CN104498192A - Preparation method and application of florists chrysanthemum extract - Google Patents
Preparation method and application of florists chrysanthemum extract Download PDFInfo
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- CN104498192A CN104498192A CN201410771801.8A CN201410771801A CN104498192A CN 104498192 A CN104498192 A CN 104498192A CN 201410771801 A CN201410771801 A CN 201410771801A CN 104498192 A CN104498192 A CN 104498192A
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- Prior art keywords
- tribute chrysanthemum
- extraction
- chrysanthemum extract
- tribute
- extract
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a preparation method and application of a florists chrysanthemum extract. The preparation method comprises the steps of drying fresh florists chrysanthemum taken as the raw material; crushing; performing supercritical CO2 extraction; filtering to obtain the florists chrysanthemum extract; dissolving the florists chrysanthemum extract with glycerol triacetate; spraying to tobacco shred based on the dosage of 0.05 to 0.9 per mill. The florists chrysanthemum extract prepared by the method is used for perfuming cigarette filter tips, and can be used for effectively improving the smoke flavor characteristic, in particular improving the flowery flavor and sweetness of cigarettes with faint scent, and the irritation of smoke can be reduced to certain extent.
Description
Technical field
The invention belongs to cigaret additive processing technique field, be specifically related to a kind of preparation method of tribute chrysanthemum extract.The invention still further relates to the application of described tribute chrysanthemum extract in cigarette filter rod perfuming simultaneously.
Background technology
It is reported, in chrysanthemum, plant chemical composition content enriches, mainly with acacetin-7-O-β-D-galactopyranoside, cosmosiin, luteolin etc. for the glucosides class of representative and with β-phellandrene, p-ymene, chrysanthenone, 1,8-eucalyptol, borneol, sabinene are the terpenoid such as monoterpene, sesquiterpene, triterpene of representative, these plant chemical ingredients are how identical with tobacco plant class aroma component.Wherein, tribute chrysanthemum is as one of China four your name chrysanthemum, and comparatively other common chrysanthemum are more abundant for formation and the conversion of its volatile compound, and content is also higher.Tribute chrysanthemum drying, solvent extraction, particularly apply supercritical CO
2the means such as extraction, a large amount of plant chemistry aroma components that tribute chrysanthemum can be produced in ripening process discharge, and therefore prepare tobacco aromatics using with tribute chrysanthemum for raw material and have good application value.Up to now, report is had no using tribute chrysanthemum extract as the research of cigarette filter rod perfuming spices.
Summary of the invention
The object of the invention is to for deficiency of the prior art, provide a kind of with tribute chrysanthemum for raw material, prepare the method for tribute chrysanthemum extract.
Meanwhile, the present invention also aims to provide the application of described tribute chrysanthemum extract in cigarette filter rod perfuming.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage ratio of the present invention is mass percent.
A preparation method for tribute chrysanthemum extract, is characterized in that: with fresh tribute chrysanthemum for raw material, drying, pulverizing, supercritical CO
2tribute chrysanthemum extract is obtained after extraction and filtration; Concrete steps are as follows:
(1) raw material prepares: cleaned by fresh tribute chrysanthemum, carry out after oven dry being ground into end, grinding particle size is less than or equal to 5mm, for subsequent use;
(2) supercritical CO
2extraction: by pulverize after tribute inulin end be placed in extraction kettle, add weight be the ethanol of described tribute chrysanthemum powder weight 0.2 ~ 1 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle is set to 30 ~ 60 DEG C, pressure is 20-40MPa, passes into CO
2extraction 0.5-5h, collects extraction liquid; Wherein, described CO
2flow control be 5-15kg/h;
(3) filter: carried out by the extraction liquid collected filtering and obtain described tribute chrysanthemum extract, described tribute chrysanthemum extract is khaki color liquid, is soluble in esters solvent.
The application of described tribute chrysanthemum extract in cigarette filter rod perfuming, is characterized in that: after being dissolved by tribute chrysanthemum extract glycerine triacetate, spray in tow with the consumption of 0.05 ~ 0.9 ‰.
