CN109198721A - A kind of middle branch cigarette filter tip and preparation method thereof containing bulky grain solid-state perfume (or spice) pearl - Google Patents
A kind of middle branch cigarette filter tip and preparation method thereof containing bulky grain solid-state perfume (or spice) pearl Download PDFInfo
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- CN109198721A CN109198721A CN201810887492.9A CN201810887492A CN109198721A CN 109198721 A CN109198721 A CN 109198721A CN 201810887492 A CN201810887492 A CN 201810887492A CN 109198721 A CN109198721 A CN 109198721A
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- pearl
- spice
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
A kind of middle branch cigarette filter tip and preparation method thereof containing bulky grain solid-state perfume (or spice) pearl, belong to essence spice for cigarette field, 19.8 ± 0.2mm of the middle branch cigarette filter tip circumference, and tow middle section is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter, solid-state perfume (or spice) pearl is using clay as primary raw material, it is prepared through special processes such as slurrying molding, calcining pore-creating, attached perfume (or spice), provides more preferable approach for the addition of thermal sensitivity flavouring essence for tobacco.In sucking process, the essence in mouth stick is not involved in burning, as flue gas slowly uniformly discharges, solves the problems, such as that the brought fragrance of burning is rotten.Advantage of the invention is that being applied in cigarette filter tip in the form of single solid-state perfume (or spice) pearl, structure is simple, nontoxic, avoids consumer to the safety concerns of the tiny additive such as biological powdered carbon, zeolite powder；Fragrant pearl preparation process is simple, and fragrant pearl concentration entirety control rate is more stable, and more preferably compared with " quick-fried pearl ", and without additional addition solvent when attached perfume, fragrance is purer for qualification rate, production stability.
Description
Technical field
The present invention relates to essence spice for cigarette field, in particular to a kind of middle branch cigarette mouth containing bulky grain solid-state perfume (or spice) pearl
Stick and preparation method thereof.
Background technique
Middle branch cigarette is that tobacco business is proposed a kind of filter tip circumference circle between the new of ramuscule cigarette and regular-size cigarette in recent years
Specification cigarette.The specification cigarette relatively positions middle and high end, therefore when designing and developing, and need to pay close attention to its aroma quality and suction interest
Taste.
In tobacco business, the development of cigarette solid meat flavor formulating technology is swift and violent, the new method, new technology especially in cigarette filter tip
Exploitation, including the quick-fried pearl of cigarette, microcapsules, nano particle, powdered granule etc..Currently, by the inspection of consumer market, cigarette is quick-fried
The whole acceptance of pearl is preferable, in Henan cigarette patent (a kind of quick-fried pearl raspberry essence of cigarette and its application in cigarette,
201710285349 .8 of application number) raspberry essence is compounded by Fructus Rubi extract with solvent Glycerin, mixed triester with caprylic acid capric acid (ODO) after
It is wrapped in quick-fried pearl, in cigarette smoking, may make fragrance to release by pinching brokenly the quick-fried pearl being placed in mouth stick.However, volume
There is also certain drawbacks for the addition of the quick-fried pearl of cigarette, dripping pill, low including ratio of briquetting, and higher cost needs to add solvent (one kind
Cigarette cigarette perfume and the insufficient quick-fried pearl of moisture feeling and preparation method thereof, 201610564325 .1 of application number can be made up) the problems such as, and it is quick-fried
Pearl, dripping pill solvent olive oil, ODO etc. there are micro bad smell so that quick-fried pearl be mainly used for wrapping up the fragrance such as ginseng, peppermint it is strong
The flavors and fragrances of gesture.In addition, Shanghai Juhua Technology Co., Ltd. patent " cigarette filter tip containing zeolite perfume (or spice) pearl and
Cigarette zeolite perfume (or spice) pearl preparation method " (201710990114 .9 of application number) is adsorbed using many zeolite fine particles as essence
Carrier, and being placed in cigarette filter tip in the form of cavity, this method can play certain essence slow release effect, but this kind of receive
The tiny additive such as rice grain, powdered granule easily causes the safety concerns of sucking of consumer, therefore promotes not satisfactory.Shanghai cigarette
Patent " disclose a kind of smoking article and its preparation method and application " (application number of careless Group Co., Ltd
201710952583.1) mass ratio for disclosing inorganic bond, inorganic adsorbing material, tobacco, atomizer, water and essence is
(400~700): (100~400): (100~400): (400~1000): (100~300): (1~30), the mixing of each component
Sequence mixes for first Alevaire, water and essence, obtains mixed solution, then mixes inorganic binder, inorganic adsorbing material and tobacco
It closes uniformly, obtains mixed dry material, mixed solution is finally added into mixed dry material.This simple mixing relies on merely inorganic adsorbent
The ability of material, limited sorption capacity.
