CN103876285A - Fragrance enhanced granular additive for filter sticks and preparation method and application thereof - Google Patents

Fragrance enhanced granular additive for filter sticks and preparation method and application thereof Download PDF

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Publication number
CN103876285A
CN103876285A CN201410076539.5A CN201410076539A CN103876285A CN 103876285 A CN103876285 A CN 103876285A CN 201410076539 A CN201410076539 A CN 201410076539A CN 103876285 A CN103876285 A CN 103876285A
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powder
filter stick
particulate additive
type filter
flavored type
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CN103876285B (en
Inventor
陈潜
金勇�
李克
赵立红
谭海风
王诗太
范红梅
喻赛波
刘琦
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Abstract

The invention discloses a fragrance enhanced granular additive for filter sticks and a preparation method and application thereof. The fragrance enhanced granular additive for the filter sticks is prepared and obtained by mixing fragrant edible powder, vegetal granular powder, a binding agent and a swelling agent via a solution, squeezing for granulation and microwave drying; the prepared fragrance enhanced granular additive for the filter sticks is added in the filter sticks of cigarettes to enhance fragrance and lower tar content in smoke; the fragrance enhanced granular additive is few in add amount and great in tar content lowering; specific composite fragrance is provided with the cigarettes are smoked, and more abundant experience in taste and smell is brought to smokers. In addition, the preparation method of the fragrance enhanced granular additive for the filter sticks is simple and low in production cost, and industrial production can be realized.

