CN105029700A - Plant composite glycerol triacetate extract and application thereof in cigarettes - Google Patents
Plant composite glycerol triacetate extract and application thereof in cigarettes Download PDFInfo
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- CN105029700A CN105029700A CN201510336787.3A CN201510336787A CN105029700A CN 105029700 A CN105029700 A CN 105029700A CN 201510336787 A CN201510336787 A CN 201510336787A CN 105029700 A CN105029700 A CN 105029700A
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- glycerol triacetate
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Abstract
The invention discloses a plant composite glycerol triacetate extract and an application thereof in cigarettes. According to the plant composite glycerol triacetate extract, vanilla beans, codonopsis pilosula, astragalus membranaceus and selfheal are taken as the raw materials, glycerol triacetate is taken as an extraction agent, and the plant composite glycerol triacetate extract is prepared by combining heating reflux extraction and ultrasonic extraction. In application, the plant composite glycerol triacetate extract is prepared into 2-5% solution by adopting glycerol triacetate as a solvent, then the prepared solution is uniformly sprayed to cellulose acetate tows with the weight being 7-8% of that of the cellulose acetate tows, and thus preparing filter sticks of the cigarettes, and finally the cigarettes with the filter sticks containing the plant composite active ingredients are prepared according to the conventional cigarette rolling process. The plant composite glycerol triacetate extract can obviously improve the smoking aroma quality o the cigarettes, the smoke volatilizes, is mellow and fine, has no irritation, and low content of other miscellaneous smell, so that the sensory quality of the cigarettes is obviously improved. The production technology is simple, and strong in operability and normalization, the raw materials are easily available, the cost is low, the industrial production is easily realized, and thus the plant composite glycerol triacetate extract has a good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of triacetyl glycerine extract of plant society.Meanwhile, the invention still further relates to the described application of plant society triacetyl glycerine extract in cigarette.
Background technology
Vanilla beans are a kind of famous and precious natural flavors, have plentiful, strong fragrance, and its fruit pod contains the Multiple components such as aldehydes and phenols, alcohols, acids, ester class, ketone, olefines and heterocyclic compound, and what wherein content was the highest is vanillic aldehyde.Due to its special odor type, be widely used as the blending raw material of the luxury foods such as high-grade cigarette, famous brand of wine, cream, coffee, chocolate.In perfuming cigarette, greatly can improve the quality scale of cigarette, have alcohol and flue gas, coordination smoke, increase cigarette perfume, make the fragrant fine and smooth soft effect of cigarette, vanilla bean tincture dipping tobacco leaf applied usually by the senior cigar of external famous brand.Radix Codonopsis is the root of Campanulaceae Radix Codonopsis, and the sweet property of taste is put down, and is Chinese medicine traditional simply.Radix Codonopsis is containing saponin, polysaccharide, phytosterol, volatile oil, phenols, vitamin, amino acid, scutellarein glucosid, saponin and alkaloid, trace element etc., there is tonifying middle-Jiao and Qi, invigorating the spleen benefit lung, anticancer step-down, anti anoxia and antidotal effect, there is the function of good stimulating central nervous system system and enhancing body immunity simultaneously.The Radix Astragali is the Chinese medicine commonly used simply, and its main chemical compositions has astragalus polyose, saponins, flavonoids and amino acid etc., pharmacologically has raising immunity of organisms, protects the liver diuresis, radioresistance, anti-ageing, resisting stress, step-down and stronger antibacterial action.Selfheal is cold in nature, taste is sweet pungent, clinically for clearing liver fire, mass dissipating and swelling eliminating, clearing heat and detoxicating, expelling phlegm and arresting coughing and cooling blood and hemostasis.Functional component is mainly containing triterpene and glycoside, sterol and glycoside, flavonoids, cumarin, organic acid, volatile oil and carbohydrate.Have sore throat in alleviation, generate heat and be widely used in accelerating wound healing etc.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of plant society extract prepared using triacetyl glycerine as extractant is provided, this extract is applied to cigarette can make cigarette flavor matter promote, smoke alcohol is good with fine and smooth, a saturating property, assorted gas and excitant alleviate, and suction quality obviously promotes.
The present invention also aims to provide the described embody rule of plant society triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of plant society triacetyl glycerine extract, is obtained by the method for following steps:
(1) vanilla beans 2 ~ 3 parts, Radix Codonopsis 1 ~ 2 part, the Radix Astragali 0 ~ 0.5 part and selfheal 4 ~ 6 parts is taken by weight, Homogeneous phase mixing after coarse crushing, then under 50 DEG C of conditions dry 10 ~ 15 hours, then to pulverize further be 20 ~ 60 object plant society powder, for subsequent use;
(2) take 1 ~ 3 part of plant society powder and be placed in round-bottomed flask, add 5 ~ 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature, after 6 ~ 15 hours, carries out refluxing extraction under 70 ~ 150 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 700W, 40kHZ condition, extract 20 ~ 60 minutes, cross the settled solution obtained after filtering filter residue and be required plant society triacetyl glycerine extract.
