CN108851213A - A kind of cigarette filter tip and preparation method thereof containing bulky grain solid-state perfume (or spice) pearl - Google Patents
A kind of cigarette filter tip and preparation method thereof containing bulky grain solid-state perfume (or spice) pearl Download PDFInfo
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- CN108851213A CN108851213A CN201810886849.1A CN201810886849A CN108851213A CN 108851213 A CN108851213 A CN 108851213A CN 201810886849 A CN201810886849 A CN 201810886849A CN 108851213 A CN108851213 A CN 108851213A
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- pearl
- spice
- perfume
- bulky grain
- filter tip
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
A kind of cigarette filter tip and preparation method thereof containing bulky grain solid-state perfume (or spice) pearl, belong to essence spice for cigarette field, the mouth stick tow middle section is loaded with a bulky grain solid-state perfume (or spice) pearl, the perfume pearl wants raw material based on porous konilite, it is prepared through techniques such as slurrying molding, calcining pore-creating, attached perfume (or spice), adds light fragrant, volatile type flavouring essence for tobacco.In sucking process, essence is slowly uniformly discharged with flue gas, solves the problems, such as that the brought fragrance of burning is rotten.The present invention is loaded in cigarette filter tip with single solid-state perfume (or spice) pearl, and structure is simple, nontoxic, avoids smoker to the safety concerns of tiny additive；Fragrant pearl preparation process is simple, and fragrant pearl concentration entirety control rate is more stable, and qualification rate, production stability are more preferable, and without additional addition solvent when attached perfume, elegant fragrance is sent out thoroughly.
Description
Technical field
The present invention relates to essence spice for cigarette field, in particular to a kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl and
Preparation method.
Background technique
In tobacco business, the development of cigarette solid meat flavor formulating technology is swift and violent, the new method, new technology especially in cigarette filter tip
Exploitation, including the quick-fried pearl of cigarette, microcapsules, nano particle, powdered granule etc..Currently, by the inspection of consumer market, cigarette is quick-fried
The whole acceptance of pearl is preferable, and the additives such as microcapsules, nano particle, powdered granule easily cause consumption since particle is tiny
Person's sucks safety concerns.However, there is also certain drawbacks for the addition of the quick-fried pearl of cigarette, dripping pill, it is low including ratio of briquetting, at
The problems such as this is higher, and there are micro bad smells by quick-fried pearl, dripping pill solvent olive oil, ODO etc., so that quick-fried pearl is mainly used for wrapping up
The flavors and fragrances of the fragrance such as ginseng, peppermint advantage.Contain silica gel perfume (or spice) pearl disclosed in prior art CN201710990115.3
Cigarette filter tip and cigarette are disclosed with silica gel perfume (or spice) pearl preparation method and CN201710990114.9 containing zeolite perfume (or spice) Zhu Juanyanzui
On the basis of the preparation method of stick and cigarette with zeolite perfume (or spice) pearl, using present invention pearl and subsequent technique, so that fragrant pearl concentration is whole
Body control rate is more stable, also avoids consumer to the tiny additive such as biological powdered carbon, silica white, zeolite powder, cyclodextrin granule
Suck safety concerns.
Porous konilite belongs to a kind of Volcanic sedimentary rock, and natural partial size is thin（5 μm or so）, even particle distribution, specific surface
Product is big（8.3m*2/g）, contour structures approximate sphericity and without angular forms body of paste under high velocity agitation, can be absorbed its from
35% water of body weight, lower than diatomite common in cigarette, (diatomite can absorb 1.5~4 times of own wt of water）.But
Its thixotropy is entirely capable of as diatomite.Currently, the price of porous konilite is only the 20%~25% of diatomite.
