CN107057853A - A kind of cigarette rose composite particles and its application - Google Patents

A kind of cigarette rose composite particles and its application Download PDF

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Publication number
CN107057853A
CN107057853A CN201710029997.7A CN201710029997A CN107057853A CN 107057853 A CN107057853 A CN 107057853A CN 201710029997 A CN201710029997 A CN 201710029997A CN 107057853 A CN107057853 A CN 107057853A
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Prior art keywords
cigarette
petal
fireworks
rose
powder
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CN201710029997.7A
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CN107057853B (en
Inventor
吴恒
杨皓天
王夸平
郭生云
韩智强
徐世涛
刘劲芸
周静媛
姚响
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China Tobacco Yunnan New Material Technology Co Ltd
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China Tobacco Yunnan New Material Technology Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/285Treatment of tobacco products or tobacco substitutes by chemical substances characterised by structural features, e.g. particle shape or size
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Toxicology (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses a kind of cigarette rose composite particles and its application.Black petal of red rose and fireworks petal using freeze-drying is primary raw material, and pulverization process is carried out to two kinds of raw materials by the way that low-temperature submicron powder is broken, then tobacco jelly powder is added in raw material powder again, subsequent material sequentially passes through mixing, extruding, broken, shaping and screening process, forms the granular material that granularity is 30~60 mesh.The rose composite particles provided using the present invention, can increase cigarette flavor, improve pleasant impression, reduction stimulation and cover miscellaneous gas, the integral suction quality of cigarette is lifted with obtaining conspicuousness.

