CN104498192A - Preparation method and application of florists chrysanthemum extract - Google Patents
Preparation method and application of florists chrysanthemum extract Download PDFInfo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 235000009604 Chrysanthemum X morifolium Nutrition 0.000 title abstract 6
- 238000000605 extraction Methods 0.000 claims abstract description 36
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 21
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 5
- 241000723353 Chrysanthemum Species 0.000 claims description 58
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 56
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 4
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 229920001202 Inulin Polymers 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 238000000227 grinding Methods 0.000 claims 1
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 claims 1
- 229940029339 inulin Drugs 0.000 claims 1
- 238000002386 leaching Methods 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 235000013773 glyceryl triacetate Nutrition 0.000 abstract description 7
- 229960002622 triacetin Drugs 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 5
- 239000000796 flavoring agent Substances 0.000 abstract description 4
- 239000000779 smoke Substances 0.000 abstract description 4
- 244000061176 Nicotiana tabacum Species 0.000 abstract description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 230000007794 irritation Effects 0.000 abstract description 2
- 238000005507 spraying Methods 0.000 abstract 1
- 238000011156 evaluation Methods 0.000 description 10
- 239000001087 glyceryl triacetate Substances 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 235000017807 phytochemicals Nutrition 0.000 description 3
- 229930000223 plant secondary metabolite Natural products 0.000 description 3
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 2
- 238000000658 coextraction Methods 0.000 description 2
- 239000003759 ester based solvent Substances 0.000 description 2
- 229930182470 glycoside Natural products 0.000 description 2
- 150000002338 glycosides Chemical class 0.000 description 2
- HFPZCAJZSCWRBC-UHFFFAOYSA-N p-cymene Chemical compound CC(C)C1=CC=C(C)C=C1 HFPZCAJZSCWRBC-UHFFFAOYSA-N 0.000 description 2
- NDVASEGYNIMXJL-UHFFFAOYSA-N sabinene Chemical compound C=C1CCC2(C(C)C)C1C2 NDVASEGYNIMXJL-UHFFFAOYSA-N 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- NDVASEGYNIMXJL-NXEZZACHSA-N (+)-sabinene Natural products C=C1CC[C@@]2(C(C)C)[C@@H]1C2 NDVASEGYNIMXJL-NXEZZACHSA-N 0.000 description 1
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 description 1
- 239000001169 1-methyl-4-propan-2-ylcyclohexa-1,4-diene Substances 0.000 description 1
- NLZCOTZRUWYPTP-WHCFWRGISA-N acacetin-7-O-beta-D-galactopyranoside Chemical compound C1=CC(OC)=CC=C1C(OC1=C2)=CC(=O)C1=C(O)C=C2O[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 NLZCOTZRUWYPTP-WHCFWRGISA-N 0.000 description 1
- NLZCOTZRUWYPTP-UHFFFAOYSA-N acacetin-7-O-beta-D-galactoside Natural products C1=CC(OC)=CC=C1C(OC1=C2)=CC(=O)C1=C(O)C=C2OC1C(O)C(O)C(O)C(CO)O1 NLZCOTZRUWYPTP-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- KQAZVFVOEIRWHN-UHFFFAOYSA-N alpha-thujene Natural products CC1=CCC2(C(C)C)C1C2 KQAZVFVOEIRWHN-UHFFFAOYSA-N 0.000 description 1
- KMOUJOKENFFTPU-QNDFHXLGSA-N apigenin 7-O-beta-D-glucoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC(O)=C2C(=O)C=C(C=3C=CC(O)=CC=3)OC2=C1 KMOUJOKENFFTPU-QNDFHXLGSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 description 1
- 229940116229 borneol Drugs 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- -1 etc. Natural products 0.000 description 1
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 1
- IQPNAANSBPBGFQ-UHFFFAOYSA-N luteolin Chemical compound C=1C(O)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(O)C(O)=C1 IQPNAANSBPBGFQ-UHFFFAOYSA-N 0.000 description 1
- LRDGATPGVJTWLJ-UHFFFAOYSA-N luteolin Natural products OC1=CC(O)=CC(C=2OC3=CC(O)=CC(O)=C3C(=O)C=2)=C1 LRDGATPGVJTWLJ-UHFFFAOYSA-N 0.000 description 1
- 235000009498 luteolin Nutrition 0.000 description 1
- 150000007875 phellandrene derivatives Chemical class 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 229930006696 sabinene Natural products 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Seasonings (AREA)
Abstract
Description
技术领域technical field
本发明属于卷烟添加剂加工技术领域，具体涉及一种贡菊提取物的制备方法。同时本发明还涉及所述贡菊提取物在卷烟滤棒加香中的应用。The invention belongs to the technical field of cigarette additive processing, and in particular relates to a preparation method of tribute chrysanthemum extract. At the same time, the invention also relates to the application of the tribute chrysanthemum extract in flavoring cigarette filter sticks.
