CN104544540A - Preparation method for vacuum freeze drying fruit grain electronic cigarette liquid - Google Patents
Preparation method for vacuum freeze drying fruit grain electronic cigarette liquid Download PDFInfo
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- CN104544540A CN104544540A CN201410817941.4A CN201410817941A CN104544540A CN 104544540 A CN104544540 A CN 104544540A CN 201410817941 A CN201410817941 A CN 201410817941A CN 104544540 A CN104544540 A CN 104544540A
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- vacuum freeze
- freeze drying
- fruit
- electronic cigarette
- preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses a preparation method for vacuum freeze drying fruit grain electronic cigarette liquid. The preparation method is characterized in that 1%-90% of vacuum freeze drying fruit grains in percentage by weight are added into base oil of the electronic cigarette liquid, and the fruit grains are formed by carrying out vacuum freeze drying on fruit pulps in arbitrary proportion and then breaking the fruit pulps into grains; the base oil comprises the components in percentage by weight: 0-10% of essence and flavor, 0-15% of deionized water, 2%-80% of glycerol and the balance of propylene glycol or polyethylene glycol which is supplemented to be 100%, and the vacuum freeze drying fruit grain electronic cigarette liquid can be obtained by uniformly stirring and mixing. Natural fruit aroma can be brought for the electronic cigarette fluid through the adding of the vacuum freeze drying fruit grains, and the vacuum freeze drying fruit grains have the obvious advantage of increasing the aroma. According to the preparation method disclosed by the invention, the aroma components are immersed into the electronic cigarette liquid, so that the characteristic flavor of fruits is given to the electronic cigarette liquid, the aroma quality and the aroma amount of the electronic cigarette liquid are increased, the throat irritation caused by an atomizing agent can be better covered, and the satisfaction of a customer is increased.
Description
Technical field
The present invention relates to a kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar, belong to tobacco preparing technical field.
Background technology
Electronic cigarette has the outward appearance similar to cigarette, and tobacco tar (electronic cigarette liquid) produces fog and is similar to true cigarette flue gas under the effect of electronic smoke atomizer, but not containing the harmful substance such as tar, carbon monoxide.At present, the product that commercially available electronics tobacco tar is deployed into various essence and flavoring agent, larger with the perceptual difference distance of cigarette in fragrance, mouthfeel etc., allow people be difficult to accept or be accustomed to its fragrance and taste, even exhaust sensation that is dizzy and that feel sick.Vacuum freeze drying fruit grain effectively keeps perfume (or spice), taste, the look of original fruit, and adding of it can bring natural fruit aroma to tobacco tar, and see in tobacco tar see fruit grain, to a kind of brand-new impression of consumer and experience.
Summary of the invention
The object of this invention is to provide a kind of vacuum freeze drying fruit grain, be applied in electronics tobacco tar compatibility, promote fragrance and the quality of tobacco tar suction.
Object of the present invention is achieved through the following technical solutions.
A preparation method for vacuum freeze drying fruit grain electronics tobacco tar, preparation method is as follows:
Joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying fruit grain 1 ~ 90%, stir and evenly mix and obtain vacuum freeze drying fruit grain electronic cigarette oil product.
Described fruit grain comprises: in apple, strawberry, banana, pears, lemon, blueberry, Kiwi berry, peach, durian, dragon fruit, pineapple, jackfruit, "Hami" melon, rambutan, grape, lichee, mango, shaddock, orange, jujube the pulp of at least one fruit smash after through vacuum freeze drying, then damaged become size be 5 ~ 80 object particles.
Described vacuum freeze-drying technique condition puts into-20 DEG C ~-30 DEG C freezer precoolings 15 ~ 30 minutes in fruit loading lyophilized plate, then precooled fruit is put into vacuum freeze drier, control temperature of heating plate and rise to 50 DEG C ~ 60 DEG C dryings 30 ~ 40 hours from room temperature, controlling vacuum in heating process is 30 ~ 80pa.
