CN110403236A - A kind of dry pearl mouth stick of cigarette for sending out function thoroughly with promotion flue gas - Google Patents
A kind of dry pearl mouth stick of cigarette for sending out function thoroughly with promotion flue gas Download PDFInfo
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- CN110403236A CN110403236A CN201910607559.3A CN201910607559A CN110403236A CN 110403236 A CN110403236 A CN 110403236A CN 201910607559 A CN201910607559 A CN 201910607559A CN 110403236 A CN110403236 A CN 110403236A
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- Prior art keywords
- pearl
- cigarette
- dry
- dry pearl
- flue gas
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
- A24D1/042—Cigars; Cigarettes with mouthpieces or filter-tips with mouthpieces
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Abstract
The invention discloses a kind of dry pearl mouth sticks of cigarette for sending out function thoroughly with promotion flue gas, the mouth stick base circumference is 19.8mm, and tow middle section is loaded with the dry pearl that a diameter is 2.75 ± 0.15mm, dry pearl is using zeolite molecular sieve as primary raw material, through pelletizing, attached perfume (or spice), moulding process is prepared, it is adsorbed on dry pearl and promotes the agalloch eaglewood composite extract that flue gas sends out function thoroughly, due to the porous structure of dry pearl, during smoking property of cigarette, essence is slowly uniformly discharged with flue gas, without burning, increase the diversity for sucking mouthfeel, it can bring simultaneously and promote the effect that flue gas sends out function thoroughly.
Description
Technical field
The present invention relates to essence spice for cigarette field, in particular to a kind of dry pearl of cigarette for sending out function thoroughly with promotion flue gas
Mouth stick.
Background technique
In tobacco business, the development of cigarette solid meat flavor formulating technology is swift and violent, the new method, new technology especially in cigarette filter tip
Exploitation, including the quick-fried pearl of cigarette, microcapsules, nano particle, powdered granule etc..Currently, by the inspection of consumer market, cigarette is quick-fried
The whole acceptance of pearl is preferable, and the additives such as microcapsules, nano particle, powdered granule easily cause consumption since particle is tiny
Person's sucks safety concerns.However, there is also certain drawbacks for the addition of the quick-fried pearl of cigarette, dripping pill, it is low including ratio of briquetting, at
The problems such as this is higher, and there are micro bad smells by quick-fried pearl, dripping pill solvent olive oil, ODO etc., so that quick-fried pearl is mainly used for wrapping up
The flavors and fragrances of the fragrance such as ginseng, peppermint advantage, and miscellaneous gas is more obvious when the use of other kinds of flavors and fragrances, affects pumping
Inhale experience.Although the prior art has the cigarette filter tip prepared with silica gel perfume (or spice) pearl or zeolite perfume (or spice) pearl, these fragrant pearls are on the one hand
Preparation process is unstable, and ratio of briquetting is low, on the other hand due to the limitation of its fragrant pearl microstructure, it is difficult to which release of upper time fragrance reaches
To slow releasing function.
Agalloch eaglewood, rare spice berry apply the research in cigarette more and more popular for agalloch eaglewood in recent years, application
Mode mainly include 1) aloes powder directly add in mouth stick, 2) added in cigarette shreds in the form of flavoring by linaloe oil,
3) it is added in mouth stick in the form of dripping pill.Although the exploitation of agalloch eaglewood class essence is increasingly rich with the research progress in new material
Richness, but since agalloch eaglewood fragrance is gentle and refined long, not like the fragrance such as peppermint advantage, thus it is how miscellaneous in the inhibition of its fragrance of cigarette saliency
Gas, promoting flue gas and sending out function thoroughly is always problem urgently to be resolved.
Summary of the invention
In view of the above technical problems, the present invention provides a kind of novel dry pearl for sending out function thoroughly with promotion flue gas, applications
In cigarette filter tip, on the one hand, extract preparation agalloch eaglewood composite extract using special process, avoid naturally extracting to the greatest extent
Loss of effective components and rotten in object, so that it is guaranteed that dry pearl gives off a strong fragrance, without miscellaneous gas；On the other hand, by agalloch eaglewood composite extract
It is adsorbed in the dry pearl being prepared by zeolite molecular sieve, can reach the effect of lasting stability sustained release in cigarette smoking.This hair
The dry pearl of bright the method preparation is nontoxic, and low cost, ratio of briquetting is high, without miscellaneous gas, gives off a strong fragrance and stablizes persistently.
