CN110464040A - A kind of preparation method and application dropping the porous particle that smells good - Google Patents
A kind of preparation method and application dropping the porous particle that smells good Download PDFInfo
- Publication number
- CN110464040A CN110464040A CN201910641710.5A CN201910641710A CN110464040A CN 110464040 A CN110464040 A CN 110464040A CN 201910641710 A CN201910641710 A CN 201910641710A CN 110464040 A CN110464040 A CN 110464040A
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- CN
- China
- Prior art keywords
- porous particle
- drop
- smells good
- good
- powder
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Abstract
The present invention relates to a kind of preparation method and application for dropping the porous particle that smells good, selection drops smell good particle, plant powder and polymer binder and Ultramicro-powder porous particle is made by fluidized bed spray granulation technique；Ultramicro-powder porous particle impregnating equipment addition leavening agent is obtained into dipping porous particle；Dipping porous particle is sent into microwave equipment and is expanded, it is obtained to drop the porous particle that smells good.The drop of the technical program porous particle that smells good has good improvement result to cigarette smoke, and can adsorb and reduce the carcinogen in flue gas after making an addition to filter stick with aromatic odor.
Description
Technical field
The invention belongs to technical field of cigarettes, particularly relate to tobacco spice technology of preparing, and espespecially a kind of drop smells good porous
The preparation method and application of grain.
Background technique
Drop smells good, also known as drop is true, dalbergia wood, Thickleaf Croton Root, tanarius major (unrelated with plant Chinese wistaria), is distributed mainly on China Hainan
It saves.
When drop smells good wood by extraneous factor destruction epidermis, it will start self-protective mechanism, secreted on surface a variety of
Juice forms grease solid-state condensation product, and finally callus repairs it again, grows new tissue.Time is more long, grease density
It is higher.
Li Shizhen of the Ming Dynasty is mentioned in Compendium of Material Medica: " Thickleaf Croton Root is dalbergia wood " originally goes out Hainan." perfume spectrum " reference " Nan Zhou
Note " also mention its place of production: " raw Hainan Zhu Shan ".What Nationality in Hainan Province was exhaled is also known as Hua Ligong for La diu (the best fragrant material of implied meaning).
The ancient book in the Hainan Miao Shu native country " precipice state will " also on the books " flower pears, aubergine smell good similar to drop "." lattice will " records " flower pears
Wood goes out Hainan, Guangdong, and aubergine and drop smell good wooden similar, also there is perfume (or spice) ".And Hainan Miao ethnic group is called agalloch eaglewood public affairs, green agalloch eaglewood, green perfume (or spice)
Tree, the wooden dalbergia wood.
Smell good containing alkaloids, phenols and volatile oil compound drop, and drop smells good leaf with aromatic odor, can treat sense
It emits, cough, ripe fruit is edible, and pulp is sweet, micro-strip numb feeling in the tongue, and it is aid digestion to be used as medicine, and root can stop blooding analgesic therapy, detumescence and promoting granulation, flat
Asthma, resin have the effects that antipyretic, stop dysentery.Modern pharmacological studies have shown that drop smells good with antitumor, antibacterial and cytotoxicity
Etc. bioactivity.
Drop is smelt good to be used in cigarette also only be related to drop and smells good extract as feed liquid or flavouring essence for tobacco, it is true for drop
Perfume (or spice) is processed into porous particle, is especially used in cigarette field there is not yet relevant report.
Summary of the invention
The object of the present invention is to provide a kind of preparation method and applications for dropping the porous particle that smells good, and are being rolled up with improving to drop to smell good
The application of cigarette technical field.Contain the novel of the cigarette filter rod for dropping the porous particle that smells good it is a further object of the present invention to provide a kind of
Smoking material.
The present invention is achieved by the following technical solutions；
A kind of preparation method dropping the porous particle that smells good, comprising the following steps:
1) it chooses smell good particle, plant powder and polymer binder of drop and ultra micro is made by fluidized bed spray granulation technique
Powder porous particle；
2) the Ultramicro-powder porous particle is added in impregnating equipment, the impregnating equipment is vacuumized, is set to dipping
Standby middle addition leavening agent, and it is filled with nitrogen, so that pressure in the impregnating equipment is reached the first setting pressure, in 60 DEG C of -100 DEG C of leachings
Stain 30min obtains dipping porous particle；
3) dipping porous particle is sent into microwave equipment, uses power density for 8-9kW/m in 100 DEG C -120 DEG C2
Microwave equipment expanded, Bulking Time 60s, obtained drop smells good porous particle.
The plant powder is porous plant powder.
The plant powder is porous kudzu-vine root powder.
The polymer binder is edible gelatin.
By mass percentage, the edible gelatin accounts for the Ultramicro-powder porous particle no more than 5%.
Further include pretreatment process before the step 2), the moisture content of the Ultramicro-powder porous particle is reached
15%-17%.
Described first sets pressure as 0.6MPa.
The drop of any of the above-described smells good porous particle in the filter stick of cigarette.
During filter stick formation, the porous particle that smells good will be dropped and evenly spread in the fibre bundle of filter stick.
The drop smells good dosage of the porous particle in fibre bundle as 1-3mg/mm.
The beneficial effects of the present invention are:
The drop of the technical program porous particle that smells good has cigarette smoke good after making an addition to filter stick with aromatic odor
Good improvement result, and can adsorb and reduce the carcinogen in flue gas.
Specific embodiment
Carry out the technical solution that the present invention will be described in detail by the following examples, embodiment below is merely exemplary, only
It can be used to explanation and illustration technical solution of the present invention, and be not to be construed as the limitation to technical solution of the present invention.
The application provides a kind of preparation method for dropping the porous particle that smells good, comprising the following steps:
1) it chooses smell good particle, plant powder and polymer binder of drop and ultra micro is made by fluidized bed spray granulation technique
Powder porous particle；In this application, it chooses Hainan drop to smell good, is ground into the particle of 200 mesh, plant powder is porous Plant Powder
End, plant powder is porous kudzu-vine root powder, in the other embodiments of the application, or other porous plant powders, drop are true
The mass ratio of fragrant particle and plant powder is such as the 1-10:1-10 according to needing to be adjusted, in the technical scheme without
Specific regulation.
Polymer binder is edible gelatin.By mass percentage, edible gelatin accounts for Ultramicro-powder porous particle and is no more than
5%.
In this application, the fluidized bed spray granulation technique used is existing food, common technique in drug, herein not into
Row detailed description.
2) Ultramicro-powder porous particle is added in impregnating equipment, impregnating equipment is vacuumized, be added into impregnating equipment
Leavening agent, and it is filled with nitrogen, so that pressure in impregnating equipment is reached 0.6MPa, in 60 DEG C of -100 DEG C of dipping 30min, preferable temperature is
80 DEG C -100 DEG C, obtain dipping porous particle；In this application, impregnating equipment is only for realizing setting for technical scheme
Standby, all equipment that can be realized dipping function are intended merely to vacuumizing function, after the vacuumizing of the application, pressure
Lower than 0.05MPa.
In this application, swelling agent includes ketone, the 2-12 carbon atom of the alcohol of 4-12 carbon atom, 4-12 carbon atom
One of halogen ether, the alkane of 3-12 carbon atom or the alkane of 3-12 carbon atom that is replaced by 2 or more halogen atoms group
Point or two or more components mixture.
Further include pretreatment process before step 2), the moisture content of Ultramicro-powder porous particle is reached into 15%-17%.
3) dipping porous particle is sent into microwave equipment, uses power density for 8-9kW/m in 100 DEG C -120 DEG C2
Microwave equipment expanded, Bulking Time 60s, obtained drop smells good porous particle.
The application also provides a kind of application for dropping the porous particle that smells good, during filter stick formation, by any of the above-described
It drops the porous particle that smells good to evenly spread in the fibre bundle of filter stick, the filter stick fibre bundle of the application can be common acetic acid
Fibre bundle is also possible to other fibre bundles for being suitable for preparing filter stick.Dropping the porous particle that smells good in the dosage of filter stick is 1-
3mg/mm refers to every millimeter of fibre bundle, is smelt good porous particle using the drop of 1-3mg.
The drop of the technical program porous particle that smells good has cigarette smoke good after making an addition to filter stick with aromatic odor
Good improvement result, and can adsorb and reduce the carcinogen in flue gas.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And deformation, the scope of the present invention is by appended claims and its equivalent limits.
Claims (10)
- The preparation method of porous particle 1. a kind of drop smells good, which comprises the following steps:1) it chooses drop and smells good that by fluidized bed spray granulation technique Ultramicro-powder to be made more for particle, plant powder and polymer binder Hole particle；2) the Ultramicro-powder porous particle is added in impregnating equipment, the impregnating equipment is vacuumized, into impregnating equipment Leavening agent is added, and is filled with nitrogen, pressure in the impregnating equipment is made to reach the first setting pressure, in 60 DEG C of -100 DEG C of dippings 30min obtains dipping porous particle；3) dipping porous particle is sent into microwave equipment, uses power density for 8-9kW/m in 100 DEG C -120 DEG C2Microwave Equipment is expanded, Bulking Time 60s, and obtained drop smells good porous particle.
- The preparation method of porous particle 2. drop according to claim 1 smells good, which is characterized in that the plant powder is more Hole plant powder.
- The preparation method of porous particle 3. drop according to claim 2 smells good, which is characterized in that the plant powder is more Hole kudzu-vine root powder.
- The preparation method of porous particle 4. drop according to claim 1 smells good, which is characterized in that the polymer binder For edible gelatin.
- The preparation method of porous particle 5. drop according to claim 4 smells good, which is characterized in that by mass percentage, The edible gelatin accounts for the Ultramicro-powder porous particle no more than 5%.
- The preparation method of porous particle 6. drop according to claim 1 smells good, which is characterized in that before the step 2) Further include pretreatment process, the moisture content of the Ultramicro-powder porous particle is reached into 15%-17%.
- The preparation method of porous particle 7. drop according to claim 1 smells good, which is characterized in that the first setting pressure For 0.6MPa.
- 8. the drop of any of the above-described smells good, porous particle is in the filter stick of cigarette.
- 9. filter stick according to claim 8, which is characterized in that during filter stick formation, the drop porous particle that smells good is equal It is even to be distributed in the fibre bundle of filter stick.
- 10. filter stick according to claim 9, which is characterized in that described to drop use of the porous particle in fibre bundle that smells good Amount is 1-3mg/mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910641710.5A CN110464040A (en) | 2019-07-16 | 2019-07-16 | A kind of preparation method and application dropping the porous particle that smells good |
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|---|---|---|---|
| CN201910641710.5A CN110464040A (en) | 2019-07-16 | 2019-07-16 | A kind of preparation method and application dropping the porous particle that smells good |
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| CN110464040A true CN110464040A (en) | 2019-11-19 |
Family
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| CN201910641710.5A Pending CN110464040A (en) | 2019-07-16 | 2019-07-16 | A kind of preparation method and application dropping the porous particle that smells good |
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Citations (9)
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|---|---|---|---|---|
| CN1307843A (en) * | 2000-12-12 | 2001-08-15 | 吴凡 | Cigarette with Chinese herbal medicine |
| CN101601502A (en) * | 2009-07-01 | 2009-12-16 | 云南瑞升烟草技术（集团）有限公司 | A kind of preparation method of cabo particle |
| CN102462831A (en) * | 2010-11-10 | 2012-05-23 | 姜晓烨 | Healthcare composition providing cigarettes with throat-moistening and refreshing functions, and production method thereof |
| CN103876285A (en) * | 2014-03-04 | 2014-06-25 | 湖南中烟工业有限责任公司 | Fragrance enhanced granular additive for filter sticks and preparation method and application thereof |
| CN103932394A (en) * | 2013-01-23 | 2014-07-23 | 湖南中烟工业有限责任公司 | Multi-section composite cigarette filtering stick, preparation method thereof and application of turgid plant granules |
| CN103689801B (en) * | 2013-12-03 | 2015-04-08 | 红云红河烟草(集团)有限责任公司 | Kudzuvine root porous particles and application thereof to cigarettes |
| WO2015075452A1 (en) * | 2013-11-22 | 2015-05-28 | British American Tobacco (Investments) Limited | Adsorbent materials |
| CN104687246A (en) * | 2015-01-05 | 2015-06-10 | 云南中烟工业有限责任公司 | Porous moringa oleifera particles, preparation method of porous moringa oleifera particles as well as cigarette filter stick containing porous particles |
| CN105670792A (en) * | 2016-02-03 | 2016-06-15 | 云南中烟工业有限责任公司 | Preparing method and application of cigarette filter tip expansion granular material |
-
2019
- 2019-07-16 CN CN201910641710.5A patent/CN110464040A/en active Pending
Patent Citations (9)
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| CN1307843A (en) * | 2000-12-12 | 2001-08-15 | 吴凡 | Cigarette with Chinese herbal medicine |
| CN101601502A (en) * | 2009-07-01 | 2009-12-16 | 云南瑞升烟草技术（集团）有限公司 | A kind of preparation method of cabo particle |
| CN102462831A (en) * | 2010-11-10 | 2012-05-23 | 姜晓烨 | Healthcare composition providing cigarettes with throat-moistening and refreshing functions, and production method thereof |
| CN103932394A (en) * | 2013-01-23 | 2014-07-23 | 湖南中烟工业有限责任公司 | Multi-section composite cigarette filtering stick, preparation method thereof and application of turgid plant granules |
| WO2015075452A1 (en) * | 2013-11-22 | 2015-05-28 | British American Tobacco (Investments) Limited | Adsorbent materials |
| CN103689801B (en) * | 2013-12-03 | 2015-04-08 | 红云红河烟草(集团)有限责任公司 | Kudzuvine root porous particles and application thereof to cigarettes |
| CN103876285A (en) * | 2014-03-04 | 2014-06-25 | 湖南中烟工业有限责任公司 | Fragrance enhanced granular additive for filter sticks and preparation method and application thereof |
| CN104687246A (en) * | 2015-01-05 | 2015-06-10 | 云南中烟工业有限责任公司 | Porous moringa oleifera particles, preparation method of porous moringa oleifera particles as well as cigarette filter stick containing porous particles |
| CN105670792A (en) * | 2016-02-03 | 2016-06-15 | 云南中烟工业有限责任公司 | Preparing method and application of cigarette filter tip expansion granular material |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20191119 |
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| RJ01 | Rejection of invention patent application after publication |