CN103211304A - Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate - Google Patents

Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate Download PDF

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Publication number
CN103211304A
CN103211304A CN2013101751643A CN201310175164A CN103211304A CN 103211304 A CN103211304 A CN 103211304A CN 2013101751643 A CN2013101751643 A CN 2013101751643A CN 201310175164 A CN201310175164 A CN 201310175164A CN 103211304 A CN103211304 A CN 103211304A
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CN
China
Prior art keywords
cigarette
filter stick
harm reduction
capsule
synergist
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101751643A
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Chinese (zh)
Inventor
宋旭艳
陈义坤
李冉
刘冰
罗诚浩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
China Tobacco Hubei Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hunan Industrial Co Ltd, Wuhan Huanghelou Science and Technology Park Co Ltd filed Critical China Tobacco Hunan Industrial Co Ltd
Priority to CN2013101751643A priority Critical patent/CN103211304A/en
Publication of CN103211304A publication Critical patent/CN103211304A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a preparation method of a filter stick using a cigarette harm-reducing synergistic agent containing glycerol triacetate. The preparation method comprises the following steps: (1) blending 60-90% mass percent of fat-soluble solvent, 5-35% mass percent of glycerol triacetate and 0.01-5% mass percent of tobacco flavor, stirring and mixing evenly to obtain the cigarette harm-reducing synergistic agent, wherein the fat-soluble solvent is food-grade fatty acid, alcohol or a grease solvent; and (2) coating the cigarette harm-reducing synergistic agent in capsules as core materials to be added into cigarette filter stick by adopting capsule addition technology of the cigarette filter stick. The method is wide in raw material source, low in cost, capable of obviously reducing the content of phenol in cigarette smoke and also endowing smoke with special aroma and taste.