Described base oil comprises essence and flavoring agent 0 ~ 10%, deionized water 0 ~ 15%, glycerine 2 ~ 80%, and surplus supplies 100% weight with propane diols or polyethylene glycol again.
Described vacuum freeze drying fruit grain does not add any additive and anticorrisive agent.
Described essence and flavoring agent, glycerine, propane diols or polyethylene glycol, be edible rank.
The invention has the beneficial effects as follows:
The present invention breaches the bottleneck of the fragrance nature sensory experience deficiency that existing electronic cigarette tobacco tar exists, give tobacco tar lasting, excellent, natural aroma experience, for electronic cigarette tobacco tar industry provides fragrance matter adding technique and the product of more high-quality, improve and add cigarette oil added value.
Detailed description of the invention
For convenience of understanding the present invention better, be illustrated by following instance.These examples belong to protection scope of the present invention, but do not limit the scope of the invention.
Embodiment 1
Get apple pulp, load in lyophilized plate and put into-30 DEG C of freezer precoolings 15 minutes, smash and briquet; Then the one-tenth block apple of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 30 hours, controlling vacuum in heating process is 30pa, and the breakage after vacuum freeze drying becomes 5 object spheric granules.Take the apple grain 10g after vacuum freeze drying, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 150g: 150g: 650g: 50g be mixed and made into 1000g base oil) 990g, be uniformly mixed and obtain performing vacuum freeze drying on apple grain electronic cigarette oil product.
Embodiment 2
Get in strawberry pulp loading lyophilized plate and put into-28 DEG C of freezer precoolings 25 minutes, smash and briquet; Then the one-tenth block strawberry of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 55 DEG C dry 35 hours, controlling vacuum in heating process is 60pa.Damaged one-tenth 20 object spheric granules after vacuum freeze drying, measure the strawberry grain 500g after vacuum freeze drying by weight percentage, join in base oil (by deionized water: glycerine: propane diols is 100g: 800g: 100g be mixed and made into 1000g base oil) 500g, be uniformly mixed and obtain vacuum freeze drying strawberry grain electronic cigarette oil product.
Embodiment 3
Get in peach pulp loading lyophilized plate and put into-28 DEG C of freezer precoolings 25 minutes, smash and briquet; Then the one-tenth block peach of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 22 hours, controlling vacuum in heating process is 30pa.Damaged one-tenth 80 object irregular particles after vacuum freeze drying, measure the peach grain after vacuum freeze drying by weight percentage: essence and flavoring agent 900g, join in base oil (by essence and flavoring agent: glycerine: polyethylene glycol is 150g: 700g: 150g be mixed and made into 1000g base oil) 100g, be uniformly mixed and obtain vacuum freeze drying peach grain electronic cigarette oil product.
Embodiment 4
Get mango, dragon fruit, pineapple pulp to load in lyophilized plate by weight 50: 30: 20 and put into-20 DEG C of freezer precoolings 30 minutes, smash mixing and briquet; Then the one-tenth block fruit of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 30 hours, controlling vacuum in heating process is 50pa.Damaged one-tenth 40 object spheric granules after vacuum freeze drying, measure the mixed fruit grain 200g after vacuum freeze drying by weight percentage, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 100g: 100g: 500g: 300g be mixed and made into 1000g base oil) 800g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronic cigarette oil product.
Embodiment 5
Get rambutan, lichee, grapefruit flesh to load in any proportion in lyophilized plate and put into-28 DEG C of freezer precoolings 25 minutes, smash mixing and briquet; Then the one-tenth block fruit of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C dry 40 hours, controlling vacuum in heating process is 60pa.Damaged one-tenth 50 object spheric granules after vacuum freeze drying, measure the mixed fruit grain 400g after vacuum freeze drying by weight percentage, join in base oil (by essence and flavoring agent: deionized water: glycerine: polyethylene glycol is 50g: 150g: 750g: 50g be mixed and made into 1000g base oil) 600g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronic cigarette oil product.
