CN104544541B - A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil - Google Patents
A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil Download PDFInfo
- Publication number
- CN104544541B CN104544541B CN201410817943.3A CN201410817943A CN104544541B CN 104544541 B CN104544541 B CN 104544541B CN 201410817943 A CN201410817943 A CN 201410817943A CN 104544541 B CN104544541 B CN 104544541B
- Authority
- CN
- China
- Prior art keywords
- flos
- flower
- oil
- vacuum lyophilization
- grain
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses the preparation method of a kind of vacuum lyophilization flower grain electronics ree-oil.Joined in electronic cigarette oil base oil by the weight ratio of vacuum lyophilization flower grain 1～90%; flower grain includes: Flos Nelumbinis, oriental cherry, Cymbidium ensifolium (L.) Sw., rape flower, osmanthus flower tea, Flos Lonicerae, Flos Trollii, Flos Rosae Rugosae, jasmine, Flos Magnoliae, Flos Inulae, etc. at least one smash mixing briquet final vacuum lyophilization in any proportion, then damaged become granule；Base oil includes essence and flavoring agent 0～10%, deionized water 0～15%, glycerol 2～80%, and surplus supplies 100% weight with propylene glycol or Polyethylene Glycol again, and stirring and evenly mixing i.e. obtains vacuum lyophilization flower grain electronic cigarette oil product.The present invention makes these fragrance components immerse electronics ree-oil, gives electronic cigarette oil bloom characteristic perfume, can promote aroma quality and the perfume quantity of electronic cigarette, preferably masks the thorn larynx that propellant brings, and improves the gratification of consumer.
Description
Technical field
The present invention relates to the preparation method of a kind of vacuum lyophilization flower grain electronics ree-oil, belong to Nicotiana tabacum L. technology of preparing
Field.
Background technology
Electronic cigarette is a kind of on-fuel cigarette class substituted type product, has the outward appearance similar to medicated cigarette, ree-oil
(electronic cigarette liquid) produces fog under the effect of electronic smoke atomizer and is similar to true cigarette
Flue gas, meets pleasant sensation and the use habit of smoker, but have substantially from medicated cigarette different, do not burn,
Without the harmful substance such as tar, carbon monoxide.At present, commercially available electronics ree-oil is to allocate with various essence and flavoring agents
The product become, at the aspect such as fragrance, mouthfeel with the perceptual difference of medicated cigarette away from bigger, allows people be difficult to accept or practise
Its fragrance used and taste, even exhaust sensation that is dizzy and that feel sick.Flower not only can bring us visually
Aesthetic feeling, it is also possible to as spice.Flower have left water and soil earth, the most just loses original glamour.At present,
Vacuum Freezing & Drying Technology is considered as one of state-of-the-art store and processing technology, can preserve fresh feed color,
Fragrant, taste, fragrance matter loss is little, have the advantages such as loose good, the long shelf-life of loose structure dissolubility.
With fresh flowers as material, briquet after vacuum lyophilization, then in damaged one-tenth granule heating ree-oil,
Its addition can bring natural flowery odour to ree-oil, and ree-oil is seen see colored grain, to consumer one
Plant brand-new impression and experience.
Summary of the invention
It is an object of the invention to provide a kind of vacuum lyophilization flower grain, be applied in electronics ree-oil compatibility, promote
The fragrance of ree-oil suction and quality.
The purpose of the present invention is achieved through the following technical solutions.
A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil, preparation method is as follows:
Being joined in electronic cigarette oil base oil by the weight ratio of vacuum lyophilization flower grain 1～90%, stirring is mixed
Even i.e. obtain vacuum lyophilization flower grain electronic cigarette oil product.
