CN103211304A - Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate - Google Patents
Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate Download PDFInfo
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- CN103211304A CN103211304A CN2013101751643A CN201310175164A CN103211304A CN 103211304 A CN103211304 A CN 103211304A CN 2013101751643 A CN2013101751643 A CN 2013101751643A CN 201310175164 A CN201310175164 A CN 201310175164A CN 103211304 A CN103211304 A CN 103211304A
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- Prior art keywords
- cigarette
- filter stick
- harm reduction
- capsule
- synergist
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 79
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 title claims abstract description 64
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000012747 synergistic agent Substances 0.000 title abstract 4
- 235000013773 glyceryl triacetate Nutrition 0.000 title abstract 3
- 229960002622 triacetin Drugs 0.000 title abstract 3
- 239000002775 capsule Substances 0.000 claims abstract description 35
- 239000002904 solvent Substances 0.000 claims abstract description 19
- 238000005516 engineering process Methods 0.000 claims abstract description 14
- 241000208125 Nicotiana Species 0.000 claims abstract description 10
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 10
- 239000004519 grease Substances 0.000 claims abstract description 3
- 230000009467 reduction Effects 0.000 claims description 45
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 6
- 235000019082 Osmanthus Nutrition 0.000 claims description 4
- 241000333181 Osmanthus Species 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- 239000003205 fragrance Substances 0.000 claims description 4
- TYSYCALJZQGVLT-UHFFFAOYSA-N 3-acetyl-3,4-dihydroxy-4-(hydroxymethyl)hexane-2,5-dione Chemical class CC(=O)C(O)(CO)C(O)(C(C)=O)C(C)=O TYSYCALJZQGVLT-UHFFFAOYSA-N 0.000 claims description 2
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 125000001931 aliphatic group Chemical group 0.000 claims description 2
- 235000013305 food Nutrition 0.000 claims description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract description 12
- 239000000779 smoke Substances 0.000 abstract description 10
- 238000000034 method Methods 0.000 abstract description 9
- 238000007792 addition Methods 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 239000011162 core material Substances 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 abstract 1
- 235000019634 flavors Nutrition 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 230000000391 smoking effect Effects 0.000 description 15
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 12
- 239000003546 flue gas Substances 0.000 description 12
- 230000000694 effects Effects 0.000 description 7
- 230000008569 process Effects 0.000 description 7
- 241000723353 Chrysanthemum Species 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000000654 additive Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000002304 perfume Substances 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 230000009471 action Effects 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 239000004014 plasticizer Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000013538 functional additive Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
The invention discloses a preparation method of a filter stick using a cigarette harm-reducing synergistic agent containing glycerol triacetate. The preparation method comprises the following steps: (1) blending 60-90% mass percent of fat-soluble solvent, 5-35% mass percent of glycerol triacetate and 0.01-5% mass percent of tobacco flavor, stirring and mixing evenly to obtain the cigarette harm-reducing synergistic agent, wherein the fat-soluble solvent is food-grade fatty acid, alcohol or a grease solvent; and (2) coating the cigarette harm-reducing synergistic agent in capsules as core materials to be added into cigarette filter stick by adopting capsule addition technology of the cigarette filter stick. The method is wide in raw material source, low in cost, capable of obviously reducing the content of phenol in cigarette smoke and also endowing smoke with special aroma and taste.
Description
Technical field
The present invention relates to technical field of cigarettes, be meant a kind of filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine particularly.
Background technology
Filter stick, especially novel special filter stick plays an important role in reducing cigarette tar and reducing harm reduction, flavouring humectation technology.Through unremitting research for many years, novel special filter stick has developed into a kind of important techniques measure of reducing cigarette tar and reducing harm reduction.Along with national governments are more and more stricter to the restriction of cigarette, and the consumer strengthens day by day to the concern of smoking with health, only be difficult to satisfy the growth requirement in cigarette market with a kind of special filter stick of single functional additive, special filter stick is developed to the multi-functional direction of multiple additives by a kind of additive list kind function.According to market and cigarette designing requirement, there is purpose selectively various technology organically to be combined, develop multi-functional special filter stick with desirable lowering harm and decreasing coking or flavouring humectation effect, especially both had the perfuming effect, have the special filter stick that reduces multiple harmful smoke composition again, have fairly obvious economic benefit and great social significance.