The technical solution of the present invention is as follows:
A kind of dry pearl mouth stick of cigarette for sending out function thoroughly with promotion flue gas, which is characterized in that the cigarette filter tip bottom surface circle
Zhou Zhouchang 19.8mm is loaded with the dry pearl of a 2.75 ± 0.15mm of diameter in tow middle section, and dry pearl is based on zeolite molecular sieve
Raw material is wanted, is prepared through pelletizing, attached fragrant, moulding process, is adsorbed with to promote flue gas and send out the agalloch eaglewood of function thoroughly on dry pearl and compound mentions
Take object.
A kind of preparation method of the dry pearl mouth stick of cigarette that sending out function thoroughly with promotion flue gas, comprising the following steps:
1) pelletizing: taking a certain amount of zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content 25~
50%) the two is uniformly mixed by=2:1~5 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out 2~6h of calcining by the qualified samples of 0.15mm at 1000~1300 DEG C, and washing, drying are made with more
The dry pearl of pore structure；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 2:1~4, and sealing is placed in 150
Rev/min the attached fragrant 6~12h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, 40~50
DEG C air-dry 2~4h, attached smoked bean curd pearl is made；
3) mouth stick form: by attached smoked bean curd pearl be added to cigarette mouth stick tow middle section molding to get.
Preferably, the agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then according to 5:10~20:10~20:2~5:100 mass ratio by aloes powder,
Saliva bar leaf tobacco extract, Brazilian leaf tobacco extract, burley tobaccos extract and water are uniformly mixed, first with 0.1~0.2% composite plant
Hydrolase and 0.1~0.2% beta-glucosidase carry out 1~4h of enzymatic hydrolysis at 30~50 DEG C.After the completion of enzymatic hydrolysis, gemma is added
Bacillus carries out fermentation 4~10 days to fermentation substrate, obtains composite fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get agalloch eaglewood is compound
Take object.
Saliva bar leaf tobacco extract of the present invention, Brazilian leaf tobacco extract, burley tobaccos extract is commercially available buys, can also
It voluntarily prepares, preferably medicinal extract class extract.Preferably, aloes powder, saliva bar leaf tobacco extract, Brazilian leaf tobacco extract, white rib
The compound proportion of tobacco extract and water is preferred with 5:15~20:10~15:2~4:100 mass ratio.
Composite plant hydrolase and beta-glucosidase of the present invention are commercially available to be bought, such as Novi believes composite plant
Hydrolase Viscozyme L and beta-glucosidase HARVEY.
Zeolite molecular sieve model of the present invention is preferably one of 4A type, 5A type, Y type, ZSM-5 type.
Preferably, the bacillus is bacillus BA-01, and separation screening has preferable flavouring from tobacco leaf surface
Energy；Bacillus BA-01 of the present invention, systematic name Bacillus amyloliquefaciens, depositary institution is wide
East saves Culture Collection, and preservation address is in 5 building, the building of compound the 59th of Xianlie Middle Road, Guangzhou City 100 Guangdong Province microorganism
Research institute, preservation date on April 26th, 2017, deposit number are GDMCC No:60171.
The additive amount of bacillus is the 0.1~0.5% of substrate quality.
Preferably, the attached fragrant rate of the dry pearl is controlled 15~30%, wherein attached perfume rate=(it is attached it is fragrant after the attached perfume (or spice) of weight-
Preceding weight)/it is attached it is fragrant before weight.
The dry pearl of the method for the invention preparation is in microcosmic porous structure, it is preferred that the microcosmic porous average pore size
In 0.5~1nm, attached fragrant and sustained release performance is more excellent.