Description

A kind of flavored type filter stick particulate additive and its preparation method and application
Technical field
The present invention relates to a kind of flavored type filter stick particulate additive and its preparation method and application, belong to production of cigarettes technical field.
Background technology
In recent years, both at home and abroad tobacco has carried out a large amount of research to the composite filter tip of multiple sorbing material, and research shows, cigarette filter is the important of a kind of reducing tar and reducing harm and effective means.Along with deepening continuously of the forming characteristic of various filter tip materials and strobe utility research, the exploitation of composite filter tip and apply the research emphasis becoming just gradually in one period at present and in the future.
The particulate adsorbent material that is applied at present cigarette filter material mostly is inorganic material as diatomite, active carbon, silica gel etc., they have special configuration of surface and many cavity structures, cigarette smoke is produced to efficient selective adsorption capacity, but had the problem such as assorted gas, change cigarette smoking style of introducing.And adopt the technological means such as expanding tobacco particle to realize the object of reducing tar and reducing harm, but in coke tar in cigarette, contain a large amount of fragrance matters, when reducing tar, lose tobacco suction taste.Therefore, how in reducing tar content in tobacco, to guarantee that do not lose fragrance and taste is the problem that industry emphasis is considered as far as possible.
Summary of the invention
For the deficiencies in the prior art, the object of the present invention is to provide one can discharge lastingly compound fragrant, and the flavored type filter stick particulate additive of while energy reducing tar and reducing harm.
Another object of the present invention is a kind of method that is to provide low cost, the described flavored type filter stick of simple and quick preparation particulate additive, and the method meets suitability for industrialized production.
The 3rd object of the present invention is to be to provide the application of flavored type filter stick particulate additive in cigarette filter rod, and flavored type filter stick additive is added in cigarette filter rod can effectively reduce tarry matters in smoke content, makes flue gas flavouring simultaneously.
The invention provides a kind of flavored type filter stick particulate additive, this additive is by compound the obtaining of following mass parts component:
1~10 part of dulcet edibility powder;
20~80 parts, plant granule powder;
1~5 part of binding agent;
1~5 part of swelling agent;
The dulcet edibility powder of described tool is one or more in ground coffee, cocoa power, rosemary, Xue MingRosma rinus officinalis powder, milk powder, fennel powder, coconut face powder;
Described plant granule powder is one or more in rice husk fine powder, walnut shell fine powder, corncob fine powder, pomelo peel fine powder.
Described binding agent is one or more in modified starch, shitosan, sodium alginate, pectin.
The described swelling agent of stating is one or more in ammonium nitrate, yeast powder, sodium bicarbonate, ammonia bicarbonate, alum, baking powder.
Described flavored type filter stick particulate additive biodiversity content control is 5%~12%.
Described flavored type filter stick particulate additive particle diameter is 30~60 orders.
Described flavored type filter stick particulate additive is prepared through solution mixing, extruder grain, microwave drying by the dulcet edibility powder of tool, plant granule powder, binding agent and swelling agent.
The present invention also provides a kind of preparation method of described flavored type filter stick particulate additive, and this preparation method mixes dulcet tool edibility powder, plant granule powder, binding agent and swelling agent, obtains dry powder material; In gained dry powder material, add after the water of 0.5~3 times of quality of dry powder material, be uniformly mixed, until mixture can pinch with hand time, is sent mixture into comminutor extruder grain, prepare 20~80 object wet granulars; Gained wet granular, sieves until moisture is not more than 12wt% by microwave drying, to obtain final product.
Described plant granule powder diameter is preferably 60~100 orders.
The quality optimization that adds water in described preparation method is dry powder material 1~2 times.
Described microwave drying is until moisture is preferably 5wt%~12wt%.
Described comminutor is preferably swing comminutor.
The present invention also provides a kind of application of described flavored type filter stick particulate additive, and this application is that described flavored type filter stick particulate additive is added in cigarette filter rod and is applied to cigarette smoke perfuming and reduces tarry matters in smoke content.
Described flavored type filter stick particulate additive is added in cigarette filter rod tow.
The addition of described flavored type filter stick particle in cigarette filter rod tow is 1mg/mm~3mg/mm.
Described flavored type filter stick particulate additive is evenly sprinkled upon cigarette in tow base material and becomes unit filter stick, then gained unit filter stick is further compound with the fine unit filter stick of vinegar or groove unit filter stick, obtains binary or multi-element composite filter stick.
Beneficial effect of the present invention: the present invention first by dulcet tool edibility powder and cheap plant granule powder by binding agent organic composite, introduce expanded reagent simultaneously and carry out microwave bulking, obtain a kind of swelling granular, be applied in cigarette filter rod, not only can lasting stability discharge the compound fragrance of pleasant, and can reducing tar and reducing harm.The plants particles material that the present invention selects is plant-derived discarded object all, cheap, safety non-toxic, resistance to good processability, be conducive to reduce the cost of compound additive, and these plants particles materials of selecting have abundant hole, particularly after the auxiliary lower microwave bulking of a small amount of expanded reagent, pore structure is more flourishing, the dulcet edibility powder of tool can be filled in hole well, and retain abundant micropore, make on the one hand the dulcet edibility powder of tool be subject to the stable lasting fragrance that discharges under heat effect, on the other hand, microcellular structure can adsorb harmful substances such as tar in flue gas.Flavouring filter stick additive of the present invention has the unrivaled technique effect of prior art: in cigarette filter rod, add consumption few, and large to tar reducing amount; When suction, there is special compound fragrant, contain the composite flavor of light plant delicate fragrance and the dulcet edibility powder of tool fragrance, the sense of taste, the scent experience of more enriching to smoker; Its preparation method is simple simultaneously, and low production cost, can suitability for industrialized production.
The specific embodiment