Add capsule in cigarette filter rod, wherein wrapping up essence, to increase the cigarette smoking quality be an emerging technology research field.But at present, what the technical staff mainly paid close attention to is the physical property that how to improve capsule, strengthen the processability of capsule and the adaptability of using in cigarette product, capsule is added mostly is traditional essence, more lacks the technical research that parcel is had harm reduction effect material.
Triacetyl glycerine is the primary raw material in the acetate silk filter stick formation technology, is used for the plasticizer of filter stick tow.Triacetyl glycerine adds in filter stick too much, can cause filter stick hardness to increase, and fusion hole appears in the filter stick tow; Triacetyl glycerine adds very few in filter stick, can cause filtering rod to descend, and filter stick reduces smoke filtration efficient.Domestic scholars has been studied different triacetyl glycerine additions to harmful components burst size in the cigarette smoke especially influence of aldehydes matter, has also studied the influence to the cigarette organoleptic quality simultaneously.The result shows that along with the increase of triacetyl glycerine consumption, filter stick Pyrogentisinic Acid's filter efficiency increases gradually, and is little to the influence of cigarette organoleptic quality.But, can cause adverse effect in the filter stick formation process to the physical property and the outward appearance of filter stick because of triacetyl glycerine adds too much.Therefore, it is still inapplicable in cigarette product to the filter efficiency of flue gas to want to strengthen filter stick by the consumption that improves triacetyl glycerine.
Summary of the invention
At the above-mentioned deficiency of prior art, utilize the chemical characteristic of triacetyl glycerine, can produce hydrogen bond action with phenol, the Pyrogentisinic Acid has certain dissolubility simultaneously.Purpose of the present invention is exactly that a kind of filter stick preparation method that can reduce phenol content in the cigarette smoke and give the cigarette harm reduction synergist that contains triacetyl glycerine of flue gas special aroma will be provided, the harm reduction synergist is used the core of capsule as cigarette, capsule joins in the cigarette filter rod, when cigarette smoking, pinch brokenly capsule, discharge triacetyl glycerine and essence, reach and reduce the flue gas phenol content, improve the purpose of cigarette smoking quality.
For achieving the above object, the filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine provided by the invention, it comprises following steps:
(1) be that the flavouring essence for tobacco of 60～90% fat-soluble solvent, 5～35% triacetyl glycerines and 0.01～5% is allocated with mass percent, be uniformly mixed to form cigarette harm reduction synergist, described fat-soluble solvent is aliphatic acid, alcohols or the grease kind solvent of food grade;
(2) with the cigarette harm reduction synergist that makes as core, cigarette harm reduction synergist is wrapped in the capsule, adopt the adding technology of capsule at cigarette filter rod, join in the cigarette filter rod.
As preferred version, the flavouring essence for tobacco in the described step (1) is chrysanthemum essence or osmanthus flower fragrance.
Further, the total addition level of described step (2) cigarette harm reduction synergist in cigarette filter rod is 0.01 ~ 0.5mg.
The present invention obtains the harm reduction synergist as the core of cigarette with capsule with configuration, is wrapped in capsule.The consumer pinches brokenly capsule in the filter stick before cigarette smoking, discharges the harm reduction synergist that wraps up in the capsule, aspirates then, and when flue gas passed through, the harm reduction synergist played the effect that effective reduction phenol improves the cigarette smoking quality.
The invention has the advantages that:
One, triacetyl glycerine can be dissolved in the fat-soluble double solvents well, need not to add new technical process, does not influence the preparation technology and the capsule quality of capsule fully.