Compared with prior art, advantages of the present invention and generation good effect are:
1) the dry pearl of the method for the invention preparation is in porous structure, and aperture is fine and compact, has the absorption of good essence
And sustained release performance, it is capable of providing continual and steady flavouring experience.
2) present invention has adsorbed agalloch eaglewood composite extract using the dry pearl of zeolite preparation, slowly releases during the smoking process
Fragrance is put, is burnt due to being not involved in, the small-molecule substance in extract enters throat with cigarette smoke, can play promotion cigarette
The effect of the flue gas property sent out thoroughly.
3) agalloch eaglewood composite extract of the present invention avoids natural extract using raw material compounding, enzymatic hydrolysis, composite fermentation technique
In the effectively loss of fragrance component and rotten so that the extract agalloch eaglewood fragrance is obvious, the property sent out enhances flue gas thoroughly when suction, distributes
Graceful tobacco aroma and without miscellaneous gas, can coordinate with cigarette cigarette perfume.
4) mouth stick circumference circle of the present invention be 19.8mm, the tow middle section of the mouth stick be loaded with a diameter 2.75 ±
The attached smoked bean curd pearl of 0.15mm, the dry pearl are prepared with zeolite molecular sieve, silica solution, similar to the quick-fried pearl size of cigarette and with single pearl
Form apply in cigarette filter tip, zeolite little particle, microcapsules are safer, hold fragrant stabilization relative to directlying adopt, by this
It invents the technique and prepares adsorption effect and be better than the prior art, avoid consumer to biological powdered carbon, silica white, zeolite powder, ring
The tiny additive such as dextrin particle sucks safety concerns.
5) compared with the quick-fried pearl of traditional cigarette, dripping pill, without pinching brokenly fragrant pearl when consumer sucks cigarette, solvent-free exudation makes
With safer convenience.
Detailed description of the invention
Fig. 1 is cigarette filter tip schematic diagram；
In figure: 1- filter stick aspiration end, the dry pearl of 2-, 3- cigarette bobbin paper, 4- pipe tobacco.
Specific embodiment
The present invention is described in further detail combined with specific embodiments below.But this should not be interpreted as in the present invention
The range for stating theme is only limitted to embodiment below, all that model of the invention is belonged to based on the technology that the content of present invention is realized
It encloses.
The technical scheme in the embodiments of the invention will be clearly and completely described below.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1
The dry pearl mouth stick of cigarette is prepared by the following method:
1) pelletizing: taking a certain amount of 5A zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
25%) the two is uniformly mixed by=2:1 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out calcining 6h by the qualified samples of 0.15mm at 1300 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 1:1, sealing, be placed in 150 turns/
Point the attached perfume 6h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, in 40~50 DEG C of air-dried 2h,
Attached smoked bean curd pearl is made；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 19.8mm to get.
Wherein, agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the mass ratio of 5:20:10:2:100
Object, Brazilian leaf tobacco extract, burley tobaccos extract, water is taken to be uniformly mixed, first with 0.1% composite plant hydrolase, the Portugal 0.1% β-
Polyglycoside enzyme carries out enzymatic hydrolysis 4h at 35 DEG C；After the completion of enzymatic hydrolysis, bacillus subtilis is added, fermentation 5 days is carried out to fermentation substrate,
Obtain composite fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get agalloch eaglewood is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.64nm, and attached perfume rate is 18.3%.
Embodiment 2
The dry pearl mouth stick of cigarette is prepared by the following method:
1) pelletizing: taking a certain amount of Y-type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
50%) the two is uniformly mixed by=2:3 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out calcining 2h by the qualified samples of 0.15mm at 1300 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 1:1, sealing, be placed in 150 turns/
Point the attached perfume 6h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, in 40~50 DEG C of air-dried 2h,
Attached smoked bean curd pearl is made；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 19.8mm to get.