The present invention is on the basis of cigarette solid blending, for the addition demand of light fragrant, volatile type flavouring essence for tobacco, exploitation
A solid-state perfume (or spice) pearl cigarette filter tip for being not involved in burning, bulky grain with essence slow-release function is obtained, periporate stone is used
The natural china clay raw material such as English, waterglass is prepared, nontoxic, low cost, and ratio of briquetting is high；And the application in the form of single solid-state perfume (or spice) pearl
Intuitionistic and concise in cigarette filter tip, production stability is more preferable；Cell quartz has natural porous structure, so that solid-state perfume (or spice) pearl
It is better than quick-fried pearl in terms of essence sustained release, and without pinching brokenly, solvent-free exudation, 1~20 μm of micropore release structures are in light fragrant, Yi Hui
There is significant advantage in the use of hair style flavouring essence for tobacco；The cigarette filter tip of bulky grain perfume (or spice) pearl with porous structure, compared to biography
The cigarette filter tip of system, essence are slowly uniformly discharged with flue gas, solve the problems, such as that the brought fragrance of burning is rotten.
Summary of the invention
In view of the above technical problems, the present invention provides one kind, to be not involved in burning, nontoxic, stable molding, fragrant pearl concentration whole
The cigarette filter tip and its system for the bulky grain solid-state perfume (or spice) pearl that body control rate is more stable, is unlikely to deteriorate with essence slow-release function, fragrance
Preparation Method.
To solve the above-mentioned problems, the technical scheme is that：
A kind of preparation method of the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, will be made the bulky grain with slow-release function and does
Pearl, attached perfume (or spice), the bulky grain solid-state perfume (or spice) pearl after attached perfume is added in the mouth stick tow of cigarette according to a certain percentage.
Further, the method specifically includes following steps：
1）Slurrying molding：By porous konilite, waterglass, silester, atoleine and distilled water according to 100~200：10~
50：10~50：1~2：500~1000 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 1~15：1 grinding 2~
Then 4h goes out slurry with screen filtration, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C baking
Dry 2~4h, obtains dry pearl green body.
2）Calcine pore-creating：Pearl green body is carried out to 2~6 h of calcining at 1000~1300 DEG C, tool is made in washing, drying
There is the dry pearl of the bulky grain of porous property；
3）Attached perfume (or spice)：By dry pearl and flavouring essence for tobacco according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 6~12h, is made flavouring essence for tobacco
Uniform adsorption air-dries 2~4h in the porous channel of dry pearl, at 40~50 DEG C, and bulky grain solid-state perfume (or spice) pearl is made；
4）The molding of mouth stick：By bulky grain solid-state perfume (or spice) pearl be added to cigarette mouth stick tow middle section molding to get.
Further, the step 1）In porous konilite, waterglass, silester, atoleine and distilled water according to
100~200：20~50：20~50：1~2：500~700 mass ratio uniformly mixes more excellent.
Further, the step 1）Middle slurry is according to ratio of grinding media to material 5~10：1 grinding 2h is more excellent；And during making training,
In view of micro- deformation can occur in calcining for pearl green body, therefore spherical mold is opened according to diameter 3.65mm.
Further, the step 2）It is more excellent that middle pearl green body carries out 4~6 h of calcining at 1200~1300 DEG C.
Further, the step 1）In porous konilite be through washing purification fine white powder, dioxide-containing silica>
99.5%。
Further, the step 3）Middle flavouring essence for tobacco is dried orange peel extracts, in rose extract, Fructus Rubi extract
It is one or more of.
Further, the step 3）The attached fragrant rate of middle bulky grain solid-state perfume (or spice) pearl is controlled 20~40%, wherein attached perfume rate
=（Weight before the attached perfume of weight-after attached perfume）/ it is attached it is fragrant before weight.
Further, the step 3）In middle step, during attached perfume, 40~50 DEG C of air-dried 2~3h are optimal, control big
The attached fragrant rate of grain solid-state perfume (or spice) pearl is 30~40%.
Further, the step 4）Middle bulky grain solid-state perfume (or spice) pearl is in microcosmic porous structure, is surveyed through scanning tunneling microscope
Amount, microcosmic porous average pore size is at 1~20 μm.