Description

A kind of cigarette rose composite particles and its application
Technical field
The invention belongs to cigarette supplementary technical field, and in particular to a kind of rose that can improve flavor quality of cigarette is combined Particle.Meanwhile, the invention further relates to concrete application of the rose composite particles in production of cigarettes.
Background technology
As the public is to smoking and the pay attention to day by day of health problem, produces and be harmful in low-coke tar cigarette, reduction cigarette smoke One of content of material, raising smoking property of cigarette security, main direction of studying as tobacco researcher.
By numerous studies and experiment, it can be designed by tobacco leaf formulation and cigarette realizes cigarette with the system design of auxiliary material The purpose of lowering harm and decreasing coking.In tobacco leaf formulation design process, using materials such as reconstituted tobacoo, expanded cut stem, expanding tobacco particles, Significantly reduce cigarette tar content;In auxiliary material design process, filtered by high porosity plug wrap paper, hole-punching huon pine paper, high resistance to suction Rod, high material and the skill such as filter stick (such as papery composite filter, activated carbon composite filter) of cigarette paper and high adsorption base material thoroughly The application of art, realizes the reduction of coke tar in cigarette and flue gas harmful substance contents.But by these technologies, materials application in cigarette Afterwards, although harmfulness is reduced, but the sucking quality of cigarette is also adversely affected.
Cigarette how is balanced while reducing tar and reducing harm sucks mouthfeel and quality, scientific research personnel from essence spice for cigarette and Cigarette filter-tip additive agent and material set out, and have carried out numerous studies and experiment.Wherein, although the use of essence spice for cigarette can be with The fragrance loss after Harm reduction techniques tar reduction is made up, the sweet sense of cigarette smoke is improved, reduces the excitant of cigarette smoke, but cigarette Participated in essence and flavoring agent during pipe tobacco is burnt and sucked due to complicated heat scission reaction so that original Flavoring Components It can change, so as to influence its original Objective fragrance, it is therefore desirable to which adjustment formula can be with pipe tobacco phase repeatedly, in large quantities Matching, reaching improves the effect of cigarette smoking quality.At present, the utilization of the technology is quite ripe, further improves cigarette and inhales The space of food matter is little.
In addition, tobacco scientific research personnel is also attempted from natural perfume plant particle, the physics eluted using cigarette smoke The fragrance matter introduced into cigarette smoke with cigarette flavor phase harmony is acted on, to reach the purpose for improving smoking property of cigarette quality, Some achievements are had been achieved at present.For example:Patent CN103126072A《It is a kind of to increase cigarette sweet rhythm and the natural plant of infiltration sense Composition granule and its application》The particle of announcement passes through crushing, granulation and heated-air drying formation finished product using rose and peppermint as raw material Grain, with lifting infiltration sense and the effect of comfortableness while sweet tea rhythm is increased.Patent CN105132167A《One kind increases profit and carries fragrant Plant granule and its preparation method and application》Disclosed particle with Aplotaxis auriculata, Tibet inula root, fragrant purple perilla, rose, lavender, peppermint, Radix Angelicae Sinensis and rice tea extraction are raw material, by extruding granulation, are dried and the fragrant formation finished particle of load;Patent CN105124758A 《One kind increases profit and carries fragrant plant granule and preparation method thereof and use》The particle of announcement with rose, peppermint, Momordica grosvenori, rosemary, Tribute chrysanthemum and rice tea extraction are raw material;Patent CN101912161B《A kind of cigarette peppermint filter stick and preparation method thereof》Disclosed filter Peppermint, blackberry lily and tobacco leaf particle are with the addition of in rod fiber base material, with wetting one's whistle, moisturizing, reduces the irritating effect of flue gas.
In terms of preparation method of granules, disclosed method mainly has fluidized bed granulation one-step method and wet granulation knot at present Close and dry two-step method.Although particle prepared by both approaches can improve or improve cigarette smoking quality to a certain extent, But due to there is also some problems in preparation method and raw material selection and in terms of assembling so that existing plants particles material addition Advantage function into cigarette filter rod also fails to give full play of.
For one-step preparation process, there are 2 points of deficiencies:1) particle surface covering macromolecule membrane layer made from, certain Migration of the vegetable material aroma substance to cigarette smoke has been obstructed in degree;2) in granulation process, because air-flow is to plant material The flushing repeatedly and elution of material, have lost most of aroma substance of script in vegetable material.
For two-step method preparation technology, there are 3 points of deficiencies:1) drying temperature is high, is easily caused the damage of vegetable material aroma substance Become estranged destruction;2) if heated-air drying, hot blast can also take away part aroma substance in vegetable material;3) wet granulation is formed Wet granular contains substantial amounts of moisture, in the drying process, and part aroma substance can dissipate with the evaporation of moisture in vegetable material Lose.
Selection as raw material and assemble, each plant material and the harmony of cigarette flavor that prior art is announced are still Need to improve, this perfume of tobacco enriches not enough, also to be improved.