Wherein, agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the mass ratio of 5:20:20:2:100
Object, Brazilian leaf tobacco extract, burley tobaccos extract, water is taken to be uniformly mixed, first with 0.1% composite plant hydrolase, the Portugal 0.1% β-
Polyglycoside enzyme carries out enzymatic hydrolysis 1h at 35 DEG C；After the completion of enzymatic hydrolysis, (depositary institution is the micro- life in Guangdong Province to addition bacillus BA-01
Object Culture Collection Center, preservation address in 5 building, the building of compound the 59th of Xianlie Middle Road, Guangzhou City 100 Guangdong Microbes Inst,
Preservation date on April 26th, 2017, deposit number are GDMCC No:60171), fermentation 10 days is carried out to fermentation substrate, is obtained compound
Fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get agalloch eaglewood is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.55nm, and attached perfume rate is 22.6%.
Embodiment 3
The dry pearl mouth stick of cigarette is prepared by the following method:
1) pelletizing: taking a certain amount of 4A zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
30%) the two is uniformly mixed by=2:3 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 2:3, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 2h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 19.8mm to get.
Wherein, agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the mass ratio of 5:20:10:2:100
Object, Brazilian leaf tobacco extract, burley tobaccos extract, water is taken to be uniformly mixed, first with 0.1% composite plant hydrolase, the Portugal 0.1% β-
Polyglycoside enzyme carries out enzymatic hydrolysis 3h at 45 DEG C；After the completion of enzymatic hydrolysis, (depositary institution is the micro- life in Guangdong Province to addition bacillus BA-01
Object Culture Collection Center, preservation address in 5 building, the building of compound the 59th of Xianlie Middle Road, Guangzhou City 100 Guangdong Microbes Inst,
Preservation date on April 26th, 2017, deposit number are GDMCC No:60171), fermentation 5 days is carried out to fermentation substrate, is obtained compound
Fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get agalloch eaglewood is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.73nm, and attached perfume rate is 25.2%.
Embodiment 4
The dry pearl mouth stick of cigarette is prepared by the following method:
1) pelletizing: taking a certain amount of 5A zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
30%) the two is uniformly mixed by=2:3 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1300 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 2:3, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 2h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 19.8mm to get.
Wherein, agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the weight ratio of 5:10:20:2:100
Object, Brazilian leaf tobacco extract, burley tobaccos extract, water is taken to be uniformly mixed, first with 0.1% composite plant hydrolase, the Portugal 0.1% β-
Polyglycoside enzyme carries out enzymatic hydrolysis 2h at 50 DEG C；After the completion of enzymatic hydrolysis, bacillus pumilus is added, fermentation 5 days is carried out to fermentation substrate,
Obtain composite fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, be added concentrate quality 20% 1,2-PD mentioned to get agalloch eaglewood is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.66nm, and attached perfume rate is 18.8%.
Embodiment 5
The dry pearl mouth stick of cigarette is prepared by the following method:
1) pelletizing: taking a certain amount of ZSM-5 type zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (admittedly contain
The two is uniformly mixed by amount 40%)=2:5 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out calcining 4h by the qualified samples of 0.15mm at 1000 DEG C, and washing, drying are made with porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 1:2, sealing, be placed in 150 turns/
Point the attached perfume 8h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, in 40~50 DEG C of air-dried 2h,
Attached smoked bean curd pearl is made；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, the cigarette filter tip bottom
Face circumference circle 19.8mm to get.
Wherein, agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the mass ratio of 5:20:15:2:100
Object, Brazilian leaf tobacco extract, burley tobaccos extract, water is taken to be uniformly mixed, first with 0.1% composite plant hydrolase, the Portugal 0.2% β-
Polyglycoside enzyme carries out enzymatic hydrolysis 2h at 40 DEG C；After the completion of enzymatic hydrolysis, (depositary institution is the micro- life in Guangdong Province to addition bacillus BA-01
Object Culture Collection Center, preservation address in 5 building, the building of compound the 59th of Xianlie Middle Road, Guangzhou City 100 Guangdong Microbes Inst,
Preservation date on April 26th, 2017, deposit number are GDMCC No:60171), fermentation 7 days is carried out to fermentation substrate, is obtained compound
Fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, decompression
Being concentrated into medicinal extract density is 1.05~1.10g/cm3, and the 1,2-PD that concentrate quality 20% is added mentions to get agalloch eaglewood is compound
Take object.
