CN103271441B - Application of moringa oleifera seed extractive to cigarette filter stick and cigarette filter stick - Google Patents
Application of moringa oleifera seed extractive to cigarette filter stick and cigarette filter stick Download PDFInfo
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- CN103271441B CN103271441B CN201310159094.2A CN201310159094A CN103271441B CN 103271441 B CN103271441 B CN 103271441B CN 201310159094 A CN201310159094 A CN 201310159094A CN 103271441 B CN103271441 B CN 103271441B
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Abstract
The invention provides the application of moringa oleifera seed extractive to a cigarette filter stick. The application of the moringa oleifera seed extractive to the cigarette filter stick is characterized in that the moringa oleifera seed extractive serving as essence fragrance is added to the filter stick of the cigarette, and 5-20 microliters of moringa oleifera seed extractive is added to the filter element of the filter stick of each cigarette. According to the preparation method of the moringa oleifera seed extractive, the moringa oleifera seed extractive is extracted form a moringa oleifera seed oil cake with oil expelled by means of ethanol water or water. The application of the moringa oleifera seed extractive to the cigarette filter stick and the cigarette filter stick have the advantages that due to the fact that the moringa oleifera seed extractive which has special fragrance and a good absorbing function and is capable of enabling sweetness lingered over the mouth is added to the filter stick of the cigarette, the fragrance of the cigarette is enriched, the sweetness lingered over the mouth can be enhanced, the absorbing capacity of the filter stick is enhanced, the hazards of the cigarette are further reduced, and the high-qualified cigarette is manufactured.
Description
Technical field
the present invention relates to cigarette filter rod technical field, more specifically, relate to the application of moringa seeds extract in cigarette filter rod and filter stick and preparation method containing moringa seeds extract.
Background technology
in cigarette smoke, include particulate, be conventionally referred to as tar.In tar, containing a large amount of chemical compositions, have 4000 to 5000 kinds, is all the unburnt product of tobacco.Except tar, in cigarette smoke, also include other gaseous substances and half volatile material.Cigarette filter rod can filter smoke composition.The filter stick of cigarette is made up of filter core and forming paper.Filter stick is the important component part of cigarette, utilizes sorbing material and additive thereof in cigarette filter can filter out the harmful substance in cigarette main flume.
China is tobacco big country, and annual production and the consumption of cigarette rank first in the world.In recent years, for meeting consumer to cigarette consumption and healthy dual pursuit, the art is constantly studied the cigarette composition of reducing tar and reducing harm.But cigarette also inevitable fragrance that must lose cigarette itself and jealous in reducing tar and reducing harm.The technical barrier that simultaneously solves harm reduction and flavouring becomes study hotspot and the emphasis of the art, comprises the technical research that relates to filter stick.
Moringa (
moringa oleifera) be Moringaceae Moringa perennial plant, originate in arid or the semiarid zone of the torrid zone, south subtropics.Planting and can blossom and bear fruit after 6 months, is multipurpose fast-growing arbor species Moringa.Complete stool all can be utilized, and root and bark are traditional medicine raw materials, and tender leaf and tender fruit pod are delicious flavour and nutritious vegetables, contain abundant Flavonoid substances in leaf.Moringa has brings down a fever, anti-inflammatory, row's stone, diuresis, step-down, pain relieving, cardiac stimulant, urges the functions such as wish.The diseases such as tradition India medicine is usually used in treating under diabetes, hypertension, cardiovascular disease, obesity, skin disease, eye illness, immunity, scurvy, anaemia, rickets, depression, arthritis, rheumatism, solid, digestive organs tumour.Studies have shown that in a large number the medical health care function of Moringa, blade, fruit and root contain and reduce blood pressure and the functional component of cholesterol, cholesterol in serum, liver and the kidney of the high fat mouse of energy reduction, can change Mouse Blood urea, plasma proteins, bilirubin and cholesterol significantly.Blade contains the superoxide dismutase (SOD) and the catalase (CAT) that regulate thyroxine and liver lipid peroxidation effect (LPO).