背景技术Background technique
据报道，菊花中植物类化学成分含量丰富，主要是以金合欢素-7-O-β-D-吡喃半乳糖苷、大波斯菊苷、木犀草素等为代表的糖苷类以及以β-水芹烯、对聚伞花烯、菊烯酮、1,8-桉油精、冰片、桧烯为代表的单萜、倍半萜、三萜等萜类化合物，这些植物化学成分，多与烟草植物类香气成分相同。其中，贡菊作为我国四大名菊之一，其香气化合物的形成与转化较其他普通菊花而言更为充分，含量也较高。贡菊经烘干、溶剂提取，特别是应用超临界CO2萃取等手段，能将贡菊在成熟过程中所产生的大量植物类化学香气成分释放出来，因此以贡菊为原料制备烟用香料具有较好的应用意义。截止目前，以贡菊提取物作为卷烟滤棒加香用香料的研究未见报道。According to reports, chrysanthemum is rich in phytochemical components, mainly glycosides represented by acacetin-7-O-β-D-galactopyranoside, cosmoside, luteolin, etc., and glycosides represented by β -Monoterpenes, sesquiterpenes, triterpenes and other terpenoids represented by phellandrene, p-cymene, inrenone, 1,8-cineole, borneol, and sabinene. These phytochemical components, many The same aroma components as tobacco plants. Among them, tribute chrysanthemum is one of the four famous chrysanthemums in my country. The formation and transformation of its aroma compounds are more sufficient and higher in content than other common chrysanthemums. Tribute chrysanthemum can release a large number of phytochemical aroma components produced during the ripening process of tribute chrysanthemum through drying and solvent extraction, especially by supercritical CO 2 extraction. Therefore, tribute chrysanthemum is used as raw material to prepare tobacco flavors It has good application significance. So far, there has been no report on the use of chrysanthemum extract as a flavoring spice for cigarette filter sticks.
发明内容Contents of the invention
本发明的目的在于针对现有技术中的不足，提供一种以贡菊为原料，制备贡菊提取物的方法。The object of the present invention is to aim at the deficiencies in the prior art and provide a method for preparing the extract of tribute chrysanthemum using tribute chrysanthemum as raw material.
同时，本发明的目的还在于提供所述贡菊提取物在卷烟滤棒加香中的应用。At the same time, the object of the present invention is also to provide the application of the tribute chrysanthemum extract in cigarette filter stick flavoring.
本发明的目的通过以下技术方案予以实现。The purpose of the present invention is achieved through the following technical solutions.
除非另有说明，本发明所采用的百分数均为质量百分数。Unless otherwise specified, the percentages used in the present invention are all mass percentages.
一种贡菊提取物的制备方法，其特征在于：以新鲜贡菊为原料，经烘干、粉碎、超临界CO2萃取及过滤后获得贡菊提取物；具体步骤如下：A kind of preparation method of tribute chrysanthemum extract, it is characterized in that: take fresh tribute chrysanthemum as raw material, obtain tribute chrysanthemum extract after drying, pulverizing, supercritical CO Extraction and filtration; Concrete steps are as follows:
(1)原料准备：将新鲜贡菊洗净，烘干后进行粉碎成末，粉碎粒度小于等于5mm，备用；(1) Raw material preparation: wash the fresh chrysanthemum, dry it and crush it into powder, the particle size of which is less than or equal to 5mm, and set aside;
(2)超临界CO2萃取：将粉碎后的贡菊粉末置于萃取釜内，加入重量为所述贡菊粉末重量0.2～1倍的乙醇作为浸提助剂，搅拌均匀后密封萃取釜；萃取釜内的温度设置为30～60℃、压力为20-40MPa，通入CO2萃取0.5-5h，收集萃取液；其中，所述CO2的流量控制为5-15kg/h；(2) Supercritical CO Extraction: place the pulverized chrysanthemum powder in the extraction kettle, add ethanol with a weight of 0.2 to 1 times the weight of the tribute chrysanthemum powder as an extraction aid, and seal the extraction kettle after stirring; The temperature in the extraction tank is set to 30-60°C, the pressure is 20-40MPa, and CO 2 is introduced to extract for 0.5-5h, and the extract is collected; wherein, the flow of CO 2 is controlled at 5-15kg/h;
(3)过滤：将收集到的萃取液进行过滤即得所述贡菊提取物，所述贡菊提取物为土黄色液体，易溶于酯类溶剂。(3) Filtration: the collected extract is filtered to obtain the chrysanthemum extract, which is a khaki liquid and easily soluble in ester solvents.