Through detecting, the average pore size of dry pearl is 0.60nm, and attached perfume rate is 23.4%.
Embodiment 6
The dry pearl mouth stick of cigarette is prepared by the following method:
1) pelletizing: taking a certain amount of 4A zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content
35%) the two is uniformly mixed by=1:2 mass ratio, is placed in pelletizer and is carried out roller forming, and screening diameter 2.75 ±
Pearl green body is carried out calcining 6h by the qualified samples of 0.15mm at 1000~1300 DEG C, and washing, drying are made with porous
The dry pearl of structure；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 2:3, sealing, be placed in 150 turns/
The attached perfume 12h of shaking table divided, is then allowed to stand 12h, makes essence uniform adsorption in the porous channel of dry pearl, air-dries at 40~50 DEG C
Attached smoked bean curd pearl is made in 4h；
3) mouth stick forms: the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette being formed, cigarette filter tip bottom surface circle
Zhou Zhouchang 19.8mm to get.
Wherein, agalloch eaglewood composite extract preparation method the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then extract aloes powder, saliva bar tobacco leaf according to the ratio of 5:20:10:4:100
Object, Brazilian leaf tobacco extract, burley tobaccos extract, water are uniformly mixed, first with 0.2% composite plant hydrolase, 0.2% β-grape
Glycosidase carries out enzymatic hydrolysis 4h at 40 DEG C；After the completion of enzymatic hydrolysis, (depositary institution is Guangdong Province microorganism to addition bacillus BA-01
Culture Collection Center, preservation address are protected in 5 building, the building of compound the 59th of Xianlie Middle Road, Guangzhou City 100 Guangdong Microbes Inst
Hide April 26 2017 date, deposit number is GDMCC No:60171), fermentation 7 days is carried out to fermentation substrate, obtains compound hair
Zymotic fluid；95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, and filtering is concentrated under reduced pressure into
Medicinal extract density is 1.05~1.10g/cm3, the 1,2-PD of concentrate quality 20% is added to get agalloch eaglewood composite extract.
Through detecting, the average pore size of dry pearl is 0.58nm, and attached perfume rate is 27.9%.
Comparative example 1
1) agalloch eaglewood is sliced, impregnates 2h with 50% ethyl alcohol of 3 times of weight, 68 DEG C heating and refluxing extraction 2 times, merge and extract
Liquid is condensed into medicinal extract, and the 1,2-PD of concentrate quality 20% is added, obtains Lignum Aquilariae Resinatum extract；
1) calcium chloride of extract quality 30% is added in Lignum Aquilariae Resinatum extract, is uniformly mixing to obtain fragrance solution, takes one
Quantitative 5A zeolite molecular sieve carries out calcining 6h at 1300 DEG C, and then washing, drying are added in fragrance solution, sealing is set
In the attached perfume 12h of 150 revs/min of shaking tables, it is then allowed to stand 12h, in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
2) the attached equiponderant attached smoked bean curd pearl of smoked bean curd pearl prepared with embodiment 1 is taken, base circumference perimeter is added to
In the tow of 19.8mm cigarette filter tip to get.
Through detecting, the average pore size of dry pearl is 0.76nm, and attached perfume rate is 10.7%.
Comparative example 2
1) a certain amount of 4A zeolite molecular sieve is taken, after grinding, according to zeolite molecular sieve: silica solution (solid content 25%)=2:
The two is uniformly mixed by 1 mass ratio, is placed in pelletizer and is carried out roller forming, and the qualification of 2.75 ± 0.15mm of diameter is screened
Pearl green body is carried out calcining 6h by sample at 800 DEG C, and dry pearl is made in washing, drying；
2) agalloch eaglewood is sliced, impregnates 2h with 50% ethyl alcohol of 3 times of weight, 68 DEG C heating and refluxing extraction 2 times, merge and extract
Liquid is condensed into medicinal extract, and the 1,2-PD of concentrate quality 20% is added, obtains Lignum Aquilariae Resinatum extract；
3) dry pearl and Lignum Aquilariae Resinatum extract are uniformly mixed according to the mass ratio of 1:2, seal, it is attached is placed in 150 revs/min of shaking table
Fragrant 12h, is then allowed to stand 12h, and in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
4) the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette is formed, the mouth stick base circumference perimeter of cigarette
19.8mm to get.