Embodiment 6
Get durian, jackfruit, Hami melon pulp to load in lyophilized plate by weight 20: 50: 30 and put into-30 DEG C of freezer precoolings 20 minutes, smash mixing and briquet; Then the one-tenth block fruit of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 30 hours, controlling vacuum in heating process is 50pa.Damaged one-tenth 60 object spheric granules after vacuum freeze drying, measure the mixed fruit grain 100g after vacuum freeze drying by weight percentage, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 150g: 150g: 20g: 680g be mixed and made into 1000g base oil) 900g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronic cigarette oil product.
Embodiment 7
Get apple, strawberry, banana, pears, lemon, blueberry, Kiwi berry, peach, durian, dragon fruit, pineapple, jackfruit, "Hami" melon, rambutan, grape, lichee, mango, shaddock, orange, jujube pulp by arbitrarily putting into-30 DEG C of freezer precoolings 30 minutes than loading in lyophilized plate, smash mixing also briquet; Then the one-tenth block fruit of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C dry 40 hours, controlling vacuum in heating process is 30pa.Damaged one-tenth 80 object spheric granules after vacuum freeze drying, measure the mixed fruit grain 600g after vacuum freeze drying by weight percentage, join in base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 150g: 150g: 200g: 500g be mixed and made into 1000g base oil) 400g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronic cigarette oil product.
Claims (6)
1. the preparation method of a vacuum freeze drying fruit grain electronics tobacco tar, it is characterized in that, preparation method is as follows: joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying fruit grain 1 ~ 90%, stirs and evenly mixs and obtain vacuum freeze drying fruit grain electronic cigarette oil product.
2. the preparation method of a kind of vacuum freeze drying fruit grain electronics tobacco tar according to claim 1, it is characterized in that: described fruit grain comprises: the pulp of at least one fruit vacuum freeze drying in any proportion in apple, strawberry, banana, pears, lemon, blueberry, Kiwi berry, peach, durian, dragon fruit, pineapple, jackfruit, "Hami" melon, rambutan, grape, lichee, mango, shaddock, orange, jujube, then damaged one-tenth size is 5 ~ 80 object particles.
3. the preparation method of a kind of vacuum freeze drying fruit grain electronics tobacco tar according to claim 1, it is characterized in that: described vacuum freeze-drying technique condition puts into-20 DEG C ~-30 DEG C freezer precoolings 15 ~ 30 minutes in fruit loading lyophilized plate, smash mixing and briquet, then precooled fruit chunk is put into vacuum freeze drier, control temperature of heating plate and rise to 50 DEG C ~ 60 DEG C dryings 30 ~ 40 hours from room temperature, controlling vacuum in heating process is 30 ~ 80pa.
4. according to the preparation method of the arbitrary described a kind of vacuum freeze drying fruit grain electronics tobacco tar of claim 1-3, it is characterized in that: described base oil comprises essence and flavoring agent 0 ~ 10%, deionized water 0 ~ 15%, glycerine 2 ~ 80%, surplus supplies 100% weight with propane diols or polyethylene glycol again.
5., according to the preparation method of the arbitrary described a kind of vacuum freeze drying fruit grain electronics tobacco tar of claim 1-3, it is characterized in that: described vacuum freeze drying fruit grain does not add any additive and anticorrisive agent.
6., according to the preparation method of the arbitrary described a kind of vacuum freeze drying fruit grain electronics tobacco tar of claim 1-3, it is characterized in that: described essence and flavoring agent, glycerine, propane diols or polyethylene glycol, be edible rank.
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| CN201410817941.4A CN104544540B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar |
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| CN201410817941.4A CN104544540B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar |
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| CN104544540A true CN104544540A (en) | 2015-04-29 |
| CN104544540B CN104544540B (en) | 2016-05-04 |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106108102A (en) * | 2016-08-23 | 2016-11-16 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of red pitaya wine odor type electronic cigarette tobacco tar |
| CN106136298A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of litchi spirit odor type electronic cigarette tobacco tar |
| CN106136301A (en) * | 2016-07-15 | 2016-11-23 | 广西中烟工业有限责任公司 | The preparation method of a kind of Hylocereus undatus extract and the application in Medicated cigarette thereof |
| CN106307601A (en) * | 2016-08-23 | 2017-01-11 | 广西壮族自治区农业科学院农产品加工研究所 | Longan wine scent type electronic cigarette liquid |
| CN106723306A (en) * | 2017-01-16 | 2017-05-31 | 云南中烟新材料科技有限公司 | A kind of method that American mint prepares cigarette filter rod additive |
| CN107853750A (en) * | 2017-10-11 | 2018-03-30 | 吴雷 | A kind of solid tobacco tar and its processing method |
| CN109757783A (en) * | 2019-03-05 | 2019-05-17 | 铂德（深圳）科技有限公司 | Fragaia ananassa Duchesne extract solution, strawberry electronics tobacco tar and preparation method thereof |
| CN109984372A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Mango extract solution, mango electronics tobacco tar and preparation method thereof |
| CN110655986A (en) * | 2019-09-25 | 2020-01-07 | 武汉黄鹤楼香精香料有限公司 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
| CN111629607A (en) * | 2017-11-01 | 2020-09-04 | 尼科创业贸易有限公司 | Flavored vaporizable formulations |
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| CN103054171A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from flat-flavor tobacco |
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| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
| CN104068468A (en) * | 2014-07-11 | 2014-10-01 | 张伟滨 | Hookah fruit tobacco for electronic smoking set and traditional hookah smoking set and preparing method of hookah fruit tobacco |
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Patent Citations (4)
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| CN103404965A (en) * | 2012-12-28 | 2013-11-27 | 昌宁德康生物科技有限公司 | Method for producing pulp applied to electronic smoking set and traditional water pipe with shredded tobacco |
| CN103054171A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from flat-flavor tobacco |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
| CN104068468A (en) * | 2014-07-11 | 2014-10-01 | 张伟滨 | Hookah fruit tobacco for electronic smoking set and traditional hookah smoking set and preparing method of hookah fruit tobacco |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106136301A (en) * | 2016-07-15 | 2016-11-23 | 广西中烟工业有限责任公司 | The preparation method of a kind of Hylocereus undatus extract and the application in Medicated cigarette thereof |
| CN106108102A (en) * | 2016-08-23 | 2016-11-16 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of red pitaya wine odor type electronic cigarette tobacco tar |
| CN106136298A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of litchi spirit odor type electronic cigarette tobacco tar |
| CN106307601A (en) * | 2016-08-23 | 2017-01-11 | 广西壮族自治区农业科学院农产品加工研究所 | Longan wine scent type electronic cigarette liquid |
| CN106723306A (en) * | 2017-01-16 | 2017-05-31 | 云南中烟新材料科技有限公司 | A kind of method that American mint prepares cigarette filter rod additive |
| CN106723306B (en) * | 2017-01-16 | 2018-05-18 | 云南中烟新材料科技有限公司 | A kind of method that cigarette filter rod additive is prepared with American mint |
| CN107853750A (en) * | 2017-10-11 | 2018-03-30 | 吴雷 | A kind of solid tobacco tar and its processing method |
| CN111629607A (en) * | 2017-11-01 | 2020-09-04 | 尼科创业贸易有限公司 | Flavored vaporizable formulations |
| CN109757783A (en) * | 2019-03-05 | 2019-05-17 | 铂德（深圳）科技有限公司 | Fragaia ananassa Duchesne extract solution, strawberry electronics tobacco tar and preparation method thereof |
| CN109984372A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Mango extract solution, mango electronics tobacco tar and preparation method thereof |
| CN110655986A (en) * | 2019-09-25 | 2020-01-07 | 武汉黄鹤楼香精香料有限公司 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
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| CN104544540B (en) | 2016-05-04 |
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