CN104544541A - Preparation method for vacuum freeze drying flower grain electronic cigarette liquid - Google Patents
Preparation method for vacuum freeze drying flower grain electronic cigarette liquid Download PDFInfo
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- CN104544541A CN104544541A CN201410817943.3A CN201410817943A CN104544541A CN 104544541 A CN104544541 A CN 104544541A CN 201410817943 A CN201410817943 A CN 201410817943A CN 104544541 A CN104544541 A CN 104544541A
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- flower
- vacuum freeze
- freeze drying
- electronic cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses a preparation method for vacuum freeze drying flower grain electronic cigarette liquid. The preparation method is characterized in that 1%-90% of vacuum freeze drying flower grains in percentage by weight are added into base oil of the electronic cigarette liquid, and the flower grains are formed by smashing and mixing at least one of lotus, oriental cherry, orchid, rape flower, osmanthus tea, honeysuckle, trollflower, rose, jasmine, magnolia flower, calendula and the like, pressing the flower mixture into blocks, carrying out vacuum freeze drying, and then breaking the blocks into grains; the base oil comprises the components in percentage by weight: 0-10% of essence and flavor, 0-15% of deionized water, 2%-80% of glycerol and the balance of propylene glycol or polyethylene glycol which is supplemented to be 100%, and the vacuum freeze drying flower grain electronic cigarette liquid can be obtained by uniformly stirring and mixing. According to the preparation method disclosed by the invention, the aroma components are immersed into the electronic cigarette liquid, so that the characteristic flavor of flowers is given to the electronic cigarette liquid, the aroma quality and the aroma amount of the electronic cigarette liquid are increased, the throat irritation caused by an atomizing agent can be better covered, and the satisfaction of a customer is increased.
Description
Technical field
The present invention relates to the preparation method of a kind of vacuum freeze drying flower grain electronics tobacco tar, belong to tobacco preparing technical field.
Background technology
Electronic cigarette is a kind of on-fuel cigarette class substituted type product, there is the outward appearance similar to cigarette, tobacco tar (electronic cigarette liquid) produces fog and is similar to true cigarette flue gas under the effect of electronic smoke atomizer, meet pleasant sensation and the use habit of smoker, but from cigarette, to have in essence different, do not burn, not containing the harmful substance such as tar, carbon monoxide.At present, commercially available electronics tobacco tar is the product be deployed into various essence and flavoring agent, larger with the perceptual difference distance of cigarette in fragrance, mouthfeel etc., allows people be difficult to accept or be accustomed to its fragrance and taste, even exhausts sensation that is dizzy and that feel sick.Fresh flower not only can bring us visual aesthetic feeling, can also as spices.Fresh flower have left water and soil, also just loses original glamour.At present, Vacuum Freezing & Drying Technology is considered to one of state-of-the-art store and processing technology, can preserve the color of fresh feed, fragrance matter loss little, there is the advantages such as loose loose structure dissolubility is good, long shelf-life.With fresh flowers for material, briquet after vacuum freeze drying, then damaged become in heating particles tobacco tar, adding of it can bring natural flowery odour to tobacco tar, and see in tobacco tar see colored grain, to a kind of brand-new impression of consumer and experience.
Summary of the invention
The object of this invention is to provide a kind of vacuum freeze drying flower grain, be applied in electronics tobacco tar compatibility, promote fragrance and the quality of tobacco tar suction.
Object of the present invention is achieved through the following technical solutions.
A preparation method for vacuum freeze drying flower grain electronics tobacco tar, preparation method is as follows:
Joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying flower grain 1 ~ 90%, stir and evenly mix and obtain vacuum freeze drying flower grain electronic cigarette oil product.