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, using preparation method as described above, the cigarette mouth
Stick base circumference perimeter 24mm is loaded with the bulky grain solid-state perfume (or spice) pearl of a 3.65 ± 0.15mm of diameter, the perfume in tow middle section
Pearl wants raw material to be prepared based on porous konilite, is adsorbed with light fragrant, volatile type flavouring essence for tobacco.
Further, the volatile type flavouring essence for tobacco is mainly the natural light perfume (or spice) such as cedar wood oil, ylang ylang oil, attar of rose
Type essence.
A kind of application of the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl in cigarette, using such as above-mentioned preparation method,
The cigarette filter tip is applied in the production for the cigarette that cigarette filter tip circumference circle is 24mm, and it is light fragrant, volatile can to play sustained release
The effect of type flavouring essence for tobacco.
Compared with prior art, advantages of the present invention and generation good effect are：
1）Bulky grain solid-state perfume (or spice) pearl in the mouth stick, is in porous structure, and average pore size at 1~20 μm there is good essence to inhale
Sustained release performance is echoed, the pore size of fragrant pearl particle can be controlled by changing pore creating material addition.Especially slurrying of the invention,
Under the conditions of pore-creating, attached fragrant and its subsequent technique, this is also inventive point place of the invention, and the attached fragrant rate of fragrant pearl is integrally controlled 20
~40%, than existing fragrant pearl entirety control rate（Existing perfume pearl concentration entirety difference is big）It is more stable, it is optimal can control to 30~
40%, absorption property is in a saturated state, during smoking property of cigarette, can play sustained release fragrance, and will not be to this perfume of cigarette
Have an impact；
2）It is applied in cigarette filter tip in the form of single solid-state perfume (or spice) pearl, it is intuitionistic and concise, nontoxic, relative to being added to micro- glue
It is thin to biological powdered carbon, silica white, zeolite powder, cyclodextrin granule etc. to avoid consumer for this kind of cigarette filter tip of capsule, powdered granule
Small additive sucks safety concerns；
3）Perfume pearl preparation process is simple, and relative to this kind of cigarette filter tip for being added to quick-fried pearl, dripping pill, qualification rate, production are stablized
Property it is more preferable, and without additional addition solvent when fragrant pearl is attached fragrant, fragrance is purer；
4）The mouth stick is a kind of mouth stick applied to middle branch cigarette, and mouth stick circumference circle is 24mm, between ramuscule cigarette and common volume
Cigarette, the application of the mouth stick can become the innovation burst point after this kind of middle branch cigarette listing.The tow middle section of the mouth stick is loaded with one
The bulky grain solid-state perfume (or spice) pearl of 3.65 ± 0.15mm of diameter, the perfume pearl is using porous konilite, waterglass, silester as primary raw material
It is prepared, prepares adsorption effect by technique of the present invention and be better than the prior art.
5）Compared with the quick-fried pearl of traditional cigarette, dripping pill, without pinching brokenly fragrant pearl, solvent-free exudation when consumer sucks cigarette.
Detailed description of the invention
Fig. 1 is cigarette filter tip schematic diagram；
Fig. 2 is the SEM figure of bulky grain solid-state perfume (or spice) pearl in embodiment 2（Before adsorbing essence）；
Fig. 3 is the SEM figure of bulky grain solid-state perfume (or spice) pearl in embodiment 2（After adsorbing essence）.
In figure：1- filter stick aspiration end, 2- bulky grain solid-state perfume (or spice) pearl, 3- cigarette bobbin paper, 4- pipe tobacco.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip circumference circle 24mm are loaded in tow middle section
There is the bulky grain solid-state perfume (or spice) pearl of a 3.65 ± 0.15mm of diameter.This contains the preparation side of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl
Method includes the following steps：
Step 1：Slurrying molding.It will be by porous konilite, waterglass, silester, atoleine and distilled water according to 100：
20：10：2：500 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 5：1 grinding 2h, is then gone out with screen filtration
Slurry, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C of drying 4h obtain dry pearl
Green body.
The porous konilite is the fine white powder through washing purification, wherein dioxide-containing silica>99.5%.
