CN101828769B - Preparation method of cigarette flavor compensating particles - Google Patents

Preparation method of cigarette flavor compensating particles Download PDF

Info

Publication number
CN101828769B
CN101828769B CN2010101486822A CN201010148682A CN101828769B CN 101828769 B CN101828769 B CN 101828769B CN 2010101486822 A CN2010101486822 A CN 2010101486822A CN 201010148682 A CN201010148682 A CN 201010148682A CN 101828769 B CN101828769 B CN 101828769B
Authority
CN
China
Prior art keywords
silicic acid
preparation method
particles
acid rock
cigarette
Prior art date
Application number
CN2010101486822A
Other languages
Chinese (zh)
Other versions
CN101828769A (en
Inventor
孙晓刚
沈彦文
范馨雷
洪学晖
杨涛
Original Assignee
云南正邦生物技术有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 云南正邦生物技术有限公司 filed Critical 云南正邦生物技术有限公司
Priority to CN2010101486822A priority Critical patent/CN101828769B/en
Publication of CN101828769A publication Critical patent/CN101828769A/en
Application granted granted Critical
Publication of CN101828769B publication Critical patent/CN101828769B/en

Links

Abstract

The invention relates to a preparation method of cigarette flavor compensating particles, in particular to a filtering material added to a cigarette filter and the preparation method of the material, belonging to the technical field of a cigarette auxiliary material. The cigarette flavor compensating particles are mainly composed of a silicic acid rock base material and a flavor carrying agent; bulking silicic acid rock is taken as a raw material; a loading agent is added; and finally the silicic acid rock load particles are formed by loading, drying, granulating and other processes. In the preparation method, particle materials are from the silicic acid rock and a natural plant material, and the silicic acid rock has better absorption characteristics; after loading and microwave treatment, the silicic acid rock particles have no influence on cigarette flavor, and the employed loading agent has the action of synergetic harm reduction at the same time; and a formula plant extract and plant fiber loaded on the surface of the particles can effectively release quantitative flavor elements and transfers the flavor elements to sucked smoke. The silicic acid rock particles prepared by the method can be used for directly combining with the current filter tip forming process, thus achieving convenient industrialized application.

Description

The preparation method of cigarette flavor compensating particles

Technical field

The invention belongs to cigarette auxiliary material technical field, particularly the filtering material that adds in the cigarette filter and this preparation methods.

Background technology

Pipe tobacco and cigarette paper produce flue gas by burning, the cigarette filter flue gas that dams, the flue gas that finally forms the consumer and sucked.Filter tip can become one of key link of cigarette smoke quality-improving.The form of filter tip is rich and varied at present has excellent filter tip in binary composite filter tip, ternary composite filter tip, hollow filter tip, the rod, spices line filter tip and adsorbs line filter tip etc.Under the big situation of reducing tar and reducing harm, the unconspicuous problem of fragrance deficiency or characteristic can appear in various brand cigarettes unavoidably.Here the compensation technique of specialize fragrance and the fragrance concentration in the flue gas becomes a research and development focus.

Chinese patent application " silicic acid rock cigarette with filter tip ", application number: 200420104785.9, disclose a kind of one or more silicic acid rock by the cigarette with filter tip of cigarette filter axially-aligned in the mouth rod, mentioned this filter tip in the invention and can obviously reduce the cigarette harmfulness.But silicic acid rock structure is fluffy, frangible, do not have at present technology and equipment can with its according to the filter tip axially-aligned in the acetate fiber or the third fine mouth rod, can't industrialization.And this silicic acid rock particle does not have functional flue gas compensate function.The present invention strengthens loose silicic acid rock in technology, makes its quality and density be satisfied with the demand of industrial applications.

Chinese patent application numbers 200710066121.6 discloses a kind of with the technology that joins after the granulation of microwave expansion offal in the mouth rod, though the cabo particle that this technology is used has certain cigarette perfume (or spice), but it does not have, and when the flue gas colloidal sol of uniform temperature flows through, discharges the effect of fragrance rapidly.It compensates the functional unsatisfactory of fragrance.

At present the actual adsorption particle that uses is mainly activated carbon granule in cigarette, and its little molecule ability of damming is stronger, the harm that can lower cigarette, but it is very limited to lowering tar, and carbon granule can drop to the plume end and causes influencing cigarette odor-absorbing.