The present invention develops a kind of solid-state perfume (or spice) pearl of bulky grain on the basis of the above-mentioned prior art, using kaolin, swollen
The natural clays such as profit soil, illite are prepared as a raw material.Clay generally by being formed after silicate mineral at the earth's surface weathering,
It is a kind of phyllosilicate, synusia is made of oxygen-octahedron and alumina octahedral.Main component is tin oxide and aluminium oxide, color
White and fire resisting, for the primary raw material for preparing china clay.Clay by its structure can be divided into kaolinite race, montmorillonite race, illite race,
Chlorite race etc., this kind of silicate mineral are chiefly used in the production preparation of ceramics, and materials are convenient, at low cost, nontoxic, and have
Fire resisting, free from extraneous odour advantage, can be used for the exploitation of cigarette new material.And it is applied in the form of single solid-state perfume (or spice) pearl in filter tip circumference week
In the middle branch cigarette of long 19.8 ± 0.2mm, intuitionistic and concise, production stability is more preferable, nontoxic, avoids consumer to biology
The safety concerns of the tiny additive such as powdered carbon, zeolite powder；Porous structure makes solid-state perfume (or spice) pearl in essence sustained release, reasonable rate, production
It is better than quick-fried pearl in terms of stability, and without pinching brokenly, solvent-free exudation has significant advantage in the addition of thermal sensitivity essence.
The cigarette filter tip of bulky grain perfume (or spice) pearl with porous structure, compared to traditional cigarette filter tip and existing simple by adsorbent material
Porous structure, without additional addition solvent when attached fragrant, fragrance is purer, provides ideal way for the addition of thermal sensitivity flavouring essence for tobacco
Diameter, essence are slowly uniformly discharged with flue gas, solve the problems, such as that the brought fragrance of burning is rotten.
Summary of the invention
In view of the above technical problems, the present invention provides one kind, to be not involved in burning, nontoxic, stable molding, fragrant pearl concentration whole
The middle branch cigarette mouth containing bulky grain solid-state perfume (or spice) pearl that body control rate is more stable, is unlikely to deteriorate with essence slow-release function, fragrance
Stick and preparation method thereof.
To solve the above-mentioned problems, the technical solution of the present invention is as follows:
A kind of preparation method of the middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, will be made the bulky grain with slow-release function
Dry pearl, attached perfume (or spice), the bulky grain solid-state perfume (or spice) pearl after attached perfume is added in the mouth stick tow of middle branch cigarette according to a certain percentage.
Further, it the described method comprises the following steps:
1) slurrying forms: by activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and distillation
Water uniformly mixes simultaneously according to 200~400:50~100:50~100:1~2:1~2:5~10:800~1000 mass ratio
Grinder is added, grinds 1~4h by 2~10:1 of ratio of grinding media to material, then goes out slurry with screen filtration, by processed polyurethane foam
After immersing slurry, is formed using the spherical mold pressing mold of diameter 3.25mm, 6~12h is dried at 70 DEG C, obtains dry pearl base
Body；
2) it calcines pore-creating: pearl green body being subjected to 2~6h of calcining at 550~1200 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property；
3) attached perfume (or spice): dry pearl and thermal sensitivity flavouring essence for tobacco are uniformly mixed according to the mass ratio of 1:2,6~12h is slowly stirred, makes cigarette
With essence uniform adsorption in the porous channel of dry pearl, 2~4h is air-dried at 40~50 DEG C, bulky grain solid-state perfume (or spice) pearl is made；
4) mouth stick form: by bulky grain solid-state perfume (or spice) pearl be added to middle branch cigarette mouth stick tow middle section molding to get.
