CN110226774A - A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling - Google Patents
A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling Download PDFInfo
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- CN110226774A CN110226774A CN201910600952.XA CN201910600952A CN110226774A CN 110226774 A CN110226774 A CN 110226774A CN 201910600952 A CN201910600952 A CN 201910600952A CN 110226774 A CN110226774 A CN 110226774A
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- cigarette
- pearl
- dry
- dry pearl
- sea
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
- A24D1/042—Cigars; Cigarettes with mouthpieces or filter-tips with mouthpieces
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling, the mouth stick base circumference is 24mm, and tow middle section is loaded with the dry pearl of a 3.25 ± 0.15mm of diameter, dry pearl is using zeolite molecular sieve as primary raw material, it is prepared through pelletizing, attached fragrant, moulding process, the sea-buckthorn composite extract for promoting cigarette sweet moisture feeling is adsorbed on dry pearl, due to the porous structure of dry pearl, during smoking property of cigarette, essence is slowly uniformly discharged with flue gas, without burning, increase the diversity for sucking mouthfeel, while the effect for sweetening and increasing profit can be brought.
Description
Technical field
The present invention relates to essence spice for cigarette field, in particular to a kind of cigarette that can promote cigarette sweet moisture feeling does Zhu Zui
Stick.
Background technique
In tobacco business, the development of cigarette solid meat flavor formulating technology is swift and violent, the new method, new technology especially in cigarette filter tip
Exploitation, including the quick-fried pearl of cigarette, microcapsules, nano particle, powdered granule etc..Currently, by the inspection of consumer market, cigarette is quick-fried
The whole acceptance of pearl is preferable, and the additives such as microcapsules, nano particle, powdered granule easily cause consumption since particle is tiny
Person's sucks safety concerns.However, there is also certain drawbacks for the addition of the quick-fried pearl of cigarette, dripping pill, it is low including ratio of briquetting, at
The problems such as this is higher, and there are micro bad smells by quick-fried pearl, dripping pill solvent olive oil, ODO etc., so that quick-fried pearl is mainly used for wrapping up
The flavors and fragrances of the fragrance such as ginseng, peppermint advantage, and miscellaneous gas is more obvious when the use of other kinds of flavors and fragrances, affects pumping
Inhale experience.Although the prior art has the cigarette filter tip prepared with silica gel perfume (or spice) pearl or zeolite perfume (or spice) pearl, these fragrant pearls are on the one hand
Preparation process is unstable, and ratio of briquetting is low, on the other hand due to the limitation of its fragrant pearl microstructure, it is difficult to which release of upper time fragrance reaches
To slow releasing function.
Sea-buckthorn, nutriment and bioactive substance rich in have effects that cough-relieving, resolving sputum, relieving asthma, although existing
There is technology to there is trial to be added into sea-buckthorn as cigarette flavors in cigarette holder filter stick, but due to its sour-puckery flavor, suction is experienced always not
It is good.Therefore, it is also desirable to develop and the astringent taste ingredient in sea-buckthorn is removed and retains its flavor component, and keep its flue gas soft sweet
Method.
Summary of the invention
In view of the above technical problems, it is adsorbed with the present invention provides a kind of with the sea-buckthorn compound collecting for sweetening increasing profit effect
The novel dry pearl of object is applied in cigarette filter tip, since this dry pearl is not involved in burning, on the one hand, acid sea-buckthorn naturally mentions
It takes object to can be used for neutralizing cigarette smoke pH, plays the role of reducing cigarette stimulation, on the other hand, the extracts such as sea-buckthorn and dandelion
In small-molecule substance enter throat with cigarette smoke, can play the role of promoting cigarette sweet moisture feeling, and this use
The dry pearl of zeolite of specific process preparation can be very good to adsorb and fixed fragrance, when suction fragrance can stablize it is lasting distribute, tie up
Hold suction experience pleasant for a long time.