And report multiple falls burnt additive such as porous-starch, silicates as (sepiolite, bentonite, medical stone, zeolite and molecular screen material that some are synthetic or the like), tar and harmful components all there is separately advantage, but these materials all have the adding technology complexity, can introduce the deficiency of assorted gas after the burning.And this type of report does not all appear at the technology that the particle surface load discharges fragrance component.

Therefore, how to pass through the extraction and the complex technique of natural material, produce when flue gas is flowed through and balancedly to discharge fragrance, and have the composite tip stick particle of the availability of mouth rod suitability for industrialized production.It is the product technology that present cigarette product very needs.

Summary of the invention

Purpose of the present invention is intended to overcome the defective of prior art, and providing a kind of is the method for feedstock production cigarette flavor compensating particles with silicic acid rock and vegetable material and natural plant extracts.

The real cigarette supplementary field that belongs to of the silicic acid batholith plinth preparation methods of cigarette flavor compensating particles, use expanded silicic acid rock and load-carrying agent to be raw material, by load-carrying, dry, granulation, form silicic acid rock loaded particle etc. technology, it has the proportion of appropriateness, abundant porous, in the mouth rod, add the characteristics that can not introduce assorted gas and dust sense, use natural plant material and silicic acid batholith plinth material to be raw material simultaneously, by extracting, load, cure, steps such as granulation obtain cigarette flavor compensating particles, it has the proportion of appropriateness, abundant porous, very easily, in the mouth rod, add the characteristic perfume characteristics that to introduce with the tobacco harmony by the surface microscopic feature of aerosol wash-out.Its preparation method is:

A, select materials: choose moisture≤4%, the expanded silicic acid rock of particle diameter between 20~100 orders;

B, the load-carrying agent is water-soluble adds on the silicic acid rock, stirs, and normal temperature and pressure was stored 1~12 hour down;

C, with step b gained silicic acid rock oven dry, dry to moisture≤4%;

D, the silicic acid rock after will drying sieve, and particle diameter is greater than 20 purpose silicic acid rock particle granulations once more, grade at 20~100 orders with the interior silicic acid batholith material that promptly gets;

E, at least a vegetable material in Radix Glycyrrhizae, Momordica grosvenori, honeysuckle, ginkgo leaf, loguat leaf, Chloranthus glaber, cocoa, coffee, tree moss, oak moss, burley tobaccos, solarization tobacco, Zimbabwe's tobacco leaf, Yuxi tobacco leaf, fragrant citrus, wrinkled giant hyssop, little eggplant perfume (or spice) and the rush used the mixed solvent refluxing extraction of ethanol, water, propane diols respectively, at least a plant residue after extracting is dried respectively, and be ground into respectively less than 80 purpose fine powders, to extract at least a extract and at least a residue fine powder and mix, and make and carry pastil;

F, will carry in the base material that pastil joins gained in the steps d, mix, place 1 to 6 hours;

G, with the compound that obtains among the step f, dry once more to moisture be 8%~14%, granulate, particle sieves, sieve is got 20~100 purpose particles and is qualified cigarette flavor compensating particles.

The bulk density of the described expanded silicic acid rock of step a is 0.01~0.2g/cm 3

The addition of the described load-carrying agent of step b is: the weight part ratio of raw material and load-carrying agent is 1: 1~9.

The described oven dry of step c is a microwave drying.

The described oven dry of step g is a microwave drying.

The described silicic acid batholith of steps d material, proportion is at 0.1~2.5g/cm 3Between.

The described vegetable material of step e is plant extraction liquid and string.

The described load-carrying agent of step b is one or more the combination in NaCl, natrium citricum, potassium citrate, natrium malicum, the potassium malate.When the load-carrying agent was in NaCl, natrium citricum, potassium citrate, natrium malicum, the potassium malate two kinds, it mixed part than being: 1: 1-5.

The preparation method of cigarette flavor compensating particles of the present invention, the cigarette flavor compensating particles that the step g preparation is got directly adds in the mouth rod of cigarette, and addition is that every millimeter mouth rod adds 0.1mg~3.0mg.

According to preparation method's gained cigarette flavor compensating particles of cigarette flavor compensating particles of the present invention, this kind particle can directly be passed to the characteristic perfume of vegetable material, damp sense, pharmacology active ingredient in the flue gas.Because do not pass through violent combustion reaction, the effect of the real genus of this kind flavor compensating method aerosol wash-out combines with distillation, so can intactly transmit these compositions.