They are two years old, capsulated triacetyl glycerine is in cigarette preparation, storing process among the present invention, all be wrapped in cigarette with in the capsule, can not increase outward appearances such as filter stick hardness or generation tow fusion hole and change, can ensure the presentation quality of cigarette product well with stable state.
They are three years old, cigarette discharges triacetyl glycerine when suction, can produce hydrogen bond action with the phenol in the flue gas, simultaneously can also bring into play the polarity effect of mixing, dissolving part phenol, greatly reduce the burst size of phenol in the flue gas, brought into play triacetyl glycerine fully except that as the harm reduction effect that is possessed the filter stick plasticizer.
Its four, cigarette belongs to additive essential in the filter stick formation technology with the triacetyl glycerine that wraps up in the capsule, self colorless and odorless can not have a negative impact to cigarette odor-absorbing, has avoided existing harm reduction material to add the defective that influences the cigarette style and features in cigarette.
Its five, cigarette can promote flue gas matter and exhaust gas volumn with the essence in the capsule, enriches the style and features of cigarette, improves the cigarette smoking quality.
The specific embodiment
The present invention is described in further detail below in conjunction with specific embodiment.
Embodiment one: the proportioning of harm reduction synergist of the present invention is as follows:
| Composition | Percentage |
| Fat-soluble solvent | 85 |
| Triacetyl glycerine | 14.5 |
| Tobacco extract | 0.5 |
Preparation method of the present invention is as follows: it is to be that the tobacco extract of 85% fat-soluble solvent, 14.5% triacetyl glycerine and 0.5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, this perfume (or spice) of tobacco of cigarette is stronger, and strength is more sufficient, and phenol content also has obvious reduction in the flue gas.
Smoke components test result of the present invention is as follows:
Embodiment two: the proportioning of harm reduction synergist of the present invention is as follows:
| Composition | Percentage |
| Fat-soluble solvent | 78 |
| Triacetyl glycerine | 20.5 |
| Osmanthus flower fragrance | 1.5 |
Preparation method of the present invention is as follows: it is to be that the osmanthus flower fragrance of 78% fat-soluble solvent, 20.5% triacetyl glycerine and 1.5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, that flue gas attenuates is greasy soft, stronger fragrant and sweet sense is arranged, and the suction quality of cigarette has obtained lifting, and phenol content also has obvious reduction in the flue gas.
Smoke components test result of the present invention is as follows:
Embodiment three: the proportioning of harm reduction synergist of the present invention is as follows:
| Composition | Percentage |
| Fat-soluble solvent | 60 |
| Triacetyl glycerine | 35 |
| Chrysanthemum essence | 5 |
Preparation method of the present invention is as follows: it is to be that the chrysanthemum essence of 60% fat-soluble solvent, 35% triacetyl glycerine and 5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Because of fat-soluble solvent percentage is lower, the overall viscosity of harm reduction synergist is less, and surface tension of liquid is less, makes difficulty of capsule shaping.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, the essence breath is overweight, has suppressed this perfume (or spice) of tobacco, but phenol content reduces obviously in the flue gas.
Smoke components test result of the present invention is as follows:
Embodiment four: the proportioning of harm reduction synergist of the present invention is as follows:
| Composition | Percentage |
| Fat-soluble solvent | 90 |
| Triacetyl glycerine | 5 |
| Chrysanthemum essence | 5 |
Preparation method of the present invention is as follows: it is to be that the chrysanthemum essence of 90% fat-soluble solvent, 5% triacetyl glycerine and 5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, this perfume (or spice) of tobacco of cigarette is stronger, and strength is more sufficient, and phenol content also has obvious reduction in the flue gas.
Smoke components test result of the present invention is as follows:
Claims (3)
1. filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine, it comprises following steps:
(1) be that the flavouring essence for tobacco of 60～90% fat-soluble solvent, 5～35% triacetyl glycerines and 0.01～5% is allocated with mass percent, be uniformly mixed to form cigarette harm reduction synergist, described fat-soluble solvent is aliphatic acid, alcohols or the grease kind solvent of food grade;
(2) with the cigarette harm reduction synergist that makes as core, cigarette harm reduction synergist is wrapped in the capsule, adopt the adding technology of capsule at cigarette filter rod, join in the cigarette filter rod.