For disadvantages mentioned above, appropriate material and technology how are selected, lifting granular materials is in increase cigarette smoke Effect in terms of sweet sense and sense of promoting the production of body fluid, it is irritating simultaneously in reduction cigarette smoke, assign cigarette certain characteristic perfume, just As the technical problem for needing further to solve.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to a kind of cigarette rose composite particles be provided, with harmony Cigarette perfume, the release for reducing fragrance matter in particle when fragrance loss in particulate production, promotion cigarette are burnt and sucked.
The present invention also aims to provide a kind of cigarette with rose composite particles in production of cigarettes specifically should Use mode.
Unless otherwise indicated, percentage of the present invention is percetage by weight.
The purpose of the present invention is achieved by the following technical programs.
A kind of cigarette rose composite particles, it is characterised in that prepared by following methods:
(1) vacuum freeze drying:To fresh ink petal of red rose and fireworks petal precooling 12 hours under the conditions of -20 DEG C, so It is afterwards 8%~10% by its vacuum freeze drying to moisture content under the conditions of -110 DEG C of condenser temperature;
(2) raw material is crushed:The black petal of red rose after freeze-drying and fireworks are spent respectively using the broken machine of low-temperature submicron powder Valve carries out pulverization process, its micro powder granule is passed through 100 eye mesh screens;
(3) get the raw materials ready:Black 55~70 parts of petal of red rose powder, 5~15 parts of fireworks petal powder and tobacco fruit are weighed by mass parts 20~30 parts of rubber powder is standby;
(4) raw material is mixed:Each raw material of step (3) is mixed, the water equivalent to mixture weight 2%~5% is then added It is well mixed with high-speed mixer;
(5) extrude:Extruding film-making is carried out to well mixed raw material using water-cooled dry granulating machine, the thickness of tabletting is controlled Degree is in 1.5~2.5mm, and pressure roller cooling coolant-temperature gage is at 30~45 DEG C;
(6) tabletting is crushed:Break process is carried out to raw material tabletting using hammer crusher;
(7) particle shaping:Shaping is carried out to the granular materials after broken using pelletizing machine, makes it completely by 30 mesh shapings Net;
(8) particle screening:Coarse granule and fine powder are removed using vibratory sieve, the bulk material of isolated 30~60 mesh, i.e., Cigarette for needed for rose composite particles.
Fireworks petal described in step (1), kind is K326 fireworks, the big gold dollar fireworks of safflower, or two kinds of fireworks Mixture.
Application method of the described cigarette with rose composite particles in production of cigarettes, be specially:Add by every millimeter of filter stick Plus 1~prepared rose composite particles are added in cigarette filter rod tow by 3mg consumption.
The black red rose that the present invention is selected is by hybrid tea Chinese rose (Rosahvbrida Hvbrid Tea Roses) and miscellaneous Plant Changchun Chinese rose (Hybridperpetualsroses) hybridization to form, its contained aroma substance is mainly bergamio, lemon Alkene, methylanisole, citronellol, ethyl acetate, carypohyllene, linalool, n-hexyl alcohol, with the graceful fragrance of a flower and strong sweet tea Perfume (or spice), fragrance is compared with horn of plenty, and sweet taste is pure, lasting, intensity is high, can improve flue gas elegance and sophistication, increase fresh and sweet rhythm, Assign the savory gas of cigarette sweet.The fireworks petal and tobacco jelly powder that the present invention is selected are originated tobacco plant, itself and cigarette cigarette Silk is of the same clan homologous, with excellent hamony and matching.Note elegance that fireworks petal is fresh and sweet, aroma substance extremely enrich, example Such as damascenone, Megastigmatrienone, dihydroactinidiolide, benzaldehyde;Tobacco jelly powder is a kind of polysaccharide hydrocarbonization Compound, not only with excellent caking property, and with cigarette flavor phase harmony, functions and effects be different from natural plant, Other caking property materials such as starch.
Compared to the combination of other vegetable materials, the particle being composited by three of the above plant material can not only be effective Ground improves flue gas elegance and sophistication, increases fresh and sweet rhythm, reduces cigarette smoke excitant, comfortable during lifting cigarette smoking Property, and sweet tea sense, moisture feeling and the sense of promoting the production of body fluid of cigarette smoke more can be effectively lifted, alleviate the sense of discomfort of smoking cigarette, and assign Give a kind of relatively comfortable sweet feel of cigarette.
Relative to prior art, the present invention has advantages below and effect:
(1) fragrance harmony:Using fireworks petal powder and the black red rose of tobacco jelly powder auxiliary, black red rose can be made The cigarette perfume of fragrance and cigarette combines together, produces harmonious, graceful, abundant sweet taste cigarette perfume.Gained rose particle addition of the invention Flue gas elegance and sophistication can be improved into cigarette filter rod tow, increases fresh and sweet rhythm, cigarette smoke excitant is reduced, makes cigarette Suction quality lifted with obtaining conspicuousness.
(2) fragrance loss is low in preparation process:Raw material uses freeze-drying method, reduces aroma substance in drying process Scatter and disappear.Material is pelletized using water-cooled dry granulating machine, and the control nip rolls cooling water temperature in pelletization.From Granular material does not pass through drying to finished granule whole process, compared with other method of granulating, effectively reduces raw material The loss of aroma substance;