Adopt the method for the invention preparation and cigarette flavor compensating particles, silicic acid rock microstructure is loose multi-pore structure, has aeration preferably, but silicic acid rock proportion own kicks the beam, and makes brokenly easily, and can not add in the mouth rod.The silicic acid rock itself has a kind of dust sense, can influence the suction flavor of cigarette, and the aesthetic quality is had negative effect, can not directly use in cigarette.Raw material of the present invention uses the silicic acid rock, after the load-carrying processing, crystal in the loose multi-pore structure plays the effect of flow-disturbing flue gas, the load-carrying agent of Jia Ruing simultaneously itself has the function that absorbs harmful ingredients in flue gas, can assist to fall evil, and particle proportion increases, intensity rises, the dust sense of silicic acid rock is removed, and adds prescription plant extracts and string in the silicic acid rock of handling, and makes its surface have the penetrating fragrant structure of loose government official.Thereby formed a kind of new material that in cigarette filter tip, adds.

The preparation method of cigarette flavor compensating particles of the present invention, granular materials derives from silicic acid rock and natural plant material, and the silicic acid rock has possessed characterization of adsorption preferably; After load-carrying, microwave treatment, silicic acid rock particle does not have influence to cigarette odor-absorbing, and the load-carrying agent of being adopted has the collaborative harmful effect of falling simultaneously.The prescription plant extracts and the string that are carried on particle surface can discharge quantitative fragrance component effectively, are delivered in the flue gas of suction.The silicic acid rock particle that preparation gets according to the method for the invention directly can directly use in conjunction with present mouth rod forming technology, and industrial applications is convenient.

Description of drawings

Fig. 1 is the preparation method's of a cigarette flavor compensating particles of the present invention process chart.

Fig. 2 is silicic acid rock raw material Electronic Speculum figure.

The cigarette flavor compensating particles finished particle Electronic Speculum figure of Fig. 3 for adopting preparation method of the present invention to make.

The specific embodiment

Below by embodiment, the invention will be further described for associative list 1 and table 2, but they are not limitation of the invention.

Embodiment 1

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, and bulk density is 0.01g/cm 3Expanded silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 1kg sodium chloride, 1kg natrium malicum, 12kg water, be mixed with the load-carrying agent;

C, with the load-carrying agent for preparing, add on the expanded silicic acid rock;

D, stir, stored 6 hours;

E, microwave drying are handled, and below the moisture drying to 4.0%, get silicic acid batholith material;

F, will cure the silicic acid rock that finishes and sieve, and choose particle diameter 20 to 80 purpose products, particle diameter is greater than the granulation once more of 20 purposes;

G, the ginkgo leaf with dry and high quality, Radix Glycyrrhizae pulverizing are the water of 55% ethanol and 10% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 3 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders, string;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid batholith material among the f;

J, mix, placed 1 hour, microwave cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 30 to 40 purpose products.

Select 30~40 order particles, add the 1.2mg amount according to every millimeter mouth rod and make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Inhale flavor and introduced new feature, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases.See Table 2.

Embodiment 2

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, density 0.2g/cm 3The silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 500g sodium chloride, 1kg natrium malicum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir, stored 1 hour;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, and choose 20 to 40 purpose particles, particle diameter is greater than the granulation once more of 20 purposes;

G, the Momordica grosvenori with dry and high quality, Radix Glycyrrhizae pulverizing are the water of 65% ethanol, 15% propane diols and surplus with weight ratio, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders, string;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid rock of gained among the f;

J, mix, placed 6 hours, microwave cure to moisture be 8% to 10%;

K, the product that obtains among the j is granulated, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 0.12mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.It is pure to inhale the sweet rhythm of flavor, and the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases.See Table 2.

Embodiment 3

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, select bulk density 0.1g/cm 3The silicic acid rock, material particle size should be below 40 orders;

B, with 2kg sodium chloride, 500g natrium citricum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 2 hours down;

E, microwave drying are handled, below the moisture drying to 10.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 40 to 60 purpose particles, silicic acid batholith material particle;

G, the Momordica grosvenori with dry and high quality, Radix Glycyrrhizae, honeysuckle, loguat leaf are pulverized, and are the water of 75% ethanol, 5% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid batholith material particle among the f;

J, mix, placed 3.5 hours, microwave cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 40 to 60 purpose products.

