CN101633864B - Apple-flavored essence for tobacco, preparation method and application thereof - Google Patents
Apple-flavored essence for tobacco, preparation method and application thereof Download PDFInfo
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- CN101633864B CN101633864B CN 200910040925 CN200910040925A CN101633864B CN 101633864 B CN101633864 B CN 101633864B CN 200910040925 CN200910040925 CN 200910040925 CN 200910040925 A CN200910040925 A CN 200910040925A CN 101633864 B CN101633864 B CN 101633864B
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Abstract
The invention discloses an apple-flavored essence for tobacco, a preparing method and an application thereof. The apple-flavored essence for tobacco is prepared, by weight percent, from the following materials: 5-30% of apple juice, 4-20% of amino acid, 0.5-5% of malic acid, 0.5-5% of acetaldehyde and the balance of glycerine in which water accounts for 10-40%. The preparing method of the apple-flavored essence for tobacco comprises the following steps: using the glycerine in which water accounts for 10-40% as a reaction medium and adding the amino acid, malic acid and acetaldehyde into the apple juice to form mixed liquid by blending; and carrying out Maillard reaction on obtained mixed liquid to obtain the apple-flavored essence for tobacco. The application is to add the apple-flavored essence for tobacco into a leave formulation according to a proportion of 0.1-5 per mill of the weight of leaves so as to be used for tobacco production. The invention further confirms the adding proportion of the essence for tobacco, reduces thorn, removes impurities, and improves the comfort of the mouth and nose to smoke; in addition, the invention enriches aroma and offers apple-flavored note, thus improving the quality and volume of aroma of the cigarettes.
Description
Technical field
The invention belongs to the tobacco production technical field, be specifically related to a kind of apple-flavored essence for tobacco and its preparation method and application.
Background technology
The kind of tobacco aromatics using comprises natural perfume, synthetic perfume, mono-isolate and browning reaction spices four large classes at present; And being specialized in the seasoning of tobacco product perfuming, the flavouring essence for tobacco that tobacco aromatics using forms through allotment uses, therefore it is different that it requires with bread and cheese essence, after adding in the cigarette, to coordinate with Gas phase Smoke, improve cigarette odor-absorbing, flavouring and do not increase assorted gas and peculiar smell, so the essence of the usefulness such as numerous food product, beverage, makeup can not be directly used in the production of cigarettes.
Along with the raising of modern life level, the taste of cigarette constantly gets a promotion, and taste is also constantly improved, and the smoking personage is to the requirement of cigarette fragrance also more and more levels.Healthy, the fine natural fruit charm essence that improves the cigarette mouthfeel of energy have no report.
Apple is rich in the materials such as robust fibre, carbohydrate, polyphenol, flavonoid, and its characteristic perfume can be alleviated the human body stress, and also having refreshes oneself puies forward the effect of brain.Apple perfume (or spice) wherein contains the organic compositions such as alcohol, ester, and its unique local flavor can't synthetic.Chinese patent ZL03112555.7 discloses a kind of " preparation method of high natural apple essence ", overcome and easily produce peculiar smell and the low problem of cycles of concentration in the preparation process of apple flavour, but this apple flavour is because high volatility, poor stability, production efficiency is low and the high in cost of production reason is not easy to directly be used in the production of cigarettes.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of come from natural fruit, stable in properties, cost a kind of apple-flavored essence for tobacco low, that have unique note.
Another object of the present invention provides the preparation method of above-mentioned flavouring essence for tobacco.
A further object of the invention provides the application of described flavouring essence for tobacco.
The present invention is achieved through the following technical solutions the foregoing invention purpose:
A kind of apple-flavored essence for tobacco, made by the material of following weight percent:
Sucus Mali pumilae 5～30%; Amino acid 4～20%; Oxysuccinic acid 0.5～5%; Acetaldehyde 0.5～5%; The glycerol that contains weight percent 10～40% moisture is surplus.
For realizing better purpose of the present invention, the present invention preferably adopts the Sucus Mali pumilae of following methods preparation to prepare described flavouring essence for tobacco; The preparation method of described Sucus Mali pumilae may further comprise the steps:
With apple broken the apple slurries of pulling an oar; The composite plant lytic enzyme Viscozyme L and 0.1 ‰～6 ‰ polygalacturonases hydrolysis apple slurries that add its weight 0.1 ‰～6 ‰ in described apple slurries get enzymolysis solution; The described enzymolysis solution of squeeze and filter gets Sucus Mali pumilae filtrate; Described Sucus Mali pumilae filtrate evaporation concentration is got Sucus Mali pumilae.