The present invention provides a kind of dry pearl mouth sticks of cigarette that can promote cigarette sweet moisture feeling, which is characterized in that the cigarette mouth
Stick base circumference perimeter 24mm is loaded with the dry pearl of a 3.25 ± 0.15mm of diameter in tow middle section, and dry pearl is with zeolite molecules
Sieve is primary raw material, is prepared through pelletizing, attached fragrant, moulding process, the sea-buckthorn that promotion cigarette sweet moisture feeling is adsorbed on dry pearl is multiple
Close extract.
The present invention also provides the preparation methods of the dry pearl mouth stick of the cigarette that can promote cigarette sweet moisture feeling, which is characterized in that institute
State method the following steps are included:
1) pelletizing: taking a certain amount of zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content 25~
50%) the two is uniformly mixed by=2:1~5 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out 2~6h of calcining by the qualified samples of 0.15mm at 1000~1300 DEG C, and washing, drying are made with more
The dry pearl of pore structure；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:1~4, and sealing is placed in 150
Rev/min the attached fragrant 6~12h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, 40~50
DEG C air-dry 2~4h, attached smoked bean curd pearl is made；
3) mouth stick form: by attached smoked bean curd pearl be added to cigarette mouth stick tow middle section molding to get.
Preferably, the sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, pulp is squeezed into juice, subsequent addition 0.1%~0.2% pectase of Hippophae Rhamnoides L. juice quality,
0.05%~0.1% flavor protease, constant temperature digest 0.5~4h, and temperature is 40~50 DEG C, obtain sea-buckthorn zymolyte；Further, excellent
0.1% pectase, 0.05% flavor protease are selected, 40~45 DEG C of hydrolysis temperature best.
2) according to 100:10~20:2~5:1~2 mass ratio by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco
Extract, dandelion extract are uniformly mixed, and are added bacillus, are carried out fermentation 4~10 days to fermentation substrate, obtain composite fermentation
Liquid.
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get sea-buckthorn is compound
Take object.
Saliva bar tobacco extract of the present invention, Sun cured tobacco extract, dandelion extract can be by commercially available acquisitions, also
It can make by oneself, preferably medicinal extract class extract, additive amount is preferred with 100:10~15:2~4:1~2.
Pectase and flavor protease of the present invention are commercially available to be bought.
Further, the zeolite molecular sieve model is preferably one of 4A, 5A type, Y type.
Further, the solid content of the silica solution preferably 30~40%.
Preferably, the bacillus is bacillus BA-01, and separation screening has preferable flavouring from tobacco leaf surface
Energy.
Bacillus BA-01 of the present invention, systematic name Bacillus amyloliquefaciens, depositary institution
For China Tobacco Jiangxi Industrial LLC, preservation date on April 26th, 2017, it is preserved in Guangdong Province's Microbiological Culture Collection
The heart, deposit number are GDMCC No.60171.Depositary institution address is No. 59 building of the compound of XianLie Middle Road, GuangZhou City, GuangDong Province 100
5 buildings.
Preferably, the attached fragrant rate of the dry pearl is controlled 15~30%, wherein attached perfume rate=(it is attached it is fragrant after the attached perfume (or spice) of weight-
Preceding weight)/it is attached it is fragrant before weight.
Preferably, the dry pearl is in microcosmic porous structure, and average pore size is in 0.5~1nm, and attached fragrant and sustained release performance is more
It is excellent.
Compared with prior art, advantages of the present invention and generation good effect are:
1) the dry pearl in the mouth stick is in porous structure, has the absorption of good essence and sustained release performance, is capable of providing persistently
Stable flavouring experience.
2) hippophae rhamnoides, saliva bar tobacco, Sun cured tobacco grass and dandelion extract compounding are prepared into sea-buckthorn and answered by the present invention
Extract is closed, is sustained in cigarette smoking, due to being not involved in burning, on the one hand, acid natural extract can be used for neutralizing cigarette
Flue gas pH plays the role of reducing cigarette stimulation, on the other hand, small-molecule substance in the extracts such as dandelion, sea-buckthorn with
Cigarette smoke enters throat, can play the role of promoting cigarette sweet moisture feeling, and the cigarette of its fragrance and saliva bar tobacco, Sun cured tobacco grass
Hay-scented mixes reconciliation well, and for the flue gas finally generated without astringent sense, aromatic flavour is sweet.
