CN106539124B - A kind of preparation method of cigarette filter tip additive - Google Patents
A kind of preparation method of cigarette filter tip additive Download PDFInfo
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- CN106539124B CN106539124B CN201610914660.XA CN201610914660A CN106539124B CN 106539124 B CN106539124 B CN 106539124B CN 201610914660 A CN201610914660 A CN 201610914660A CN 106539124 B CN106539124 B CN 106539124B
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- Prior art keywords
- filter tip
- white
- cigarette filter
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- preparation
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a kind of cigarette filter tip additive and preparation method thereof, cigarette filter tip additive composition is in parts by weight：White 1~5 part of conopsea extraction of member, 5~10 parts of polyalcohol, 0.001~0.005 part of sweetener, 1~10 part of glyceryl triacetate；Cigarette filter tip additive prepared by the present invention can improve the sense organ comfort level of cigarette smoke.The present invention is easy to operate, and equipment is easy to get, at low cost, is easy to be extended and applied.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of cigarette filter tip additive and preparation method thereof.
Background technology
China's cigarette product there is flue gas drying, it is pungent stimulate, the low suction organoleptic issues of sweet degree, therefore, it is necessary to
This is solved the problems, such as by adding humectant.Humectant, which refers to be applied in tobacco product process in tobacco, to be enhanced
Tobacco product performance of keeping humidity increases flexibility, reduces broken substance.Applying humectant is beneficial to improve in tobacco product in matter
Amount, can reduce irritation, make jealous good, in addition, humectant can also make the fragrance of application reduce volatilization, maintain tobacco product
Stable quality.Cigarette flavouring humectation technology always is the key point of prominent tobacco product characteristic chicken flavor and personalized style.This
Outside, cigarette humid keeping performance is an important factor for influencing cigarette fragrance and suction comfort level.At present, domestic cigarette enterprise mainly passes through
The polyhydroxy substances such as addition propylene glycol, glycerine improve the humid keeping performance of cigarette as humectant, but see with practical conditions, cigarette
Humectation effect is unsatisfactory, still has moisture in cut tobacco and scatters and disappears that fast, main flume moisture is relatively low, irritation is bigger than normal, dry sensation is apparent
And the common problems such as oral cavity abundant expectoration.Natural plants flavouring humectant is combined separation is extracted with moisturizing humid keeping performance, is being built
Cigarette feature note in terms of improving suction comfort, embodies unique advantage and significant application effect.
Bai Yuancan also known as false bark of ash, Bai Yun Shen, white American ginseng, native Radix Glycyrrhizae, white radix scrophulariae, pungent ginseng etc.；Lijing Nahsi language claims " thick
Bow "；For Labiatae (Lamiaceae) Paraphlomis herbaceous plant, rhizome is plump, knob-like series connection；The western regions of the Yunnan Province, Eastern Tibet are originated in,
The western Sichuan North Sea is pulled out on 2700~3000 meters of grass plot, hayashishita or careless slope, is the sweet-tasting plant of NW YUNNAN specialty.White clouds
Join as Yunnan Tibetan common traditional Tibetan medicine among the people, be used as medicine with root block, it is among the people to control abscess of throat, tripe swollen (food poisoning),
Collywobbles, diarrhea and anemofrigid cold etc.；Spleen and other effects is opened with pharynx-clearing throat-benefiting, kobadrin, stomach invigorating.In hundred radix scrophulariae containing high sweet taste into
Divide hundred radix scrophulariae glucosides, sweet taste is 500 times of sucrose, and sweet taste is lasting, can remain 1h or so in oral cavity；Its extract and sweet taste
Hundred radix scrophulariae glucoside of ingredient can substantially increase the sweet sense of cigarette smoking, have preferable effect of promoting the production of body fluid, but white radix scrophulariae gives birth to applied to cigarette
Production not yet has been reported that.It is an object of the invention to be directed to deficiency of the prior art, with hundred yuan of conopsea extractions and its main sweet taste
Hundred radix scrophulariae glucoside of ingredient is key component, provides a kind of additive of cigarette filter stick preparation side easy to operate, being suitble to large-scale production
Method.