Following examples are intended to illustrate content of the present invention, rather than further restriction to protection domain of the present invention.
Embodiment 1
1, divide 5 parts of ground coffees of another name, 50 parts of 60~100 object powdered rice hulls, 1 part of water soluble chitosan, 5 parts of baking powders, fully mix, add 50 parts of running water to stir to obtain wet feed;
2, above-mentioned wet feed is sent into swing comminutor extruder grain, being prepared into order number is 20~80 object wet granulars;
3, above-mentioned wet granular material being used to microwave drying to pellet moisture is 5~12wt%, and further 30~60 object particles are got in screening, obtain filter stick particulate additive.
4, add this filter stick particulate additive in cigarette filter rod granulation base rod according to the addition of 1.5mg/mm fiber base material, be further complex as binary compound filter candle with the fine white rod of vinegar.This binary compound filter candle is applied in cigarette, compare and can reduce Cigarette grain phase 0.6mg left and right in the same old way, simultaneously before suction, can provide joyful coffee aroma to people, aspirate that seasonal consumer experiences joyful coffee pleasant impression and light rice husk toasts fragrant compound fragrant.
By the cigarette and the common fiber tow filter rods cigarette that adopt the present embodiment binary compound filter candle to make, transfer to specialized review person to smoke panel test, it is as shown in the table for smoking result:
Figure BDA0000472782550000041
Embodiment 2
1, divide 8 parts of milk powders of another name, 50 parts of 60~100 object maize cob meals, 1 part of sodium alginate, 5 parts of saleratus powers, fully mix, add 60 parts of running water to stir to obtain wet feed;
2, above-mentioned wet feed is sent into swing comminutor extruder grain, being prepared into order number is 20~80 object wet granulars;
3, use microwave drying to pellet moisture 5~12wt% in above-mentioned wet granular material, further 30~60 object particles are got in screening, obtain filter stick particulate additive.
4, add filter stick particulate additive in cigarette filter rod granulation base rod according to the addition of 2mg/mm fiber base material, be further complex as binary compound filter candle with the fine white rod of vinegar.This binary compound filter candle is applied in cigarette, compare and can reduce Cigarette grain phase 0.8mg left and right in the same old way, simultaneously before suction, can provide joyful milk fragrance to people, aspirate that seasonal consumer experiences joyful milk pleasant impression and light corn toasts fragrant compound fragrant.
By the cigarette and the common fiber tow filter rods cigarette that adopt the present embodiment filter stick to prepare, transfer to specialized review person to smoke panel test, it is as shown in the table for smoking result:
Figure BDA0000472782550000042
Embodiment 3
1, divide 3 parts, another name rosemary, Xue MingRosma rinus officinalis powder, 2 parts of fennel powders, 80 parts of 60~100 object walnut shell powders, 2 parts of modified starches, 3 parts of baking powders, fully mix, add 90 parts of running water to stir to obtain wet feed;
2, above-mentioned wet feed is sent into swing comminutor extruder grain, being prepared into order number is 20~80 object wet granulars;
3, above-mentioned wet granular material being used to microwave drying to pellet moisture is 7~12wt%, and further 30~60 object particles are got in screening, obtain filter stick particulate additive.
4, add this filter stick particulate additive in cigarette filter rod granulation base rod according to the addition of 1.5mg/mm fiber base material, be further complex as binary compound filter candle with the fine white rod of vinegar.This binary compound filter candle is applied in cigarette, compare and can reduce Cigarette grain phase 0.5mg left and right in the same old way, before suction, can provide joyful rosemary, Xue MingRosma rinus officinalis taste and fennel taste to people, aspirate seasonal consumer and experience joyful herbal and Xin Xiang compound fragrant simultaneously.
By the cigarette and the common fiber tow filter rods cigarette that adopt the present embodiment binary compound filter candle to make, transfer to specialized review person to smoke panel test, it is as shown in the table for smoking result:
Embodiment 4
1, divide 3 parts of milk powders of another name, 5 parts of ground coffees, 30 parts of 60~100 object maize cob meals, 1 part of pectin, 5 parts of ammonia bicarbonates, fully mix, add 60 parts of running water to stir to obtain wet feed;
2, above-mentioned wet feed is sent into swing comminutor extruder grain, being prepared into order number is 20~80 object wet granulars;
3, use microwave drying to pellet moisture 5~10wt% in above-mentioned wet granular material, further 30~60 object particles are got in screening, obtain filter stick particulate additive.
4, add this filter stick particulate additive in cigarette filter rod granulation base rod according to the addition of 2.5mg/mm fiber base material, be further complex as binary compound filter candle with the fine white rod of vinegar.This binary compound filter candle is applied in cigarette, compare and can reduce Cigarette grain phase 0.8mg left and right in the same old way, simultaneously before suction, can provide joyful coffee with milk compound fragrant to people, aspirate seasonal consumer and experience joyful milk and coffee pleasant impression and light corn and toast fragrant compound fragrant.
Cigarette and common fiber tow filter rods cigarette that the binary compound filter candle that adopts the present embodiment to make is made, transfer to specialized review person to smoke panel test, and it is as shown in the table for smoking result:
Figure BDA0000472782550000061
Embodiment 5
1, divide 1 part of milk powder of another name, 4 parts of coconut powders, 60~100 50 parts, object pomelo peel powder, 1 part of pectin, 5 parts of baking powders, fully mix, add 60 parts of running water to stir to obtain wet feed;
2, above-mentioned wet feed is sent into swing comminutor extruder grain, being prepared into order number is 20~80 object wet granulars;
3, use microwave drying to pellet moisture 7~10wt% in above-mentioned wet granular material, further 30~60 object particles are got in screening, obtain cigarette filter rod particulate additive.
4, add this cigarette filter rod particulate additive in cigarette filter rod granulation base rod according to the addition of 1.2mg/mm fiber base material, be further complex as binary compound filter candle with the fine white rod of vinegar.This binary compound filter candle is applied in cigarette, compare and can reduce Cigarette grain phase 0.8mg left and right in the same old way, simultaneously before suction, can provide joyful coffee with milk compound fragrant to people, aspirate seasonal consumer and experience the compound fragrant of joyful milk and fruit perfume (or spice).
Cigarette and common fiber tow filter rods cigarette that the binary compound filter candle that adopts the present embodiment to make is made, transfer to specialized review person to smoke panel test, and it is as shown in the table for smoking result:
Figure BDA0000472782550000062