Further, in the step 1) activate kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose,
Silica solution and distilled water are uniform according to 300~400:50~100:50~100:1:1:8~10:800~1000 mass ratio
It mixes more excellent.
Further, slurry is more excellent according to 2~10:1 of ratio of grinding media to material grinding, 1~2h in the step 1)；And in training process processed
In, it is contemplated that micro- deformation can occur in calcining for pearl green body, therefore spherical mold is opened according to diameter 3.25mm.
Further, that 4~6 h of calcining is carried out at 800~1000 DEG C is more excellent for pearl green body in the step 2.
Further, kaolin is activated in the step 1) is after kaolinite original soil beats powder, 800~900 in Muffle furnace
DEG C roasting 2h activation after gained.
Further, thermal sensitivity flavouring essence for tobacco is dried orange peel extracts, rose extract, raspberry extraction in the step 3)
One of object or several.
Further, 40~50 DEG C of air-dried 2~3h are optimal in the step 3), the attached fragrant rate control of bulky grain solid-state perfume (or spice) pearl
30~40%, wherein weight before attached perfume rate=(weight before the attached perfume of weight-after attached perfume)/attached perfume.
Further, bulky grain solid-state perfume (or spice) pearl is in microcosmic porous structure in the step 3, is surveyed through scanning tunneling microscope
Amount, microcosmic porous average pore size is at 20~100 μm.
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, using system as described in any one in claim 1-5
Preparation Method, the cigarette filter tip are branch cigarette filter tips in one kind, and circumference circle is 19.8 ± 0.2mm, are loaded in tow middle section
One is adsorbed with the bulky grain solid-state perfume (or spice) pearl of thermal sensitivity flavouring essence for tobacco, 3.25 ± 0.15 mm of diameter, and the solid-state perfume (or spice) pearl is to activate
Kaolin, bentonite, illite are made of raw material.
A kind of application of the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl in cigarette, it is any using such as claim 1-5
Preparation method described in, the cigarette filter tip are applied to the middle branch cigarette that cigarette filter tip circumference circle is 19.8 ± 0.2mm
In production, it can play the role of being sustained thermal sensitivity essence.
Compared with prior art, advantages of the present invention and generation good effect are:
1) the bulky grain solid-state perfume (or spice) pearl in the mouth stick, is in porous structure, and average pore size has good essence at 20~100 μm
Absorption property.It is under the conditions of slurrying of the invention, pore-creating, attached fragrant and its subsequent technique, this is also inventive point of the invention
Place, the attached fragrant rate of fragrant pearl are integrally controlled 38~40%, than existing fragrant pearl entirety control rate (existing perfume pearl concentration entirety difference
Greatly) more stable, absorption property is in a saturated state, during smoking property of cigarette, can play sustained release fragrance, and will not be right
This perfume (or spice) of cigarette has an impact；
2) it is applied in cigarette filter tip in the form of single solid-state perfume (or spice) pearl, it is intuitionistic and concise, nontoxic, relative to being added to micro- glue
It is thin to biological powdered carbon, silica white, zeolite powder, cyclodextrin granule etc. to avoid consumer for this kind of cigarette filter tip of capsule, powdered granule
Small additive sucks safety concerns；
3) perfume pearl preparation process is simple, and relative to this kind of cigarette filter tip for being added to quick-fried pearl, dripping pill, qualification rate, production are stablized
Property it is more preferable, and without additional addition solvent when fragrant pearl is attached fragrant, fragrance is purer；
4) the mouth stick is a kind of mouth stick applied to middle branch cigarette, and mouth stick circumference circle is 19.8 ± 0.2mm, between ramuscule cigarette and
Regular-size cigarette, the application of the mouth stick can innovation burst points after this kind of middle branch cigarette listing of ingredient.The perfume pearl be with activate kaolin,
Bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and distilled water are prepared for primary raw material, by the present invention
The technique prepares adsorption effect and is significantly stronger than the prior art；
5) compared with the quick-fried pearl of traditional cigarette, dripping pill, without pinching brokenly fragrant pearl, solvent-free exudation when consumer sucks cigarette.
