CN105733810A - Angelica sinensis glycerol triacetate extract and application thereof to cigarettes - Google Patents
Angelica sinensis glycerol triacetate extract and application thereof to cigarettes Download PDFInfo
- Publication number
- CN105733810A CN105733810A CN201610156100.2A CN201610156100A CN105733810A CN 105733810 A CN105733810 A CN 105733810A CN 201610156100 A CN201610156100 A CN 201610156100A CN 105733810 A CN105733810 A CN 105733810A
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- China
- Prior art keywords
- extract
- angelica sinensis
- glycerol triacetate
- radix angelicae
- angelicae sinensis
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
Abstract
The invention discloses angelica sinensis glycerol triacetate extract and application thereof to cigarettes.A preparation method of the angelica sinensis glycerol triacetate extract includes: using angelica sinensis powder obtained by sieving crushed dried angelica sinensis as the raw material and glycerol triacetate as extracting agent, and sequentially using ultrasonic extraction, microwave extraction and heating reflux extraction to obtain the angelica sinensis glycerol triacetate extract.A method for applying the angelica sinensis glycerol triacetate extract to the cigarettes includes: using glycerol triacetate as the solvent to prepare the angelica sinensis glycerol triacetate extract into a solution with the concentration being 0.05-0.10%, spraying the solution to filter stick tows according to a proportion that the weight of the solution accounts for 7-8% of the weight of cellulose acetate tows so as to obtain cigarette filter sticks, and using a conventional cigarette connecting procedure to produce the cigarettes with the filter sticks containing the effective components of angelica sinensis.The angelica sinensis glycerol triacetate extract can enrich the fragrance of the cigarettes, increase the sweetness of the cigarettes and evidently increase the smoking quality of the cigarettes.The preparation method is high in operability and normalization, easy in raw material obtaining, low in cost, simple in production process, convenient to achieve industrial production and promising in application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of Radix Angelicae Sinensis triacetyl glycerine extract.Meanwhile, the invention still further relates to the application in Medicated cigarette of the described Radix Angelicae Sinensis triacetyl glycerine extract.
Background technology
Radix Angelicae Sinensis, RadixAngelicaeSinensis, another name Radix Angelicae Sinensis, cloud are returned, western Radix Angelicae Sinensis, rise abruptly Radix Angelicae Sinensis.Current medical material Radix Angelicae Sinensis refers to the root of umbelliferae angelica.After the process of preparing Chinese medicine, medical material is closely cylindrical, and a plurality of supporting root, long 15～35cm are arranged at bottom.Surface yellowish-brown to palm fibre exhausts color, and tool indulges wrinkle and hole skin of growing crosswise.Root head diameter 1.5～4.0cm, has ring grain, has purple or yellow green stem, leaf residue, main root surface irregularity；Supporting root diameter 0.3～l.0cm, upper coarse and lower fine, distort more.Matter is pliable and tough, section yellow-white or fallow, and skin zone is thick, has crack and brown oil drop.Gas is special, sweet in the mouth, hardship pungent, micro-.Radix Angelicae Sinensis is rich in lactone active component, and contains ferulic acid, nicotinic acid, sucrose and several amino acids, and sesquiterpenoids etc..