Claims (14)

1. a flavored type filter stick particulate additive, is characterized in that, by compound the obtaining of following mass parts component:
1~10 part of the dulcet edibility powder of tool;
20~80 parts, plant granule powder;
1~5 part of binding agent;
1~5 part of swelling agent;
The dulcet edibility powder of described tool is one or more in ground coffee, cocoa power, rosemary, Xue MingRosma rinus officinalis powder, milk powder, fennel powder, coconut face powder;
Described plant granule powder is one or more in rice husk fine powder, walnut shell fine powder, corncob fine powder, pomelo peel fine powder.
2. flavored type filter stick particulate additive as claimed in claim 1, is characterized in that, described binding agent is one or more in modified starch, shitosan, sodium alginate, pectin.
3. flavored type filter stick particulate additive as claimed in claim 1, is characterized in that, described swelling agent is one or more in ammonium nitrate, yeast powder, sodium bicarbonate, ammonia bicarbonate, alum, baking powder.
4. flavored type filter stick particulate additive as claimed in claim 1, is characterized in that, described flavored type filter stick particulate additive biodiversity content control is 5%~12%.
5. flavored type filter stick particulate additive as claimed in claim 1, is characterized in that, described particulate additive particle diameter is 30~60 orders.
6. the flavored type filter stick particulate additive as described in claim 1~5 any one, it is characterized in that, described flavored type filter stick particulate additive is prepared through solution mixing, extruder grain, microwave drying by the dulcet edibility powder of tool, plant granule powder, binding agent and swelling agent.
7. a preparation method for the flavored type filter stick particulate additive as described in claim 1~5 any one, is characterized in that, dulcet tool edibility powder, plant granule powder, binding agent and swelling agent are mixed, and obtains dry powder material; In gained dry powder material, add after the water of 0.5~3 times of quality of dry powder material, be uniformly mixed, until mixture can pinch with hand time, is sent mixture into comminutor extruder grain, prepare 20~80 object wet granulars; Gained wet granular, sieves until moisture is not more than 12wt% by microwave drying, to obtain final product.
8. preparation method as claimed in claim 7, is characterized in that, described plant granule powder diameter is 60~100 orders.
9. preparation method as claimed in claim 7, is characterized in that, the quality that adds water is dry powder material 1~2 times.
10. preparation method as claimed in claim 7, is characterized in that, described microwave drying is until moisture is 5wt%~12wt%.
The application of 11. 1 kinds of flavored type filter stick particulate additives as described in claim 1~5 any one, is characterized in that, described flavored type filter stick particulate additive is added in cigarette filter rod and is applied to cigarette smoke perfuming and reduces tarry matters in smoke content.
12. application as claimed in claim 11, is characterized in that, described flavored type filter stick particulate additive is added in cigarette filter rod tow.
13. application as claimed in claim 12, is characterized in that, the addition of described flavored type filter stick particulate additive in cigarette filter rod tow is 1mg/mm~3mg/mm.
14. application as claimed in claim 11, it is characterized in that, described flavored type filter stick particulate additive is evenly sprinkled upon cigarette in tow base material and becomes unit filter stick, then gained unit filter stick is further compound with the fine unit filter stick of vinegar or groove unit filter stick, obtains binary or multi-element composite filter stick.
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Cited By (13)