(3) aroma substance release is easy:Because the black petal of red rose after freeze-drying and fireworks Petal structure are dredged Pine is porous, and it has larger specific surface area by the particle crushed, granulation is formed so that rose particle has with cigarette smoke Larger mass exchange area, enhances the eluting effect of cigarette smoke, promotes migration of the particulate aroma material to cigarette smoke.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, by the following examples to the present invention It is described in further detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not to this The restriction of inventive technique scheme.
Exemplified by preparing 100 kilograms of plant composite particles products, the present invention is specifically described.
Embodiment 1:The preparation of rose composite particles is completed by following steps:
First under the conditions of -20 DEG C to fresh ink petal of red rose and fireworks petal precooling 12 hours, then condenser temperature - By black petal of red rose and fireworks petal vacuum freeze drying to moisture content it is 9% state under the conditions of 110 DEG C, using low temperature ultra micro Pulverizer is crushed to the black petal of red rose and fireworks petal after freeze-drying respectively, its micro powder granule is passed through 100 eye mesh screens;70 kilograms of black petal of red rose powder, 5 kilograms of K326 fireworks petals powder, the big gold dollar cigarettes of 5 kilograms of safflowers are weighed respectively Flower petal powder, 20 kilograms of tobacco jelly powder input high-speed mixers, and 3 kg of water are additionally added into mixer, afterwards, carry out It is sufficiently stirred for;Extruding film-making is carried out to well mixed material using water-cooled dry granulating machine, and controls the thickness of tabletting to exist 1.5~2.0mm, nip rolls cooling water temperature is at 35~45 DEG C.Break process is carried out to materials result using hammer crusher. Shaping is carried out to the granular materials after broken using pelletizing machine, makes it completely by 30 mesh shaping nets.Removed using vibratory sieve thick Particle and fine powder, the bulk material of isolated 30~60 mesh.
By 1.5mg/mm consumption, prepared rose composite particles are added in filter stick tow, formation charge bar, then with White rod is combined, and is prepared into binary compound filter candle, and roll into cigarette.It is control sample to set the cigarette added without particle, and sense organ is commented Suction the results are shown in Table 1.
Embodiment 2:
Embodiment 1 is repeated, there is following difference:Black petal of red rose and fireworks petal vacuum freeze drying to moisture content are 10% state.Weigh 60 kilograms of black petal of red rose powder, 8 kilograms of K326 fireworks petals powder, the big gold dollar fireworks petals of 4 kilograms of safflowers Powder, 28 kilograms of tobacco jelly powders, and add 3.5 kg of water.The thickness of tabletting is controlled in 2.0~2.5mm, nip rolls coolant water temperature Degree is at 30~40 DEG C.By 1.0mg/mm consumption, the rose composite particles of the gained of embodiment 2 are added in filter stick tow.
Embodiment 3:
Embodiment 1 is repeated, there is following difference:Black petal of red rose and fireworks petal vacuum freeze drying to moisture content are 8% state.Weigh 55 kilograms of black petal of red rose powder, 10 kilograms of K326 fireworks petals powder, the big gold dollar fireworks petals of 5 kilograms of safflowers Powder, 30 kilograms of tobacco jelly powders, and add 2 kg of water.The thickness of tabletting is controlled in 1.5~2.0mm, nip rolls cooling water temperature At 30~40 DEG C.By 2.0mg/mm consumption, the rose composite particles of the gained of embodiment 3 are added in filter stick tow.
Embodiment 4:
Embodiment 1 is repeated, there is following difference:Black petal of red rose and fireworks petal vacuum freeze drying to moisture content are 10% state.Weigh the big gold dollar fireworks flower of 65 kilograms of black petal of red rose powder, 5 kilograms of K326 fireworks petals powder, 10 kilograms of safflowers Valve powder, 20 kilograms of tobacco jelly powders, and add 4 kg of water.The thickness of tabletting is controlled in 2.0~2.5mm, nip rolls coolant water temperature Degree is at 35~45 DEG C.By 2.5mg/mm consumption, the rose composite particles of the gained of embodiment 4 are added in filter stick tow.
Embodiment 5:
Embodiment 1 is repeated, there is following difference:Black petal of red rose and fireworks petal vacuum freeze drying to moisture content are 8% state.70 kilograms of black petal of red rose powder, the big gold dollar fireworks petal powder of 5 kilograms of safflowers, 25 kilograms of tobacco jelly powders are weighed, And add 5 kg of water.Control the thickness of tabletting in 1.5~2.0mm, nip rolls cooling water temperature is at 30~40 DEG C.By 3.0mg/ Mm consumption, the rose composite particles of the gained of embodiment 5 are added in filter stick tow.
The cigarette sensory evaluating smoking's result of table 1
As seen from the above table, the present invention gained rose composite particles be added in cigarette filter rod tow can increase cigarette flavor, Improving pleasant impression, reduction stimulates and covers miscellaneous gas, the integral suction quality of cigarette is lifted with obtaining conspicuousness.It is main in terms of flavouring Lifting flue gas elegance and sophistication are shown as, this perfume of increase tobacco assigns the savory gas of cigarette sweet;Main table in terms of pleasant impression improvement It is now the sweet sense of supplement and sense of promoting the production of body fluid;Miscellaneous gas covers aspect and covers effect substantially to wooden, raw blue foreign smell, has one to dried-up miscellaneous gas Fixed covers effect;The thorn of stining that throat and lingual surface can substantially be reduced by being mainly shown as in terms of drop thorn is felt.