The described application of plant society triacetyl glycerine extract in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described plant society triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the plant society triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that prior art exists when vegetable composition is mixed be fitted in plasticizer as filter stick additive.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in described plant society fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained plant society triacetyl glycerine extract can make cigarette flavor matter promote, and smoke alcohol is good with fine and smooth, a saturating property, and assorted gas and excitant alleviate, and suction quality obviously promotes.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Get 3 parts of vanilla beans, 1 part of Radix Codonopsis, 0.5 part of Radix Astragali and 4 portions of selfheals, carry out coarse crushing, after Homogeneous phase mixing under 50 DEG C of conditions dry 10 hours, pulverize further again as 20-40 object plant society powder, take 1 part of plant society powder according to weight portion and be placed in round-bottomed flask, add 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 6 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 8 hours, to be cooled to room temperature, plant society after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (400W, 40kHZ), extract 40 minutes, cross after filtering filter residue and obtain settled solution, be required plant society triacetyl glycerine extract.
Take triacetyl glycerine as solvent, plant society triacetyl glycerine extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains plant society active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flavor matter of adding above-mentioned plant society triacetyl glycerine extract is improved, and oral cavity is sweet, promote the production of body fluid, and flue gas is sent out thoroughly, and pleasant impression is totally comfortable.
Embodiment 2
Get 2 parts of vanilla beans, 2 parts of Radix Codonopsis and 6 portions of selfheals, carry out coarse crushing, after Homogeneous phase mixing under 50 DEG C of conditions dry 15 hours, pulverize further again as 20-60 object vegetable composition powder, take 3 parts of plant society powder according to weight portion and be placed in round-bottomed flask, add 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 10 hours, refluxing extraction is carried out under 100 DEG C of conditions, extraction time is 8 hours, to be cooled to room temperature, plant society after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (700W, 40kHZ), extract 30 minutes, cross after filtering filter residue and obtain settled solution, required plant society triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, plant society triacetyl glycerine extract is mixed with the solution that concentration is 1%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains plant society active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned plant society triacetyl glycerine extract is obvious, and aroma quality and perfume quantity increase, and excitant and assorted gas alleviate, and suction comfortableness promotes.
Embodiment 3
Get 2 parts of vanilla beans, 2 parts of Radix Codonopsis, 0.5 part of Radix Astragali and 5 portions of selfheals, carry out coarse crushing, after Homogeneous phase mixing under 50 DEG C of conditions dry 10 hours, pulverize further again as 40-60 object vegetable composition powder, take 1 part of plant society powder according to weight portion and be placed in round-bottomed flask, add 5 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 15 hours, refluxing extraction is carried out under 120 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, plant society after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (400W, 40kHZ), extract 60 minutes, cross after filtering filter residue and obtain settled solution, required plant society three triacetin extract can be obtained.
Take triacetyl glycerine as solvent, plant society triacetyl glycerine extract is mixed with the solution that concentration is 4%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains plant society active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned plant society triacetyl glycerine extract is obvious, and fragrant plentiful of cigarette, aroma quality promote, and flue gas excitant obviously reduces, and suction quality obviously promotes.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a plant society triacetyl glycerine extract, is obtained by the method for following steps:
(1) vanilla beans 2 ~ 3 parts, Radix Codonopsis 1 ~ 2 part, the Radix Astragali 0 ~ 0.5 part and selfheal 4 ~ 6 parts is taken by weight, Homogeneous phase mixing after coarse crushing, then under 50 DEG C of conditions dry 10 ~ 15 hours, then to pulverize further be 20 ~ 60 object plant society powder, for subsequent use;
(2) take 1 ~ 3 part of plant society powder and be placed in round-bottomed flask, add 5 ~ 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature, after 6 ~ 15 hours, carries out refluxing extraction under 70 ~ 150 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 700W, 40kHZ condition, extract 20 ~ 60 minutes, cross the settled solution obtained after filtering filter residue and be required plant society triacetyl glycerine extract.
2. the application of plant society triacetyl glycerine extract according to claim 1 in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described plant society triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105581374A (en) * | 2016-03-18 | 2016-05-18 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
| CN106539124A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | A kind of cigarette filter tip additive and preparation method thereof |
| CN111990689A (en) * | 2020-08-20 | 2020-11-27 | 广西中烟工业有限责任公司 | Preparation method of chestnut shell pigment cigarette filter stick |
| CN112075661A (en) * | 2020-09-07 | 2020-12-15 | 广西中烟工业有限责任公司 | Preparation method of persimmon leaf flavonoid cigarette filter stick |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105581374A (en) * | 2016-03-18 | 2016-05-18 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
| CN106539124A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | A kind of cigarette filter tip additive and preparation method thereof |
| CN106539124B (en) * | 2016-10-20 | 2018-05-29 | 云南中烟工业有限责任公司 | A kind of preparation method of cigarette filter tip additive |
| CN111990689A (en) * | 2020-08-20 | 2020-11-27 | 广西中烟工业有限责任公司 | Preparation method of chestnut shell pigment cigarette filter stick |
| CN112075661A (en) * | 2020-09-07 | 2020-12-15 | 广西中烟工业有限责任公司 | Preparation method of persimmon leaf flavonoid cigarette filter stick |
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Application publication date: 20151111 |