3) sea-buckthorn composite extract so that the sour-sweet fragrance of the extract is prominent, and is had using enzymatic hydrolysis, composite fermentation technique
The graceful tobacco aroma of hair thoroughly, can coordinate with cigarette cigarette perfume.
4) the mouth stick circumference circle is 24mm, and the tow middle section of the mouth stick is loaded with the attached of a 3.25 ± 0.15mm of diameter
Smoked bean curd pearl, the dry pearl are prepared with zeolite molecular sieve, silica solution, relative to directlying adopt zeolite little particle, microcapsules more
Safely, fragrant stabilization is held, adsorption effect is prepared by technique of the present invention and is better than the prior art, avoids consumer to charcoal
The tiny additive such as powder, silica white, zeolite powder, cyclodextrin granule sucks safety concerns；
5) compared with the quick-fried pearl of traditional cigarette, dripping pill, without pinching brokenly fragrant pearl when consumer sucks cigarette, solvent-free exudation makes
With safer convenience.
Detailed description of the invention
Fig. 1 is cigarette filter tip schematic diagram；
In figure: 1- filter stick aspiration end, the dry pearl of 2-, 3- cigarette bobbin paper, 4- pipe tobacco.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1
The dry pearl mouth stick of cigarette is prepared as follows, comprising the following steps:
1) pelletizing: taking a certain amount of Y-type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
50%) the two is uniformly mixed by=2:3 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:2, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 4h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 24mm to get.
Wherein, sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, 0.1% pectase of Hippophae Rhamnoides L. juice quality, 0.05% flavor is then added at juice in pulp squeezing
Protease, constant temperature digest 2h, and temperature is 40 DEG C, obtain sea-buckthorn zymolyte；
2) according to the mass ratio of 100:10:2:1 by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco extract, Pu Gong
English extract is uniformly mixed, and adds the Lyceum bacillus of substrate quality 0.5%, is carried out fermentation 5 days to fermentation substrate, is obtained compound
Fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, and the 1,2-PD that concentrate quality 20% is added mentions to get sea-buckthorn is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.72nm, and attached perfume rate is 19.9%.
Embodiment 2
The dry pearl mouth stick of cigarette is prepared as follows, comprising the following steps:
1) pelletizing: taking a certain amount of 5A type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
25%) the two is uniformly mixed by=2:3 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:2, sealing, be placed in 150 turns/
Point the attached perfume 6h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, in 40~50 DEG C of air-dried 4h,
Attached smoked bean curd pearl is made；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 24mm to get.
Wherein, sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, 0.1% pectase of Hippophae Rhamnoides L. juice quality, 0.1% flavor egg is then added at juice in pulp squeezing
White enzyme, constant temperature digest 4h, and temperature is 45 DEG C, obtain sea-buckthorn zymolyte；
2) according to the mass ratio of 100:20:3:2 by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco extract, Pu Gong
English extract is uniformly mixed, and adds the bacillus pumilus of substrate quality 0.1%, is carried out fermentation 5 days to fermentation substrate, is obtained compound
Fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get sea-buckthorn is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.77nm, and attached perfume rate is 21.5%.
Embodiment 3
The dry pearl mouth stick of cigarette is prepared as follows, comprising the following steps:
1) pelletizing: taking a certain amount of ZSM-5 type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (admittedly contain
The two is uniformly mixed by amount 35%)=2:3 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:3, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 4h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 24mm to get.
Wherein, sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, pulp is squeezed into juice；0.1% pectase of Hippophae Rhamnoides L. juice quality, 0.1% flavor egg is then added
White enzyme, constant temperature digest 4h, and temperature is 45 DEG C, obtain sea-buckthorn zymolyte；
2) according to the mass ratio of 100:20:3:2 by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco extract, Pu Gong
English extract is uniformly mixed, and adds the bacillus subtilis of substrate quality 0.1%, is carried out fermentation 5 days to fermentation substrate, is obtained compound
Fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get sea-buckthorn is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.82nm, and attached perfume rate is 18.7%.
