, specific formula：12% small blue or green mandarin orange extract, 1.5% fourth
Diketone, 0.4% Ethyl vanillin, 0.7% methyl cinnamate, 0.35% geraniol, 1.5% orange oil and 83.55% it is pungent
Glycerol decanoate.
It is to be understood that different essence are different according to purposes, it, which is formulated, is generally particular design, described herein small
The blue or green savory essence of mandarin orange be with reference to the quick-fried pearl of cigarette production technology characteristic, while according in final cigarette purposes carry out particular design,
So as to can preferably realize regulation flue gas mass on quick-fried pearl quality base is ensured, improve the result of cigarette sucking quality.
Using the quick-fried pearl of the cigarette with the small blue or green quick-fried pearl of mandarin orange taste cigarette prepared by the savory essence of small blue or green mandarin orange, the quick-fried pearl of cigarette is
Finger natural macromolecular material or synthesis high polymer material, essence and flavoring agent is wrapped among a closed quick-fried pearl, one is formed
Kind with the quick-fried pearl of sealing of circular different colours in the majority, a diameter of 2.0 ~ 4.0mm of quick-fried pearl, essence content is 20 ~ 25 μ in quick-fried pearl
L/；Specifically for example：The quick-fried a diameter of 3.65mm of pearl, weight are 23mg/；Essence content is 23 μ L/ in quick-fried pearl, in a word, its
The concrete specification can be adjusted according to machinery equipment difference and institute using filter stick specification difference.
Application of the small blue or green quick-fried pearl of mandarin orange taste cigarette in cigarette, the quick-fried pearl of cigarette is made an addition to commonly（Circumference 24.3mm）Volume
In cigarette filter, quick-fried pearl position is that, apart from lip end 12.5mm, every cigarette adds a quick-fried pearl.
The quick-fried pearl of cigarette has obvious draft fragrant with the small blue or green savory essence of mandarin orange provided in the application, and these fragrance are cigarette
Most important note feature in flue gas；It is prepared into " quick-fried pearl " product form and applied to after cigarette, product are inhaled result and shown：Phase
Compared with control sample, after the small blue or green quick-fried pearl cigarette smoking of mandarin orange taste cigarette, cigarette smoke aromatic style can not only not changed
Under the premise of, and can significantly improve that flue gas fragrance is rich, strengthen the satiety of flue gas by with it is rich, and then improve perfume (or spice)
Gas and the harmony of product sensory quality, add the interest of cigarette smoking；Simultaneously because small blue or green mandarin orange has qi-regulating stomach invigorating, dispelled
Phlegm wets one's whistle, arousing brain, raising spirit the effects such as so that the application have to a certain degree mitigate smoking property of cigarette harm effect.
In general, the small blue or green savory essence of mandarin orange employed in the application, by being obtained to be extracted from natural small blue or green mandarin orange,
Therefore these aroma substances can reduce the excitant of flue gas after cigarette smoke is entered, and lift the soft mellow and full of cigarette smoke
Degree, fragrance richness and plumpness, and then improve its sucking quality and sense organ comfort level.
In a word, the application is by providing a kind of small blue or green savory essence of mandarin orange for being specifically used for the quick-fried pearl of cigarette and combining more perfect
Quick-fried pearl production technology, can prepare Forming Quality stabilization, the uniform quick-fried pearl product of cigarette, the quick-fried pearl is inserted into cigarette filter
Afterwards, it can preferably weaken the excitant of cigarette, improve and abundant cigarette flavor, the fragrance for being obviously improved cigarette is rich, sense organ
Quality and the interest of suction, and due to being wet one's whistle with certain qi-regulating stomach invigorating, eliminating the phlegm, arousing brain, raising spirit, reduction cigarette harm etc. work(
Effect, thus there is preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.
Embodiment
Explanation is further explained to the present invention with reference to embodiment.Before specific embodiment is introduced, first to following
The preparation process of the quick-fried pearl of cigarette described in embodiment is briefly discussed below.