Particle is added the 3.0mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Inhaling flavor has sweet rhythm, and in an elegant style, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases.See Table 2.

Embodiment 4

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening, bulk density 0.2g/cm 3The silicic acid rock, material particle size should be between 20 to 60 orders;

B, with 1.5kg sodium chloride, 1kg natrium malicum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 8.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, the cocoa with dry and high quality, coffee pulverizing are the water of 65% ethanol, 15% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid rock among the f;

J, mix, placed 4 hours, microwave cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 1.6mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Cocoa and coffee perfume (or spice) obviously embody in fragrance, and the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, flue gas concentration and rich rising.See Table 2.

Embodiment 5

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material are chosen, bulk density 0.03g/cm 3The silicic acid rock, material particle size should be between 20 to 40 orders;

B, with 2kg sodium chloride, 1kg natrium citricum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, the tree moss with dry and high quality, oak moss pulverizing are the water of 65% ethanol, 15% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid rock among the f;

J, mix, placed 5 hours, microwave cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 1.5mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Inhale flavor and introduced plain graceful bearing, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and fragrance enriches degree to be increased.See Table 2.

Embodiment 6

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, bulk density 0.12g/cm 3The silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 500g sodium chloride, 1kg natrium malicum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, with burley tobaccos, shine tobacco and pulverize, be the water of 65% ethanol, 15% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid rock among the f;

J, mix, microwave cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 1.4mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Inhale flavor and introduced the style of blended type cigarette, flue gas concentration obviously strengthens, and fragrance enriches degree and rises.See Table 2.

Embodiment 7

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, bulk density 0.18g/cm 3The silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 1.51g sodium chloride, 1.5kg natrium malicum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, Zimbabwe's tobacco leaf, Yuxi tobacco leaf, Chloranthus glaber (can leave out) being pulverized, is the water of 65% ethanol, 15% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid rock among the f;

J, mix, place 2 hours microwaves cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 1.6mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.This perfume of flue gas of Virginian-type cigarette significantly increases, the rich increase of fragrance, and the flue gas soften rises.See Table 2.

Embodiment 8

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, bulk density 0.05g/cm 3The silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 2kg sodium chloride, 2kg natrium citricum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, the honeysuckle with dry and high quality, fragrant citrus pulverizing are the water of 65% ethanol, 15% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid among the rock f;

J, mix, place 6 hours microwaves cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 1.2mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Inhale flavor and introduced the fruital and the fragrance of a flower, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases.See Table 2.

Embodiment 9

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, bulk density 0.11g/cm 3The silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 750g sodium chloride, 500kg natrium malicum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, the wrinkled giant hyssop with dry and high quality, fennel seeds pulverizing are the water of 65% ethanol, 15% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicic acid rock among the f;

J, mix, placed 2 hours, microwave cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 20 to 40 purpose products.

Particle is added the 1.9mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.Inhale in the flavor and introduced traditional spices style, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, the rich rising of fragrance, and throat's comfort level increases.See Table 2.

Embodiment 10

The preparation method of cigarette flavor compensating particles of the present invention is the flavor compensating particles of making by following process:

A, raw material screening are selected the density homogeneous, bulk density 0.1g/cm 3The silicic acid rock, material particle size should be between 80 to 20 orders;

B, with 600g sodium chloride, 1.5kg natrium malicum, 12kg water, be mixed with the load-carrying agent of homogeneous;

C, with the load-carrying agent for preparing, add on the silicic acid rock;

D, stir normal temperature and pressure storage 1 hour down;

E, microwave drying are handled, below the moisture drying to 6.0%;

F, will cure the silicic acid rock that finishes and sieve, choose 20 to 40 purpose particles;

G, the rush of dry and high quality being pulverized, is the water of 45% ethanol, 25% propane diols and surplus with percentage by weight, mixed solvent refluxing extraction 2 hours;

H, with the residue crushed after being dried of extract among the g, sieve is got the following fine powder of 80 orders;

I, the string that obtains among the h and the extract among the g mixed after, join in the silicate among the f;

J, mix, place 5.5 hours microwaves cure to moisture be 8% to 10%;

K, with the product that obtains among the j, sieve, sieve is got 40 to 60 purpose products.

Particle is added the 1.2mg amount according to every millimeter mouth rod make composite tip stick, make cigarette, fume indication sees Table the test sample one in 1 compared with the control.The suction flavor is light partially, and feature is if the flue gas soften rises, throat's comfort level increase.See Table 2.