The content of the invention
The object of the present invention is to provide a kind of cigarette filter tip flavouring humectations that can be enriched cigarette perfume, provide cigarette sense organ comfort level
Additive and preparation method thereof.It is formed in parts by weight as white first 1~5 part of conopsea extraction, 5~10 parts of polyalcohol, sweet taste
0.001~0.005 part of agent, 1~10 part of glyceryl triacetate.The present invention using reaching abundant cigarette perfume in white member conopsea extraction,
The problem of improving flue gas drying, improves the purpose of sense organ comfort level.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 2~5 parts of absolute ethyl alcohols is added in, using surname extraction, heats back
4~8h is flowed, extracting solution is concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The preparation method of the cigarette filter tip additive, it is characterised in that：
(1) 40~70 DEG C are warming up to after polyalcohol is mixed with sweetener, under 600~1600rpm stir 5~
10min；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasound about 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 40~70 DEG C after mixing, 600~
5~10min is stirred under 1600rpm to get to cigarette filter tip additive.
Cigarette filter tip additive prepared by the present invention can improve flue gas moistening degree, aesthetic quality and comfort level.The present invention
Easy to operate, equipment is easy to get, at low cost, is easy to be extended and applied.
Description of the drawings
Nothing.
Specific embodiment
The present invention is further described with reference to embodiment, but protection scope of the present invention is not limited to this.
Embodiment 1
Its composition of this cigarette filter tip additive is in parts by weight white first 1 part of conopsea extraction, 5 parts of polyalcohol, sweetener
0.001 part, 1 part of glyceryl triacetate.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 2 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
4h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The preparation method of the cigarette filter tip additive, it is characterised in that：
(1) 40 DEG C are warming up to after polyalcohol is mixed with sweetener, stirs 5min at 600 rpm；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasound about 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 40 DEG C after mixing, at 600 rpm
5min is stirred to get to cigarette filter tip additive.
Embodiment 2
Its composition of this cigarette filter tip additive is in parts by weight white first 2 parts of conopsea extraction, 6 parts of polyalcohol, sweetener
0.002 part, 3 parts of glyceryl triacetate.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 3 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
5h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The preparation method of the cigarette filter tip additive, it is characterised in that：
(1) 50 DEG C are warming up to after polyalcohol is mixed with sweetener, stirs 6min at 800 rpm；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasound about 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 50 DEG C after mixing, at 800 rpm
6min is stirred to get to cigarette filter tip additive.
Embodiment 3
Its composition of this cigarette filter tip additive is in parts by weight white first 3 parts of conopsea extraction, 7 parts of polyalcohol, sweetener
0.003 part, 5 parts of glyceryl triacetate.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 3.5 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
6h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The preparation method of the cigarette filter tip additive, it is characterised in that：
(1) 55 DEG C are warming up to after polyalcohol is mixed with sweetener, 7min is stirred under 1200rpm；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasound about 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 55 DEG C after mixing, under 1200rpm
7min is stirred to get to cigarette filter tip additive.
Embodiment 4
Its composition of this cigarette filter tip additive is in parts by weight white first 4 parts of conopsea extraction, 9 parts of polyalcohol, sweetener
0.004 part, 7 parts of glyceryl triacetate.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 4 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
7h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The preparation method of the cigarette filter tip additive, it is characterised in that：
(1) 60 DEG C are warming up to after polyalcohol is mixed with sweetener, 8min is stirred under 1400rpm；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasound about 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 60 DEG C after mixing, under 1400rpm
8min is stirred to get to cigarette filter tip additive.
Embodiment 5
Its composition of this cigarette filter tip additive is in parts by weight white first 5 parts of conopsea extraction, 10 parts of polyalcohol, sweetener
0.005 part, 10 parts of glyceryl triacetate.
The polyalcohol is one or more of propylene glycol, glycerine, xylitol, sorbierite mixture.
The sweetener is the mixing of one or more of Sucralose, neotame, Talin, steviol glycoside, baiyunoside
Object.
The extracting method of white first conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, 5 parts of absolute ethyl alcohols is added in, using surname extraction, is heated to reflux
8h, extracting solution are concentrated under the conditions of 25~85 DEG C of pressure of temperature is 0.02~0.04MPa up to white first conopsea extraction.
