CN106281683A - A kind of Flos Inulae extract flavouring essence for tobacco and preparation method thereof - Google Patents

A kind of Flos Inulae extract flavouring essence for tobacco and preparation method thereof Download PDF

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Publication number
CN106281683A
CN106281683A CN201610742869.2A CN201610742869A CN106281683A CN 106281683 A CN106281683 A CN 106281683A CN 201610742869 A CN201610742869 A CN 201610742869A CN 106281683 A CN106281683 A CN 106281683A
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parts
tobacco
flavouring essence
flos inulae
extract
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Chinese (zh)
Inventor
堵育明
王勇均
黄英
翟金朋
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Hunan Mount Everest Technology Co Ltd
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Hunan Mount Everest Technology Co Ltd
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Priority to CN201610742869.2A priority Critical patent/CN106281683A/en
Publication of CN106281683A publication Critical patent/CN106281683A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses a kind of Flos Inulae extract flavouring essence for tobacco and preparation method thereof, described flavouring essence for tobacco is prepared from by the raw material of following weight portion: Flos Inulae extract 16~20 parts, laurel fat 13~15 parts, ethyl maltol 10~12 parts, Salanesol 10~12 parts, ethyl phenylacetate 8~10 parts, heliotropin 8~10 parts, linalool 8~10 parts, Semen Myristicae oil 6~8 parts, Dendranthema indicum quintessence oil 6~8 parts, Oleum lavandula angustifolia 3~5 parts, Mel 3~5 parts.The flavouring essence for tobacco that the present invention provides, cigarette flavor, soft flue gas can be effectively improved, reduce stimulation, lifting mouthfeel, simultaneously because Flos Inulae has effect of nourishing the lung to arrest cough, in sucking process, Flos Inulae effective ingredient can be in suction body, play lung moistening, reduce phlegm, the effect of cough-relieving, thus alleviate the flue gas stimulation to respiratory mucosa, reduce the harm of Medicated cigarette.

Description

A kind of Flos Inulae extract flavouring essence for tobacco and preparation method thereof
Technical field
The invention belongs to cigarette additive field, be specifically related to a kind of Flos Inulae extract flavouring essence for tobacco and preparation side thereof Method.
Background technology
Along with fast development, the formation of famous brand of tobacco industry, and Nicotiana tabacum L. category is the most perfect, to high-quality The demand of tobacco aromatics using essence also grows with each passing day.Tobacco business use spices and essence can suppress the pungent zest of cigarette, cover Miscellaneous QI, rectification are inhaled taste, are increased cigarette perfume.But traditional tobacco aromatics using essence uses chemical method to prepare, although price is low Honest and clean, but chemicals sucked multipair smoker, and healthy meeting has a great impact, and also can not in purification process That avoids also exists solvent and the problem of reactant residual.
There is abundant Chinese herbal medicine resource in China, from fragrant rich in extracting suitable cigarette the medicine-food two-purpose Chinese herbal medicine of fragrance Material essence, can not only improve the pungent zest of cigarette, cover miscellaneous QI, and can give the local flavor that medicated cigarette is different, simultaneously because be Extract from medicine food dual purpose plant and obtain, health of smokers is safe from harm, thus is welcome by market and consumer.
Flos Inulae has another name called Jin Fohua, Herba Inulae, belongs to Compositae, Inula herbaceos perennial, is distributed in Hunan, wide The ground such as west, Guizhou and Yunnan.Flos Inulae is put down, and mildly bitter flavor has the therapeutic method to keep the adverse QI flowing downwards, Hang Shui, nourishing the lung to arrest cough, clearing away heat and expelling pathogen in the exterior, lowering the adverse-rising QI and dispelling phlegm Etc. effect.At present, Flos Inulae is mainly used in Chinese crude drug field, cures mainly pertussis, bronchial asthma, the disease such as have a headache and fever, still Not finding the report as tobacco aromatics using essence, the extraction to Flos Inulae active component mainly has soxhlet extraction, extraction, decocts The methods such as cooking method, the Flos Inulae active component using existing method and technique to extract adds in Medicated cigarette, can bring muddy to flue gas Turbid sense, and stimulation is big, oral cavity residual is serious, greatly reduces the quality of Medicated cigarette.
Summary of the invention
It is an object of the invention to provide a kind of flavouring essence for tobacco containing Flos Inulae extract, this essence adds in Medicated cigarette, The fragrance of Medicated cigarette, soft flue gas can be increased, reduce stimulation, lifting mouthfeel, present invention also offers the preparation side of this flavouring essence for tobacco Method.