Embodiment 4
The dry pearl mouth stick of cigarette is prepared as follows, comprising the following steps:
1) pelletizing: taking a certain amount of Y-type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
35%) the two is uniformly mixed by=1:1 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:2, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 4h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 24mm to get.
Wherein, sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, 0.1% pectase of Hippophae Rhamnoides L. juice quality, 0.1% flavor egg is then added at juice in pulp squeezing
White enzyme, constant temperature digest 4h, and temperature is 45 DEG C, obtain sea-buckthorn zymolyte；
2) according to the mass ratio of 100:20:3:2 by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco extract, Pu Gong
English extract is uniformly mixed, and adds bacillus BA-01 (preservation date on April 26th, 2017, the preservation of substrate quality 0.5%
In Guangdong Province's Culture Collection, deposit number is GDMCC No.60171), fermentation 5 days is carried out to fermentation substrate, is obtained
Composite fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get sea-buckthorn is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.55nm, and attached perfume rate is 26.4%.
Embodiment 5
The dry pearl mouth stick of cigarette is prepared as follows, comprising the following steps:
1) pelletizing: taking a certain amount of 5A type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
35%) the two is uniformly mixed by=2:5 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out calcining 2h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:2, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 4h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 24mm to get.
Wherein, sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, 0.1% pectase of Hippophae Rhamnoides L. juice quality, 0.1% flavor egg is then added at juice in pulp squeezing
White enzyme, constant temperature digest 4h, and temperature is 45 DEG C, obtain sea-buckthorn zymolyte；
2) according to the mass ratio of 100:20:3:2 by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco extract, Pu Gong
English extract is uniformly mixed, and adds bacillus BA-01 (preservation date on April 26th, 2017, the preservation of substrate quality 0.25%
In Guangdong Province's Culture Collection, deposit number is GDMCC No.60171), fermentation 5 days is carried out to fermentation substrate,
Obtain composite fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, and the 1,2-PD that concentrate quality 20% is added mentions to get sea-buckthorn is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.71nm, and attached perfume rate is 22.7%.
Embodiment 6
The dry pearl mouth stick of cigarette is prepared as follows, comprising the following steps:
1) pelletizing: taking a certain amount of 4A type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
30%) the two is uniformly mixed by=1:2 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 3.25 ±
Pearl green body is carried out calcining 6h by the qualified samples of 0.15mm at 1200 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:2, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 4h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 24mm to get.
Wherein, sea-buckthorn composite extract preparation method the following steps are included:
1) after cleaning sea-buckthorn, 0.1% pectase of Hippophae Rhamnoides L. juice quality, 0.1% flavor egg is then added at juice in pulp squeezing
White enzyme, constant temperature digest 1h, and temperature is 45 DEG C, obtain sea-buckthorn zymolyte；
2) according to the mass ratio of 100:10:2:1 by sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco extract, Pu Gong
English extract is uniformly mixed, and adds bacillus BA-01 (preservation date on April 26th, 2017, the preservation of substrate quality 0.1%
In Guangdong Province's Culture Collection, deposit number is GDMCC No.60171), fermentation 5 days is carried out to fermentation substrate, is obtained
Composite fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get sea-buckthorn is compound
Take object.
Comparative example 1
1) after cleaning sea-buckthorn, 75% ethanol solution of 5 times of amounts, 70 DEG C of heating and refluxing extractions 2 are added at juice in pulp squeezing
Secondary, combined extract is condensed into medicinal extract, and the 1,2-PD of concentrate quality 20% is added, obtains hippophae rhamnoides；
1) calcium chloride of extract quality 30% is added in hippophae rhamnoides, is uniformly mixing to obtain fragrance solution, takes one
Quantitative 5A zeolite molecular sieve carries out calcining 6h at 1300 DEG C, and then washing, drying are added in fragrance solution, sealing is set
In the attached perfume 12h of 150 revs/min of shaking tables, it is then allowed to stand 12h, in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
2) the attached equiponderant attached smoked bean curd pearl of smoked bean curd pearl prepared with embodiment 1 is taken, base circumference perimeter is added to
In the tow of 24mm cigarette filter tip to get.