Detailed description of the invention
Fig. 1 is cigarette sticks schematic diagram；
The solid-state perfume (or spice) pearl fragment SEM figure of 200 times of amplifications in Fig. 2 embodiment 2；
The solid-state perfume (or spice) pearl fragment SEM figure of 3000 times of amplifications in Fig. 3 embodiment 2.
In figure: 1- filter stick aspiration end, 2- bulky grain solid-state perfume (or spice) pearl, 3- cigarette bobbin paper, 4- pipe tobacco.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip is branch cigarette filter tip in one kind, circumference
19.8 ± 0.2mm of perimeter is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter in tow middle section.This contains
The preparation method of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl, includes the following steps:
Step 1: slurrying molding.Will activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and
Distilled water is uniformly mixed and added into grinder according to the mass ratio of 200:50:50:1:1:5:800, grinds by ratio of grinding media to material 2:1
Then 1h goes out ceramic slurry with screen filtration；After processed polyurethane foam is immersed slurry, using the spherical mould of 3.25mm
Have pressing mold molding, dries 6h at 70 DEG C, obtain dry pearl green body.
The activation kaolin is the gained after 800 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder.
Step 2: calcining pore-creating.Pearl green body is carried out to 2 h of calcining at 800 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property.
Step 3: attached perfume (or spice).Dry pearl and dried orange peel extracts are uniformly mixed according to the mass ratio of 1:2,12h is slowly stirred, makes
In the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made in flavouring essence for tobacco uniform adsorption, controls attached fragrant rate
35~40%。
Step 4: mouth stick molding.Bulky grain solid-state perfume (or spice) pearl is added to the middle branch cigarette filter tip that circumference circle is 19.8mm
Tow middle section formed to get.
Embodiment 2
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip is branch cigarette filter tip in one kind, circumference
19.8 ± 0.2mm of perimeter is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter in tow middle section.This contains
The preparation method of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl, includes the following steps:
Step 1: slurrying molding.Will activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and
Distilled water is uniformly mixed and added into grinder according to the mass ratio of 400:100:100:1:1:5:800, grinds by ratio of grinding media to material 1.5:1
1h is ground, then goes out ceramic slurry with screen filtration；After processed polyurethane foam is immersed slurry, using the ball of 3.25 mm
Shape mold pressing mold forms, and dries 12h at 70 DEG C, obtains dry pearl green body.
The activation kaolin is the gained after 800 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder.
Step 2: calcining pore-creating.Pearl green body is carried out to 4 h of calcining at 800 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property.
Step 3: attached perfume (or spice).Dry pearl and dried orange peel extracts are uniformly mixed according to the mass ratio of 1:2,12h is slowly stirred, makes
In the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made in flavouring essence for tobacco uniform adsorption, controls attached fragrant rate
35~40%。
Step 4: mouth stick molding.Bulky grain solid-state perfume (or spice) pearl is added to the middle branch cigarette filter tip that circumference circle is 19.8mm
Tow middle section formed to get.
Embodiment 3
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip is branch cigarette filter tip in one kind, circumference
19.8 ± 0.2mm of perimeter is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter in tow middle section.This contains
The preparation method of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl, includes the following steps:
Step 1: slurrying molding.Will activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and
Distilled water is uniformly mixed and added into grinder according to the mass ratio of 400:100:100:2:1:5:1000, grinds by ratio of grinding media to material 2:1
1h is ground, then goes out ceramic slurry with screen filtration；After processed polyurethane foam is immersed slurry, using the ball of 3.25 mm
Shape mold pressing mold forms, and dries 12h at 70 DEG C, obtains dry pearl green body.
The activation kaolin is the gained after 800 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder.
Step 2: calcining pore-creating.Pearl green body is carried out to 6 h of calcining at 900 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property.