The preparation method of the cigarette filter tip additive, it is characterised in that：
(1) 70 DEG C are warming up to after polyalcohol is mixed with sweetener, stirs 10min at 1600 rpm；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasound about 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 70 DEG C after mixing, at 1600 rpm
10min is stirred to get to cigarette filter tip additive.
By cigarette filter tip additive made from the present embodiment, by the amount of 5 μ L/ branch cigarette, uniformly injected with essence injector
Into cigarette filter tip, the cigarette of the additive containing cigarette filter tip is made, carries out sense organ comfort level performance test.
Cigarette filter tip additive prepared by embodiment 1-3 carries out sense organ Comfort Evaluation (the main irritation and remaining investigated
Taste two indices), 1 is the results are shown in Table, which carries out according to tobacco business standard, and result is score value, and score value is higher to be illustrated to feel
Official's comfort level is better.
Table 1：Cigarette filter tip additive sense organ Comfort Evaluation
| Cigarette filter tip additive | Irritation (full marks 20) | Pleasant impression (full marks 25 divide) |
| Blank control sample | 17.5 | 22.0 |
| 1 product of embodiment | 19.0 | 23.5 |
| 2 product of embodiment | 18.5 | 22.5 |
| 3 product of embodiment | 18.5 | 23.0 |
As shown in Table 1, by the way that sense organ comfort test, product of the present invention is superior to blank in terms of irritation and pleasant impression
Control sample.
Claims (3)
1. a kind of preparation method of cigarette filter tip additive, the composition of the cigarette filter tip additive are in parts by weight：In vain
First 1~5 part of conopsea extraction, 5~10 parts of polyalcohol, 0.001~0.005 part of sweetener, 1~10 part of glyceryl triacetate；It is described
The extracting method of white member conopsea extraction is to carry out gained according to the following steps：
1 part of white radix scrophulariae is ground into powder with pulverizer, adds in 2~5 parts of absolute ethyl alcohols, using surname extraction, it is heated to reflux 4~
8h, extracting solution are concentrated under the conditions of 25~85 DEG C of temperature, pressure is 0.02~0.04MPa up to white first conopsea extraction；
It is characterized in that, preparation method includes the following steps：
(1) 40~70 DEG C are warming up to after polyalcohol is mixed with sweetener, 5~10min is stirred under 600~1600rpm；
(2) after white first conopsea extraction and glyceryl triacetate being mixed, ultrasonic 30min, filtering, removing insoluble matter；
(3) liquid prepared by the liquid and step (2) prepared step (1) is warming up to 40~70 DEG C after mixing, 600~
5~10min is stirred under 1600rpm to get to cigarette filter tip additive.
2. preparation method according to claim 1, it is characterised in that：Polyalcohol is glycerine, in xylitol, sorbierite
One or more of mixtures.
3. preparation method according to claim 1, it is characterised in that：Sweetener is Sucralose, neotame, Talin, sweet tea
One or more of synanthrin glycosides, baiyunoside mixture.
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| CN201610914660.XA CN106539124B (en) | 2016-10-20 | 2016-10-20 | A kind of preparation method of cigarette filter tip additive |
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| CN106539124B true CN106539124B (en) | 2018-05-29 |
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| CN108252154A (en) * | 2018-02-28 | 2018-07-06 | 吉林长白山包装材料有限公司 | A kind of seasoning composition added in cigarette tipping paper |
| CN109156895A (en) * | 2018-08-07 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage |
| CN109288125B (en) * | 2018-09-20 | 2021-01-29 | 云南中烟工业有限责任公司 | Filter tip additive mainly containing refined radix glycyrrhizae preparata sweet components and preparation method thereof |
| CN111635825A (en) * | 2020-05-18 | 2020-09-08 | 云南中烟工业有限责任公司 | Snow mountain liquorice essence for cigarette bead blasting, bead blasting prepared from snow mountain liquorice essence and cigarette |
| CN112998304B (en) * | 2021-03-01 | 2022-03-25 | 云南中烟工业有限责任公司 | Preparation method and application of baked and fermented gentiana macrophylla spice |
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