CN110655986A - Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof - Google Patents
Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof Download PDFInfo
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- CN110655986A CN110655986A CN201910909298.0A CN201910909298A CN110655986A CN 110655986 A CN110655986 A CN 110655986A CN 201910909298 A CN201910909298 A CN 201910909298A CN 110655986 A CN110655986 A CN 110655986A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to the technical field of tobacco essence and flavor, in particular to honey pomelo compound-flavor electronic cigarette oil and a preparation method thereof. The electronic cigarette oil comprises, by mass, 0.5-3 parts of phenethyl acetate, 0.1-0.5 part of phenylacetic acid, 0.2-1.0 part of p-cresol acetate, 0.5-3 parts of methyl phenylacetate, 0.1-0.5 part of menthyl acetate, 1.5-5.0 parts of isobutyl phenylacetate, 0.2-0.8 part of ethyl phenylacetate, 0.5-3.5 parts of damascenone, 0.2-0.8 part of natural citral, 0.5-3 parts of beeswax absolute, 0.3-1 part of amyl phenylacetate, 0.2-1.0 part of vanillin, 10-20 parts of benzyl alcohol, 1-5 parts of ethyl laurate, 0.5-3 parts of oxidized isophorone, 2-8 parts of nootkatone, 0.2-1.0 part of bruton oil, 0.2-0 part of bitter almond oil, 1.5-5.5 parts of ethyl maltol and 850 parts of propylene glycol. The electronic cigarette oil with the fragrance of honey pomelo, harmonious and natural fragrance, soft and exquisite smoke and comfortable mouthfeel is obtained by matching a plurality of components, and the electronic cigarette oil is simple in preparation method, low in cost and applicable to large-scale industrial production.
Description
Technical Field
The invention relates to the technical field of tobacco essence and flavor, in particular to honey pomelo compound-flavor electronic cigarette oil and a preparation method thereof.
Background
The electronic cigarette is an electronic product simulating a cigarette, and has the same appearance, smoke, taste and sensation as the cigarette. It is a product which is absorbed by users after nicotine and the like are changed into steam by means of atomization and the like.
The electronic cigarette liquid is electronic atomized liquid used in cooperation with an electronic cigarette, is also a food additive, and can generate mist like cigarettes by heating through an electronic cigarette atomizer. The components are as follows: propylene glycol, vegetable glycerin, flavoring essence and natural extract and nicotine.
At present, the electronic cigarette still has certain deficiencies in the aspects of smoking quality, aroma style characteristics and the like, the development of an essence product suitable for the electronic cigarette is delayed, and a novel essence suitable for the electronic cigarette is urgently needed to solve the problems, so that the aroma amount is increased, the personalized requirements of consumers on aroma are met, and the problems are avoided.
Honey is produced by natural fermentation of honey in honeycomb, and is a yellow-white sticky liquid which contains various inorganic salts with similar concentration to human serum, various organic acids such as vitamins, iron, calcium, copper, manganese, potassium and phosphorus, trace elements beneficial to human health, fructose, glucose, amylase, oxidase, reductase and the like, has the effects of nourishing, moistening dryness, detoxifying, whitening, beautifying and relaxing bowel, and is known as the most perfect nutritional food in nature. The pomelo is a tree of Citrus of Rutaceae, contains abundant nutritional values, contains a large amount of nutritional elements, including protein, organic acid, multiple vitamins, calcium, phosphorus, magnesium, sodium and other trace elements necessary for human body, and the pomelo meat contains abundant vitamin C, insulin-like and other components, so that the pomelo has the effects of reducing blood sugar, blood fat, weight, skin care and beautifying. The honey and grapefruit composite flavor type electronic cigarette oil can endow the electronic cigarette with new flavor type in the application of the electronic cigarette, increase the fragrance amount, improve the smoking quality of the electronic cigarette, and meet the personalized requirements of consumers.
Disclosure of Invention
The invention aims to solve the problems and provides the electronic cigarette oil which has the fragrance of honey pomelo, harmonious and natural fragrance, soft and exquisite smoke and comfortable mouthfeel and the preparation method thereof.
The technical scheme for solving the problems is to provide honey pomelo compound-flavor electronic cigarette oil which comprises, by mass, 0.5-3 parts of phenethyl phenylacetate, 0.1-0.5 part of phenylacetic acid, 0.2-1.0 part of p-cresol acetate, 0.5-3 parts of methyl phenylacetate, 0.1-0.5 part of menthyl acetate, 1.5-5.0 parts of isobutyl phenylacetate, 0.2-0.8 part of ethyl phenylacetate, 0.5-3.5 parts of damascenone, 0.2-0.8 part of natural citral, 0.5-3 parts of beeswax absolute, 0.3-1 part of amyl phenylacetate, 0.2-1.0 part of vanillin, 10-20 parts of benzyl alcohol, 1-5 parts of ethyl laurate, 0.5-3 parts of oxidized isophorone, 2-8 parts of parapomelo ketone, 0.2-1.0 part of buchu oil, 0.2-0.8 part of almond oil and 1.5-5 parts of ethyl phenol, 750 portions of propylene glycol and 850 portions of propylene glycol.