Step 3: attached perfume (or spice).Dry pearl and rose extract are uniformly mixed according to the mass ratio of 1:2,12h is slowly stirred, makes
In the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made in flavouring essence for tobacco uniform adsorption, controls attached fragrant rate
35~40%。
Step 4: mouth stick molding.Bulky grain solid-state perfume (or spice) pearl is added to the middle branch cigarette filter tip that circumference circle is 19.8mm
Tow middle section formed to get.
Embodiment 4
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip is branch cigarette filter tip in one kind, circumference
19.8 ± 0.2mm of perimeter is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter in tow middle section.This contains
The preparation method of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl, includes the following steps:
Step 1: slurrying molding.Will activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and
Distilled water is uniformly mixed and added into grinder according to the mass ratio of 400:100:100:2:1:5:1000, grinds by ratio of grinding media to material 2:1
1h is ground, then goes out ceramic slurry with screen filtration；After processed polyurethane foam is immersed slurry, using the ball of 3.25 mm
Shape mold pressing mold forms, and dries 12h at 70 DEG C, obtains dry pearl green body.
The activation kaolin is the gained after 800 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder.
Step 2: calcining pore-creating.Pearl green body is carried out to 6 h of calcining at 900 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property.
Step 3: attached perfume (or spice).Dry pearl and Fructus Rubi extract are uniformly mixed according to the mass ratio of 1:2, are slowly stirred 12h,
Make flavouring essence for tobacco uniform adsorption in the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made, controls attached perfume (or spice)
Rate 35 ~ 40%.
Step 4: mouth stick molding.Bulky grain solid-state perfume (or spice) pearl is added to the middle branch cigarette filter tip that circumference circle is 19.8mm
Tow middle section formed to get.
Embodiment 5
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip is branch cigarette filter tip in one kind, circumference
19.8 ± 0.2mm of perimeter is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter in tow middle section.This contains
The preparation method of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl, includes the following steps:
Step 1: slurrying molding.Will activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and
Distilled water is uniformly mixed and added into grinder according to the mass ratio of 400:100:100:2:1:5:1000, grinds by ratio of grinding media to material 5:1
1h is ground, then goes out ceramic slurry with screen filtration；After processed polyurethane foam is immersed slurry, using the ball of 3.25 mm
Shape mold pressing mold forms, and dries 12h at 70 DEG C, obtains dry pearl green body.
The activation kaolin is the gained after 800 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder.
Step 2: calcining pore-creating.Pearl green body is carried out to 6 h of calcining at 900 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property.
Step 3: attached perfume (or spice).Dry pearl and Fructus Rubi extract are uniformly mixed according to the mass ratio of 1:2,8h is slowly stirred, makes
In the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made in flavouring essence for tobacco uniform adsorption, controls attached fragrant rate
30~35%。
Step 4: mouth stick molding.Bulky grain solid-state perfume (or spice) pearl is added to the middle branch cigarette filter tip that circumference circle is 19.8mm
Tow middle section formed to get.
Embodiment 6
A kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip is branch cigarette filter tip in one kind, circumference
19.8 ± 0.2mm of perimeter is loaded with the bulky grain solid-state perfume (or spice) pearl of 3.25 ± 0.15 mm of diameter in tow middle section.This contains
The preparation method of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl, includes the following steps:
Step 1: slurrying molding.Will activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and
Distilled water is uniformly mixed and added into grinder according to the mass ratio of 400:100:100:2:1:5:1000, grinds by ratio of grinding media to material 5:1
1h is ground, then goes out ceramic slurry with screen filtration；After processed polyurethane foam is immersed slurry, using the ball of 3.25 mm
Shape mold pressing mold forms, and dries 12h at 70 DEG C, obtains dry pearl green body.
The activation kaolin is the gained after 800 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder.
Step 2: calcining pore-creating.Pearl green body is carried out to 6 h of calcining at 900 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property.