Along with smoking increasingly receives publicity with healthy problem, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also brings along Medicated cigarette gratification and natural cigarette perfume (or spice) is more or less lost, therefore, each tobacco productive corporation will promote Medicated cigarette gratification and Nicotiana tabacum L. nature fragrance gradually as researching and developing key task.Cigarette smoking quality can be effectively improved by cigarette tobacco leaf formulation flavoring and casing, but this mode finally needs that carrying out burns brings more complicated product, R&D worker will become a kind of simple and feasible application mode by adding some in filter stick and have flavouring, mend extracts of the effect such as fragrant.R&D worker has carried out the work of some correlational studyes, and obtains certain achievement.The filtering material of such as a kind of cigarette filter rod and cigarette filter rod (200810219901.4), a kind of Radix Et Rhizoma Fagopyri Tatarici cigarette filter rod (201410372333.7) with burnt odor, the application in cigarette filter rod of the moringa seeds extract and cigarette filter rod (201310159094.2) thereof, a kind of Pelargonium gravelens porous particle and the application (201310643496.X) etc. in Medicated cigarette thereof, but the filter stick additive described in above-mentioned patent mainly first passes through extraction or allotment additive dissolves in triacetyl glycerine and adds in Medicated cigarette, maybe interpolation granule is applied directly in cigarette filter rod by increasing interpolation operation.On the one hand, there is complicated process of preparation, triacetyl glycerine in this interpolation application mode, the solvability of additive is limited, Medicated cigarette much has flavouring, the extract of benefit Xiang Gong effect is difficult to be dissolved in triacetyl glycerine, limits the application in cigarette filter rod of such extract.On the other hand, if being not that carrier carries out filter stick perfuming by triacetyl glycerine, but additive being applied directly in cigarette filter rod, can produce to filter stick and bring bigger difficulty, dramatically increasing production cost, being unfavorable for large-scale popularization and application.For meeting tobacco business demand in Medicated cigarette flavouring, benefit perfume, how adopting suitable Technology, the additive of cigarette filter stick of the applicable Production requirement of preparation needs the technical barrier of solution badly by becoming this field.
Summary of the invention
Present invention aims to the deficiencies in the prior art, a kind of Radix Angelicae Sinensis extract prepared as extractant using triacetyl glycerine is provided, this extract can be directly appended in triacetyl glycerine to be applied to cigarette filter tip shaping, can be effectively increased that cigarette flavor is rich, promote sweet sense, be obviously improved cigarette sensory quality.
The present invention also aims to provide described Radix Angelicae Sinensis triacetyl glycerine extract specifically applying in production of cigarettes.
The purpose of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percent adopted in the present invention is mass percent.
A kind of Radix Angelicae Sinensis triacetyl glycerine extract, is prepared by the method for following steps:
(1) take the Radix Angelicae Sinensis root of dryness in the sun, pulverize through pulverizer after stripping and slicing, cross 40～60 mesh sieves and obtain Chinese Angelica Root, standby；
(2) weigh 300～500g Chinese Angelica Root and be placed in extraction flask, glycerol triacetate for tobacco is added as extractant in the ratio of solid-liquid ratio 1:10～20, soak 2～4 hours after stirring, ultrasonic extraction is carried out under 40～50 DEG C of conditions, extraction power is 400～600W, 40kHZ, 40～80 minutes extraction times, standby after being cooled to room temperature；
(3) it is placed in microwave extraction device again by step (2) gains hydrotropy, at 200～400W, under 40～50 DEG C of conditions, extracts 30～60 minutes, standby after being cooled to room temperature；
(4) by step (3) gains, carrying out reflux, extract, 3～6 hours under 70～90 DEG C of conditions, the settled solution obtained after elimination residue after being cooled to room temperature is required Radix Angelicae Sinensis triacetyl glycerine extract.
The application in Medicated cigarette of the described Radix Angelicae Sinensis triacetyl glycerine extract, it is characterized in that: with triacetyl glycerine for solvent, described Radix Angelicae Sinensis triacetyl glycerine extract is configured to the solution that concentration is 0.05～0.10%, it is sprayed onto on tow by the ratio uniform of acetate silk weight 7～8%, make cigarette filter rod, and this filter stick is applied to Medicated cigarette.
Compared with prior art, the invention have the advantages that
1. the present invention adopts triacetyl glycerine to be that extractant extracts Radix Angelicae Sinensis, the effective efficiency composition being dissolved in triacetyl glycerine in Radix Angelicae Sinensis fully can be extracted, it is to avoid adopt other solvent to carry out extracting and redissolve the loss of effective efficiency composition during to triacetyl glycerine again；The safety of production of cigarettes will not be had a negative impact simultaneously.
2. gained Radix Angelicae Sinensis triacetyl glycerine extract can enrich cigarette flavor, effectively promotes the flue gas property sent out thoroughly, increases sweet sense, cover cigarette foreign gas, improves effect of suction quality.