The main preparation process of the quick-fried pearl of cigarette of prior art is as described below：
The mainstream technology of quick-fried pearl production mainly prepares technique using drop method in shunting-liquid and produced, that is, utilizes cooling oil
The shearing force cut-out glue post liquidated, completes quick-fried droplet system；Specifically：Exist first with two different cooling oils of incident angle
Shearing force is formed in solenoid, the wall material during lower drop and core liquid are cut off, finally by surface tension in cooling oil
Effect condenses balling-up, then the quick-fried pearl of final finished product is made after the program such as deoiling, drying, sieve；It is prepared in following embodiments
Quick-fried pearl entrusts company of Shanghai Huabao Biotechnology Co., Ltd. to machine using the method；
It should be noted that, material employed in following embodiments：Diacetyl, Ethyl vanillin, methyl cinnamate, geraniol,
Orange oil and Glycerin, mixed triester with caprylic acid capric acid etc. are also Shanghai Huabao Biotechnology Co., Ltd.'s Products；
Small blue or green mandarin orange is the plant tea being made from still immature " infantile period " citrus with yunnan puer tea for raw material, institute
With small blue or green mandarin orange in company of Xinhui of Guangdong Province stochastic buying.
Small blue or green mandarin orange extract, is prepared as follows employed in following embodiments：
（1）After dried small blue or green mandarin orange is crushed, 50 mesh sieves are crossed, small blue or green mandarin orange powder is prepared；
（2）To step（1）Small blue or green mandarin orange powder in add the ethanol solution of volume fraction 75%, water-bath heat backflow 4h at 70 DEG C；Small green grass or young crops
The solid-liquid ratio of mandarin orange powder and ethanol solution is, small blue or green mandarin orange powder：Ethanol=1g：5mL；
（3）By step（2）It is unchanged that middle hot phegma is concentrated under reduced pressure into volume under the conditions of 60 DEG C, 70Kpa, it is extract obtained i.e.
For small blue or green mandarin orange extract.
Embodiment 1
The quick-fried pearl of cigarette in the present embodiment is calculated in mass percent with the small blue or green savory essence of mandarin orange, composed of the following components：
10% small blue or green mandarin orange extract, 1.0% diacetyl, 0.3% Ethyl vanillin, 0.5% methyl cinnamate, 0.2% perfume (or spice)
Leaf-alcohol, 1.0% orange oil and 87.0% Glycerin, mixed triester with caprylic acid capric acid.
This small blue or green savory essence of mandarin orange is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl
Content is 23 μ L/, the as small blue or green quick-fried pearl of mandarin orange taste cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, common circumference is made an addition to
（24.3mm）In cigarette filter rod, quick-fried pearl position is that, apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter
It is the small blue or green quick-fried pearl cigarette of mandarin orange taste after rod, and cigarette cigarette sample.
To the prepared small blue or green quick-fried pearl cigarette of mandarin orange taste, by 7 professional sensory evaluation personnel to the sample and reference examples blank
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the small blue or green quick-fried pearl of mandarin orange taste cigarette,
Substantially, the fragrance of flue gas is rich certain lifting to " small blue or green mandarin orange is fragrant " fragrance of cigarette sample, and fresh and sweet fragrant and burnt fragrant and sweet impression increases
By force, there is back sweet tea sense, excitant reduction, miscellaneous gas is reduced, and flue gas sophistication is improved, and pleasant impression makes moderate progress.
Embodiment 2
The quick-fried pearl of cigarette in the present embodiment is calculated in mass percent with the small blue or green savory essence of mandarin orange, composed of the following components：
12% small blue or green mandarin orange extract, 1.5% diacetyl, 0.4% Ethyl vanillin, 0.7% methyl cinnamate, 0.35%
Geraniol, 1.5% orange oil and 83.55% Glycerin, mixed triester with caprylic acid capric acid.
This small blue or green savory essence of mandarin orange is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl
Content is 23 μ L/, the as small blue or green quick-fried pearl of mandarin orange taste cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And be the small blue or green quick-fried pearl cigarette of mandarin orange taste after cigarette cigarette sample.
To the prepared small blue or green quick-fried pearl cigarette of mandarin orange taste, by 7 professional sensory evaluation personnel to the sample and reference examples blank
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the small blue or green quick-fried pearl of mandarin orange taste cigarette,
" small blue or green mandarin orange is fragrant " of cigarette sample is obvious, and flue gas fragrance is rich to be dramatically increased, and fresh and sweet fragrant and burnt fragrant and sweet impression substantially increases
By force, have and significantly return sweet tea sense, excitant is significantly reduced, miscellaneous gas is reduced, flue gas sophistication is significantly improved, and pleasant impression is obviously improved.