The condition of described hydrolysis is: stirring at normal temperature, speed 5～40r/min, hydrolysis time 1～6 hour.
The Brix of described Sucus Mali pumilae is preferably 10～40.
Described amino acid is selected from any one or the two or more mixture that mixes by any part by weight in L-glutamic acid, glycine, proline(Pro), α-amino-isovaleric acid or the alanyl-glycine.
The preparation method of above-mentioned apple-flavored essence for tobacco may further comprise the steps:
(1) take the glycerol that contains weight percent 10～40% moisture as reaction medium, amino acid, oxysuccinic acid and acetaldehyde are added Sucus Mali pumilae allocate and obtain mixed solution;
(2) mixed solution that obtains is carried out Maillard reaction and make apple-flavored essence for tobacco.
The pH value of mixed solution is preferably 4.0～7.0 described in the above-mentioned steps (1); Described pH value phosphoric acid or potassium hydroxide are regulated.
The condition of Maillard reaction is described in the above-mentioned steps (2): under the sealed environment, temperature is 90～125 ℃, mixing speed 10～30r/min, the reaction times is 1.5～4 hours.
The present invention provides the application of described apple-flavored essence for tobacco simultaneously, is described flavouring essence for tobacco to be joined tobacco leaf formulation with 0.1 ‰～5 ‰ ratio of leaf group weight be applied to during tobacco produces.
The invention has the beneficial effects as follows, from natural fruit, prepared a kind of flavor essence that is successfully applied in the tobacco production, get the natural note of apple, make flue gas become more mellow and fuller, fine and smooth after joining in the tobacco tobacco leaf formulation, the flue gas form there is certain modification, the present invention has further determined the additional proportion of described essence, falls the thorn removal of impurities, improves the comfort level that flue gas gives the oral cavity nasal cavity; Make simultaneously fragrance become abundanter, give the apple shape note, cigarette flavor matter, perfume quantity are all had castering action.
Embodiment
Further describe the present invention below in conjunction with specific embodiment.
Embodiment 1
Preparation Sucus Mali pumilae: with the broken apple slurries 1000g (almost not having loss) that gets of commercially available apple 1Kg making beating; Adding composite plant lytic enzyme Viscozyme L 1g and polygalacturonase 6g hydrolysis apple slurries get enzymolysis solution in described apple slurries; The described enzymolysis solution of squeeze and filter gets Sucus Mali pumilae filtrate; Described Sucus Mali pumilae filtrate is evaporated to get Sucus Mali pumilae.Because the Sucus Mali pumilae sugar content need to improve in order to improve the apple-flavored of essence, the present embodiment adopts double-effect evaporator that the Sucus Mali pumilae that makes is carried out evaporation concentration and processes, and obtains Brix and be 10 Sucus Mali pumilae concentrated solution.
Embodiment 2
Preparation Sucus Mali pumilae: with the broken apple slurries 1000g (almost not having loss) that gets of commercially available apple 1Kg making beating; Adding composite plant lytic enzyme Viscozyme L 6g and polygalacturonase 1g hydrolysis apple slurries get enzymolysis solution in described apple slurries; The described enzymolysis solution of squeeze and filter gets Sucus Mali pumilae filtrate; Described Sucus Mali pumilae filtrate is evaporated to get Sucus Mali pumilae.Because the Sucus Mali pumilae sugar content need to improve in order to improve the apple-flavored of essence, the present embodiment adopts double-effect evaporator that the Sucus Mali pumilae that makes is carried out evaporation concentration and processes, and obtains Brix and be 40 Sucus Mali pumilae concentrated solution.
Embodiment 3
Prepare apple-flavored type essence 100g, the weight percent of each component is among the 100g: Sucus Mali pumilae 5%; Amino acid 20%; Oxysuccinic acid 0.5%; Acetaldehyde 5%; The glycerol that contains weight percent 10% moisture is surplus; Amino acid is L-glutamic acid in the present embodiment: the glycine weight ratio is to be mixed at 1: 1.