Moringa seed is rich in plant oil content, is used for extracting oil obtaining oil ben, and oil ben is very well sold and in short supply in the international market.After its bean powder or oil expression, remaining oil cake is mainly used to the flocculant purifying as water.
At present, have no other application of the oil cake after moringa seeds oil expression, especially have no the technology report of the application aspect production of cigarettes.
Summary of the invention
The technical problem to be solved in the present invention is the reutilization technology deficiency for the oil cake after moringa seeds oil expression, and the application in cigarette filter rod of extract based on described oil cake is provided.
Another technical problem that the present invention will solve is to provide the preparation method of described cigarette filter rod.
A present invention also technical problem that will solve is to provide the filter stick of having applied moringa seeds oil cake extract.
Object of the present invention is achieved by the following technical programs:
The application of moringa seeds extract in cigarette filter rod is provided, moringa seeds extract is joined by adding the mode of essence and flavoring agent in the filter stick of cigarette, applied amount is: in the filter core of every filter stick, add 5～20 microlitre moringa seeds extracts.
The preparation method of described moringa seeds extract is: get the moringa seeds oil cake after oil expression, obtain by ethanol water or water extraction.
In the time that solvent is ethanol water, the volume by volume concentration of ethanol is preferably 50～99%, and preferably 70%.The temperature of alcohol extract is 50～70 DEG C, and the time of extraction is 0.5～2 hour, and extraction time is 2～4 times.
Preferably, the consumption of described ethanol water is that 15～25:1 determines according to: the mass ratio of ethanol water and moringa seeds oil cake.Preferably, the mass ratio of ethanol water and moringa seeds oil cake is 20:1.
Most preferably, adopt the condition of the extraction moringa seeds oil cake of ethanol water to be: the volume by volume concentration of ethanol is 70%, and consumption is that the mass ratio of ethanol water and moringa seeds oil cake is 20:1, and the temperature of extraction is 60 DEG C, the time of extracting is 0.5 hour, and extraction time is 3 times.
In the time that extraction solvent is water, the temperature of extraction is 60～80 DEG C, and the time of extraction is 1～2 hour, and extraction time is 2～4 times.
Preferably, extracting the water of use and the mass ratio of moringa seeds oil cake is 5～10:1.Preferably 5:1.
The most preferably, while adopting water to prepare moringa seeds oil cake extract for extracting solvent, the temperature of extraction is 70 DEG C, and the time of extraction is 0.5 hour, and extraction time is 3 times, and the mass ratio of water and moringa seeds oil cake is 5:1.
Described moringa seeds oil cake can adopt castaway slag or the moringa seeds powder after conventional moringa seeds oil expression.
Preferably, the preparation method who the invention provides moringa seeds oil cake is as follows: get shelling moringa seeds, under the condition of 40～50 DEG C of pressing temperatures, 40～60MPa squeeze pressure, squeeze 3～6 times, squeeze 20～30 min at every turn, obtain moringa seeds oil cake.Squeeze oil ben can reserve for other use.
Preferably, the preparation method of described moringa seeds oil cake is: fresh Moringa seed (moringa seeds) is rinsed well to natural air drying.Get the shelling moringa seeds of a certain amount of (1～2kg), wrap the squeezing thorax that has vertical fuel-displaced gap of putting into Korean style hydraulic oil press with white Kanakin, be increased to gradually under the condition of 40～60MPa squeezing 20～30 min, afterwards release in 40～50 DEG C of pressing temperatures, squeezing gun pressure power, in squeezing thorax, take out the moringa seeds bag of compacting, by after its manual loosening, again put into squeezing thorax and squeeze, so squeeze 3～6 times, obtain moringa seeds oil cake, squeeze oil ben reserve for other use.
The preferred acetate fiber of material of the filter core of described filter stick.
Further, the invention provides a kind of method of preparing the cigarette filter rod that contains moringa seeds extract, comprise the following steps:
S1. adopt ethanol water or water extraction to get the oil cake after moringa seeds oil expression, obtain moringa seeds ethanol extract or moringa seeds aqueous extract;
S2. S1 gained moringa seeds ethanol extract or moringa seeds aqueous extract are joined in the material for core of cigarette filter rod, obtain filter stick according to conventional method parcel forming paper etc.