Through detecting, the average pore size of dry pearl is 0.63nm, and attached perfume rate is 18.4%.
Comparative example 3
1) a certain amount of 4A zeolite molecular sieve is taken, after grinding, according to zeolite molecular sieve: silica solution (solid content 30%)=2:
The two is uniformly mixed by 5 mass ratio, is placed in pelletizer and is carried out roller forming, and the qualification of 2.75 ± 0.15mm of diameter is screened
Pearl green body is carried out calcining 4h by sample at 1200 DEG C, and dry pearl is made in washing, drying；
2) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the mass ratio of 5:10:20:2:200
Object, Brazilian leaf tobacco extract, burley tobaccos extract and water is taken to be uniformly mixed, then ultrasonic 45min is impregnated for 24 hours, obtained after filtering
After reduced pressure, the 1,2-PD of concentrate quality 20% is added to get agalloch eaglewood composite extract in compound extracted solution；
3) dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 1:2, are sealed, be placed in 150 revs/min and shake
The attached perfume 12h of bed, is then allowed to stand 12h, in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
4) the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette is formed, the mouth stick base circumference perimeter of cigarette
19.8mm to get.
Through detecting, the average pore size of dry pearl is 0.54nm, and attached perfume rate is 20.4%.
Comparative example 4
1) a certain amount of 4A zeolite molecular sieve is taken, after grinding, according to zeolite molecular sieve: silica solution (solid content 30%)=2:
The two is uniformly mixed by 5 mass ratio, is placed in pelletizer and is carried out roller forming, and the qualification of 2.75 ± 0.15mm of diameter is screened
Pearl green body is carried out calcining 4h by sample at 1200 DEG C, and dry pearl is made in washing, drying；
2) agalloch eaglewood is sliced, beats powder, then mention aloes powder, saliva bar tobacco leaf according to the mass ratio of 5:10:20:2:200
It takes object, Brazilian leaf tobacco extract, burley tobaccos extract and water to be uniformly mixed, 0.15% pectase and 0.2% cellulose water is added
Solution enzyme obtains composite fermentation liquid after the completion of 35 DEG C of enzymatic hydrolysis 3h, enzymatic hydrolysis after filtering, in 95% second that 3 times of weight is wherein added
Alcohol alcohol precipitation, 4 DEG C stand filtering for 24 hours, and being concentrated under reduced pressure into medicinal extract density is 1.05~1.10g/cm3, concentrate quality is added
20% 1,2-PD is to get agalloch eaglewood composite extract；
3) dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 1:2, are sealed, be placed in 150 revs/min and shake
The attached perfume 12h of bed, is then allowed to stand 12h, in 40~50 DEG C of air-dried 2h, attached smoked bean curd pearl is made；
4) the mouth stick tow middle section that an attached smoked bean curd pearl is added to cigarette is formed, the mouth stick base circumference perimeter of cigarette
19.8mm to get.
Through detecting, the average pore size of dry pearl is 0.62nm, and attached perfume rate is 23.4%.
Test effect:
It is applied in cigarette via the dry pearl mouth stick of cigarette made from Examples 1 to 6 and comparative example 1~4, and not using dry
Regular-size cigarette made from pearl mouth stick is control sample.Tissue has the smoke panel test expert of qualification of national cigarette and inhales five ginsengs of group is commented to shine
GB5606.4-2005 " the 4th part of cigarette: sense organ technical requirements " and YC/T 497-2014 " cigarette Chinese-style cigarette style sense organ
Evaluation method " it smokes panel test to using cigarette made from 1~6 mouth stick of the embodiment of the present invention, it the results are shown in Table 1.