3. the Radix Angelicae Sinensis triacetyl glycerine extract prepared by and triacetyl glycerine ratio of dissolving each other is wider, and extract is evenly distributed in filter stick tow, solves the problem that quality that Medicated cigarette brings because of spice inequality is unstable.
4. operability of the present invention and standardization are strong, and raw material is easy to get, with low cost, and production technology is simple, it is simple to realize industrialized production, have a good application prospect.
5. material used herein is food stage, has higher safety in utilization.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, is not limited to the technical solution.
Embodiment 1
Take the Radix Angelicae Sinensis root of dryness in the sun, pulverize through pulverizer after stripping and slicing, cross 40 mesh sieves and obtain Chinese Angelica Root；Weigh 300g Chinese Angelica Root and be placed in extraction flask, glycerol triacetate for tobacco is added in the ratio of solid-liquid ratio 1:10, soak 2 hours after stirring, ultrasonic extraction is carried out under 40 DEG C of conditions, extraction power is 400W, 40kHZ, 40 minutes extraction times, it is cooled to room temperature, gains is placed in microwave extraction device and extracts (200W again, 40 DEG C), extract 30 minutes, withdraw from microwave extraction device, by gains reflux, extract, 3 hours under 70 DEG C of conditions, after being cooled to room temperature, elimination residue obtains settled solution, is required Radix Angelicae Sinensis triacetyl glycerine extract.
With triacetyl glycerine for solvent, Radix Angelicae Sinensis triacetyl glycerine extract is configured to the solution that concentration is 0.05%, it is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8%, make cigarette filter rod, make the Medicated cigarette containing Radix Angelicae Sinensis effective ingredient filter stick by conventional cigarette tipping program.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds that the cigarette flavor of above-mentioned Radix Angelicae Sinensis triacetyl glycerine extract is rich to be increased to some extent, and comfortableness increases.
Embodiment 2
Take the Radix Angelicae Sinensis root of dryness in the sun, pulverize through pulverizer after stripping and slicing, cross 50 mesh sieves and obtain Chinese Angelica Root；Weigh 400g Chinese Angelica Root and be placed in extraction flask, glycerol triacetate for tobacco is added in the ratio of solid-liquid ratio 1:15, soak 3 hours after stirring, ultrasonic extraction is carried out under 45 DEG C of conditions, extraction power is 500W, 40kHZ, 60 minutes extraction times, it is cooled to room temperature, gains is placed in microwave extraction device and extracts (300W again, 40 DEG C), extract 40 minutes, withdraw from microwave extraction device, by gains reflux, extract, 4 hours under 80 DEG C of conditions, after being cooled to room temperature, elimination residue obtains settled solution, is required Radix Angelicae Sinensis triacetyl glycerine extract.
With triacetyl glycerine for solvent, Radix Angelicae Sinensis triacetyl glycerine extract is configured to the solution that concentration is 0.08%, it is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8%, make cigarette filter rod, make the Medicated cigarette containing Radix Angelicae Sinensis effective ingredient filter stick by conventional cigarette tipping program.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds that the cigarette flavor of above-mentioned Radix Angelicae Sinensis triacetyl glycerine extract is rich to be increased to some extent, and sweet sense and comfortableness increase.
Embodiment 3
Take the Radix Angelicae Sinensis root of dryness in the sun, pulverize through pulverizer after stripping and slicing, cross 60 mesh sieves and obtain Chinese Angelica Root；Weigh 500g Chinese Angelica Root and be placed in extraction flask, glycerol triacetate for tobacco is added in the ratio of solid-liquid ratio 1:10, soak 4 hours after stirring, ultrasonic extraction is carried out under 50 DEG C of conditions, extraction power is 600W, 40kHZ, 80 minutes extraction times, it is cooled to room temperature, gains is placed in microwave extraction device and extracts (400W again, 50 DEG C), extract 60 minutes, withdraw from microwave extraction device, by gains reflux, extract, 6 hours under 90 DEG C of conditions, after being cooled to room temperature, elimination residue obtains settled solution, is required Radix Angelicae Sinensis triacetyl glycerine extract.
With triacetyl glycerine for solvent, Radix Angelicae Sinensis triacetyl glycerine extract is configured to the solution that concentration is 0.10%, it is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make the Medicated cigarette containing Radix Angelicae Sinensis effective ingredient filter stick by conventional cigarette tipping program.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds the submissive harmony of cigarette smoke of above-mentioned Radix Angelicae Sinensis triacetyl glycerine extract, and fragrance is rich to be increased to some extent, and pleasant impression is clean.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all any amendment, equivalent replacement and improvement etc. made within the spirit and principles in the present invention, should be included within protection scope of the present invention.
Claims (2)
1. a Radix Angelicae Sinensis triacetyl glycerine extract, is prepared by the method for following steps:
(1) take the Radix Angelicae Sinensis root of dryness in the sun, pulverize through pulverizer after stripping and slicing, cross 40～60 mesh sieves and obtain Chinese Angelica Root, standby；
(2) weigh 300～500g Chinese Angelica Root and be placed in extraction flask, glycerol triacetate for tobacco is added as extractant in the ratio of solid-liquid ratio 1:10～20, soak 2～4 hours after stirring, ultrasonic extraction is carried out under 40～50 DEG C of conditions, extraction power is 400～600W, 40kHZ, 40～80 minutes extraction times, standby after being cooled to room temperature；
(3) it is placed in microwave extraction device again by step (2) gains hydrotropy, at 200～400W, under 40～50 DEG C of conditions, extracts 30～60 minutes, standby after being cooled to room temperature；
(4) by step (3) gains, carrying out reflux, extract, 3～6 hours under 70～90 DEG C of conditions, the settled solution obtained after elimination residue after being cooled to room temperature is required Radix Angelicae Sinensis triacetyl glycerine extract.
2. the application in Medicated cigarette of the Radix Angelicae Sinensis triacetyl glycerine extract described in claim 1, it is characterized in that: with triacetyl glycerine for solvent, described Radix Angelicae Sinensis triacetyl glycerine extract is configured to the solution that concentration is 0.05～0.10%, it is sprayed onto on tow by the ratio uniform of acetate silk weight 7～8%, make cigarette filter rod, and this filter stick is applied to Medicated cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610156100.2A CN105733810A (en) | 2016-03-18 | 2016-03-18 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610156100.2A CN105733810A (en) | 2016-03-18 | 2016-03-18 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
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| CN105733810A true CN105733810A (en) | 2016-07-06 |
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| CN201610156100.2A Pending CN105733810A (en) | 2016-03-18 | 2016-03-18 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107723092A (en) * | 2017-11-29 | 2018-02-23 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications with fragrant and sweet fermentation angelica extract |
| CN112980574A (en) * | 2021-01-20 | 2021-06-18 | 广东澳大新化工有限公司 | Glycerol triacetate reactant of cordyceps sinensis and application of glycerol triacetate reactant in cigarettes |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104095289A (en) * | 2014-08-05 | 2014-10-15 | 云南中烟工业有限责任公司 | Cigarette filter with slow-release flavor plate and application thereof |
| CN104921288A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
| CN105132162A (en) * | 2015-06-17 | 2015-12-09 | 云南中烟工业有限责任公司 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
-
2016
- 2016-03-18 CN CN201610156100.2A patent/CN105733810A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104095289A (en) * | 2014-08-05 | 2014-10-15 | 云南中烟工业有限责任公司 | Cigarette filter with slow-release flavor plate and application thereof |
| CN104921288A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
| CN105132162A (en) * | 2015-06-17 | 2015-12-09 | 云南中烟工业有限责任公司 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107723092A (en) * | 2017-11-29 | 2018-02-23 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications with fragrant and sweet fermentation angelica extract |
| CN112980574A (en) * | 2021-01-20 | 2021-06-18 | 广东澳大新化工有限公司 | Glycerol triacetate reactant of cordyceps sinensis and application of glycerol triacetate reactant in cigarettes |
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Application publication date: 20160706 |
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