S1 gained moringa seeds ethanol extract or moringa seeds aqueous extract are joined to cigarette filter rod can add by the injection of essence and flavoring agent injector.
In the time that solvent is ethanol water, the volume by volume concentration of ethanol is preferably 50～99%, and preferably 70%.The temperature of alcohol extract is 50～70 DEG C, and the time of extraction is 0.5～2 hour, and extraction time is 2～4 times.
Preferably, the consumption of described ethanol water is that 15～25:1 determines according to: the mass ratio of ethanol water and moringa seeds.Preferably, the mass ratio of ethanol water and moringa seeds is 15:1.
Most preferably, adopt the condition of the extraction moringa seeds oil cake of ethanol water to be: the volume by volume concentration of ethanol is 70%, and consumption is that the mass ratio of ethanol water and moringa seeds is 15:1, and the temperature of extraction is 60 DEG C, the time of extracting is 0.5 hour, and extraction time is 3 times.
In the time that extraction solvent is water, the temperature of extraction is 60～80 DEG C, and the time of extraction is 1～2 hour, and extraction time is 2～4 times.
Preferably, extracting the water of use and the mass ratio of moringa seeds oil cake is 5～10:1.Preferably 5:1.
The most preferably, while adopting water level extraction solvent to prepare moringa seeds oil cake extract, the temperature of extraction is 70 DEG C, and the time of extraction is 0.5 hour, and extraction time is 3 times, and the mass ratio of water and moringa seeds oil cake is 5:1.
The invention provides the filter stick containing moringa seeds (oil cake) extract.
The invention has the beneficial effects as follows:
The present invention by special fragrance, there is stronger adsorption function and oral cavity and return sweet moringa seeds extract and join in cigarette filter rod, both can enrich the fragrance of cigarette, increase returning of oral cavity sweet, can increase again the adsorption capacity of filter stick, thereby further reduce the harm of cigarette, thereby prepare the cigarette product of high-quality.The application of a kind of moringa seeds extract in cigarette filter rod is provided, expanded the range of application of moringa seeds extract.
2. the present invention contains moringa seeds extract and is added into cigarette filter rod, can adopt existing cigarette flavors to add equipment, does not need to change existing production technology production line, and technique is simple, and operability is high, has important practical extending application value.
Detailed description of the invention
Further describe the present invention below in conjunction with the drawings and specific embodiments.Unless stated otherwise, reagent, equipment and the method that the present invention adopts is the conventional commercial reagent of the art, equipment and the conventional method using.
Described moringa seeds oil cake can adopt castaway slag or the moringa seeds powder after conventional moringa seeds oil expression.In the embodiment of the present invention, provide the preparation method of moringa seeds oil cake as follows:
Fresh moringa seeds (market purchasing) is rinsed well to natural air drying.Get the shelling moringa seeds of a certain amount of (1～2kg), wrap the squeezing thorax that has vertical fuel-displaced gap of putting into Korean style hydraulic oil press with white Kanakin, be increased to gradually under the condition of 40～60MPa squeezing 20～30 min, afterwards release in 40～50 DEG C of pressing temperatures, squeezing gun pressure power, in squeezing thorax, take out the moringa seeds bag of compacting, by after its manual loosening, again put into squeezing thorax and squeeze, so squeeze 3～6 times, obtain moringa seeds oil cake, squeeze oil ben reserve for other use.
Embodiment 1
S1. the preparation of moringa seeds ethanol extract: get moringa seeds oil cake, the ethanol water using volume by volume concentration as 70% is as extractant, and is 1:20 by solid-liquid ratio, and temperature is 60 DEG C, extracts 3 times, and each 0.5h, obtains moringa seeds ethanol extract.
S2. by S1 gained moringa seeds ethanol extract by essence and flavoring agent injector (existing routine? each cigarette factory has, and within one minute, can complete a cigarette.Large-scale production can consider extract to be applied in fibroin, makes filter stick.) join in the filter stick of 20cm, applied amount 10 microlitres, to obtain final product.