Compared with prior art, the present invention has following beneficial effect:
1, the tribute chrysanthemum extract prepared of the present invention is for cigarette filter rod perfuming, effectively can promote smoke transportation, particularly increases the floral notes of scent type cigarette and sweet sense, reduces flue gas pungency to a certain extent.
2, tribute chrysanthemum extract solvability in esters solvent of preparing of the present invention is good, can be directly used in cigarette filter rod perfuming, and application is convenient.
3, the inventive method is simple, and technique, equipment are ripe, can realize industrialization.
Embodiment
Below in conjunction with embodiment, invention is described in detail; it should be noted that; embodiment is only used to further illustrate the present invention; but embodiment should not be construed as limiting the scope of the invention; the non-intrinsically safe that those skilled in the art's training centre according to the present invention is made improves and adjustment, all falls into protection scope of the present invention.
Embodiment 1
By fresh tribute chrysanthemum clean, dry after, take the tribute chrysanthemum 100 grams of oven dry, pulverize for granularity be less than or equal to 5mm tribute inulin end, be placed in extraction kettle; Add weight be the ethanol of described tribute chrysanthemum powder weight 0.2 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle is set to 30 DEG C, pressure is 40MPa, passes into the CO that flow is 15kg/h
2, extraction 2.5h, collects extraction liquid, filtration is prepared tribute chrysanthemum extract.
After being dissolved with glycerine triacetate by this extract, spray in cigarette filter rod according to the addition of tow quality 0.05 ‰, contrast with former finished cigarettes, ask expert to carry out sensory evaluating smoking, smoking result is in table 1.
Embodiment 2
By fresh tribute chrysanthemum clean, dry after, take the tribute chrysanthemum 100 grams of oven dry, pulverize for granularity be less than or equal to 5mm tribute inulin end, be placed in extraction kettle; Add weight be the ethanol of described tribute chrysanthemum powder weight 1 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle is set to 40 DEG C, pressure is 20MPa, passes into the CO that flow is 5kg/h
2, extraction 5h, collects extraction liquid, filtration is prepared tribute chrysanthemum extract.
After being dissolved with glycerine triacetate by this extract, spray in cigarette filter rod according to the addition of tow quality 0.1 ‰, contrast with former finished cigarettes, ask expert to carry out sensory evaluating smoking, smoking result is in table 1.
Embodiment 3
By fresh tribute chrysanthemum clean, dry after, take the tribute chrysanthemum 100 grams of oven dry, pulverize for granularity be less than or equal to 5mm tribute inulin end, be placed in extraction kettle; Add weight be the ethanol of described tribute chrysanthemum powder weight 0.3 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle is set to 60 DEG C, pressure is 20MPa, passes into the CO that flow is 8kg/h
2, extraction 0.5h, collects extraction liquid, filtration is prepared tribute chrysanthemum extract.
After being dissolved with glycerine triacetate by this extract, spray in cigarette filter rod according to the addition of tow quality 0.3 ‰, contrast with former finished cigarettes, ask expert to carry out sensory evaluating smoking, smoking result is in table 1.
Embodiment 4
By fresh tribute chrysanthemum clean, dry after, take the tribute chrysanthemum 100 grams of oven dry, pulverize for granularity be less than or equal to 5mm tribute inulin end, be placed in extraction kettle; Add weight be the ethanol of described tribute chrysanthemum powder weight 0.8 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle is set to 35 DEG C, pressure is 25MPa, passes into the CO that flow is 6kg/h
2, extraction 1h, collects extraction liquid, filtration is prepared tribute chrysanthemum extract.
After being dissolved with glycerine triacetate by this extract, spray in cigarette filter rod according to the addition of tow quality 0.5 ‰, contrast with former finished cigarettes, ask expert to carry out sensory evaluating smoking, smoking result is in table 1.