Embodiment 3
The quick-fried pearl of cigarette in the present embodiment is calculated in mass percent with the small blue or green savory essence of mandarin orange, composed of the following components：
15% small blue or green mandarin orange extract, 2.0% diacetyl, 0.6% Ethyl vanillin, 1.0% methyl cinnamate, 0.5% perfume (or spice)
Leaf-alcohol, 2.0% orange oil and 78.9% Glycerin, mixed triester with caprylic acid capric acid.
This small blue or green savory essence of mandarin orange is prepared into essence in the quick-fried pearl of cigarette that a diameter of 3.65mm, weight are 23mg/, quick-fried pearl
Content is 23 μ L/, the as small blue or green quick-fried pearl of mandarin orange taste cigarette.
By existing filter stick production technology, quick-fried pearl is inserted by filter stick center by filter-stick forming device, made an addition to common（Circumference
24.3mm）In cigarette filter rod, quick-fried pearl position is that apart from lip end 12.5mm, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick,
And be the small blue or green quick-fried pearl cigarette of mandarin orange taste after cigarette cigarette sample.
To the prepared small blue or green quick-fried pearl cigarette of mandarin orange taste, by 7 professional sensory evaluation personnel to the sample and reference examples blank
Cigarette sample（Same position adds the quick-fried pearl of blank）Suction is detected and is contrasted to evaluate.
Flue gas inspection and specific suction evaluate score value referring to successive table.
Suction evaluation result shows that 7 cigarette personnel that smoke panel test unanimously think, after it with the addition of the small blue or green quick-fried pearl of mandarin orange taste cigarette,
" small blue or green mandarin orange is fragrant " of cigarette sample is fairly obvious, and flue gas fragrance harmony reduction, excitant increase, miscellaneous gas is reduced, and flue gas is coordinated
Property difference and have a uncomfortable sweet sense, pleasant impression is not so good as normal cigarette（Control sample cigarette）.
Quick-fried pearl product prepared by not be the same as Example is detected, while being carried out to prepared cigarette in above-described embodiment
Conventional detection, with to the physical and chemical index of diacetate fiber sample, the physical index of filter stick sample, the reason of cigarette sample in cigarette sample
Change index to be measured, further according to《The conventional analysis of the cigarette of GB/T 19609-2004 with smoking machine determine TPM and
Tar》Method determine the index such as TPM, tar, nicotine and moisture in cigarette mainstream flue gas and detected, specific knot
It is really as shown in the table.
Table 1, not in be the same as Example prepared quick-fried pearl testing result：
。
The testing result of table 2, the not prepared filter stick containing quick-fried pearl of be the same as Example：
。
Table 3, the physical index and main flume testing result of kinds of cigarettes sample：
。
It is can be seen that from the above-mentioned data of table 2 compared with normal diacetate fiber filter stick, place the filter stick physics of the small blue or green quick-fried pearl of mandarin orange
Index there occurs significant changes without significant difference, mainly filter stick pressure drop.As can be seen from Table 3, with reference examples normal volume
Cigarette is compared, and the main flume of the small blue or green quick-fried pearl cigarette of mandarin orange taste is varied from, but after quick-fried pearl pinches brokenly, the key of influence cigarette sense organ refers to
Mark tar and nicotine do not have significant changes.
Table 4, kinds of cigarettes sample sensory quality assessment result：
。
As can be seen from Table 4, cigarette sensory quality can be made to significantly improve by using the small blue or green quick-fried pearl of mandarin orange, it is felt
Official's scoring highest can improve 1.15 points, and fragrance is significantly improved, and pleasant impression improves, and excitant and miscellaneous gas also have larger reduction.
To sum up, it is formulated by targetedly designing the quick-fried pearl of specific fragrance, is applied to after cigarette, can be obviously improved
Impression is sucked in odor characteristic during smoking property of cigarette, abundant and raising, simultaneously because the special efficacy that small blue or green mandarin orange possesses can also be reduced
Cigarette endangers.Therefore the application highlights cigarette " small blue or green mandarin orange " note, improvement sucking quality as one kind, reduces the new of cigarette harm
The small blue or green quick-fried pearl of mandarin orange of type, in industry with definitely application value.