Preferably, the cleaning agent comprises, by mass, 2 parts of phenylethyl phenylacetate, 0.8 part of phenylacetic acid, 0.6 part of p-cresol acetate, 2 parts of methyl phenylacetate, 0.3 part of menthyl acetate, 3 parts of isobutyl phenylacetate, 0.6 part of ethyl phenylacetate, 2.2 parts of damascenone, 0.5 part of natural citral, 1.2 parts of beeswax absolute, 0.6 part of amyl phenylacetate, 0.7 part of vanillin, 15 parts of benzyl alcohol, 3.2 parts of ethyl laurate, 1.8 parts of oxidized isophorone, 6 parts of paraquat ketone, 0.6 part of brunaxseed oil, 0.6 part of bitter almond oil, 3 parts of ethyl maltol and 785 parts of propylene glycol.
The invention also aims to provide a preparation method of the honey pomelo compound-flavor electronic cigarette oil, which comprises the following steps: the components are evenly mixed according to the mass portion and then diluted to 900-1100 portions.
Preferably, it is diluted with glycerol.
The invention has the beneficial effects that:
1. the natural honey fragrance is prepared by matching and using raw materials such as phenethyl phenylacetate, phenylacetic acid, p-cresol acetate, methyl phenylacetate, menthyl acetate, isobutyl phenylacetate, ethyl phenylacetate, damascenone, natural citral, beeswax absolute, amyl phenylacetate, vanillin, benzyl alcohol, ethyl laurate, isophorone oxide and the like, and the natural honey fragrance is natural, and is transparent and lasting. The main fragrance of the grapefruit is prepared by reasonably matching and using the raw materials such as natural citral, 6 parts of paraguazone, 0.6 part of buchu oil, 0.6 part of bitter almond oil, fruit fragrance such as ethyl maltol and the like, herb fragrance and the like, and the use of the raw materials can improve the overall quality of the essence to different degrees. The essence has high quality, no impurity is separated out during suction, and the feasibility is reliably guaranteed through production verification.
2. Presents the fragrance of the compound honey and the grapefruit and is suitable for the field of electronic cigarette manufacture. The honey pomelo composite fragrance type fruit and fruit vinegar contains various fragrance components including fruity, sour, burnt, sweet, baking, herbal and other fragrance notes, is rich in fragrance note and natural in transition, can better highlight the main fragrance note of the honey pomelo composite fragrance type, is harmonious and natural in fragrance note, soft and fine in smoke and comfortable in taste, improves sensory experience, and meets the individual requirements of consumers.
3. The preparation method is simple and convenient, has low cost, can be used for large-scale industrial production, and has strong practicability.
Detailed Description
The following are specific embodiments of the present invention and further describe the technical solutions of the present invention, but the present invention is not limited to these examples.
Example 1
Weighing the following raw materials in parts by weight: 0.6 part of phenethyl acetate, 0.2 part of phenylacetic acid, 0.3 part of p-cresol acetate, 0.6 part of methyl phenylacetate, 0.2 part of menthyl acetate, 1.8 parts of isobutyl phenylacetate, 0.3 part of ethyl phenylacetate, 0.9 part of damascenone, 0.3 part of natural citral, 0.6 part of beeswax absolute, 0.4 part of amyl phenylacetate, 0.3 part of vanillin, 12 parts of benzyl alcohol, 1.2 parts of ethyl laurate, 0.6 part of oxidized isophorone, 3 parts of naringenone, 0.3 part of buchu oil, 0.3 part of bitter almond oil, 1.7 parts of ethyl maltol and 760 parts of propylene glycol, and then the components are diluted to 1000 parts by glycerol and uniformly stirred to prepare the honey and pomelo compound fragrance electronic cigarette oil 1 for standby.
According to the procedure of adding electronic cigarette oil in the production of electronic cigarettes, the honey pomelo compound fragrance type electronic cigarette oil 1 is added to prepare an electronic cigarette product A.
Example 2
Weighing the following raw materials in parts by weight: 2.9 parts of phenethyl phenylacetate, 0.45 part of phenylacetic acid, 0.9 part of p-cresol acetate, 2.8 parts of methyl phenylacetate, 0.4 part of menthyl acetate, 4.7 parts of isobutyl phenylacetate, 0.7 part of ethyl phenylacetate, 3.3 parts of damascenone, 0.7 part of natural citral, 2.8 parts of beeswax absolute, 0.9 part of amyl phenylacetate, 0.8 part of vanillin, 18 parts of benzyl alcohol, 4.5 parts of ethyl laurate, 2.8 parts of oxidized isophorone, 7.4 parts of pomelo garden ketone, 0.9 part of buchu oil, 0.75 part of bitter almond oil, 5.3 parts of ethyl maltol and 835 parts of propylene glycol, then diluting to 1000 parts by using glycerol, and stirring uniformly to prepare the shaddock compound flavor electronic cigarette oil 2 for later use.
According to the procedure of adding electronic cigarette oil in the production of electronic cigarettes, the honey pomelo compound fragrance type electronic cigarette oil 2 is added to prepare an electronic cigarette product B.
Example 3
Weighing the following raw materials in parts by weight: 1.8 parts of phenethyl phenylacetate, 0.8 part of phenylacetic acid, 0.65 part of p-cresol acetate, 1.6 parts of methyl phenylacetate, 0.35 part of menthyl acetate, 3 parts of isobutyl phenylacetate, 0.45 part of ethyl phenylacetate, 2 parts of damascenone, 0.65 part of natural citral, 2 parts of beeswax absolute, 0.6 part of amyl phenylacetate, 0.6 part of vanillin, 15 parts of benzyl alcohol, 3 parts of ethyl laurate, 1.7 parts of oxidized isophorone, 5 parts of parapummelone, 0.65 part of buchu oil, 0.5 part of bitter almond oil, 3.6 parts of ethyl maltol and 800 parts of propylene glycol, then diluting the mixture to 1000 parts by using glycerol, and stirring the mixture uniformly to prepare the honey and grapefruit composite flavor type electronic cigarette oil 3 for later use.
And (3) adding the honey pomelo compound-flavor electronic cigarette oil 3 according to the procedure of adding electronic cigarette oil in the electronic cigarette production to prepare an electronic cigarette product C.
In the case of the example 4, the following examples are given,
weighing the following raw materials in parts by weight: 2 parts of phenethyl acetate, 0.8 part of phenylacetic acid, 0.6 part of p-cresol acetate, 2 parts of methyl phenylacetate, 0.3 part of menthyl acetate, 3 parts of isobutyl phenylacetate, 0.6 part of ethyl phenylacetate, 2.2 parts of damascone, 0.5 part of natural citral, 1.2 parts of beeswax absolute, 0.6 part of amyl phenylacetate, 0.7 part of vanillin, 15 parts of benzyl alcohol, 3.2 parts of ethyl laurate, 1.8 parts of oxidized isophorone, 6 parts of nootkatone, 0.6 part of buchu oil, 0.6 part of bitter almond oil, 3 parts of ethyl maltol and 785 parts of propylene glycol, then diluting the mixture to 1000 parts by using 170.3 parts of glycerol, and stirring the mixture uniformly to prepare the honey and grapefruit composite flavor electronic cigarette oil 4 for later use.
And (3) adding the honey pomelo compound fragrance type electronic cigarette oil 4 according to the procedure of adding electronic cigarette oil in the electronic cigarette production to prepare an electronic cigarette product D.
Comparative example 1
760 parts of propylene glycol is weighed, diluted to 1000 parts by using glycerol and uniformly stirred by adopting the same method as in example 1 to prepare blank electronic cigarette oil, and then the blank electronic cigarette oil is prepared into a blank electronic cigarette control.
The evaluation is carried out according to the national bureau smoking evaluation standard, a smoking evaluation group consists of 7 cigarette sensory evaluation experts, sensory evaluation is carried out and scoring is carried out in a dark evaluation mode according to the cigarette sensory quality evaluation standard in the national standard GB 5606.5-2005, and the sensory evaluation scoring table is shown in the following table 1:
as can be seen from table 1, the electronic cigarette tobacco product prepared by adding the honey pomelo compound-flavor electronic cigarette oil into the electronic cigarette has fresh and natural honey and pomelo fragrance in the smoking process, has lasting fragrance, unique fragrance style, full fragrance, slightly improved texture, soft and fine smoke, reduced miscellaneous gas, reduced irritation, comfortable oral cavity, no influence on fragrance harmony, and improved sensory experience of consumers.
The specific embodiments described herein are merely illustrative of the spirit of the invention. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the invention as defined in the appended claims.