Claims (3)

1. a kind of cigarette rose composite particles, it is characterised in that prepared by following methods:
(1) vacuum freeze drying:To fresh ink petal of red rose and fireworks petal precooling 12 hours, Ran Hou under the conditions of -20 DEG C Under the conditions of -110 DEG C of condenser temperature by its vacuum freeze drying to moisture content be 8%~10%;
(2) raw material is crushed:The black petal of red rose and fireworks petal after freeze-drying are entered respectively using the broken machine of low-temperature submicron powder Row pulverization process, enables its micro powder granule to pass through 100 eye mesh screens;
(3) get the raw materials ready:Black 55~70 parts of petal of red rose powder, 5~15 parts of fireworks petal powder and tobacco jelly powder are weighed by mass parts 20~30 parts standby;
(4) raw material is mixed:Each raw material of step (3) is mixed, then adds high equivalent to the water of mixture weight 2%~5% Fast mixer is well mixed;
(5) extrude:Extruding film-making is carried out to well mixed raw material using water-cooled dry granulating machine, the thickness of control tabletting exists 1.5~2.5mm, pressure roller cooling coolant-temperature gage is at 30~45 DEG C;
(6) tabletting is crushed:Break process is carried out to raw material tabletting using hammer crusher;
(7) particle shaping:Shaping is carried out to the granular materials after broken using pelletizing machine, makes it completely by 30 mesh shaping nets;
(8) particle screening:Coarse granule and fine powder, the as bulk material of isolated 30~60 mesh, institute are removed using vibratory sieve The cigarette rose composite particles needed.
2. cigarette according to claim 1 rose composite particles, it is characterised in that:Fireworks flower described in step (1) Valve, kind is the mixture of K326 fireworks, the big gold dollar fireworks of safflower, or two kinds of fireworks.
3. application method of the cigarette described in claim 1 with rose composite particles in production of cigarettes, it is characterised in that:By every milli Prepared rose composite particles are added in cigarette filter rod tow by the consumption that rice filter stick adds 1~3mg.
CN201710029997.7A 2017-01-16 2017-01-16 Rose composite particles for cigarettes and application thereof Active CN107057853B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107594621A (en) * 2017-09-25 2018-01-19 云南程耀生物科技有限公司 A kind of fruity flavor composite particles and its preparation method and application
CN108143005A (en) * 2017-12-22 2018-06-12 安徽中烟工业有限责任公司 A kind of peripheral electrical heating aerosol generation system for including tobacco particle
CN109602068A (en) * 2018-11-16 2019-04-12 深圳市凯神科技股份有限公司 Plantflakesare, cigarette substitute and preparation method thereof and cigarette

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CN1826996A (en) * 2006-04-03 2006-09-06 张保民 Method for preparing health cigarette
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CN103190693A (en) * 2013-04-19 2013-07-10 安徽中烟工业有限责任公司 Extracting method for tobacco flower extract and application thereof
CN104544541A (en) * 2014-12-24 2015-04-29 广西中烟工业有限责任公司 Preparation method for vacuum freeze drying flower grain electronic cigarette liquid
CN105273842A (en) * 2015-11-17 2016-01-27 鹰潭中投科技有限公司 Preparation method of rose perfume
CN105595421A (en) * 2015-10-23 2016-05-25 云南中烟工业有限责任公司 Plant compound particles for cigarette filter and preparation method thereof

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CN85104502A (en) * 1985-06-12 1986-12-10 菲利普莫里斯公司 Cohesive tobacco composition
CN1826996A (en) * 2006-04-03 2006-09-06 张保民 Method for preparing health cigarette
CN102161936A (en) * 2011-03-02 2011-08-24 广州市澳键香料有限公司 Formula of tobacco additive essence containing tobacco flower bud extract
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107594621A (en) * 2017-09-25 2018-01-19 云南程耀生物科技有限公司 A kind of fruity flavor composite particles and its preparation method and application
CN108143005A (en) * 2017-12-22 2018-06-12 安徽中烟工业有限责任公司 A kind of peripheral electrical heating aerosol generation system for including tobacco particle
CN109602068A (en) * 2018-11-16 2019-04-12 深圳市凯神科技股份有限公司 Plantflakesare, cigarette substitute and preparation method thereof and cigarette

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