It is emphasized that above-mentioned quick-fried pearl formula is directed to conventional formulation cigarette improvement design, when applied to ramuscule cigarette,
Equally there is preferable application effect, but need to be added according to specific tobacco blend and design requirement to quick-fried pearl specification and in filter stick
Amount is suitably adjusted, and will not be described in detail herein.
Claims (6)
1. a kind of quick-fried pearl of cigarette is with the small blue or green savory essence of mandarin orange, it is characterised in that be calculated in mass percent, composed of the following components：
10.0 ~ 15.0% small blue or green mandarin orange extract,
1.0 ~ 2.0% diacetyl,
0.3 ~ 0.6% Ethyl vanillin,
0.5 ~ 1.0% methyl cinnamate,
0.2 ~ 0.5% geraniol,
1.0 ~ 2.0% orange oil,
78.9 ~ 87.0% Glycerin, mixed triester with caprylic acid capric acid；
The small blue or green mandarin orange extract is the ethanol extract of small blue or green mandarin orange.
2. the quick-fried pearl of cigarette as claimed in claim 1 is with the small blue or green savory essence of mandarin orange, it is characterised in that 12% small blue or green mandarin orange extract, 1.5%
Diacetyl, 0.4% Ethyl vanillin, 0.7% methyl cinnamate, 0.35% geraniol, 1.5% orange oil and 83.55%
Glycerin, mixed triester with caprylic acid capric acid.
3. the quick-fried pearl of cigarette described in claim 1 is utilized with the small blue or green quick-fried pearl of mandarin orange taste cigarette prepared by the small blue or green savory essence of mandarin orange, its feature
It is, a diameter of 2.0 ~ 4.0mm of quick-fried pearl, essence content is 20 ~ 25 μ L/ in quick-fried pearl.
4. the small blue or green quick-fried pearl of mandarin orange taste cigarette as claimed in claim 3, it is characterised in that the quick-fried a diameter of 3.65mm of pearl, weight are 23mg/
Essence content is 23 μ L/ in grain, quick-fried pearl.
5. application of the small blue or green quick-fried pearl of mandarin orange taste cigarette in cigarette described in claim 3, it is characterised in that make an addition to the quick-fried pearl of cigarette
In filter stick.
6. application of the small blue or green quick-fried pearl of mandarin orange taste cigarette in cigarette as claimed in claim 5, it is characterised in that the quick-fried pearl of cigarette is located at filter
In the middle part of rod, a quick-fried pearl is added in every cigarette filter rod.
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| CN109393571A (en) * | 2018-11-14 | 2019-03-01 | 湖北中烟工业有限责任公司 | Orange sweet wine taste essence and preparation method thereof for electric heating low temperature cigarette filter stick |
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| CN109868184A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of Radix Glycyrrhizae cigarette quick-fried pearl essence and its application in cigarette |
| CN109965045A (en) * | 2019-03-20 | 2019-07-05 | 福建绿色黄金生物科技有限公司 | One grows tea and green mandarin orange composition, preparation method and applications |
| CN110574962A (en) * | 2018-06-08 | 2019-12-17 | 湖南中烟工业有限责任公司 | Preparation method of tea-flavored essence for cigarettes, and beads and bead-popping cigarettes for cigarettes |
| CN110819457A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Sweet tea flavor and preparation method and application thereof |
| CN110819456A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Green lemon essence for bead blasting and application of green lemon essence in cigarettes |
| CN111254015A (en) * | 2020-03-20 | 2020-06-09 | 云南中烟工业有限责任公司 | Pu' er tea essence bead for cigarettes and preparation method thereof |