Step 3: attached perfume (or spice).By dry pearl and thermal sensitivity essence (Fructus Rubi extract, dried orange peel extracts mass ratio 1:1 are mixed)
It is uniformly mixed according to the mass ratio of 1:2, is slowly stirred 12h, makes flavouring essence for tobacco uniform adsorption in the porous channel of dry pearl, 40
Bulky grain solid-state perfume (or spice) pearl is made in DEG C air-dried 4h, controls attached fragrant rate 35 ~ 40%.
Step 4: mouth stick molding.Bulky grain solid-state perfume (or spice) pearl is added to the middle branch cigarette filter tip that circumference circle is 19.8mm
Tow middle section formed to get.
Test effect:
It is applied in cigarette via the middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl made from embodiment 1 ~ 6, mouth stick is made
Circumference circle is the middle branch cigarette of 19.8 ± 0.2mm.
Tissue have national cigarette smoke panel test qualification expert inhale comment five ginsengs of group according to GB5606.4-2005 " the 4th part of cigarette:
Sense organ technical requirements " and YC/T 497-2014 " cigarette Chinese-style cigarette style sensory evaluation method " to use the embodiment of the present invention 1
The cigarette of ~ 6 mouth sticks is smoked panel test, and to be not added with the control sample of the mouth stick of bulky grain solid-state perfume (or spice) pearl, and optimal for effect
Fragrant pearl carries out SEM scanning in embodiment, observes its porous structure, the results are shown in Table 1.
1 cigarette sensory evaluation result of table
Middle branch cigarette (mouth stick circumference made from the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl using the embodiment of the present invention 1 ~ 6
19.8 ± 0.2mm of Zhou Changwei) compared with control sample, " sweet taste " style becomes apparent from product, and the abundant degree of fragrance obviously increases,
The property sent out is promoted flue gas thoroughly.Using cigarette highest scoring made from 2 mouth stick of embodiment, main reason is that dried orange peel fragrance with
Cigarette odor-absorbing is more coordinated, and the sustained release performance of solid-state perfume (or spice) pearl is best, it can be seen that, in fragrant pearl preparation process, slurry grinder
It is preferable that 4 h effects of calcining are carried out by ratio of grinding media to material 3:1 and at 800 DEG C.
SEM scanning has been carried out after smashing present invention is alternatively directed to the fragrant pearl in the optimal embodiment 2 of application effect, it is more to observe it
Pore structure and adsorption capacity.Wherein Fig. 2 is the solid-state perfume (or spice) pearl fragment SEM figure of 200 times of amplifications, and Fig. 3 is the solid-state of 3000 times of amplifications
Fragrant pearl fragment SEM figure, it can be seen that, fragrant hole of bead diameter is at 40 ~ 60 μm or so in the embodiment.
Above-described embodiment is only more excellent embodiment of the invention, is implemented according to the technical essence of the invention to above
Any simple modification, modification and the alternate variation that example is made, belong in the range of technical solution of the present invention.
Claims (7)
1. a kind of preparation method of the middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, it is characterised in that: will be made to have and delay
The dry pearl of bulky grain of function is released, according to a certain percentage attached perfume (or spice), the bulky grain solid-state perfume (or spice) pearl after attached perfume is added to middle branch cigarette
In mouth stick tow.
2. a kind of preparation method of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl according to claim 1, special
Sign is: it the described method comprises the following steps:
Slurrying molding: by activation kaolin, bentonite, illite, polyphosphate sodium, carboxymethyl cellulose, silica solution and distilled water
It uniformly mixes and adds according to 200~400:50~100:50~100:1~2:1~2:5~10:800~1000 mass ratio
Enter grinder, grinds 1~4h by 2~10:1 of ratio of grinding media to material, then go out slurry with screen filtration, processed polyurethane foam is soaked
After entering slurry, is formed using the spherical mold pressing mold of diameter 3.25mm, 6~12h is dried at 70 DEG C, obtains dry pearl base
Body;
Calcining pore-creating: pearl green body is carried out to 2~6 h of calcining at 550~1200 DEG C, washing, drying, being made has porosity
The dry pearl of the bulky grain of matter；
Attached perfume (or spice): dry pearl and thermal sensitivity flavouring essence for tobacco are uniformly mixed according to the mass ratio of 1:2,6~12h is slowly stirred, uses cigarette
Essence uniform adsorption air-dries 2~4h in the porous channel of dry pearl, at 40~50 DEG C, and bulky grain solid-state perfume (or spice) pearl is made；
Mouth stick molding: by bulky grain solid-state perfume (or spice) pearl be added to middle branch cigarette mouth stick tow middle section molding to get.