Preparation process is:
(1) take the glycerol that contains 10% moisture as reaction medium, add Sucus Mali pumilae, amino acid, oxysuccinic acid and acetaldehyde, mix; Adjust system pH 4.0 with potassium hydroxide, phosphoric acid, sealing;
(2) Mei Lade (Maillard) reaction: under the sealed environment, stirring reaction; Temperature is 90 ℃, mixing speed 10r/min, and the reaction times is 4 hours.React complete after, rapidly cooling process is carried out in cooling.Deng being cooled to normal temperature, namely get the product apple-flavored essence for tobacco.
Embodiment 4
Prepare apple-flavored type essence 100g, the weight percent of each component is among the 100g: Sucus Mali pumilae 30%; Amino acid 4%; Oxysuccinic acid 5%; Acetaldehyde 0.5%; The glycerol that contains weight percent 40% moisture is surplus; Amino acid is proline(Pro) in the present embodiment: α-amino-isovaleric acid: the alanyl-glycine weight ratio is to be mixed at 1: 1: 1.
Preparation process is:
(1) take the glycerol that contains 40% moisture as reaction medium, add Sucus Mali pumilae, amino acid, oxysuccinic acid and acetaldehyde, mix; Adjust system pH 7.0 with potassium hydroxide, phosphoric acid, sealing;
(2) Mei Lade (Maillard) reaction: under the sealed environment, stirring reaction; Temperature is 125 ℃, mixing speed 30r/min, and the reaction times is 1.5 hours.React complete after, rapidly cooling process is carried out in cooling.Deng being cooled to normal temperature, namely get the product apple-flavored essence for tobacco.
The application experiment of embodiment 5 flavouring essence for tobaccos of the present invention
Be divided into two groups behind the normal flavoring and casing of Ye Zujing of certain trade mark specification cigarette A, one group is not added in contrast sample of the apple-flavored type essence of the present invention, the apple-flavored type essence that another group makes embodiment 3 adds wherein according to 0.1 ‰ adding proportion of leaf group weight, mix, after the cigarette wrapping machine rolls into cigarette, place a week, then carry out the sensory evaluating smoking.The result shows, compare with the cigarette control sample of not adding apple-flavored type essence, the flue gas that adds apple-flavored essence for tobacco becomes soft continuous fine and smooth, sweet sense increases to some extent, and oral cavity nasal cavity comfort level makes moderate progress, and fragrance matter and perfume quantity all promote to some extent, feel that more horn of plenty is full, have simultaneously good Harmony, and the assorted gas in the flue gas, pungency descend to some extent all, the cigarette quality totally promotes to some extent.
The application experiment of embodiment 6 flavouring essence for tobaccos of the present invention
Be divided into two groups behind the normal flavoring and casing of Ye Zujing of certain trade mark specification cigarette B, one group is not added in contrast sample of the apple-flavored type essence of the present invention, the apple-flavored type essence that another group makes embodiment 4 adds wherein according to 0.5 ‰ adding proportion of leaf group weight, mix, after the cigarette wrapping machine rolls into cigarette, place a week, then carry out the sensory evaluating smoking.The result shows, compare with the cigarette control sample of not adding apple-flavored type essence, the flue gas that adds apple-flavored essence for tobacco is softer continuous fine and smooth, sweet sense obviously increases, and oral cavity nasal cavity comfort level has larger improvement, and fragrance matter and perfume quantity all promote to some extent, feel that more horn of plenty is full, have simultaneously good Harmony, and the assorted gas in the flue gas, pungency descend obviously all, the cigarette quality totally has a distinct increment.
Claims (4)
1. an apple-flavored essence for tobacco is characterized in that being made by the material of following weight percent: Sucus Mali pumilae 5～30%; Amino acid 4～20%; Oxysuccinic acid 0.5～5%; Acetaldehyde 0.5～5%; The glycerol that contains weight percent 10～40% moisture is surplus; Described Sucus Mali pumilae is the Sucus Mali pumilae that makes by following preparation method, and described preparation method is with apple broken the apple slurries of pulling an oar; In described apple slurries, add the composite plant lytic enzyme Viscozyme L of its weight 0.1 ‰～6 ‰ and 0.1 ‰～6 ‰ polygalacturonase hydrolysis apple slurries and get enzymolysis solution; The described enzymolysis solution of squeeze and filter gets Sucus Mali pumilae filtrate; Described Sucus Mali pumilae filtrate evaporation concentration is got Sucus Mali pumilae; The condition of described hydrolysis is: stirring at normal temperature, speed 5～40r/min, hydrolysis time 1～6 hour; The Brix of described Sucus Mali pumilae is 10～40; Described amino acid is selected from any one or the two or more mixture that mixes by any part by weight in L-glutamic acid, glycine, proline(Pro), α-amino-isovaleric acid or the alanyl-glycine;
Described flavouring essence for tobacco is got by the preparation method's preparation that may further comprise the steps:
(1) take the glycerol that contains weight percent 10～40% moisture as reaction medium, amino acid, oxysuccinic acid and acetaldehyde are added Sucus Mali pumilae allocate and obtain mixed solution;
(2) mixed solution that obtains is carried out Maillard reaction and make apple-flavored essence for tobacco.