The flavouring essence for tobacco that the present invention provides, is prepared from by the raw material of following weight portion: Flos Inulae extract 16~20 parts, Laurel fat 13~15 parts, ethyl maltol 10~12 parts, Salanesol 10~12 parts, ethyl phenylacetate 8~10 parts, heliotropin 8 ~10 parts, linalool 8~10 parts, Semen Myristicae oil 6~8 parts, Dendranthema indicum quintessence oil 6~8 parts, Oleum lavandula angustifolia 3~5 parts, Mel 3~ 5 parts.
Applicant is devoted for years in the research and development of tobacco aromatics using essence, finds in great many of experiments, and Flos Inulae extract is used for Flavouring essence for tobacco, can improve the flue gas of Medicated cigarette to a certain extent, reduces zest, further study show that, by laurel fat, ethyl wheat Bud alcohol, Salanesol, ethyl phenylacetate, heliotropin, linalool, Semen Myristicae oil, Dendranthema indicum quintessence oil, Oleum lavandula angustifolia, Mel with The flavouring essence for tobacco that Flos Inulae extract is mixed with, is significantly improved effect to the flue gas tool of Medicated cigarette.
As preferably, described flavouring essence for tobacco, the raw material of following weight portion it is prepared from: Flos Inulae extract 18 parts, Laurel fat 14 parts, ethyl maltol 11 parts, Salanesol 11 parts, ethyl phenylacetate 9 parts, heliotropin 9 parts, linalool 9 parts, lima bean Cool oily 7 parts, Dendranthema indicum quintessence oil 7 parts, Oleum lavandula angustifolia 4 parts, Mel 4 parts.
As preferably, the extracting method of described Flos Inulae extract is as follows:
(1) british inula root was pulverized 80 mesh sieves, obtained british inula root powder;
(2) british inula root powder is mixed by solid-liquid ratio 28~30g/L with ethanol, then in mixed liquor, add british inula root The arabinose of powder quality 14%~20%, after mixed liquor mix homogeneously, uses ultrasonic extraction to obtain extracting solution;
(3) being filtered by extracting solution, filtrate is 1.25 through being concentrated in vacuo to relative density, obtains Flos Inulae extract.
The present invention uses ultrasonic extraction british inula root, can improve the extraction ratio of effective ingredient in british inula root, exists simultaneously The arabinose of british inula root powder quality 14%~18% it is additionally added during extraction, anti-to carry out a certain degree of U.S. rad Should.In this method, the addition controlling arabinose is abnormal crucial, if addition is less than 14%, then Flos Inulae extract does not has Improving the effect of cigarette smoke, if addition is higher than 20%, then Flos Inulae extract not only can not improve cigarette smoke, makes on the contrary Flue gas is more muddy, stimulates bigger.Wherein above-mentioned steps (3), concentrating the filtrate to relative density is 1.25, and measuring temperature is 30 ℃。
As preferably, in above-mentioned steps (2), the temperature of ultrasonic extraction is 65~70 DEG C.Temperature not only affects Flos Inulae and carries Taking the extraction ratio of thing, also can affect Maillard reaction, Extracting temperature is set to 65~70 DEG C, both can ensure higher extraction ratio, Can also make to have through the Flos Inulae extract of Maillard reaction preferably to improve the effect of cigarette smoke.
As preferably, in above-mentioned steps (2), the time of ultrasonic extraction is 1.5~2h.
As preferably, in above-mentioned steps (2), the power of ultrasonic extraction is 500~700W.
As preferably, in above-mentioned steps (2), the volume fraction of ethanol is 65~70%.In ethanol, the content of moisture also can shadow Ringing Maillard reaction, moisture is too high or too low all can be affected and extract the Flos Inulae extract that obtains and improve the effect of flue gas, this The volume fraction of bright middle ethanol is most preferably 68%.
As preferably, in above-mentioned steps (2), arabinose addition is 17%.
Present invention also offers the preparation method of flavouring essence for tobacco as above, step is: first by heliotropin, Lignum cinnamomi camphorae Alcohol, Semen Myristicae oil, Dendranthema indicum quintessence oil, Oleum lavandula angustifolia and Mel mixing, after stirring, then add Flos Inulae in mixed liquor Extract and laurel fat, ethyl maltol, Salanesol, ethyl phenylacetate, mix homogeneously i.e. obtains flavouring essence for tobacco.