3. the preparation method of the middle branch cigarette filter tip according to claim 1 or 2 containing bulky grain solid-state perfume (or spice) pearl, feature
Be: it is 800~900 DEG C of roasting 2h activation in Muffle furnace after kaolinite original soil beats powder that kaolin is activated in the step 1)
Gained afterwards.
4. the preparation method of the middle branch cigarette filter tip according to claim 1 or 2 containing bulky grain solid-state perfume (or spice) pearl, feature
Be: in the step 3) thermal sensitivity flavouring essence for tobacco be one of dried orange peel extracts, rose extract, Fructus Rubi extract or
It is several.
5. the preparation method of the middle branch cigarette filter tip according to claim 1 or 2 containing bulky grain solid-state perfume (or spice) pearl, feature
Be: the attached fragrant rate of bulky grain solid-state perfume (or spice) pearl is controlled 30~40% in the step 3), wherein attached perfume rate=(heavy after attached perfume
Amount-it is attached it is fragrant before weight)/it is attached it is fragrant before weight.
6. a kind of middle branch cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, it is characterised in that: using such as any one of claim 1-5
The preparation method, the cigarette filter tip are branch cigarette filter tips in one kind, and circumference circle is 19.8 ± 0.2mm, in tow
Section is loaded with the bulky grain solid-state perfume (or spice) pearl for being adsorbed with thermal sensitivity flavouring essence for tobacco, 3.25 ± 0.15 mm of diameter, and the solid-state is fragrant
Pearl is made using activating kaolin, bentonite, illite of raw material.
7. a kind of application of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl in cigarette, it is characterised in that: wanted using such as right
The described in any item preparation methods of 1-5 are sought, it is in 19.8 ± 0.2mm that the cigarette filter tip, which is applied to cigarette filter tip circumference circle,
In the production of branch cigarette.
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| CN201810887492.9A CN109198721B (en) | 2018-08-06 | 2018-08-06 | Medium cigarette filter tip containing large-particle solid aromatic beads and preparation method thereof |
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| CN201810887492.9A CN109198721B (en) | 2018-08-06 | 2018-08-06 | Medium cigarette filter tip containing large-particle solid aromatic beads and preparation method thereof |
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| CN115337858A (en) * | 2022-08-12 | 2022-11-15 | 广东中烟工业有限责任公司 | Visual herbal fragrance sustained-release granules and preparation method and application thereof |
| CN115318197A (en) * | 2022-08-12 | 2022-11-11 | 广东中烟工业有限责任公司 | Visual fragrance sustained-release particles and preparation method and application thereof |
| CN115430353A (en) * | 2022-08-16 | 2022-12-06 | 广东中烟工业有限责任公司 | Modified visual coloring flavor sustained-release particles and preparation method and application thereof |
| CN115430353B (en) * | 2022-08-16 | 2023-11-17 | 广东中烟工业有限责任公司 | Modified visual coloring fragrance slow-release particles and preparation method and application thereof |
| CN115337859A (en) * | 2022-08-16 | 2022-11-15 | 广东中烟工业有限责任公司 | Acid-modified visual flavor sustained-release particles and preparation method and application thereof |
| CN115337859B (en) * | 2022-08-16 | 2023-11-17 | 广东中烟工业有限责任公司 | Acid modified visual fragrance slow-release particles and preparation method and application thereof |
| CN115382462A (en) * | 2022-09-07 | 2022-11-25 | 广东中烟工业有限责任公司 | Preparation method of colored aromatic bead, product and application thereof |
| CN115382463A (en) * | 2022-09-07 | 2022-11-25 | 广东中烟工业有限责任公司 | Preparation method of composite modified visible fragrant bead, product and application thereof |
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