Described colored grain comprises: lotus, oriental cherry, orchid, rape flower, osmanthus flower tea, honeysuckle, trollflower, forget-me-not, carnation, flower of Panax ginseng, sanchi flower, rose, jasmine, Flos Magnoliae Liliflorae, pot marigold, Roselle, gardenia, peach blossom, tribute chrysanthemum, chamomile, globe amaranth, shrub althea flower, lilac, feltwort, bigarabe flower, flores aurantii, robiniae,flos, safflower, mother chrysanthemum, magnolia, peony, lavandulae flos, pot marigold, yellow chamomile, bitter citrus immature flower, broom top, leek, yellow giner, gillyflower, plum blossom, in Flos Papaveris rhoeadis, at least one fresh flowers raw material loads in lyophilized plate in any proportion, put into-20 DEG C ~-30 DEG C freezer precoolings 15 ~ 30 minutes and briquet, then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate and rise to 50 DEG C ~ 60 DEG C dryings 20 ~ 50 hours from room temperature, controlling vacuum in heating process is 30 ~ 80pa, then being broken into size after vacuum freeze drying is 5 ~ 80 object particles.
Described base oil comprises essence and flavoring agent 0 ~ 10%, deionized water 0 ~ 15%, glycerine 2 ~ 80%, and surplus supplies 100% weight with propane diols or polyethylene glycol again.
Described vacuum freeze drying flower grain does not add any additive and anticorrisive agent.
Described essence and flavoring agent, glycerine, propane diols or polyethylene glycol, be edible rank.
The invention has the beneficial effects as follows:
The present invention breaches the bottleneck of the fragrance nature sensory experience deficiency that existing electronic cigarette tobacco tar exists, give tobacco tar lasting, excellent, natural flowery odour impression, for electronic cigarette tobacco tar industry provides fragrance matter adding technique and the product of more high-quality, improve and add cigarette oil added value.
Detailed description of the invention
For convenience of understanding the present invention better, be illustrated by following instance.These examples belong to protection scope of the present invention, but do not limit the scope of the invention.
Embodiment 1
Trollflower loads in lyophilized plate puts into-25 DEG C of freezer precoolings 25 minutes and briquet; Then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 55 DEG C dry 30 hours, controlling vacuum in heating process is 50pa, after vacuum freeze drying damaged become 5 object spheric granules.Take the trollflower grain 10g after vacuum freeze drying, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 100g: 150g: 500g: 250g be mixed and made into 1000g base oil) 990g, be uniformly mixed and obtain vacuum freeze drying trollflower grain electronic cigarette oil product.
Embodiment 2
Rape flower loads in lyophilized plate puts into-30 DEG C of freezer precoolings 28 minutes and briquet; Then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C dry 40 hours, controlling vacuum in heating process is 30pa, after vacuum freeze drying damaged become 20 object spheric granules.Take the rape flower 500g after vacuum freeze drying, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 80g: 150g: 20g: 750g be mixed and made into 1000g base oil) 500g, be uniformly mixed and obtain vacuum freeze drying rape flower grain electronic cigarette oil product.
Embodiment 3
Lilac loads in lyophilized plate puts into-20 DEG C of freezer precoolings 30 minutes and briquet; Then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 20 hours, controlling vacuum in heating process is 30pa, after vacuum freeze drying damaged become 80 object irregular particles.Take the lilac grain 900g after vacuum freeze drying, join in base oil (by deionized water: glycerine: polyethylene glycol is 150g: 100g: 750g be mixed and made into 1000g base oil) 100g, be uniformly mixed and obtain vacuum freeze drying lilac grain electronic cigarette oil product.
Embodiment 4
Flower of Panax ginseng, sanchi flower load in lyophilized plate by weight 50: 50 puts into-28 DEG C of freezer precoolings 26 minutes and briquet; Then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 40 hours, controlling vacuum in heating process is 60pa, after vacuum freeze drying damaged become 50 object spheric granules.Take the flower of the mixing after vacuum freeze drying grain 200g, join in base oil (by essence and flavoring agent: glycerine: propane diols is 50g: 100g: 850g be mixed and made into 1000g base oil) 100g, be uniformly mixed and obtain vacuum freeze drying mixing flower grain electronic cigarette oil product.
Embodiment 5
Gillyflower, lavandulae flos, chamomile load in lyophilized plate by weight 10: 30: 60 puts into-30 DEG C of freezer precoolings 15 minutes and briquet; Then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C dry 50 hours, controlling vacuum in heating process is 60pa, damaged one-tenth 40 object spheric granules after vacuum freeze drying, take the flower of the mixing after vacuum freeze drying grain 300g, join in base oil (by essence and flavoring agent: deionized water: glycerine: polyethylene glycol is 50g: 150g: 350g: 450g be mixed and made into 1000g base oil) 100g, be uniformly mixed and obtain vacuum freeze drying mixing flower grain electronic cigarette oil product.
Embodiment 6
Forget-me-not, carnation, Flos Papaveris rhoeadis, jasmine, Flos Magnoliae Liliflorae, pot marigold, Roselle are by putting into-25 DEG C of freezer precoolings 26 minutes and briquet than in loading lyophilized plate arbitrarily; Then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 40 hours, controlling vacuum in heating process is 60pa, after vacuum freeze drying damaged become 10 object spheric granules.Take the flower of the mixing after vacuum freeze drying grain 400g, join in base oil (by essence and flavoring agent: deionized water: glycerine is 50g: 150g: 800g be mixed and made into 1000g base oil) 100g, be uniformly mixed and obtain vacuum freeze drying mixing flower grain electronic cigarette oil product.
Embodiment 7
Lotus, oriental cherry, orchid, rape flower, osmanthus flower tea, honeysuckle, trollflower, forget-me-not, carnation, flower of Panax ginseng, sanchi flower, rose, jasmine, Flos Magnoliae Liliflorae, pot marigold, Roselle, gardenia, peach blossom, tribute chrysanthemum, chamomile, globe amaranth, shrub althea flower, lilac, feltwort, bigarabe flower, flores aurantii, robiniae,flos, safflower, mother chrysanthemum, magnolia, peony, lavandulae flos, pot marigold, yellow chamomile, bitter citrus immature flower, broom top, leek, yellow giner, gillyflower, plum blossom, Flos Papaveris rhoeadis puts into-30 DEG C of freezer precoolings 30 minutes and briquet by any weight ratio loading lyophilized plate, then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C dry 42 hours, controlling vacuum in heating process is 30pa.Damaged one-tenth 20 object spheric granules after vacuum freeze drying, take the flower of the mixing after vacuum freeze drying grain 600g, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is be mixed and made into 1000g base oil at 10g: 150g: 700g: 140) 100g and be uniformly mixed and obtain vacuum freeze drying mixing flower grain electronic cigarette oil product.
Claims (5)
1. the preparation method of a vacuum freeze drying flower grain electronics tobacco tar, it is characterized in that, preparation method is as follows: joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying flower grain 1 ~ 90%, stirs and evenly mixs and obtain vacuum freeze drying flower grain electronic cigarette oil product.
2. the preparation method of a kind of vacuum freeze drying flower grain electronics tobacco tar according to claim 1, it is characterized in that, described colored grain comprises: lotus, oriental cherry, orchid, rape flower, osmanthus flower tea, honeysuckle, trollflower, forget-me-not, carnation, flower of Panax ginseng, sanchi flower, rose, jasmine, Flos Magnoliae Liliflorae, pot marigold, Roselle, gardenia, peach blossom, tribute chrysanthemum, chamomile, globe amaranth, shrub althea flower, lilac, feltwort, bigarabe flower, flores aurantii, robiniae,flos, safflower, mother chrysanthemum, magnolia, peony, lavandulae flos, pot marigold, yellow chamomile, bitter citrus immature flower, broom top, leek, yellow giner, gillyflower, plum blossom, in Flos Papaveris rhoeadis, at least one fresh flowers raw material loads in lyophilized plate in any proportion, put into-20 DEG C ~-30 DEG C freezer precoolings 15 ~ 30 minutes and briquet, then the one-tenth block of precooling flower raw material is put into vacuum freeze drier, control temperature of heating plate and rise to 50 DEG C ~ 60 DEG C dryings 20 ~ 50 hours from room temperature, controlling vacuum in heating process is 30 ~ 80pa, then being broken into size after vacuum freeze drying is 5 ~ 80 object particles.
3. the preparation method of a kind of vacuum freeze drying flower grain electronics tobacco tar according to claim 1, it is characterized in that, described base oil comprises essence and flavoring agent 0 ~ 10%, deionized water 0 ~ 15%, glycerine 2 ~ 80%, surplus supplies 100% weight with propane diols or polyethylene glycol again.