2. the filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine according to claim 1, it is characterized in that: the flavouring essence for tobacco in the described step (1) is chrysanthemum essence or osmanthus flower fragrance.
3. the filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine according to claim 1 and 2 is characterized in that: the total addition level of described step (2) cigarette harm reduction synergist in cigarette filter rod is 0.01 ~ 0.5mg.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013101751643A CN103211304A (en) | 2013-05-13 | 2013-05-13 | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013101751643A CN103211304A (en) | 2013-05-13 | 2013-05-13 | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103211304A true CN103211304A (en) | 2013-07-24 |
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|---|---|---|---|
| CN2013101751643A Pending CN103211304A (en) | 2013-05-13 | 2013-05-13 | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103361173A (en) * | 2013-07-26 | 2013-10-23 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
| CN103504475A (en) * | 2013-10-11 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moisture-increasing modifying agent for cigarette filter rods and application thereof |
| CN104498192A (en) * | 2014-12-15 | 2015-04-08 | 云南中烟工业有限责任公司 | Preparation method and application of florists chrysanthemum extract |
| CN106136312A (en) * | 2016-06-28 | 2016-11-23 | 云南瑞升烟草技术（集团）有限公司 | A kind of capsule filter stick reducing harmful substances from flue gases burst size |
| CN106263015A (en) * | 2016-08-30 | 2017-01-04 | 云南中烟工业有限责任公司 | A kind of reduce cigarette smoke phenol the method highlighting its delicate fragrance type main body note |
| CN106418669A (en) * | 2016-11-11 | 2017-02-22 | 湖北中烟工业有限责任公司 | High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice |
| CN109998165A (en) * | 2019-04-03 | 2019-07-12 | 红云红河烟草(集团)有限责任公司 | A kind of cigarette filter rod plasticizer and preparation method thereof and cigarette filter rod |
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| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN102783713A (en) * | 2012-08-16 | 2012-11-21 | 贵州中烟工业有限责任公司 | Bouquet-type capsule filter tip and preparation technology thereof |
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2013
- 2013-05-13 CN CN2013101751643A patent/CN103211304A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0920816A2 (en) * | 1993-09-30 | 1999-06-09 | British American Tobacco (Investments) Limited | Improvements relating to tobacco smoke filter elements |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103361173A (en) * | 2013-07-26 | 2013-10-23 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
| CN103361173B (en) * | 2013-07-26 | 2014-11-26 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
| CN103504475A (en) * | 2013-10-11 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moisture-increasing modifying agent for cigarette filter rods and application thereof |
| CN103504475B (en) * | 2013-10-11 | 2015-06-17 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moisture-increasing modifying agent for cigarette filter rods and application thereof |
| CN104498192A (en) * | 2014-12-15 | 2015-04-08 | 云南中烟工业有限责任公司 | Preparation method and application of florists chrysanthemum extract |
| CN106136312A (en) * | 2016-06-28 | 2016-11-23 | 云南瑞升烟草技术（集团）有限公司 | A kind of capsule filter stick reducing harmful substances from flue gases burst size |
| CN106263015A (en) * | 2016-08-30 | 2017-01-04 | 云南中烟工业有限责任公司 | A kind of reduce cigarette smoke phenol the method highlighting its delicate fragrance type main body note |
| CN106418669A (en) * | 2016-11-11 | 2017-02-22 | 湖北中烟工业有限责任公司 | High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice |
| CN106418669B (en) * | 2016-11-11 | 2018-06-01 | 湖北中烟工业有限责任公司 | A kind of high time sweet tea sense tobacco aromaticss and its preparation method and application |
| CN109998165A (en) * | 2019-04-03 | 2019-07-12 | 红云红河烟草(集团)有限责任公司 | A kind of cigarette filter rod plasticizer and preparation method thereof and cigarette filter rod |
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Application publication date: 20130724 |