Through detecting, the average pore size of dry pearl is 0.68nm, and attached perfume rate is 12.4%.
Comparative example 2
1) a certain amount of 4A zeolite molecular sieve is taken, after grinding, according to zeolite molecular sieve: silica solution (solid content 25%)=2:
The two is uniformly mixed by 1 mass ratio, is placed in pelletizer and is carried out roller forming, and the qualification of 3.25 ± 0.15mm of diameter is screened
Pearl green body is carried out calcining 6h by sample at 800 DEG C, and dry pearl is made in washing, drying；
2) after cleaning sea-buckthorn, 75% ethanol solution of 5 times of amounts, 70 DEG C of heating and refluxing extractions 2 are added at juice in pulp squeezing
Secondary, combined extract is condensed into medicinal extract, and the 1,2-PD of concentrate quality 20% is added, obtains hippophae rhamnoides；
3) dry pearl and hippophae rhamnoides are uniformly mixed according to the mass ratio of 1:2, seal, it is attached is placed in 150 revs/min of shaking table
Fragrant 12h, is then allowed to stand 12h, and in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
4) the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette is formed, the mouth stick base circumference perimeter of cigarette
24mm to get.
Through detecting, the average pore size of dry pearl is 0.76nm, and attached perfume rate is 18.8%.
Comparative example 3
1) a certain amount of 5A zeolite molecular sieve is taken, after grinding, according to zeolite molecular sieve: silica solution (solid content 30%)=2:
The two is uniformly mixed by 5 mass ratio, is placed in pelletizer and is carried out roller forming, and the qualification of 3.25 ± 0.15mm of diameter is screened
Pearl green body is carried out calcining 4h by sample at 1200 DEG C, and dry pearl is made in washing, drying；
2) after cleaning sea-buckthorn, pulp is squeezed at juice, by Hippophae Rhamnoides L. juice, saliva bar tobacco extract, Sun cured tobacco extract and Pu
Public English extract is uniformly mixed according to the mass ratio of 100:10:5:2, adds 0.1% cellulolytic enzyme, 0.1% composite plant
Protease, 35 DEG C ferment 5 days, obtain composite fermentation liquid,
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get sea-buckthorn is compound
Take object；
4) dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:2, are sealed, be placed in 150 revs/min and shake
The attached perfume 12h of bed, is then allowed to stand 12h, in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
5) the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette is formed, the mouth stick base circumference perimeter of cigarette
24mm to get.
Through detecting, the average pore size of dry pearl is 0.74nm, and attached perfume rate is 21.9%.
Test effect:
It is applied in cigarette via the dry pearl mouth stick of cigarette made from Examples 1 to 6 and comparative example 1~3, and not using dry
Regular-size cigarette made from pearl mouth stick is control sample.Tissue has the smoke panel test expert of qualification of national cigarette and inhales five ginsengs of group is commented to shine
GB5606.4-2005 " the 4th part of cigarette: sense organ technical requirements " and YC/T 497-2014 " cigarette Chinese-style cigarette style sense organ
Evaluation method " it smokes panel test to using cigarette made from 1~6 mouth stick of the embodiment of the present invention, it the results are shown in Table 1.
1 cigarette sensory evaluation result of table
Using the dry pearl mouth rod product of the cigarette of the embodiment of the present invention 1~6 compared with control sample, " sour-sweet taste " style is brighter
Aobvious, the abundant degree of fragrance obviously increases, and moisture feeling is promoted.Using cigarette highest scoring made from 6 mouth stick of embodiment, mainly
Reason is that sea-buckthorn composite extract is more coordinated with cigarette odor-absorbing, and the sustained release performance of solid-state perfume (or spice) pearl is best.
Above-described embodiment is only more excellent embodiment of the invention, is implemented according to the technical essence of the invention to above
Any simple modification and alternate variation that example is made, belong to technical solution of the present invention range.