所述贡菊提取物在卷烟滤棒加香中的应用，其特征在于：将贡菊提取物用三醋酸甘油酯溶解后，以0.05～0.9‰的用量喷施于丝束中。The application of the tribute chrysanthemum extract in flavoring cigarette filter sticks is characterized in that: after the tribute chrysanthemum extract is dissolved in triacetin, it is sprayed on the tow in an amount of 0.05-0.9‰.
与现有技术相比，本发明具有如下有益效果：Compared with the prior art, the present invention has the following beneficial effects:
1、本发明制备的贡菊提取物用于卷烟滤棒加香，能够有效提升烟气特征，特别是增加清香型卷烟的花香香韵和甜润感，在一定程度上降低烟气刺激性。1. The chrysanthemum chrysanthemum extract prepared by the present invention is used for flavoring cigarette filter sticks, which can effectively improve the characteristics of smoke, especially increase the floral aroma and sweetness of light-flavor cigarettes, and reduce the irritation of smoke to a certain extent.
2、本发明制备的贡菊提取物在酯类溶剂中溶解性好，可直接用于卷烟滤棒加香，应用方便。2. The chrysanthemum chrysanthemum extract prepared by the present invention has good solubility in ester solvents, can be directly used for flavoring cigarette filter sticks, and is convenient to use.
3、本发明方法简单，工艺、设备成熟，能够实现产业化。3. The method of the present invention is simple, the technology and equipment are mature, and industrialization can be realized.
具体实施方式Detailed ways
下面结合实施例对发明进行详细描述，应当注意，实施例只用于对本发明进行进一步说明，但实施例不应理解为对本发明保护范围的限制，本领域的技术人员根据本发明的教导所作出的非本质改进和调整，均落入本发明的保护范围。The invention will be described in detail below in conjunction with the examples. It should be noted that the examples are only used to further illustrate the present invention, but the examples should not be interpreted as limiting the scope of the present invention. Those skilled in the art make according to the teachings of the present invention. All non-essential improvements and adjustments fall within the protection scope of the present invention.
实施例1Example 1
将新鲜的贡菊洗净、烘干后，称取烘干的贡菊100克，粉碎为粒度小于等于5mm的贡菊粉末，置于萃取釜内；加入重量为所述贡菊粉末重量0.2倍的乙醇作为浸提助剂，搅拌均匀后密封萃取釜；萃取釜内的温度设置为30℃、压力为40MPa，通入流量为15kg/h的CO2，萃取2.5h，收集萃取液、过滤即为所制备的贡菊提取物。After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, crush it into chrysanthemum powder with a particle size less than or equal to 5mm, and place it in the extraction kettle; the added weight is 0.2 times the weight of the chrysanthemum powder The ethanol was used as an extraction aid, and the extraction kettle was sealed after stirring evenly; the temperature in the extraction kettle was set at 30°C, the pressure was 40MPa, and CO 2 was introduced at a flow rate of 15kg/h, extracted for 2.5h, and the extract was collected and filtered. For the prepared chrysanthemum extract.
将此提取物用三醋酸甘油酯溶解后，按照丝束质量0.05‰的添加量喷施于卷烟滤棒，与原成品卷烟对照，请专家进行感官评吸，评吸结果见表1。After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the added amount of 0.05‰ of the tow mass, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.