4. the preparation method of a kind of vacuum freeze drying flower grain electronics tobacco tar according to claim 1, it is characterized in that, described vacuum freeze drying flower grain does not add any additive and anticorrisive agent.
5. the preparation method of a kind of vacuum freeze drying flower grain electronics tobacco tar according to claim 1, is characterized in that described essence and flavoring agent, glycerine, propane diols or polyethylene glycol are edible rank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410817943.3A CN104544541B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil |
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| CN201410817943.3A CN104544541B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil |
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| CN104544541A true CN104544541A (en) | 2015-04-29 |
| CN104544541B CN104544541B (en) | 2016-09-28 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107057853A (en) * | 2017-01-16 | 2017-08-18 | 云南中烟新材料科技有限公司 | A kind of cigarette rose composite particles and its application |
| CN109832654A (en) * | 2019-01-10 | 2019-06-04 | 广东中烟工业有限责任公司 | A kind of cigarette low temperature multiple roasting method and its redried of preparation |
| CN110801050A (en) * | 2019-12-07 | 2020-02-18 | 深圳波顿香料有限公司 | Electronic cigarette oil for relieving rhinitis and preparation method thereof |
| CN112851636A (en) * | 2021-01-20 | 2021-05-28 | 深圳市艾普生物科技有限公司 | Preparation method and application of synthetic nicotine salt |
| CN113897244A (en) * | 2021-10-14 | 2022-01-07 | 深圳市兰科植物保护研究中心 | Preparation method and application of healthy cigarette spice |
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| US4694842A (en) * | 1983-09-21 | 1987-09-22 | Kouzou Kobayashi | Tea-containing tobacco |
| CN101669673A (en) * | 2008-09-11 | 2010-03-17 | 吴明宗 | Cigarette substitute and preparation method thereof |
| CN102370243A (en) * | 2010-08-11 | 2012-03-14 | 时书勤 | Traditional Chinese medicine healthcare sucking product for smoking cessation and preparation method thereof |
| CN102499456A (en) * | 2011-10-27 | 2012-06-20 | 云南烟草科学研究院 | Application of Yunnan edible roses in product ingredients of cigarette |
| CN103919263A (en) * | 2014-04-10 | 2014-07-16 | 中国烟草总公司郑州烟草研究院 | Method for judging freeze drying precooling temperatures of tobacco leaf samples by aid of eutectic crystal points and eutectic melting points |
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2014
- 2014-12-24 CN CN201410817943.3A patent/CN104544541B/en active Active
Patent Citations (6)
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| US4694842A (en) * | 1983-09-21 | 1987-09-22 | Kouzou Kobayashi | Tea-containing tobacco |
| CN101669673A (en) * | 2008-09-11 | 2010-03-17 | 吴明宗 | Cigarette substitute and preparation method thereof |
| CN102370243A (en) * | 2010-08-11 | 2012-03-14 | 时书勤 | Traditional Chinese medicine healthcare sucking product for smoking cessation and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107057853A (en) * | 2017-01-16 | 2017-08-18 | 云南中烟新材料科技有限公司 | A kind of cigarette rose composite particles and its application |
| CN107057853B (en) * | 2017-01-16 | 2020-06-16 | 云南中烟新材料科技有限公司 | Rose composite particles for cigarettes and application thereof |
| CN109832654A (en) * | 2019-01-10 | 2019-06-04 | 广东中烟工业有限责任公司 | A kind of cigarette low temperature multiple roasting method and its redried of preparation |
| CN110801050A (en) * | 2019-12-07 | 2020-02-18 | 深圳波顿香料有限公司 | Electronic cigarette oil for relieving rhinitis and preparation method thereof |
| CN112851636A (en) * | 2021-01-20 | 2021-05-28 | 深圳市艾普生物科技有限公司 | Preparation method and application of synthetic nicotine salt |
| CN113897244A (en) * | 2021-10-14 | 2022-01-07 | 深圳市兰科植物保护研究中心 | Preparation method and application of healthy cigarette spice |
| CN113897244B (en) * | 2021-10-14 | 2023-10-27 | 深圳市兰科植物保护研究中心 | Preparation method and application of cigarette spice |
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| Publication number | Publication date |
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| CN104544541B (en) | 2016-09-28 |
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