Step 2：Calcine pore-creating.Pearl green body is carried out to 2 h of calcining at 1200 DEG C, washing, drying are made with more
The dry pearl of the bulky grain of porous.
Step 3：Attached perfume (or spice).By dry pearl and cedar wood oil according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 12h, is used cigarette
Essence uniform adsorption is in the porous channel of dry pearl, and in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made, control attached fragrant rate 35 ~
40%。
Step 4：The molding of mouth stick.Bulky grain solid-state perfume (or spice) pearl is added in the cigarette filter tip tow that circumference circle is 24mm
Duan Jinhang molding to get.
Embodiment 2
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip circumference circle 24mm are loaded in tow middle section
There is the bulky grain solid-state perfume (or spice) pearl of a 3.65 ± 0.15mm of diameter.This contains the preparation side of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl
Method includes the following steps：
Step 1：Slurrying molding.It will be by porous konilite, waterglass, silester, atoleine and distilled water according to 100：
20：10：1：500 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 10：1 grinding 4h, is then gone out with screen filtration
Slurry, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C of drying 4h obtain dry pearl
Green body.
The porous konilite is the fine white powder through washing purification, wherein dioxide-containing silica>99.5%.
Step 2：Calcine pore-creating.Pearl green body is carried out to 2 h of calcining at 1300 DEG C, washing, drying are made with more
The dry pearl of the bulky grain of porous.
Step 3：Attached perfume (or spice).By dry pearl and cedar wood oil according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 12h, is used cigarette
Essence uniform adsorption is in the porous channel of dry pearl, and in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made, control attached fragrant rate 25 ~
30%。
Step 4：The molding of mouth stick.Bulky grain solid-state perfume (or spice) pearl is added in the cigarette filter tip tow that circumference circle is 24mm
Duan Jinhang molding to get.
Embodiment 3
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip circumference circle 24mm are loaded in tow middle section
There is the bulky grain solid-state perfume (or spice) pearl of a 3.65 ± 0.15mm of diameter.This contains the preparation side of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl
Method includes the following steps：
Step 1：Slurrying molding.It will be by porous konilite, waterglass, silester, atoleine and distilled water according to 180：
30：20：1：700 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 10：1 grinding 4h, is then gone out with screen filtration
Slurry, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C of drying 4h obtain dry pearl
Green body.
The porous konilite is the fine white powder through washing purification, wherein dioxide-containing silica>99.5%.
Step 2：Calcine pore-creating.Pearl green body is carried out to 2 h of calcining at 1000 DEG C, washing, drying are made with more
The dry pearl of the bulky grain of porous.
Step 3：Attached perfume (or spice).By dry pearl and cedar wood oil according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 12h, is used cigarette
Essence uniform adsorption is in the porous channel of dry pearl, and in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made, control attached fragrant rate 25 ~
30%。
Step 4：The molding of mouth stick.Bulky grain solid-state perfume (or spice) pearl is added in the cigarette filter tip tow that circumference circle is 24mm
Duan Jinhang molding to get.
Embodiment 4
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip circumference circle 24mm are loaded in tow middle section
There is the bulky grain solid-state perfume (or spice) pearl of a 3.65 ± 0.15mm of diameter.This contains the preparation side of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl
Method includes the following steps：
Step 1：Slurrying molding.It will be by porous konilite, waterglass, silester, atoleine and distilled water according to 180：
30：20：1：700 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 10：1 grinding 4h, is then gone out with screen filtration
Slurry, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C of drying 4h obtain dry pearl
Green body.
The porous konilite is the fine white powder through washing purification, wherein dioxide-containing silica>99.5%.
Step 2：Calcine pore-creating.Pearl green body is carried out to 2 h of calcining at 1200 DEG C, washing, drying are made with more
The dry pearl of the bulky grain of porous.