Embodiment 5
By fresh tribute chrysanthemum clean, dry after, take the tribute chrysanthemum 100 grams of oven dry, pulverize for granularity be less than or equal to 5mm tribute inulin end, be placed in extraction kettle; Add weight be the ethanol of described tribute chrysanthemum powder weight 0.5 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle is set to 50 DEG C, pressure is 20MPa, passes into the CO that flow is 10kg/h
2, extraction 1.5h, collects extraction liquid, filtration is prepared tribute chrysanthemum extract.
After being dissolved with glycerine triacetate by this extract, spray in cigarette filter rod according to the addition of tow quality 0.9 ‰, contrast with former finished cigarettes, ask expert to carry out sensory evaluating smoking, smoking result is in table 1.
Table 1 tribute chrysanthemum extract filter stick perfuming smoking result
Claims (2)
1. a preparation method for tribute chrysanthemum extract, is characterized in that: with fresh tribute chrysanthemum for raw material, drying, pulverizing, supercritical CO
2tribute chrysanthemum extract is obtained after extraction and filtration; Concrete steps are as follows:
(1) raw material prepares: cleaned by fresh tribute chrysanthemum, carry out after oven dry being ground into end, grinding particle size is less than or equal to 5mm, for subsequent use;
(2) supercritical CO
2extraction: by pulverize after tribute inulin end be placed in extraction kettle, add weight be the ethanol of described tribute chrysanthemum powder weight 0.2 ~ 1 times as Leaching Aid, seal extraction kettle after stirring; Temperature in extraction kettle be set to 30 ~ 60 DEG C, pressure be 20 ?40MPa, pass into flow be 5 ?the CO of 15kg/h
2extract 0.5 ?5h, collect extraction liquid;
(3) filter: carried out by the extraction liquid collected filtering and obtain described tribute chrysanthemum extract, described tribute chrysanthemum extract is khaki color liquid, is soluble in esters solvent.
2. the application of tribute chrysanthemum extract according to claim 1 in cigarette filter rod perfuming, is characterized in that: after being dissolved by tribute chrysanthemum extract glycerine triacetate, spray in tow with the consumption of 0.05 ~ 0.9 ‰.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410771801.8A CN104498192A (en) | 2014-12-15 | 2014-12-15 | Preparation method and application of florists chrysanthemum extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410771801.8A CN104498192A (en) | 2014-12-15 | 2014-12-15 | Preparation method and application of florists chrysanthemum extract |
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| CN104498192A true CN104498192A (en) | 2015-04-08 |
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| CN201410771801.8A Pending CN104498192A (en) | 2014-12-15 | 2014-12-15 | Preparation method and application of florists chrysanthemum extract |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104921289A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Honeysuckle glyceryl triacetate extract and application thereof in cigarette |
| CN104939309A (en) * | 2015-06-17 | 2015-09-30 | 云南中烟工业有限责任公司 | Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes |
| CN112056613A (en) * | 2020-09-07 | 2020-12-11 | 广西中烟工业有限责任公司 | Preparation method of cigarette filter stick with gardenia fragrance |
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| CN101161801A (en) * | 2007-11-21 | 2008-04-16 | 闫克玉 | Method for extracting chrysanthemum volatile oil and method for flavouring cigarette by employing same |
| CN102100714A (en) * | 2009-12-16 | 2011-06-22 | 青岛康地恩药业有限公司 | Method for extracting active ingredients of Echinacea through supercritical carbon dioxide |
| CN103211304A (en) * | 2013-05-13 | 2013-07-24 | 湖北中烟工业有限责任公司 | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate |
| CN103242959A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of tobacco chrysanthemum absolute oil |
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Patent Citations (8)
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104921289A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Honeysuckle glyceryl triacetate extract and application thereof in cigarette |
| CN104939309A (en) * | 2015-06-17 | 2015-09-30 | 云南中烟工业有限责任公司 | Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes |
| CN112056613A (en) * | 2020-09-07 | 2020-12-11 | 广西中烟工业有限责任公司 | Preparation method of cigarette filter stick with gardenia fragrance |
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Application publication date: 20150408 |