Described colored grain includes: Flos Nelumbinis, oriental cherry, Cymbidium ensifolium (L.) Sw., rape flower, osmanthus flower tea, Flos Lonicerae, Flos Trollii,
Myosotis sylvatica, Dianthus carryophyllus, Flos Ginseng, flower of Radix Notoginseng, Flos Rosae Rugosae, jasmine, Flos Magnoliae, Flos Inulae, Hibiscus Sabdariffa Linn,
Flos Gardeniae, Flos persicae, Flos Chrysanthemi flower, Flos Matricariae chamomillae, Flos Gomphrenae, Flos Hibisci, Flos Caryophylli, Herba Verbasci Thapsi, bigarabe flower,
Orange blossom, Flos Robiniae Pseudoacaciae, Stigma Croci, Flos Chrysanthemi Indici, Flos Magnoliae Liliflorae, Flos Moutan, lavender flower, Flos Inulae, spring Huang
In Flos Chrysanthemi, Citrus aurantium L. var. amara Engl., Flos Caraganae Sinicae, flower of Folium Allii tuberosi, Hedychium flavum Roxb, gillyflower, Flos Mume, Flos Papaveris rhoeadis at least one
Kind of fresh flowers raw material loads in lyophilized plate in any proportion, put in-20 DEG C～-30 DEG C of freezers pre-cooling 15～
30 minutes and briquet；Then the in bulk flower raw material of pre-cooling is put in vacuum freeze drier, control to add
Hot plate temperature rises to 50 DEG C～60 DEG C dry 20～50 hours from room temperature, controls vacuum in heating process
It is 30～80pa；Then the granule that size is 5～80 mesh it is broken into after vacuum lyophilization.
Described base oil includes essence and flavoring agent 0～10%, deionized water 0～15%, glycerol 2～80%,
Surplus supplies 100% weight with propylene glycol or Polyethylene Glycol again.
Described vacuum lyophilization flower grain is without any additive and preservative.
Described essence and flavoring agent, glycerol, propylene glycol or Polyethylene Glycol, is edible rank.
The invention has the beneficial effects as follows:
The present invention breaches the bottleneck of the fragrance nature sensory experience deficiency that existing electronic cigarette tobacco tar exists, and composes
Give the impression of ree-oil flowery odour lasting, excellent, natural, the fragrance of more high-quality is provided for electronic cigarette tobacco tar industry
Material adding technique and product, improve and add cigarette oil added value.
Detailed description of the invention
It is more fully understood that the present invention for convenience, is illustrated by following instance.These examples belong to the present invention
Protection domain, but be not intended to protection scope of the present invention.
Embodiment 1
Flos Trollii loads puts into pre-cooling 25 minutes briquet in-25 DEG C of freezers in lyophilized plate；Then by pre-cooling
In bulk flower raw material put in vacuum freeze drier, control temperature of heating plate from room temperature rise to 55 DEG C be dried
30 hours, controlling vacuum in heating process was 50pa, and after vacuum lyophilization, damaged one-tenth 5 purposes are spherical
Granule.Weigh the Flos Trollii grain 10g after vacuum lyophilization, join base oil (by essence and flavoring agent: deionization
Water: glycerol: propylene glycol is 100g: 150g: 500g: 250g to be mixed and made into 1000g base oil) 990g
In, it is uniformly mixed and i.e. obtains vacuum lyophilization Flos Trollii grain electronic cigarette oil product.
Embodiment 2
Rape flower loads puts into pre-cooling 28 minutes briquet in-30 DEG C of freezers in lyophilized plate；Then by pre-cooling
In bulk flower raw material put in vacuum freeze drier, control temperature of heating plate from room temperature rise to 50 DEG C be dried
40 hours, controlling vacuum in heating process was 30pa, the ball of damaged one-tenth 20 mesh after vacuum lyophilization
Shape granule.Weigh the rape flower 500g after vacuum lyophilization, join base oil (by essence and flavoring agent: go from
Sub-water: glycerol: propylene glycol is 80g: 150g: 20g: 750g to be mixed and made into 1000g base oil) 500g
In, it is uniformly mixed and i.e. obtains vacuum lyophilization rape flower grain electronic cigarette oil product.
Embodiment 3
Flos Caryophylli loads puts into pre-cooling 30 minutes briquet in-20 DEG C of freezers in lyophilized plate；Then will be pre-
Cold in bulk flower raw material is put in vacuum freeze drier, controls temperature of heating plate and rises to 60 DEG C dry from room temperature
Dry 20 hours, controlling vacuum in heating process was 30pa, damaged one-tenth 80 purposes after vacuum lyophilization
Irregular particle.Weigh the Flos Caryophylli grain 900g after vacuum lyophilization, join base oil (by deionized water:
Glycerol: Polyethylene Glycol is 150g: 100g: 750g to be mixed and made into 1000g base oil) in 100g, stirring
Mix homogeneously i.e. obtains vacuum lyophilization Flos Caryophylli grain electronic cigarette oil product.