Embodiment 2
S1. the preparation of moringa seeds ethanol extract: get moringa seeds oil cake, the ethanol water using volume by volume concentration as 90% is as extractant, and is 1:20 by solid-liquid ratio, and temperature is 60 DEG C, extracts 3 times, and each 0.5h, obtains moringa seeds ethanol extract.
S2. S1 gained moringa seeds ethanol extract is joined in filter stick by essence and flavoring agent injector, applied amount 15 microlitres, to obtain final product.
Embodiment 3
S1. the preparation of moringa seeds ethanol extract: get moringa seeds oil cake, the ethanol water using volume by volume concentration as 70% is as extractant, and is 1:20 by solid-liquid ratio, and temperature is 60 DEG C, extracts 3 times, and each 0.5h, obtains moringa seeds ethanol extract.
S2. S1 gained moringa seeds ethanol extract is joined in filter stick by essence and flavoring agent injector, applied amount 5 microlitres, to obtain final product.
Embodiment 4
S1. the preparation of moringa seeds ethanol extract: get moringa seeds oil cake, the ethanol water using volume by volume concentration as 70% is as extractant, and is 1:15 by solid-liquid ratio, and temperature is 60 DEG C, extracts 4 times, and each 0.5h, obtains moringa seeds ethanol extract.
S2. S1 gained moringa seeds ethanol extract is joined in filter stick by essence and flavoring agent injector, applied amount 20 microlitres, to obtain final product.
Embodiment 5
S1. the preparation of moringa seeds aqueous extract: get moringa seeds oil cake, make extractant with pure water, solid-liquid ratio 1:5, temperature is 70 DEG C, extracts 3 times, each 0.5h, obtains moringa seeds aqueous extract.
S2. S1 gained moringa seeds aqueous extract is joined by essence and flavoring agent injector in the filter stick of cigarette, applied amount 10 microlitres, to obtain final product.
Embodiment 6
S1. the preparation of moringa seeds aqueous extract: get moringa seeds oil cake, make extractant with pure water, solid-liquid ratio 1:5, temperature is 70 DEG C, extracts 3 times, each 0.5h, obtains moringa seeds aqueous extract.
S2. S1 gained moringa seeds aqueous extract is joined by essence and flavoring agent injector in the filter stick of cigarette, applied amount 15 microlitres, to obtain final product.
Embodiment 7
S1. the preparation of moringa seeds aqueous extract: get moringa seeds oil cake, make extractant with pure water, solid-liquid ratio 1:10, temperature is 70 DEG C, extracts 3 times, each 0.5h, obtains moringa seeds aqueous extract.
S2. S1 gained moringa seeds aqueous extract is joined by essence and flavoring agent injector in the filter stick of cigarette, applied amount 20 microlitres, to obtain final product.
Embodiment 8
S1. the preparation of moringa seeds aqueous extract: get moringa seeds oil cake, make extractant with pure water, solid-liquid ratio 1:8, temperature is 70 DEG C, extracts 3 times, each 0.5h, obtains moringa seeds aqueous extract.
S2. S1 gained moringa seeds aqueous extract is joined by essence and flavoring agent injector in the filter stick of cigarette, applied amount 5 microlitres, to obtain final product.
Embodiment 9 sensory evaluations
The contrast of smokeing panel test of the cigarette that adopts the filter tip that contains moringa seeds extract that obtains of embodiment 1～8 and the cigarette that contains conventional filter tip, after being smoked panel test, on average gives a mark as shown in table 1 below by 10 test and appraisal persons.
Table 1 is inhaled evaluation and test test result
Fragrance performance and the pleasant impression of embodiment 1～4 can better, and the doing very well of the reduction of embodiment 5～8 stimulation.But the cigarette that embodiment 1～8 makes all has grace and pleasant Moringa is smelt perfume (or spice).After burning, smoke panel test through expert, the present invention adds the cigarette flavor of moringa seeds extract to be valued for nature, does not bring obvious non-tobacco breath into, especially embodiment 1,2,5,6, and mellow Tianjin is sweet, and tasty and refreshing jealous giving prominence to moistened in mouthfeel cleaning.