Step 3：Attached perfume (or spice).By dry pearl and ylang ylang oil according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 12h, is made
In the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made in flavouring essence for tobacco uniform adsorption, controls attached fragrant rate
25~30%。
Step 4：The molding of mouth stick.Bulky grain solid-state perfume (or spice) pearl is added in the cigarette filter tip tow that circumference circle is 24mm
Duan Jinhang molding to get.
Embodiment 5
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, states cigarette filter tip circumference circle 24mm, is loaded in tow middle section
The bulky grain solid-state perfume (or spice) pearl of one 3.65 ± 0.15mm of diameter.This contains the preparation side of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl
Method includes the following steps：
Step 1：Slurrying molding.It will be by porous konilite, waterglass, silester, atoleine and distilled water according to 150：
20：20：1：600 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 15：1 grinding 4h, is then gone out with screen filtration
Slurry, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C of drying 4h obtain dry pearl
Green body.
The porous konilite is the fine white powder through washing purification, wherein dioxide-containing silica>99.5%.
Step 2：Calcine pore-creating.Pearl green body is carried out to 4 h of calcining at 1200 DEG C, washing, drying are made with more
The dry pearl of the bulky grain of porous.
Step 3：Attached perfume (or spice).By dry pearl and ylang ylang oil according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 12h, is made
In the porous channel of dry pearl, in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made in flavouring essence for tobacco uniform adsorption, controls attached fragrant rate
30~35%。
Step 4：The molding of mouth stick.Bulky grain solid-state perfume (or spice) pearl is added in the cigarette filter tip tow that circumference circle is 24mm
Duan Jinhang molding to get.
Embodiment 6
A kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, the cigarette filter tip circumference circle 24mm are loaded in tow middle section
There is the bulky grain solid-state perfume (or spice) pearl of a 3.65 ± 0.15mm of diameter.This contains the preparation side of the cigarette filter tip of bulky grain solid-state perfume (or spice) pearl
Method includes the following steps：
Step 1：Slurrying molding.It will be by porous konilite, waterglass, silester, atoleine and distilled water according to 150：
20：20：1：600 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 10：1 grinding 4h, is then gone out with screen filtration
Slurry, using 3.65 mm of diameter spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C of drying 4h obtain dry pearl
Shape green body.
The porous konilite is the fine white powder through washing purification, wherein dioxide-containing silica>99.5%.
Step 2：Calcine pore-creating.Pearl green body is carried out to 3 h of calcining at 1200 DEG C, washing, drying are made with more
The dry pearl of the bulky grain of porous.
Step 3：Attached perfume (or spice).By dry pearl and attar of rose according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 12h, is used cigarette
Essence uniform adsorption is in the porous channel of dry pearl, and in 40 DEG C of air-dried 4h, bulky grain solid-state perfume (or spice) pearl is made, control attached fragrant rate 30 ~
35%。
Step 4：The molding of mouth stick.Bulky grain solid-state perfume (or spice) pearl is added in the cigarette filter tip tow that circumference circle is 24mm
Duan Jinhang molding to get.
Test effect：
It is applied in cigarette via the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl made from embodiment 1 ~ 6, is made mouth stick, and with
Do not use regular-size cigarette made from bulky grain solid-state perfume (or spice) pearl mouth stick for control sample.Tissue has the smoke panel test expert of qualification of national cigarette and inhales
Comment five ginsengs of group according to GB5606.4-2005《The 4th part of cigarette：Sense organ technical requirements》With YC/T 497-2014《Cigarette Chinese style
Cigarette style sensory evaluation method》It smokes panel test to using cigarette made from 1 ~ 6 mouth stick of the embodiment of the present invention, the results are shown in Table 1.
1 cigarette sensory evaluation result of table
Middle branch cigarette (mouth stick circumference made from the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl using the embodiment of the present invention 1 ~ 6
Zhou Changwei 24mm) compared with control sample, " sweet taste " style becomes apparent from product, and the abundant degree of fragrance obviously increases, and flue gas is saturating
Hair property is promoted.Using cigarette highest scoring made from 2 mouth stick of embodiment, main reason is that dried orange peel fragrance and cigarette odor-absorbing
More coordinate, and the sustained release performance of solid-state perfume (or spice) pearl is best, it can be seen that, in fragrant pearl preparation process, slurry grinder presses ratio of grinding media to material
3：1 and carried out at 800 DEG C calcining 4 h effects it is more preferable.