Embodiment 4
Flos Ginseng, flower of Radix Notoginseng load in lyophilized plate by weight 50: 50 puts into pre-cooling 26 points in-28 DEG C of freezers
Clock briquet；Then the in bulk flower raw material of pre-cooling is put in vacuum freeze drier, control heating plate
Temperature rises to be dried 40 hours 60 DEG C from room temperature, and controlling vacuum in heating process is 60pa, very
The spheroidal particle of damaged one-tenth 50 mesh after vacuum freecing-dry.Weigh the flower grain 200g of the mixing after vacuum lyophilization,
Join base oil (by essence and flavoring agent: glycerol: propylene glycol is 50g: 100g: 850g to be mixed and made into 1000g
Base oil) in 100g, it is uniformly mixed and i.e. obtains vacuum lyophilization mixing flower grain electronic cigarette oil product.
Embodiment 5
Gillyflower, lavender flower, Flos Matricariae chamomillae load in lyophilized plate by weight 10: 30: 60 puts into-30 DEG C
Pre-cooling 15 minutes briquet in freezer；Then the in bulk flower raw material of pre-cooling is put into vacuum freeze drier
In, control temperature of heating plate and rise to be dried 50 hours 50 DEG C from room temperature, control vacuum in heating process
Degree is 60pa, and the spheroidal particle of damaged one-tenth 40 mesh after vacuum lyophilization, after weighing vacuum lyophilization
Mixing flower grain 300g, join base oil (by essence and flavoring agent: deionized water: glycerol: Polyethylene Glycol is 50g:
150g: 350g: 450g is mixed and made into 1000g base oil) in 100g, it is uniformly mixed that i.e. to obtain vacuum cold
Freeze dry mixed flower grain electronic cigarette oil product.
Embodiment 6
Myosotis sylvatica, Dianthus carryophyllus, Flos Papaveris rhoeadis, jasmine, Flos Magnoliae, Flos Inulae, Hibiscus Sabdariffa Linn are by arbitrarily freezing than loading
Dry pan is put into pre-cooling 26 minutes briquet in-25 DEG C of freezers；Then the in bulk flower raw material of pre-cooling is put
Enter in vacuum freeze drier, control temperature of heating plate and rise to be dried 40 hours 60 DEG C from room temperature, control
In heating process processed, vacuum is 60pa, the spheroidal particle of damaged one-tenth 10 mesh after vacuum lyophilization.Weigh
Mixing flower grain 400g after vacuum lyophilization, joins base oil (by essence and flavoring agent: deionized water: the third three
Alcohol is 50g: 150g: 800g to be mixed and made into 1000g base oil) in 100g, it is uniformly mixed and i.e. obtains vacuum
Lyophilization mixing flower grain electronic cigarette oil product.
Embodiment 7
Flos Nelumbinis, oriental cherry, Cymbidium ensifolium (L.) Sw., rape flower, osmanthus flower tea, Flos Lonicerae, Flos Trollii, Myosotis sylvatica, Dianthus carryophyllus,
Flos Ginseng, flower of Radix Notoginseng, Flos Rosae Rugosae, jasmine, Flos Magnoliae, Flos Inulae, Hibiscus Sabdariffa Linn, Flos Gardeniae, Flos persicae,
Flos Chrysanthemi flower, Flos Matricariae chamomillae, Flos Gomphrenae, Flos Hibisci, Flos Caryophylli, Herba Verbasci Thapsi, bigarabe flower, orange blossom, Flos Robiniae Pseudoacaciae,
Stigma Croci, Flos Chrysanthemi Indici, Flos Magnoliae Liliflorae, Flos Moutan, lavender flower, Flos Inulae, Chamomile, Citrus aurantium L. var. amara Engl.,
Flos Caraganae Sinicae, flower of Folium Allii tuberosi, Hedychium flavum Roxb, gillyflower, Flos Mume, Flos Papaveris rhoeadis load lyophilized plate by any weight ratio
In put in-30 DEG C of freezers pre-cooling 30 minutes briquet；Then the in bulk flower raw material of pre-cooling is put into very
In vacuum freecing-dry machine, control temperature of heating plate and rise to be dried 42 hours 50 DEG C from room temperature, control to add
In thermal process, vacuum is 30pa.After vacuum lyophilization, the spheroidal particle of damaged one-tenth 20 mesh, weighs vacuum cold
Freeze dried mixing flower grain 600g, join base oil (by essence and flavoring agent: deionized water: glycerol: third
Glycol is to be mixed and made into 1000g base oil at 10g: 150g: 700g: 140) 100g is uniformly mixed i.e.