Table 1

? Cigarette Zhi Kechong Average resistance to suction TPM Moisture Smoking nicotine Tar The mouth number CO Contrast 0.92g 1020 14.4 1.6 1.1 12.7 9.7 12.2 Test sample one 0.91g 1000 14.6 1.7 1.1 11.8 9.9 11.5 Test sample two 0.93g 1080 14.7 1.7 1.1 12.4 9.6 11.8 Test sample three 0.93g 1020 15.2 1.6 1.0 12.8 9.7 10.9 Test sample four 0.92g 1000 15.8 1.8 1.1 12.3 9.4 12.0 Test sample five 0.92g 1000 16.0 1.7 1.0 11.9 9.8 11.9 Test sample six 0.93g 1020 15.1 1.9 1.1 12.4 9.5 11.0 Test sample seven 0.93g 1020 14.2 1.8 1.0 12.0 9.7 11.4 Test sample eight 0.92g 1040 15.5 1.6 0.9 12.6 9.9 11.7 Test sample nine 0.94g 1060 13.8 1.6 0.8 12.0 9.8 11.9 Test sample ten 0.94g 1060 14.9 1.6 0.9 12.3 99.7 12.1

Table 2

Describe Contrast Fragrant saturating the sending out of cigarette, flue gas concentration is owed slightly, and flue gas is soft, and pleasant impression is clean, and throat stimulates slightly; Test sample one Inhale flavor and introduced new feature, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases; Test sample two It is pure to inhale the sweet rhythm of flavor, and the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases; Test sample three Inhaling flavor has sweet rhythm, and in an elegant style, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases; Test sample four Cocoa and coffee perfume (or spice) obviously embody in fragrance, and the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, flue gas concentration and rich rising; Test sample five Inhale flavor and introduced plain graceful bearing, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and fragrance enriches degree to be increased; Test sample six Inhale flavor and introduced the style of blended type cigarette, flue gas concentration obviously strengthens, and fragrance enriches degree and rises; Test sample seven This perfume of fire-cured tobacco type flue gas significantly increases, the rich increase of fragrance, and the flue gas soften rises; Test sample eight Inhale flavor and introduced the fruital and the fragrance of a flower, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, and the flue gas soften rises, and throat's comfort level increases; Test sample nine Inhale in the flavor and introduced traditional spices style, the feature flue gas is coordinated mutually with this perfume (or spice) of tobacco, the rich rising of fragrance, and throat's comfort level increases; Test sample ten The suction flavor is light partially, and feature is if the flue gas soften rises, throat's comfort level increase.

Claims (10)

1. the preparation method of a cigarette flavor compensating particles mainly is made up of a silicic acid batholith plinth material and a year pastil, is raw material with expanded silicic acid rock, add the load-carrying agent, form silicic acid rock loaded particle by load-carrying, drying, prilling, it is characterized in that its preparation method is:
A, select materials: choose moisture≤4%, the expanded silicic acid rock of particle diameter between 20~100 orders;
B, the load-carrying agent is water-soluble adds on the silicic acid rock, stirs, and normal temperature and pressure was stored 1~12 hour down;
C, with step b gained silicic acid rock oven dry, dry to moisture≤4%;
D, the silicic acid rock after will drying sieve, and particle diameter is greater than 20 purpose silicic acid rock particle granulations once more, grade at 20~100 orders with the interior silicic acid batholith material that promptly gets;
E, at least a vegetable material in Radix Glycyrrhizae, Momordica grosvenori, honeysuckle, ginkgo leaf, loguat leaf, Chloranthus glaber, cocoa, coffee, tree moss, oak moss, burley tobaccos, solarization tobacco, Zimbabwe's tobacco leaf, Yuxi tobacco leaf, fragrant citrus, wrinkled giant hyssop, little eggplant perfume (or spice) and the rush used the mixed solvent refluxing extraction of ethanol, water, propane diols respectively, at least a plant residue after extracting is dried respectively, and be ground into respectively less than 80 purpose fine powders, at least a extract and at least a residue fine powder that extract are mixed, make and carry pastil;
F, will carry in the base material that pastil joins gained in the steps d, mix, place 1 to 6 hours;
G, with the compound that obtains among the step f, dry once more to moisture be 8%~14%, granulate, particle sieves, sieve is got 20~100 purpose particles and is qualified cigarette flavor compensating particles.
2. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the bulk density of the described expanded silicic acid rock of step a is 0.01~0.2g/cm 3
3. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the addition of the described load-carrying agent of step b is: the weight part ratio of raw material and load-carrying agent is 1: 1~9.
4. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the described oven dry of step c is a microwave drying.
5. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the described oven dry of step g is a microwave drying.
6. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that, the described silicic acid batholith of steps d material, proportion is at 0.1~2.5g/cm 3Between.
7. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the described vegetable material of step e is plant extraction liquid and string.
8. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the described load-carrying agent of step b is one or more the combination in NaCl, natrium citricum, potassium citrate, natrium malicum, the potassium malate.
9. the preparation method of described cigarette flavor compensating particles according to Claim 8 is characterized in that described load-carrying agent is two kinds in NaCl, natrium citricum, potassium citrate, natrium malicum, the potassium malate, and it mixes part than being: 1: 1-5.
10. according to the preparation method of the described cigarette flavor compensating particles of claim 1, it is characterized in that the cigarette flavor compensating particles that the step g preparation is got directly adds in the mouth rod of cigarette, addition is that every millimeter mouth rod adds 0.1mg~3.0mg.
CN2010101486822A 2010-04-16 2010-04-16 Preparation method of cigarette flavor compensating particles CN101828769B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010101486822A CN101828769B (en) 2010-04-16 2010-04-16 Preparation method of cigarette flavor compensating particles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010101486822A CN101828769B (en) 2010-04-16 2010-04-16 Preparation method of cigarette flavor compensating particles