Claims (4)
1. The honey and grapefruit compound aroma type electronic cigarette oil is characterized in that: according to the mass portion, the composition comprises 0.5-3 portions of phenethyl acetate, 0.1-0.5 portion of phenylacetic acid, 0.2-1.0 portion of p-cresol acetate, 0.5-3 portions of methyl phenylacetate, 0.1-0.5 portion of menthyl acetate, 1.5-5.0 portions of isobutyl phenylacetate, 0.2-0.8 portion of ethyl phenylacetate, 0.5-3.5 portions of damascenone, 0.2-0.8 portion of natural citral, 0.5-3 portions of beeswax absolute, 0.3-1 portion of amyl phenylacetate, 0.2-1.0 portion of vanillin, 10-20 portions of benzyl alcohol, 1-5 portions of ethyl laurate, 0.5-3 portions of oxidized isophorone, 2-8 portions of paranarione, 0.2-1.0 portion of buchu oil, 0.2-0.8 portion of bitter almond oil, 1.5-5.5 portions of ethyl maltol and 850 portions of propylene glycol.
2. The honey pomelo compound odor type electronic cigarette oil according to claim 1, characterized in that: according to the mass portion, the composition comprises 2 portions of phenethyl acetate, 0.8 portion of phenylacetic acid, 0.6 portion of p-cresol acetate, 2 portions of methyl phenylacetate, 0.3 portion of menthyl acetate, 3 portions of isobutyl phenylacetate, 0.6 portion of ethyl phenylacetate, 2.2 portions of damascenone, 0.5 portion of natural citral, 1.2 portions of beeswax absolute, 0.6 portion of amyl phenylacetate, 0.7 portion of vanillin, 15 portions of benzyl alcohol, 3.2 portions of ethyl laurate, 1.8 portions of oxidized isophorone, 6 portions of parapomelo ketone, 0.6 portion of buchu oil, 0.6 portion of bitter almond oil, 3 portions of ethyl maltol and 785 portions of propylene glycol.
3. A method for preparing honey pomelo compound scent type electronic cigarette oil according to any one of claims 1 to 2, which is characterized in that: the method comprises the following steps: the components are evenly mixed according to the mass portion and then diluted to 900-1100 portions.
4. The preparation method of the honey pomelo compound-flavor electronic cigarette oil according to claim 3, characterized by comprising the following steps: diluted with glycerol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910909298.0A CN110655986A (en) | 2019-09-25 | 2019-09-25 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910909298.0A CN110655986A (en) | 2019-09-25 | 2019-09-25 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
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| CN110655986A true CN110655986A (en) | 2020-01-07 |
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| CN201910909298.0A Pending CN110655986A (en) | 2019-09-25 | 2019-09-25 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104073347A (en) * | 2013-03-27 | 2014-10-01 | 丽华（广州）香精有限公司 | Sweet orange daily chemical essence |
| CN104431939A (en) * | 2014-12-16 | 2015-03-25 | 广东顺大食品调料有限公司 | Honey essence and preparation method thereof |
| CN104531356A (en) * | 2015-01-19 | 2015-04-22 | 川渝中烟工业有限责任公司 | Honeyed-sweet additive and electronic cigarette liquid with same |
| CN104544540A (en) * | 2014-12-24 | 2015-04-29 | 广西中烟工业有限责任公司 | Preparation method for vacuum freeze drying fruit grain electronic cigarette liquid |
| CN104830529A (en) * | 2015-04-27 | 2015-08-12 | 湖北中烟工业有限责任公司 | Honey-sweet type cigarette paper essence and preparation method thereof |
| CN110106024A (en) * | 2019-06-13 | 2019-08-09 | 广州宝士迪香精香料有限公司 | Daily use chemicals honey essence |
-
2019
- 2019-09-25 CN CN201910909298.0A patent/CN110655986A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104073347A (en) * | 2013-03-27 | 2014-10-01 | 丽华（广州）香精有限公司 | Sweet orange daily chemical essence |
| CN104431939A (en) * | 2014-12-16 | 2015-03-25 | 广东顺大食品调料有限公司 | Honey essence and preparation method thereof |
| CN104544540A (en) * | 2014-12-24 | 2015-04-29 | 广西中烟工业有限责任公司 | Preparation method for vacuum freeze drying fruit grain electronic cigarette liquid |
| CN104531356A (en) * | 2015-01-19 | 2015-04-22 | 川渝中烟工业有限责任公司 | Honeyed-sweet additive and electronic cigarette liquid with same |
| CN104830529A (en) * | 2015-04-27 | 2015-08-12 | 湖北中烟工业有限责任公司 | Honey-sweet type cigarette paper essence and preparation method thereof |
| CN110106024A (en) * | 2019-06-13 | 2019-08-09 | 广州宝士迪香精香料有限公司 | Daily use chemicals honey essence |
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