Embodiment 10 hazardous materials detect
Get the cigarette sample of embodiment 1～8 gained, carry out contrast test with the cigarette that does not add moringa seeds extract, detect with reference to the method for ISO and GB, as shown in table 2.
Table 2 becomes the detection (tar, nicotine, CO) of flue gas routine
Claims (7)
1. the application of moringa seeds extract in cigarette filter rod, it is characterized in that, moringa seeds extract is joined by adding the mode of essence and flavoring agent in the filter stick of cigarette, addition is: in the filter core of the filter stick of every cigarette, add 5～20 microlitre moringa seeds extracts, the preparation method of described moringa seeds extract is: get the moringa seeds oil cake after oil expression, obtain by ethanol water or water extraction.
2. application according to claim 1, is characterized in that, the preparation method of described moringa seeds extract is: get the moringa seeds oil cake after oil expression, extract and obtain with ethanol water; The volume by volume concentration of described ethanol water is 50～99%, and the temperature of extraction is 50～70 DEG C, and the time of extraction is 0.5～2 hour, and extraction time is 2～4 times.
3. application according to claim 2, is characterized in that, the consumption of described ethanol water is that 15～25:1 determines according to: the mass ratio of ethanol water and moringa seeds oil cake.
4. application according to claim 2, is characterized in that, the volume by volume concentration of described ethanol water is 50-99%, consumption is that the mass ratio of ethanol water and moringa seeds oil cake is 15-25:1, the temperature of extracting is 50-70 DEG C, and the time of extraction is 0.5 hour, and extraction time is 3 times.
5. application according to claim 1, is characterized in that, the preparation method of described moringa seeds extract is: get the moringa seeds oil cake after oil expression, water extracts and obtains; The temperature of extracting is 60～80 DEG C, and the time of extraction is 1～2 hour, and extraction time is 2～4 times.
6. application according to claim 5, is characterized in that, the mass ratio of the water of described extraction use and moringa seeds oil cake is 5～10:1.
7. according to the application described in claim 1 to 6 any one, it is characterized in that, the preparation method of described moringa seeds oil cake is as follows: get shelling moringa seeds, under the condition of 40～50 DEG C of pressing temperatures, 40～60MPa squeeze pressure, squeeze 3～6 times, each squeezing 20～30min, obtains moringa seeds oil cake.
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| CN104687246B (en) * | 2015-01-05 | 2018-08-17 | 云南中烟工业有限责任公司 | A kind of Moringa porous particle, preparation method and the cigarette filter rod containing the porous particle |
| CN104957763A (en) * | 2015-06-17 | 2015-10-07 | 云南中烟工业有限责任公司 | Moringa glycerol triacetate extractive and application of moringa glycerol triacetate extractive in cigarette |
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| US20060222682A1 (en) * | 2005-03-18 | 2006-10-05 | Andrews David A | Nutraceutical Moringa composition |
| WO2009066303A2 (en) * | 2007-11-22 | 2009-05-28 | Ganga Raju Gokaraju | New synergistic phytochemical composition for the treatment of obesity |
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Non-Patent Citations (4)
| Title |
|---|
| BeyeneHagosAregawi等.REMOVALOFNi(II)FROMAQUEOUSSOLUTIONUSINGLEAF BARK AND SEED OF MORINGA STENOPETALA ADSORBENTS.《Bulletin of the Chemical Society of Ethiopia》.2013 |
| Comparison of antioxidant activity of Moringa oleifera and selected vegetables in South Africa;Vusumzi Pakade等;《South African Journal of Science》;20130327;第109卷(第3/4期);全文 * |
| REMOVAL OF Ni(II) FROM AQUEOUS SOLUTION USING LEAF, BARK AND SEED OF MORINGA STENOPETALA ADSORBENTS;Beyene Hagos Aregawi等;《Bulletin of the Chemical Society of Ethiopia》;20130430;第27卷(第1期);第35-47页 * |
| Vusumzi Pakade等.Comparison of antioxidant activity of Moringa oleifera and selected vegetables in South Africa.《South African Journal of Science》.2013,第109卷(第3/4期),全文. |
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