Publications (2)

Publication Number Publication Date
CN101828769A CN101828769A (en) 2010-09-15
CN101828769B true CN101828769B (en) 2011-08-31

Family

ID=42713106

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2010101486822A CN101828769B (en) 2010-04-16 2010-04-16 Preparation method of cigarette flavor compensating particles

Country Status (1)

Country Link
CN (1) CN101828769B (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102551207B (en) * 2010-12-17 2014-09-10 江西中烟工业有限责任公司 Chinese herbal additive for reducing hydrogen cyanide in main stream smoke of cigarette, preparation method and application thereof
CN102533445B (en) * 2012-02-05 2013-09-18 云南正邦生物技术有限公司 Method for preparing active release type cigarette flavor complementing particles
CN102987561A (en) * 2012-11-28 2013-03-27 红塔烟草(集团)有限责任公司 Cigarette paper filter material containing honeysuckle fragrance
CN102987547A (en) * 2012-12-19 2013-03-27 云南瑞升烟草技术(集团)有限公司 Method for preparing cigarette fragrance compensation granules
CN103054181B (en) * 2012-12-27 2015-02-11 广东中烟工业有限责任公司 Coffee or cocoa composite particle filtering bar and manufacturing method thereof
CN103689798B (en) * 2013-12-03 2015-04-08 红云红河烟草(集团)有限责任公司 Gingko leaf porous particle and application thereof in cigarette
CN103689794B (en) * 2013-12-03 2015-04-08 红云红河烟草(集团)有限责任公司 Pelargonium graveolens porous particle and application thereof to cigarette
CN103876283B (en) * 2014-03-04 2016-02-10 湖南中烟工业有限责任公司 Filter stick compound additive with coffee or cocoa flavor and its preparation method and application
CN103876286B (en) * 2014-03-04 2016-06-08 湖南中烟工业有限责任公司 A kind of filter rod particulate additive with coffee or cocoa flavor and its preparation method and application
CN104026732B (en) * 2014-06-13 2017-01-04 广西中烟工业有限责任公司 The preparation method of a kind of Nicotiana tabacum L. glutinous rice flour composite particles and the flavouring application in filter tip thereof
CN104273648B (en) * 2014-09-25 2018-03-13 广东中烟工业有限责任公司 The cigarette filter of application and application Chinese alpine rush of the Chinese alpine rush in cigarette filter
CN105231480B (en) * 2015-11-10 2017-07-04 江苏中烟工业有限责任公司 A kind of method that calcium carbonate is applied as perfuming carrier in reconstituted tobacco coating fluid