1 cigarette sensory evaluation result of table
Using the dry pearl mouth rod product of the cigarette of the embodiment of the present invention 1~6 compared with comparative example and control sample, system of the present invention
Dry pearl cigarette " sweet taste " style of Preparation Method preparation becomes apparent from, and the abundant degree of fragrance obviously increases, and agalloch eaglewood fragrance stabilization is drawn
Enter so that cigarette smoke is sent out thoroughly is promoted.Using cigarette highest scoring made from 6 mouth stick of embodiment, more assisted with cigarette odor-absorbing
It adjusts, and the sustained release performance of dry pearl is best.
Above-described embodiment is only more excellent embodiment of the invention, is implemented according to the technical essence of the invention to above
Any simple modification and alternate variation that example is made, belong to technical solution of the present invention range.
Claims (8)
1. a kind of dry pearl mouth stick of cigarette for sending out function thoroughly with promotion flue gas, it is characterised in that the cigarette filter tip base circumference week
Long 19.8mm is loaded with the dry pearl of a 2.75 ± 0.15mm of diameter in tow middle section, and dry pearl is main former with zeolite molecular sieve
Material is prepared through pelletizing, attached fragrant, moulding process, is adsorbed on dry pearl and promotes the agalloch eaglewood composite extract that flue gas sends out function thoroughly.
2. according to claim 1 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
It is the described method comprises the following steps:
1) pelletizing: taking a certain amount of zeolite molecular sieve, after grinding, according to zeolite molecular sieve: silica solution (solid content 25~50%)
The two is uniformly mixed by the mass ratio of=2:1~5, is placed in pelletizer and is carried out roller forming, and 2.75 ± 0.15mm of diameter is screened
Qualified samples, pearl green body is subjected to 2~6h of calcining at 1000~1300 DEG C, washing, drying, being made has porous structure
Dry pearl；
2) attached perfume (or spice): dry pearl and agalloch eaglewood composite extract are uniformly mixed according to the mass ratio of 2:1~4, and sealing is placed in 150 revs/min
The attached fragrant 6~12h of shaking table, be then allowed to stand 12h, make essence uniform adsorption in the porous channel of dry pearl, 40~50 DEG C air-dry 2
Attached smoked bean curd pearl is made in~4h；
3) mouth stick form: by attached smoked bean curd pearl be added to cigarette mouth stick tow middle section molding to get.
3. according to claim 2 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
Be: the preparation method of the agalloch eaglewood composite extract the following steps are included:
1) agalloch eaglewood is sliced, beats powder, then according to 5:10~20:10~20:2~5:100 mass ratio by aloes powder, saliva bar
Leaf tobacco extract, Brazilian leaf tobacco extract, burley tobaccos extract and water are uniformly mixed, and are first hydrolyzed with 0.1~0.2% composite plant
Enzyme and 0.1~0.2% beta-glucosidase carry out 1~4h of enzymatic hydrolysis at 30~50 DEG C, after the completion of enzymatic hydrolysis, add bacillus,
Fermentation is carried out 4~10 days to fermentation substrate, obtains composite fermentation liquid；
2) 95% ethyl alcohol that 3 times of weight are added into composite fermentation liquid carries out alcohol precipitation, and 4 DEG C stand for 24 hours, filters, is concentrated under reduced pressure
It is 1.05~1.10g/cm to medicinal extract density3, the 1,2-PD of concentrate quality 20% is added to get agalloch eaglewood compound collecting
Object.
4. according to claim 2 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
It is one of the zeolite molecular sieve model 4A type, 5A type, Y type, ZSM-5 type.
5. according to claim 3 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
It is, the bacillus is bacillus BA-01, and separation screening is from tobacco leaf surface, preservation date on April 26th, 2017, is protected
It is hidden in Guangdong Province's Culture Collection, deposit number is GDMCC No.60171.
6. according to claim 3 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
The additive amount for being the bacillus is the 0.1~0.5% of substrate quality.
7. according to claim 2 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
The attached fragrant rate for being the dry pearl is 15~30%.
8. according to claim 2 have the preparation method for promoting the dry pearl mouth stick of cigarette that flue gas sends out function thoroughly, feature
It is the dry pearl in microcosmic porous structure, average pore size is in 0.5~1nm.
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