Present invention is alternatively directed to the fragrant pearls in the optimal embodiment 2 of application effect to have carried out SEM scanning, to confirm its porous knot
Structure and essence absorption property.
Above-described embodiment is only more excellent embodiment of the invention, is implemented according to the technical essence of the invention to above
Any simple modification and alternate variation that example is made, belong to technical solution of the present invention range.
Claims (7)
1. a kind of preparation method of the cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, it is characterised in that：To be made has sustained release function
The dry pearl of bulky grain of energy, the bulky grain solid-state perfume (or spice) pearl after attached perfume, is added to the mouth stick tow of cigarette by attached perfume (or spice) according to a certain percentage
In.
2. a kind of preparation method of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl according to claim 1, feature exist
In：The method specifically includes following steps：
Slurrying molding：By porous konilite, waterglass, silester, atoleine and distilled water according to 100~200：10~
50：10~50：1~2：500~1000 mass ratio is uniformly mixed and added into grinder, by ratio of grinding media to material 1~15：1 grinding 2~
Then 4h goes out slurry with screen filtration, using diameter 3.65mm spherical mold pressing mold form, drying at room temperature for 24 hours after, 45 DEG C baking
Dry 2~4h, obtains dry pearl green body；
Calcine pore-creating：Pearl green body is carried out to 2~6 h of calcining at 1000~1300 DEG C, washing, drying are made with porous
The dry pearl of the bulky grain of property；
Attached perfume (or spice)：By dry pearl and flavouring essence for tobacco according to 1:2 mass ratio is uniformly mixed, and is slowly stirred 6~12h, is kept flavouring essence for tobacco equal
In the even porous channel for being adsorbed on dry pearl, 2~4h is air-dried at 40~50 DEG C, bulky grain solid-state perfume (or spice) pearl is made；
The molding of mouth stick：By bulky grain solid-state perfume (or spice) pearl be added to cigarette mouth stick tow middle section molding to get.
3. a kind of preparation method of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl according to claim 1 or 2, feature
It is：The step 1）In porous konilite be through washing purification fine white powder, dioxide-containing silica>99.5%.
4. a kind of preparation method of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl according to claim 1 or 2, feature
It is：The step 3）Middle flavouring essence for tobacco is one or more of dried orange peel extracts, rose extract, Fructus Rubi extract.
5. a kind of preparation method of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl according to claim 1 or 2, feature
It is：The step 3）The attached fragrant rate of middle bulky grain solid-state perfume (or spice) pearl is controlled 20~40%, wherein and attached perfume rate=（Weight after attached perfume
Weight before the attached perfume of amount-）/ it is attached it is fragrant before weight.
6. a kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl, it is characterised in that：Using as described in claim any one of 1-5
Preparation method, the cigarette filter tip base circumference perimeter 24mm is loaded with a 3.65 ± 0.15mm of diameter in tow middle section
Bulky grain solid-state perfume (or spice) pearl, which wants raw material to be prepared based on porous konilite, is adsorbed with light fragrant, volatile type cigarette and uses
Essence.
7. a kind of application of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl in cigarette, it is characterised in that：It is wanted using such as right
The described in any item preparation methods of 1-5 are sought, the cigarette filter tip is applied to the life for the cigarette that cigarette filter tip circumference circle is 24mm
In production.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810886849.1A CN108851213B (en) | 2018-08-06 | 2018-08-06 | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810886849.1A CN108851213B (en) | 2018-08-06 | 2018-08-06 | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108851213A true CN108851213A (en) | 2018-11-23 |
| CN108851213B CN108851213B (en) | 2020-12-29 |
Family
ID=64307759
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| CN201810886849.1A Active CN108851213B (en) | 2018-08-06 | 2018-08-06 | Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof |
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