2. apple-flavored essence for tobacco as claimed in claim 1, the pH value that it is characterized in that mixed solution described in the step (1) is 4.0～7.0.
3. apple-flavored essence for tobacco as claimed in claim 1 is characterized in that the condition of Maillard reaction described in the step (2) is: under the sealed environment, temperature is 90～125 ℃, mixing speed 10～30r/min, the reaction times is 1.5～4 hours.
4. the application of apple-flavored essence for tobacco claimed in claim 1 is characterized in that flavouring essence for tobacco is joined tobacco leaf formulation with 0.1 ‰～5 ‰ ratio of leaf group weight to be applied to tobacco and to produce.
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| CN 200910040925 CN101633864B (en) | 2009-07-07 | 2009-07-07 | Apple-flavored essence for tobacco, preparation method and application thereof |
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| CN 200910040925 CN101633864B (en) | 2009-07-07 | 2009-07-07 | Apple-flavored essence for tobacco, preparation method and application thereof |
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| CN101633864B true CN101633864B (en) | 2013-01-30 |
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| CN102125290A (en) * | 2011-01-12 | 2011-07-20 | 宁夏夏盛实业集团有限公司 | Novel technology for clarifying apple juice |
| US20140044857A1 (en) * | 2011-03-02 | 2014-02-13 | Feellife Bioscience International Co., Ltd. | Method for Preparing Water-Soluble Tobacco Flavor in Gel State |
| CN102499360B (en) * | 2011-11-17 | 2013-12-11 | 湖北中烟工业有限责任公司 | Natural apple essence and preparation method thereof |
| CN103215131B (en) * | 2013-04-03 | 2014-07-02 | 红云红河烟草(集团)有限责任公司 | Tomato composite enzymatic hydrolysis extract preparation method and application thereof |
| CN103409238B (en) * | 2013-09-03 | 2014-12-10 | 红塔烟草(集团)有限责任公司 | Cut stem fumet for tobacco as well as preparation method and application thereof |
| CN104474997B (en) * | 2014-11-24 | 2017-02-01 | 湖北中烟工业有限责任公司 | Maillard reaction cooling device and rapid cooling method thereof |
| CN104862076A (en) * | 2015-06-04 | 2015-08-26 | 湖北中烟工业有限责任公司 | Preparing method of Maillard reactant of mixed juice for tobaccos |
| CN104893826A (en) * | 2015-06-18 | 2015-09-09 | 湖北中烟工业有限责任公司 | Preparation method of grape juice Maillard cigarette flavor |
| CN104928028A (en) * | 2015-06-18 | 2015-09-23 | 湖北中烟工业有限责任公司 | Method for preparing apple juice Maillard tobacco flavor |
| CN105167169B (en) * | 2015-08-06 | 2016-08-17 | 云南中烟工业有限责任公司 | A kind of Compound Water Fruity type electronic cigarette tobacco tar |
| CN105581371A (en) * | 2016-03-09 | 2016-05-18 | 嘉兴景程生物科技有限公司 | Cigarette spice prepared from tropical fruit extract and preparing method of spice |
| CN106235386B (en) * | 2016-09-23 | 2018-01-19 | 陕西科技大学 | A kind of method that functional form reconstituted tobacco is prepared with pomace |
| CN106520368B (en) * | 2016-11-18 | 2019-11-08 | 湖北中烟工业有限责任公司 | A kind of application of formula for preparing Amadori reaction flavor and preparation method thereof and the fragrance |
| CN108013499A (en) * | 2017-12-29 | 2018-05-11 | 深圳睿思奇科技开发有限公司 | One grow tobacco taste tobacco tar preparation method and with this method prepare tobacco tar |
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