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1099957A (en) * 1993-09-11 1995-03-15 中国烟草总公司郑州烟草研究院 Adsorbent for cigarette filter-tip
WO2007083245A2 (en) * 2006-01-17 2007-07-26 Philip, Morris, Products, S.A. Cigarette components having encapsulated catalyst particles and methods of making and use thereof
WO2009080368A1 (en) * 2007-12-20 2009-07-02 Philip Morris Products S.A. Filter including randomly-oriented fibers for reduction of particle breakthrough
CN101347266B (en) * 2008-08-28 2010-12-22 云南亚可生物科技有限公司 Method for preparing filter material of cigarette

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060260626A1 (en) * 2005-01-05 2006-11-23 Philip Morris Usa Inc. Activated carbons with molecular sieve membranes and their use as adsorbents in smoking articles

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1099957A (en) * 1993-09-11 1995-03-15 中国烟草总公司郑州烟草研究院 Adsorbent for cigarette filter-tip
WO2007083245A2 (en) * 2006-01-17 2007-07-26 Philip, Morris, Products, S.A. Cigarette components having encapsulated catalyst particles and methods of making and use thereof
WO2009080368A1 (en) * 2007-12-20 2009-07-02 Philip Morris Products S.A. Filter including randomly-oriented fibers for reduction of particle breakthrough
CN101347266B (en) * 2008-08-28 2010-12-22 云南亚可生物科技有限公司 Method for preparing filter material of cigarette

Also Published As

Publication number Publication date
CN101828769A (en) 2010-09-15

Similar Documents

Publication Publication Date Title
Demisie et al. Effect of biochar on carbon fractions and enzyme activity of red soil
US4889144A (en) Filter for tobacco smoking
RU2294675C2 (en) Encapsulated materials
RU2577838C2 (en) Smoking article comprising alkanoylated glucoside and method for production thereof
JP4940409B2 (en) Smoking articles having tobacco beads
ES2702056T3 (en) Article for smoking that includes flavoring granules
CN101810165B (en) Smokeless mosquito incense blank and preparation method thereof
DE60311769T2 (en) Cigarette filter with aerated carbon
CN104366687A (en) Smoking material for low-temperature nonflammable cigarette and preparing method thereof
US20180360099A1 (en) Tobacco composition
RU2462964C2 (en) Cigarette filter containing aromatic particles
AU734551B2 (en) Compressed mixtures of coconut coir pith and peat moss and processes for the preparation thereof
KR20140004754A (en) Smoking articles
Haimour et al. Utilization of date stones for production of activated carbon using phosphoric acid
EP1460908B1 (en) Improvements relating to smokable filler materials
EP1937092B1 (en) A reconstituted tobacco with bonded flavorant, smoking article and methods
RU2256386C2 (en) Smoking stuffing material containing fruit substance
TWI308484B (en) Improvements relating to smoking articles and smokable filler materials therefor
CN102342583B (en) Filter stick containing tobacco particles and preparation method thereof
CN103054171A (en) Electronic cigarette liquid prepared from flat-flavor tobacco
CN101642582A (en) Material with multi-functional long-acting slow-release effective components
CN104436263B (en) Multi-purpose water-containing granular air purifying agent and production method thereof
EP0756461A1 (en) Tobacco products, or substances similar to such products, containing natural substances with anti-oxidant properties, and process for producing the same
AU723466B2 (en) Smokable filler material for smoking articles
RU2436484C2 (en) Cigarette filter containing vegetal material and cigarette

Legal Events

Date Code Title Description
PB01 Publication
C06 Publication
SE01 Entry into force of request for substantive examination
C10 Entry into substantive examination
GR01 Patent grant
C14 Grant of patent or utility model
ASS Succession or assignment of patent right

Owner name: SHANGHAI HUABAO BIOTECHNOLOGY CO., LTD.

Free format text: FORMER OWNER: YUNNAN ZHENGBANG BIOLOGICAL TECHNOLOGY CO., LTD.

Effective date: 20120518

TR01 Transfer of patent right

Effective date of registration: 20120518

Address after: 201821 Shanghai Huabao biological science and Technology Co Ltd, No. 1299 Yecheng Road, Shanghai, Jiading District

Patentee after: Shanghai Huabao Biotechnology Co., Ltd.

Address before: 650118 science and technology park for university students studying abroad at No. 139, Ke FA Road, Kunming hi tech Zone, Yunnan, A2-202

Patentee before: Yunnan Zhengbang Biological Technology Co., Ltd.

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 650118 KUNMING, YUNNAN PROVINCE TO: 201821 JIADING, SHANGHAI