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CN105167185A (en) * 2015-07-28 2015-12-23 云南天宏香精香料有限公司 Natural filter rod particle material as well as preparation method and application thereof
CN108713793A (en) * 2018-07-27 2018-10-30 内蒙古昆明卷烟有限责任公司 A kind of composite filter and preparation method thereof with milk sweet fragrance
CN109123774A (en) * 2017-06-28 2019-01-04 湖南中烟工业有限责任公司 It is a kind of to assign fragrant cigarette filter rod and its preparation and application naturally
CN109123772A (en) * 2017-06-28 2019-01-04 湖南中烟工业有限责任公司 A kind of cigarette filter rod with flavoring function, preparation method and applications
CN110250565A (en) * 2019-06-10 2019-09-20 江西中烟工业有限责任公司 A kind of plant granule perfume (or spice) pearl and the preparation method and application thereof
CN110464040A (en) * 2019-07-16 2019-11-19 河南中烟工业有限责任公司 A kind of preparation method and application dropping the porous particle that smells good
CN110680008A (en) * 2019-09-19 2020-01-14 上海华宝生物科技有限公司 Porous solid aromatic bead for cigarettes and preparation method thereof
CN111567841A (en) * 2020-04-23 2020-08-25 红云红河烟草(集团)有限责任公司 Novel cigarette filter stick flavoring particle and preparation method thereof
CN111616404A (en) * 2020-06-05 2020-09-04 安徽中烟工业有限责任公司 Microwave drying method for heating particles for cigarettes
US10966453B2 (en) 2015-04-29 2021-04-06 British American Tobacco (Investments) Limited Flavouring component, and apparatus and method for manufacturing a flavouring component
CN113693276A (en) * 2021-09-03 2021-11-26 云南养瑞科技集团有限公司 Fermented glutinous rice aroma-enhancing granule and preparation method thereof
CN114621818A (en) * 2022-03-09 2022-06-14 山东省食品发酵工业研究设计院 Nano essence particles for cigarette filter stick and preparation method thereof
CN114766718A (en) * 2022-04-24 2022-07-22 云南养瑞科技集团有限公司 Cigarette aroma-carrying particle, preparation method and application thereof

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Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10966453B2 (en) 2015-04-29 2021-04-06 British American Tobacco (Investments) Limited Flavouring component, and apparatus and method for manufacturing a flavouring component
CN105167185A (en) * 2015-07-28 2015-12-23 云南天宏香精香料有限公司 Natural filter rod particle material as well as preparation method and application thereof
CN105167185B (en) * 2015-07-28 2018-09-11 云南芯韵科技开发有限公司 A kind of natural filter stick granular materials and the preparation method and application thereof
CN109123772A (en) * 2017-06-28 2019-01-04 湖南中烟工业有限责任公司 A kind of cigarette filter rod with flavoring function, preparation method and applications
CN109123774A (en) * 2017-06-28 2019-01-04 湖南中烟工业有限责任公司 It is a kind of to assign fragrant cigarette filter rod and its preparation and application naturally
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CN108713793A (en) * 2018-07-27 2018-10-30 内蒙古昆明卷烟有限责任公司 A kind of composite filter and preparation method thereof with milk sweet fragrance
CN113662243A (en) * 2018-07-27 2021-11-19 内蒙古昆明卷烟有限责任公司 Composite filter stick with milk sweet fragrance and preparation method thereof
CN110250565A (en) * 2019-06-10 2019-09-20 江西中烟工业有限责任公司 A kind of plant granule perfume (or spice) pearl and the preparation method and application thereof
CN110464040A (en) * 2019-07-16 2019-11-19 河南中烟工业有限责任公司 A kind of preparation method and application dropping the porous particle that smells good
CN110680008A (en) * 2019-09-19 2020-01-14 上海华宝生物科技有限公司 Porous solid aromatic bead for cigarettes and preparation method thereof
CN111567841A (en) * 2020-04-23 2020-08-25 红云红河烟草(集团)有限责任公司 Novel cigarette filter stick flavoring particle and preparation method thereof
CN111616404A (en) * 2020-06-05 2020-09-04 安徽中烟工业有限责任公司 Microwave drying method for heating particles for cigarettes
WO2021243937A1 (en) * 2020-06-05 2021-12-09 安徽中烟工业有限责任公司 Method for microwave drying granules for making heated cigarettes
CN113693276A (en) * 2021-09-03 2021-11-26 云南养瑞科技集团有限公司 Fermented glutinous rice aroma-enhancing granule and preparation method thereof
CN114621818A (en) * 2022-03-09 2022-06-14 山东省食品发酵工业研究设计院 Nano essence particles for cigarette filter stick and preparation method thereof
CN114766718A (en) * 2022-04-24 2022-07-22 云南养瑞科技集团有限公司 Cigarette aroma-carrying particle, preparation method and application thereof

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