Description

The filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine
Technical field
The present invention relates to technical field of cigarettes, be meant a kind of filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine particularly.
Background technology
Filter stick, especially novel special filter stick plays an important role in reducing cigarette tar and reducing harm reduction, flavouring humectation technology.Through unremitting research for many years, novel special filter stick has developed into a kind of important techniques measure of reducing cigarette tar and reducing harm reduction.Along with national governments are more and more stricter to the restriction of cigarette, and the consumer strengthens day by day to the concern of smoking with health, only be difficult to satisfy the growth requirement in cigarette market with a kind of special filter stick of single functional additive, special filter stick is developed to the multi-functional direction of multiple additives by a kind of additive list kind function.According to market and cigarette designing requirement, there is purpose selectively various technology organically to be combined, develop multi-functional special filter stick with desirable lowering harm and decreasing coking or flavouring humectation effect, especially both had the perfuming effect, have the special filter stick that reduces multiple harmful smoke composition again, have fairly obvious economic benefit and great social significance.
Add capsule in cigarette filter rod, wherein wrapping up essence, to increase the cigarette smoking quality be an emerging technology research field.But at present, what the technical staff mainly paid close attention to is the physical property that how to improve capsule, strengthen the processability of capsule and the adaptability of using in cigarette product, capsule is added mostly is traditional essence, more lacks the technical research that parcel is had harm reduction effect material.
Triacetyl glycerine is the primary raw material in the acetate silk filter stick formation technology, is used for the plasticizer of filter stick tow.Triacetyl glycerine adds in filter stick too much, can cause filter stick hardness to increase, and fusion hole appears in the filter stick tow; Triacetyl glycerine adds very few in filter stick, can cause filtering rod to descend, and filter stick reduces smoke filtration efficient.Domestic scholars has been studied different triacetyl glycerine additions to harmful components burst size in the cigarette smoke especially influence of aldehydes matter, has also studied the influence to the cigarette organoleptic quality simultaneously.The result shows that along with the increase of triacetyl glycerine consumption, filter stick Pyrogentisinic Acid's filter efficiency increases gradually, and is little to the influence of cigarette organoleptic quality.But, can cause adverse effect in the filter stick formation process to the physical property and the outward appearance of filter stick because of triacetyl glycerine adds too much.Therefore, it is still inapplicable in cigarette product to the filter efficiency of flue gas to want to strengthen filter stick by the consumption that improves triacetyl glycerine.
Summary of the invention
At the above-mentioned deficiency of prior art, utilize the chemical characteristic of triacetyl glycerine, can produce hydrogen bond action with phenol, the Pyrogentisinic Acid has certain dissolubility simultaneously.Purpose of the present invention is exactly that a kind of filter stick preparation method that can reduce phenol content in the cigarette smoke and give the cigarette harm reduction synergist that contains triacetyl glycerine of flue gas special aroma will be provided, the harm reduction synergist is used the core of capsule as cigarette, capsule joins in the cigarette filter rod, when cigarette smoking, pinch brokenly capsule, discharge triacetyl glycerine and essence, reach and reduce the flue gas phenol content, improve the purpose of cigarette smoking quality.
For achieving the above object, the filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine provided by the invention, it comprises following steps:
(1) be that the flavouring essence for tobacco of 60~90% fat-soluble solvent, 5~35% triacetyl glycerines and 0.01~5% is allocated with mass percent, be uniformly mixed to form cigarette harm reduction synergist, described fat-soluble solvent is aliphatic acid, alcohols or the grease kind solvent of food grade;
(2) with the cigarette harm reduction synergist that makes as core, cigarette harm reduction synergist is wrapped in the capsule, adopt the adding technology of capsule at cigarette filter rod, join in the cigarette filter rod.
As preferred version, the flavouring essence for tobacco in the described step (1) is chrysanthemum essence or osmanthus flower fragrance.
Further, the total addition level of described step (2) cigarette harm reduction synergist in cigarette filter rod is 0.01 ~ 0.5mg.
The present invention obtains the harm reduction synergist as the core of cigarette with capsule with configuration, is wrapped in capsule.The consumer pinches brokenly capsule in the filter stick before cigarette smoking, discharges the harm reduction synergist that wraps up in the capsule, aspirates then, and when flue gas passed through, the harm reduction synergist played the effect that effective reduction phenol improves the cigarette smoking quality.
The invention has the advantages that:
One, triacetyl glycerine can be dissolved in the fat-soluble double solvents well, need not to add new technical process, does not influence the preparation technology and the capsule quality of capsule fully.
They are two years old, capsulated triacetyl glycerine is in cigarette preparation, storing process among the present invention, all be wrapped in cigarette with in the capsule, can not increase outward appearances such as filter stick hardness or generation tow fusion hole and change, can ensure the presentation quality of cigarette product well with stable state.
They are three years old, cigarette discharges triacetyl glycerine when suction, can produce hydrogen bond action with the phenol in the flue gas, simultaneously can also bring into play the polarity effect of mixing, dissolving part phenol, greatly reduce the burst size of phenol in the flue gas, brought into play triacetyl glycerine fully except that as the harm reduction effect that is possessed the filter stick plasticizer.
Its four, cigarette belongs to additive essential in the filter stick formation technology with the triacetyl glycerine that wraps up in the capsule, self colorless and odorless can not have a negative impact to cigarette odor-absorbing, has avoided existing harm reduction material to add the defective that influences the cigarette style and features in cigarette.
Its five, cigarette can promote flue gas matter and exhaust gas volumn with the essence in the capsule, enriches the style and features of cigarette, improves the cigarette smoking quality.
The specific embodiment
The present invention is described in further detail below in conjunction with specific embodiment.
Embodiment one: the proportioning of harm reduction synergist of the present invention is as follows:
Composition Percentage
Fat-soluble solvent 85
Triacetyl glycerine 14.5
Tobacco extract 0.5
Preparation method of the present invention is as follows: it is to be that the tobacco extract of 85% fat-soluble solvent, 14.5% triacetyl glycerine and 0.5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, this perfume (or spice) of tobacco of cigarette is stronger, and strength is more sufficient, and phenol content also has obvious reduction in the flue gas.
Smoke components test result of the present invention is as follows:
Embodiment two: the proportioning of harm reduction synergist of the present invention is as follows:
Composition Percentage
Fat-soluble solvent 78
Triacetyl glycerine 20.5
Osmanthus flower fragrance 1.5
Preparation method of the present invention is as follows: it is to be that the osmanthus flower fragrance of 78% fat-soluble solvent, 20.5% triacetyl glycerine and 1.5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, that flue gas attenuates is greasy soft, stronger fragrant and sweet sense is arranged, and the suction quality of cigarette has obtained lifting, and phenol content also has obvious reduction in the flue gas.
Smoke components test result of the present invention is as follows:
Embodiment three: the proportioning of harm reduction synergist of the present invention is as follows:
Composition Percentage
Fat-soluble solvent 60
Triacetyl glycerine 35
Chrysanthemum essence 5
Preparation method of the present invention is as follows: it is to be that the chrysanthemum essence of 60% fat-soluble solvent, 35% triacetyl glycerine and 5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Because of fat-soluble solvent percentage is lower, the overall viscosity of harm reduction synergist is less, and surface tension of liquid is less, makes difficulty of capsule shaping.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, the essence breath is overweight, has suppressed this perfume (or spice) of tobacco, but phenol content reduces obviously in the flue gas.
Smoke components test result of the present invention is as follows:
Embodiment four: the proportioning of harm reduction synergist of the present invention is as follows:
Composition Percentage
Fat-soluble solvent 90
Triacetyl glycerine 5
Chrysanthemum essence 5
Preparation method of the present invention is as follows: it is to be that the chrysanthemum essence of 90% fat-soluble solvent, 5% triacetyl glycerine and 5% is allocated with mass percent, is uniformly mixed to form the harm reduction synergist; Again the harm reduction synergist is wrapped in the capsule, adopts the adding technology of capsule, join in the cigarette at cigarette filter rod.Through before cigarette smoking, the capsule in the filter stick being crumbed, discharge harm reduction synergist wherein, in the cigarette smoking process, this perfume (or spice) of tobacco of cigarette is stronger, and strength is more sufficient, and phenol content also has obvious reduction in the flue gas.
Smoke components test result of the present invention is as follows:

Claims (3)

1. filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine, it comprises following steps:
(1) be that the flavouring essence for tobacco of 60~90% fat-soluble solvent, 5~35% triacetyl glycerines and 0.01~5% is allocated with mass percent, be uniformly mixed to form cigarette harm reduction synergist, described fat-soluble solvent is aliphatic acid, alcohols or the grease kind solvent of food grade;
(2) with the cigarette harm reduction synergist that makes as core, cigarette harm reduction synergist is wrapped in the capsule, adopt the adding technology of capsule at cigarette filter rod, join in the cigarette filter rod.
2. the filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine according to claim 1, it is characterized in that: the flavouring essence for tobacco in the described step (1) is chrysanthemum essence or osmanthus flower fragrance.
3. the filter stick preparation method who contains the cigarette harm reduction synergist of triacetyl glycerine according to claim 1 and 2 is characterized in that: the total addition level of described step (2) cigarette harm reduction synergist in cigarette filter rod is 0.01 ~ 0.5mg.
CN2013101751643A 2013-05-13 2013-05-13 Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate Pending CN103211304A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103361173A (en) * 2013-07-26 2013-10-23 上海华宝生物科技有限公司 Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof
CN103504475A (en) * 2013-10-11 2014-01-15 红云红河烟草(集团)有限责任公司 Hydrophobic moisture-increasing modifying agent for cigarette filter rods and application thereof
CN104498192A (en) * 2014-12-15 2015-04-08 云南中烟工业有限责任公司 Preparation method and application of florists chrysanthemum extract
CN106136312A (en) * 2016-06-28 2016-11-23 云南瑞升烟草技术(集团)有限公司 A kind of capsule filter stick reducing harmful substances from flue gases burst size
CN106263015A (en) * 2016-08-30 2017-01-04 云南中烟工业有限责任公司 A kind of reduce cigarette smoke phenol the method highlighting its delicate fragrance type main body note
CN106418669A (en) * 2016-11-11 2017-02-22 湖北中烟工业有限责任公司 High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice
CN109998165A (en) * 2019-04-03 2019-07-12 红云红河烟草(集团)有限责任公司 A kind of cigarette filter rod plasticizer and preparation method thereof and cigarette filter rod

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0920816A2 (en) * 1993-09-30 1999-06-09 British American Tobacco (Investments) Limited Improvements relating to tobacco smoke filter elements
CN101203148A (en) * 2005-06-21 2008-06-18 玛奈·菲尔萨公司 Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule
CN102783713A (en) * 2012-08-16 2012-11-21 贵州中烟工业有限责任公司 Bouquet-type capsule filter tip and preparation technology thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0920816A2 (en) * 1993-09-30 1999-06-09 British American Tobacco (Investments) Limited Improvements relating to tobacco smoke filter elements
CN101203148A (en) * 2005-06-21 2008-06-18 玛奈·菲尔萨公司 Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule
CN102783713A (en) * 2012-08-16 2012-11-21 贵州中烟工业有限责任公司 Bouquet-type capsule filter tip and preparation technology thereof

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103361173A (en) * 2013-07-26 2013-10-23 上海华宝生物科技有限公司 Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof
CN103361173B (en) * 2013-07-26 2014-11-26 上海华宝生物科技有限公司 Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof
CN103504475A (en) * 2013-10-11 2014-01-15 红云红河烟草(集团)有限责任公司 Hydrophobic moisture-increasing modifying agent for cigarette filter rods and application thereof
CN103504475B (en) * 2013-10-11 2015-06-17 红云红河烟草(集团)有限责任公司 Hydrophobic moisture-increasing modifying agent for cigarette filter rods and application thereof
CN104498192A (en) * 2014-12-15 2015-04-08 云南中烟工业有限责任公司 Preparation method and application of florists chrysanthemum extract
CN106136312A (en) * 2016-06-28 2016-11-23 云南瑞升烟草技术(集团)有限公司 A kind of capsule filter stick reducing harmful substances from flue gases burst size
CN106263015A (en) * 2016-08-30 2017-01-04 云南中烟工业有限责任公司 A kind of reduce cigarette smoke phenol the method highlighting its delicate fragrance type main body note
CN106418669A (en) * 2016-11-11 2017-02-22 湖北中烟工业有限责任公司 High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice
CN106418669B (en) * 2016-11-11 2018-06-01 湖北中烟工业有限责任公司 A kind of high time sweet tea sense tobacco aromaticss and its preparation method and application
CN109998165A (en) * 2019-04-03 2019-07-12 红云红河烟草(集团)有限责任公司 A kind of cigarette filter rod plasticizer and preparation method thereof and cigarette filter rod

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