| CN111961531A (en) * | 2020-09-10 | 2020-11-20 | 将军烟草集团有限公司济南包装材料分公司 | Bead blasting essence for citrus reticulata blanco cigarette and preparation method and application thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102834027A (en) * | 2010-03-26 | 2012-12-19 | 菲利普莫里斯生产公司 | Methods of manufacturing cigarettes and filter subassemblies with squeezable flavor capsule |
| CN103584276A (en) * | 2013-11-13 | 2014-02-19 | 川渝中烟工业有限责任公司 | Ambergris cigarette and ambergris spices |
| CN104394718A (en) * | 2012-07-02 | 2015-03-04 | 西姆莱斯股份公司 | A method of flavouring a smoking product |
| CN104804871A (en) * | 2015-04-27 | 2015-07-29 | 湖北中烟工业有限责任公司 | Spicy spice for kretek blasting bead, preparation method and application thereof |
| GB2534210A (en) * | 2015-01-19 | 2016-07-20 | Ngip Res Ltd | Aerosol-generating article |
| CN105925376A (en) * | 2016-07-06 | 2016-09-07 | 红塔辽宁烟草有限责任公司 | Essence for cigarette blasting bead and application thereof |
-
2017
- 2017-04-27 CN CN201710288573.2A patent/CN106987314B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102834027A (en) * | 2010-03-26 | 2012-12-19 | 菲利普莫里斯生产公司 | Methods of manufacturing cigarettes and filter subassemblies with squeezable flavor capsule |
| CN104394718A (en) * | 2012-07-02 | 2015-03-04 | 西姆莱斯股份公司 | A method of flavouring a smoking product |
| CN103584276A (en) * | 2013-11-13 | 2014-02-19 | 川渝中烟工业有限责任公司 | Ambergris cigarette and ambergris spices |
| GB2534210A (en) * | 2015-01-19 | 2016-07-20 | Ngip Res Ltd | Aerosol-generating article |
| CN104804871A (en) * | 2015-04-27 | 2015-07-29 | 湖北中烟工业有限责任公司 | Spicy spice for kretek blasting bead, preparation method and application thereof |
| CN105925376A (en) * | 2016-07-06 | 2016-09-07 | 红塔辽宁烟草有限责任公司 | Essence for cigarette blasting bead and application thereof |
Cited By (12)
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| CN110574962A (en) * | 2018-06-08 | 2019-12-17 | 湖南中烟工业有限责任公司 | Preparation method of tea-flavored essence for cigarettes, and beads and bead-popping cigarettes for cigarettes |
| CN109043755A (en) * | 2018-08-29 | 2018-12-21 | 台山市精工源木制品有限公司 | A kind of preparation method and applications of the portable small green mandarin orange of arousing brain, raising spirit |
| CN109393571A (en) * | 2018-11-14 | 2019-03-01 | 湖北中烟工业有限责任公司 | Orange sweet wine taste essence and preparation method thereof for electric heating low temperature cigarette filter stick |
| CN109602081A (en) * | 2019-01-11 | 2019-04-12 | 广西中烟工业有限责任公司 | A kind of shatian pomelo cigarette quick-fried pearl essence and its application in cigarette |
| CN109868185A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of faenum graecum cigarette quick-fried pearl essence and its application in cigarette |
| CN109868184A (en) * | 2019-01-31 | 2019-06-11 | 广西中烟工业有限责任公司 | A kind of Radix Glycyrrhizae cigarette quick-fried pearl essence and its application in cigarette |
| CN109965045A (en) * | 2019-03-20 | 2019-07-05 | 福建绿色黄金生物科技有限公司 | One grows tea and green mandarin orange composition, preparation method and applications |
| CN110819457A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Sweet tea flavor and preparation method and application thereof |
| CN110819456A (en) * | 2019-12-09 | 2020-02-21 | 将军烟草集团有限公司 | Green lemon essence for bead blasting and application of green lemon essence in cigarettes |
| CN111254015A (en) * | 2020-03-20 | 2020-06-09 | 云南中烟工业有限责任公司 | Pu' er tea essence bead for cigarettes and preparation method thereof |
| CN111961531A (en) * | 2020-09-10 | 2020-11-20 | 将军烟草集团有限公司济南包装材料分公司 | Bead blasting essence for citrus reticulata blanco cigarette and preparation method and application thereof |
| CN111961531B (en) * | 2020-09-10 | 2023-09-29 | 将军烟草集团有限公司济南包装材料分公司 | Bead-explosion essence for citrus parviflora and preparation method and application thereof |
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