实施例2Example 2
将新鲜的贡菊洗净、烘干后，称取烘干的贡菊100克，粉碎为粒度小于等于5mm的贡菊粉末，置于萃取釜内；加入重量为所述贡菊粉末重量1倍的乙醇作为浸提助剂，搅拌均匀后密封萃取釜；萃取釜内的温度设置为40℃、压力为20MPa，通入流量为5kg/h的CO2，萃取5h，收集萃取液、过滤即为所制备的贡菊提取物。After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, crush it into a tribute chrysanthemum powder with a particle size less than or equal to 5mm, and place it in an extraction kettle; the added weight is 1 times the weight of the tribute chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set to 40°C, the pressure is 20MPa, the flow rate of 5kg/h CO 2 is introduced, the extraction is 5h, the extract is collected and filtered. The prepared chrysanthemum extract.
将此提取物用三醋酸甘油酯溶解后，按照丝束质量0.1‰的添加量喷施于卷烟滤棒，与原成品卷烟对照，请专家进行感官评吸，评吸结果见表1。After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the added amount of 0.1‰ of the tow mass, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.
实施例3Example 3
将新鲜的贡菊洗净、烘干后，称取烘干的贡菊100克，粉碎为粒度小于等于5mm的贡菊粉末，置于萃取釜内；加入重量为所述贡菊粉末重量0.3倍的乙醇作为浸提助剂，搅拌均匀后密封萃取釜；萃取釜内的温度设置为60℃、压力为20MPa，通入流量为8kg/h的CO2，萃取0.5h，收集萃取液、过滤即为所制备的贡菊提取物。After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, crush it into a tribute chrysanthemum powder with a particle size less than or equal to 5mm, and place it in the extraction kettle; the added weight is 0.3 times the weight of the tribute chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set at 60°C, the pressure is 20MPa, the flow rate is 8kg/h of CO 2 , the extraction is 0.5h, the extract is collected, filtered and ready to use. For the prepared chrysanthemum extract.
将此提取物用三醋酸甘油酯溶解后，按照丝束质量0.3‰的添加量喷施于卷烟滤棒，与原成品卷烟对照，请专家进行感官评吸，评吸结果见表1。After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter rod according to the tow weight of 0.3‰, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.
实施例4Example 4
将新鲜的贡菊洗净、烘干后，称取烘干的贡菊100克，粉碎为粒度小于等于5mm的贡菊粉末，置于萃取釜内；加入重量为所述贡菊粉末重量0.8倍的乙醇作为浸提助剂，搅拌均匀后密封萃取釜；萃取釜内的温度设置为35℃、压力为25MPa，通入流量为6kg/h的CO2，萃取1h，收集萃取液、过滤即为所制备的贡菊提取物。After washing and drying the fresh chrysanthemum, weigh 100 grams of dried chrysanthemum, grind it into chrysanthemum powder with a particle size less than or equal to 5mm, and place it in the extraction kettle; the added weight is 0.8 times the weight of the chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set to 35°C, the pressure is 25MPa, and the flow rate is 6kg/h of CO 2 , extracted for 1h, and the extract is collected and filtered. The prepared chrysanthemum extract.
将此提取物用三醋酸甘油酯溶解后，按照丝束质量0.5‰的添加量喷施于卷烟滤棒，与原成品卷烟对照，请专家进行感官评吸，评吸结果见表1。After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the added amount of 0.5‰ of the tow mass, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.
实施例5Example 5
将新鲜的贡菊洗净、烘干后，称取烘干的贡菊100克，粉碎为粒度小于等于5mm的贡菊粉末，置于萃取釜内；加入重量为所述贡菊粉末重量0.5倍的乙醇作为浸提助剂，搅拌均匀后密封萃取釜；萃取釜内的温度设置为50℃、压力为20MPa，通入流量为10kg/h的CO2，萃取1.5h，收集萃取液、过滤即为所制备的贡菊提取物。After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, grind it into chrysanthemum powder with a particle size less than or equal to 5mm, and place it in the extraction kettle; the added weight is 0.5 times the weight of the chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set at 50°C, the pressure is 20MPa, the flow rate is 10kg/h of CO 2 , the extraction is 1.5h, the extract is collected, filtered and then For the prepared chrysanthemum extract.
将此提取物用三醋酸甘油酯溶解后，按照丝束质量0.9‰的添加量喷施于卷烟滤棒，与原成品卷烟对照，请专家进行感官评吸，评吸结果见表1。After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the tow weight of 0.9‰, compared with the original finished cigarette, and experts were invited to conduct a sensory evaluation. The evaluation results are shown in Table 1.
表1 贡菊提取物滤棒加香评吸结果Table 1 The results of flavoring and smoking of Gongju extract filter sticks
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