Obtain vacuum lyophilization mixing flower grain electronic cigarette oil product.
Claims (5)
1. the preparation method of a vacuum lyophilization flower grain electronics ree-oil, it is characterised in that preparation method is such as
Under: being joined in electronic cigarette oil base oil by the weight ratio of vacuum lyophilization flower grain 1～90%, stirring is mixed
Even i.e. obtain vacuum lyophilization flower grain electronic cigarette oil product；
Described colored grain includes: Flos Nelumbinis, oriental cherry, Cymbidium ensifolium (L.) Sw., rape flower, osmanthus flower tea, Flos Lonicerae, Flos Trollii,
Myosotis sylvatica, Dianthus carryophyllus, Flos Ginseng, flower of Radix Notoginseng, Flos Rosae Rugosae, jasmine, Flos Magnoliae, Flos Inulae, Hibiscus Sabdariffa Linn,
Flos Gardeniae, Flos persicae, Flos Chrysanthemi flower, Flos Matricariae chamomillae, Flos Gomphrenae, Flos Hibisci, Flos Caryophylli, Herba Verbasci Thapsi, bigarabe flower,
Orange blossom, Flos Robiniae Pseudoacaciae, Stigma Croci, Flos Chrysanthemi Indici, Flos Magnoliae Liliflorae, Flos Moutan, lavender flower, Chamomile, turtle
At least one fresh flowers in turtle flower, Flos Caraganae Sinicae, flower of Folium Allii tuberosi, Hedychium flavum Roxb, gillyflower, Flos Mume, Flos Papaveris rhoeadis
Raw material loads in lyophilized plate in any proportion, puts in-20 DEG C～-30 DEG C of freezers pre-cooling 15～30 minutes also
Briquet；Then the in bulk flower raw material of pre-cooling is put in vacuum freeze drier, control temperature of heating plate
Rise to 50 DEG C～60 DEG C from room temperature and be dried 20～50 hours, control vacuum in heating process be 30～
80pa；The granule that size is 5～80 mesh it is broken into after vacuum lyophilization.
The preparation method of a kind of vacuum lyophilization the most according to claim 1 flower grain electronics ree-oil, its
Being characterised by, described base oil includes essence and flavoring agent 0～10%, deionized water 0～15%, glycerol 2～
80%, surplus supplies 100% weight with propylene glycol or Polyethylene Glycol again.
The preparation method of a kind of vacuum lyophilization the most according to claim 1 and 2 flower grain electronics ree-oil,
It is characterized in that, described vacuum lyophilization flower grain is without any additive.
The preparation method of a kind of vacuum lyophilization the most according to claim 3 flower grain electronics ree-oil, its
Being characterised by, described additive is preservative.
The preparation method of a kind of vacuum lyophilization the most according to claim 2 flower grain electronics ree-oil, its
It is characterised by that described essence and flavoring agent, glycerol, propylene glycol and Polyethylene Glycol is edible rank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410817943.3A CN104544541B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410817943.3A CN104544541B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104544541A CN104544541A (en) | 2015-04-29 |
| CN104544541B true CN104544541B (en) | 2016-09-28 |
Family
ID=53062459
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410817943.3A Active CN104544541B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104544541B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107057853B (en) * | 2017-01-16 | 2020-06-16 | 云南中烟新材料科技有限公司 | Rose composite particles for cigarettes and application thereof |
| CN109832654A (en) * | 2019-01-10 | 2019-06-04 | 广东中烟工业有限责任公司 | A kind of cigarette low temperature multiple roasting method and its redried of preparation |
| CN110801050A (en) * | 2019-12-07 | 2020-02-18 | 深圳波顿香料有限公司 | Electronic cigarette oil for relieving rhinitis and preparation method thereof |
| CN112851636B (en) * | 2021-01-20 | 2022-04-05 | 深圳市艾普生物科技有限公司 | Preparation method and application of synthetic nicotine salt |
| CN113897244B (en) * | 2021-10-14 | 2023-10-27 | 深圳市兰科植物保护研究中心 | Preparation method and application of cigarette spice |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4694842A (en) * | 1983-09-21 | 1987-09-22 | Kouzou Kobayashi | Tea-containing tobacco |
| CN101669673A (en) * | 2008-09-11 | 2010-03-17 | 吴明宗 | Cigarette substitute and preparation method thereof |