The invention has the beneficial effects as follows: the present invention provide flavouring essence for tobacco, can be effectively improved cigarette flavor, soft flue gas, Reducing stimulation, promote mouthfeel, simultaneously because Flos Inulae has effect of nourishing the lung to arrest cough, in sucking process, Flos Inulae effectively becomes Point can in suction body, play lung moistening, reduce phlegm, the effect such as cough-relieving, thus alleviate the flue gas stimulation to respiratory mucosa, reduce Medicated cigarette Harm.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described further.
If not raw material of the present invention and equipment refer in particular to, all it is commercially available or commonly used in the art, implements Method in example, if no special instructions, is the conventional method of this area.
Embodiment 1
Flavouring essence for tobacco in the present embodiment is prepared from the following materials: Flos Inulae extract 18g, laurel fat 14g, ethyl Maltol 11g, Salanesol 11g, ethyl phenylacetate 9g, heliotropin 9g, linalool 9g, Semen Myristicae oil 7g, Dendranthema indicum quintessence oil 7g, Oleum lavandula angustifolia 4g, Mel 4g.
Wherein, the extracting method of Flos Inulae extract is:
(1) british inula root cleaned and dry is pulverized 80 mesh sieves, obtain british inula root powder;
(2) british inula root powder is mixed by solid-liquid ratio 29g/L with the ethanol that volume fraction is 68%, then in mixed liquor Add the arabinose of british inula root powder quality 17%, after mixed liquor mix homogeneously, use ultrasonic extraction to obtain extracting solution, Wherein, ultrasonic extraction condition is: temperature 68 DEG C, time 100min, power 600W;
(3) being filtered by extracting solution, it is 1.25 that filtrate is concentrated in vacuo to relative density at 30 DEG C of rotated evaporimeters, obtains rotation Flos Inulae extract.
9g heliotropin, 9g linalool, 7g Semen Myristicae oil, 7g Dendranthema indicum quintessence oil, 4g Oleum lavandula angustifolia and 4g Mel are mixed Close, after stirring, then in mixed liquor, add 18g Flos Inulae extract and 14g laurel fat, 11g ethyl maltol, 11g eggplant Buddhist nun's alcohol, 9g ethyl phenylacetate, mix homogeneously i.e. obtains flavouring essence for tobacco.
Embodiment 2
Flavouring essence for tobacco in the present embodiment is prepared from the following materials: Flos Inulae extract 16g, laurel fat 13g, ethyl Maltol 10g, Salanesol 10g, ethyl phenylacetate 8g, heliotropin 8g, linalool 8g, Semen Myristicae oil 6g, Dendranthema indicum quintessence oil 6g, Oleum lavandula angustifolia 3g, Mel 3g.
Wherein, the extracting method of Flos Inulae extract is:
(1) british inula root cleaned and dry is pulverized 80 mesh sieves, obtain british inula root powder;
(2) british inula root powder is mixed by solid-liquid ratio 28g/L with the ethanol that volume fraction is 65%, then in mixed liquor Add the arabinose of british inula root powder quality 14%, after mixed liquor mix homogeneously, use ultrasonic extraction to obtain extracting solution, Wherein, ultrasonic extraction condition is: temperature 65 DEG C, time 90min, power 500W;
(3) being filtered by extracting solution, it is 1.25 that filtrate is concentrated in vacuo to relative density at 30 DEG C of rotated evaporimeters, obtains rotation Flos Inulae extract.
8g heliotropin, 8g linalool, 6g Semen Myristicae oil, 6g Dendranthema indicum quintessence oil, 3g Oleum lavandula angustifolia and 3g Mel are mixed Close, after stirring, then in mixed liquor, add 16g Flos Inulae extract and 13g laurel fat, 10g ethyl maltol, 10g eggplant Buddhist nun's alcohol, 8g ethyl phenylacetate, mix homogeneously i.e. obtains flavouring essence for tobacco.
Embodiment 3
Flavouring essence for tobacco in the present embodiment is prepared from the following materials: Flos Inulae extract 20g, laurel fat 15g, ethyl Maltol 12g, Salanesol 12g, ethyl phenylacetate 10g, heliotropin 10g, linalool 10g, Semen Myristicae oil 8g, Dendranthema indicum essence Oil 8g, Oleum lavandula angustifolia 5g, Mel 5g.
Wherein, the extracting method of Flos Inulae extract is:
(1) british inula root cleaned and dry is pulverized 80 mesh sieves, obtain british inula root powder;
(2) british inula root powder is mixed by solid-liquid ratio 30g/L with the ethanol that volume fraction is 70%, then in mixed liquor Add the arabinose of british inula root powder quality 20%, after mixed liquor mix homogeneously, use ultrasonic extraction to obtain extracting solution, Wherein, ultrasonic extraction condition is: temperature 70 C, time 120min, power 700W;
(3) being filtered by extracting solution, it is 1.25 that filtrate is concentrated in vacuo to relative density at 30 DEG C of rotated evaporimeters, obtains rotation Flos Inulae extract.
By 10g heliotropin, 10g linalool, 8g Semen Myristicae oil, 8g Dendranthema indicum quintessence oil, 5g Oleum lavandula angustifolia and 5g Mel Mixing, after stirring, then adds 20g Flos Inulae extract and 15g laurel fat, 12g ethyl maltol, 12g in mixed liquor Salanesol, 10g ethyl phenylacetate, mix homogeneously i.e. obtains flavouring essence for tobacco.
Comparative example 1
In this comparative example, flavouring essence for tobacco is prepared from the following materials: laurel fat 14g, ethyl maltol 11g, Salanesol 11g, ethyl phenylacetate 9g, heliotropin 9g, linalool 9g, Semen Myristicae oil 7g, Dendranthema indicum quintessence oil 7g, Oleum lavandula angustifolia 4g, honeybee Honey 4g.The present embodiment flavouring essence for tobacco is without Flos Inulae extract with the difference of embodiment 1.
Comparative example 2
In this comparative example, flavouring essence for tobacco only has Flos Inulae extract composition, the extracting method of Flos Inulae extract and enforcement Example 1 is identical.
Comparative example 3~7
In comparative example 3, comparative example 4, comparative example 5, comparative example 6 and comparative example 7, the flavouring essence for tobacco of each comparative example by with Lower raw material is prepared from: Flos Inulae extract 18g, laurel fat 14g, ethyl maltol 11g, Salanesol 11g, ethyl phenylacetate 9g, heliotropin 9g, linalool 9g, Semen Myristicae oil 7g, Dendranthema indicum quintessence oil 7g, Oleum lavandula angustifolia 4g, Mel 4g.
Wherein, the flavouring essence for tobacco of each comparative example, its preparation method is all identical with embodiment 1, and difference is that Flos Inulae carries Take the extraction conditions of thing, in comparative example 3, comparative example 4, comparative example 5, comparative example 6 and comparative example 7, during supersound extraction Flos Inulae, The quality adding arabinose is respectively the 8% of british inula root powder quality, 12%, 24%, 30% and 40%, other condition phases With.
Smoke panel test experiment
Being respectively used to prepare cigarette by the flavouring essence for tobacco of embodiment 1~3, comparative example 1~7 preparation, method is by tobacco shred matter The 0.01% of amount is sprayed on tobacco shred equably with laryngeal spray, after placing 2 days in climatic chamber, with cigarette-roller by upper Stating tobacco shred and be respectively prepared cigarette, be evaluated according to GB5606.4-2005 standard, evaluation criterion is shown in Table 1, embodiment 1~3 and right The evaluation result of ratio 1~7 is shown in Table 2.
Be can be seen that by the smoking result of table 2, the total of embodiment 1~3 is divided more than 89, hence it is evident that higher than comparative example 1~7, Illustrate that the flavouring essence for tobacco that the present invention provides is obvious to the improvement effect of cigarette smoke;The total of comparative example 1 divides only 74, illustrates In the case of not adding Flos Inulae extract, other components are limited to the improvement effect of cigarette smoke, with embodiment 1~3 phase Ratio, is mainly manifested in flue gas muddiness, stimulates greatly, especially stimulates throat big;The total of comparative example 2 divides also only 76, explanation It is used alone Flos Inulae extract cigarette smoke to be had some improvement effect, but the use that effect can not meet Medicated cigarette is wanted Asking, compared with comparative example 1, zest is less than normal, illustrates that Flos Inulae extract can effectively reduce the zest of flue gas;Comparative example The total of 3~7 is divided and is followed successively by 80,82,80,78,77, illustrates when ultrasonic extraction Flos Inulae, the addition pair of arabinose The essence influential effect of preparation is very big, and the addition of arabinose is on the low side, and the improvement of flue gas effect is substantially deteriorated, arabinose Addition is on the high side, and the improvement of flue gas effect also can be deteriorated, and along with the further increase of addition, improves effect and also can enter one Step is deteriorated.
Table 1 Sensory Quality of Cigarette evaluation criterion
The each embodiment of table 2 and the smoking result of comparative example flavouring essence for tobacco

Claims (9)

1. a Flos Inulae extract flavouring essence for tobacco, it is characterised in that be prepared from by the raw material of following weight portion: Flos Inulae carries Take thing 16~20 parts, laurel fat 13~15 parts, ethyl maltol 10~12 parts, Salanesol 10~12 parts, ethyl phenylacetate 8~10 Part, heliotropin 8~10 parts, linalool 8~10 parts, Semen Myristicae oil 6~8 parts, Dendranthema indicum quintessence oil 6~8 parts, Oleum lavandula angustifolia 3 ~5 parts, Mel 3~5 parts.
Flavouring essence for tobacco the most according to claim 1, it is characterised in that be prepared from by the raw material of following weight portion: sheathed Flower extract 18 parts, laurel fat 14 parts, ethyl maltol 11 parts, Salanesol 11 parts, ethyl phenylacetate 9 parts, heliotropin 9 parts, Linalool 9 parts, Semen Myristicae oil 7 parts, Dendranthema indicum quintessence oil 7 parts, Oleum lavandula angustifolia 4 parts, Mel 4 parts.
Flavouring essence for tobacco the most according to claim 1 and 2, it is characterised in that the extracting method of described Flos Inulae extract is such as Under:
(1) british inula root was pulverized 80 mesh sieves, obtained british inula root powder;
(2) british inula root powder is mixed by solid-liquid ratio 28~30g/L with ethanol, then in mixed liquor, add british inula root powder The arabinose of quality 14%~20%, after mixed liquor mix homogeneously, uses ultrasonic extraction to obtain extracting solution;
(3) being filtered by extracting solution, filtrate is 1.25 through being concentrated in vacuo to relative density, obtains Flos Inulae extract.
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) temperature of ultrasonic extraction be 65~ 70℃。
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) time of ultrasonic extraction be 1.5~ 2h。
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) power of ultrasonic extraction be 500~ 700W。
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) volume fraction of ethanol be 65%~ 70%.
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2), arabinose addition is 17%.
9. the preparation method of the flavouring essence for tobacco as described in any one of claim 1 to 8, it is characterised in that first by heliotrope Aldehyde, linalool, Semen Myristicae oil, Dendranthema indicum quintessence oil, Oleum lavandula angustifolia and Mel mixing, after stirring, then add in mixed liquor Entering Flos Inulae extract and laurel fat, ethyl maltol, Salanesol, ethyl phenylacetate, mix homogeneously i.e. obtains flavouring essence for tobacco.
CN201610742869.2A 2016-08-26 2016-08-26 A kind of Flos Inulae extract flavouring essence for tobacco and preparation method thereof Pending CN106281683A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107189861A (en) * 2017-07-19 2017-09-22 北京军秀咨询有限公司 The essence and preparation method of a kind of plant extract
CN110655983A (en) * 2018-06-29 2020-01-07 湖南中烟工业有限责任公司 Preparation method and application of essence containing solanesol

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103113989A (en) * 2013-03-07 2013-05-22 华宝食用香精香料(上海)有限公司 Tobacco essence capable of improving cigarette taste and aroma
CN103478894A (en) * 2013-09-27 2014-01-01 福建中烟工业有限责任公司 Camellia extract composition with spicy fragrance and application of same to cigarettes
CN105146731A (en) * 2015-07-10 2015-12-16 川渝中烟工业有限责任公司 Heat-not-burn cigarette additive and preparation method and application thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103113989A (en) * 2013-03-07 2013-05-22 华宝食用香精香料(上海)有限公司 Tobacco essence capable of improving cigarette taste and aroma
CN103478894A (en) * 2013-09-27 2014-01-01 福建中烟工业有限责任公司 Camellia extract composition with spicy fragrance and application of same to cigarettes
CN105146731A (en) * 2015-07-10 2015-12-16 川渝中烟工业有限责任公司 Heat-not-burn cigarette additive and preparation method and application thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107189861A (en) * 2017-07-19 2017-09-22 北京军秀咨询有限公司 The essence and preparation method of a kind of plant extract
CN110655983A (en) * 2018-06-29 2020-01-07 湖南中烟工业有限责任公司 Preparation method and application of essence containing solanesol
CN110655983B (en) * 2018-06-29 2022-11-04 湖南中烟工业有限责任公司 Preparation method and application of essence containing solanesol

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Application publication date: 20170104