Claims (8)
1. a kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling, it is characterised in that the cigarette filter tip base circumference perimeter
24mm is loaded with the dry pearl of a 3.25 ± 0.15mm of diameter in tow middle section, and dry pearl is using zeolite molecular sieve as primary raw material, warp
Pelletizing, attached fragrant, moulding process are prepared, and the sea-buckthorn composite extract for promoting cigarette sweet moisture feeling is adsorbed on dry pearl.
2. the preparation method of the cigarette dry pearl mouth stick according to claim 1 that cigarette sweet moisture feeling can be promoted, it is characterised in that
It the described method comprises the following steps:
1) pelletizing: taking a certain amount of zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content 25~50%)
The two is uniformly mixed by the mass ratio of=2:1~5, is placed in pelletizer and is carried out roller forming, and 3.25 ± 0.15mm of diameter is screened
Qualified samples, pearl green body is subjected to 2~6h of calcining at 1000~1300 DEG C, washing, drying, being made has porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and sea-buckthorn composite extract are uniformly mixed according to the mass ratio of 1:1~4, and sealing is placed in 150 revs/min
The attached fragrant 6~12h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, 40~50 DEG C air-dry 2
Attached smoked bean curd pearl is made in~4h；
3) mouth stick form: by attached smoked bean curd pearl be added to cigarette mouth stick tow middle section molding to get.
3. the preparation method of the cigarette dry pearl mouth stick according to claim 2 that cigarette sweet moisture feeling can be promoted, it is characterised in that
The preparation method of the sea-buckthorn composite extract the following steps are included:
1) after sea-buckthorn being cleaned, pulp squeezing at juice, be then added 0.1%~0.2% pectase of Hippophae Rhamnoides L. juice quality, 0.05%~
0.1% flavor protease, constant temperature digest 0.5~4h, and temperature is 40~50 DEG C, obtain sea-buckthorn zymolyte；
2) sea-buckthorn zymolyte, saliva bar tobacco extract, Sun cured tobacco are extracted according to 100:10~20:2~5:1~2 mass ratio
Object and dandelion extract are uniformly mixed, and are added bacillus, are carried out fermentation 4~10 days to fermentation substrate, obtain composite fermentation liquid；
3) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, is concentrated under reduced pressure
It is 1.05~1.10g/cm to medicinal extract density3, the 1,2-PD of concentrate quality 20% is added to get sea-buckthorn compound collecting
Object.
4. the preparation method of the cigarette dry pearl mouth stick according to claim 2 that cigarette sweet moisture feeling can be promoted, it is characterised in that
One of the zeolite molecular sieve model 4A type, 5A type, Y type, ZSM-5 type.
5. the preparation method of the cigarette dry pearl mouth stick according to claim 3 that cigarette sweet moisture feeling can be promoted, it is characterised in that
The bacillus is bacillus BA-01, and separation screening is from tobacco leaf surface, preservation date on April 26th, 2017, is preserved in wide
East saves Culture Collection, and deposit number is GDMCC No.60171.
6. the preparation method of the cigarette dry pearl mouth stick according to claim 3 that cigarette sweet moisture feeling can be promoted, it is characterised in that
The additive amount of the bacillus is the 0.1~0.5% of substrate quality.
7. the preparation method of the cigarette dry pearl mouth stick according to claim 2 that cigarette sweet moisture feeling can be promoted, it is characterised in that
The attached fragrant rate of the dry pearl is controlled 15~30%.
8. the preparation method of the cigarette dry pearl mouth stick according to claim 2 that cigarette sweet moisture feeling can be promoted, it is characterised in that
The dry pearl is in microcosmic porous structure, and average pore size is in 0.5~1nm.
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| CN110982625A (en) * | 2019-12-29 | 2020-04-10 | 亿利耐雀生物科技有限公司 | Licorice-flavored dried beads for cigarette filter tips and preparation method thereof |
| CN113229523A (en) * | 2021-04-26 | 2021-08-10 | 河南中烟工业有限责任公司 | Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick |
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