| CN102370243A (en) * | 2010-08-11 | 2012-03-14 | 时书勤 | Traditional Chinese medicine healthcare sucking product for smoking cessation and preparation method thereof |
| CN102499456A (en) * | 2011-10-27 | 2012-06-20 | 云南烟草科学研究院 | Application of Yunnan edible roses in product ingredients of cigarette |
| CN103919263A (en) * | 2014-04-10 | 2014-07-16 | 中国烟草总公司郑州烟草研究院 | Method for judging freeze drying precooling temperatures of tobacco leaf samples by aid of eutectic crystal points and eutectic melting points |
| CN104026731A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Heart nourishing and nerve soothing functional electronic cigarette juice |
-
2014
- 2014-12-24 CN CN201410817943.3A patent/CN104544541B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4694842A (en) * | 1983-09-21 | 1987-09-22 | Kouzou Kobayashi | Tea-containing tobacco |
| CN101669673A (en) * | 2008-09-11 | 2010-03-17 | 吴明宗 | Cigarette substitute and preparation method thereof |
| CN102370243A (en) * | 2010-08-11 | 2012-03-14 | 时书勤 | Traditional Chinese medicine healthcare sucking product for smoking cessation and preparation method thereof |
| CN102499456A (en) * | 2011-10-27 | 2012-06-20 | 云南烟草科学研究院 | Application of Yunnan edible roses in product ingredients of cigarette |
| CN103919263A (en) * | 2014-04-10 | 2014-07-16 | 中国烟草总公司郑州烟草研究院 | Method for judging freeze drying precooling temperatures of tobacco leaf samples by aid of eutectic crystal points and eutectic melting points |
| CN104026731A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Heart nourishing and nerve soothing functional electronic cigarette juice |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104544541A (en) | 2015-04-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104544541B (en) | A kind of preparation method of vacuum lyophilization flower grain electronics ree-oil | |
| CN106212732A (en) | A kind of spicy chilli oil and preparation method thereof | |
| CN104996627A (en) | A granular pattern tea solid beverage and a preparation method | |
| CN101828769B (en) | Preparation method of cigarette flavor compensating particles | |
| Moghbeli et al. | A Taguchi approach optimization of date powder production by spray drying with the aid of whey protein-pectin complexes | |
| CN107438367A (en) | For preparing the low bulk density composition with the dust reduced or the teabag drink of fine powder | |
| CN104642688A (en) | Preparation method of cordyceps militaris link tableted candy | |
| CN104544540A (en) | Preparation method for vacuum freeze drying fruit grain electronic cigarette liquid | |
| CN104189935A (en) | Peony fragrant bead and preparation method thereof | |
| CN101606550A (en) | A kind of natural volatile solid fruit and vegetable fresh-keeping agent and preparation method thereof | |
| CN106235243A (en) | A kind of Bulbus Allii perfume (or spice) chilli oil and preparation method thereof | |
| CN104687204A (en) | Production method of solid cordyceps militaris drink | |
| CN104686762A (en) | Scenting method for composite camellia nitidissima scented tea | |
| CN105838503A (en) | Slow aroma release type zein microcapsules and preparing method thereof | |
| CN107846949A (en) | The method for preparing sodium salt and/or sylvite product, can thus obtained product salt and application thereof | |
| CN103300178B (en) | Dry flower puer tea and preparation method thereof | |
| CN105638595A (en) | Fish bait formula and preparation method for same | |
| CN102132797A (en) | Areca-nut core substitute for areca-nut food and preparation method thereof | |
| CN107969523A (en) | A kind of preparation method of egg fruit tea | |
| CN105670792A (en) | Preparing method and application of cigarette filter tip expansion granular material | |
| CN104544542B (en) | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid | |
| CN106361980A (en) | Polygonatum kingianum lozenge and preparation method thereof | |
| CN102504964B (en) | High-stability formaldehyde eliminating clean composition and preparation method thereof | |
| CN107815358A (en) | A kind of preparation method of tea seed washing powder | |
| CN106490138A (en) | A kind of based on the kiwi fruit preservative of plants essential oil, tin foil and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |