CN104263517A - Tobacco flavor prepared from black tomato, lavender and tobacco and application of tobacco flavor - Google Patents
Tobacco flavor prepared from black tomato, lavender and tobacco and application of tobacco flavor Download PDFInfo
- Publication number
- CN104263517A CN104263517A CN201410515952.7A CN201410515952A CN104263517A CN 104263517 A CN104263517 A CN 104263517A CN 201410515952 A CN201410515952 A CN 201410515952A CN 104263517 A CN104263517 A CN 104263517A
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- China
- Prior art keywords
- tobacco
- reaction
- prepared
- tobacco flavor
- black tomato
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
- A24B15/306—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation one reactant being an amino acid or a protein, e.g. Maillard's reaction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
Abstract
The invention discloses a tobacco flavor prepared from black tomato, lavender and tobacco and application of the tobacco flavor. The tobacco flavor is prepared by the following steps: mixing black tomato, lavender and tobacco which serve as raw materials and preparing extracts; adding compound amino acid, xylose, propylene glycol and water to form a reaction system; regulating pH value, and carrying out Maillard reaction in a reaction kettle to obtain the tobacco flavor. The tobacco flavor disclosed by the invention has a more obvious and comprehensive effect of improving smoking quality in comparison with a traditional extract and specifically can obviously promote secretion of saliva and increase sweet feeling, has rich and coordinated aroma, improves a sense of being solid and thick, reduces irritation and residue, and remarkably improves overall smoking quality.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, be specifically related to one with black tomato, lavandula angustifolia and tobacco for main raw material, the tobacco aromatics using prepared after Maillard reaction.Meanwhile, the invention still further relates to the embody rule of this tobacco aromatics using in cigarette.
Background technology
Tobacco aromatics using is requisite material in production of cigarettes, is improving the mouthfeel of cigarette, and outstanding cigarette product style and features aspect has important effect.Along with people more and more pay attention to smoking and healthy problem, exploitation low tar Less harmful cigarette has become the long-term task of tobacco industry one.The insufficient fragrance on cigarette tobacco leaf formulation can be made up by the mode of flavoring and casing, assorted gas of forgoing, make the cigarette perfume (or spice) of cigarette product more abundant, sufficient, thus at suction taste, smell on perfume (or spice) there is individual style, strengthen the characteristic of cigarette product.The method of essence spice for cigarette is prepared in traditional single extraction, usually there is inaccurate coordination, acts on the defects such as single, prepares by Maillard reaction the study hotspot that novel tobacco aromatics using has been association area, the report of existing more pertinent literature and patent.
Maillard reaction is also known as " non enzymatic browning reacton ", and being that french chemist L.C.Maillard proposed in 1912, is the reaction between carbonyl compound and aminocompound, also known as carbonyl ammonia react.The fields such as food, medicine and tobacco are widely used in, in multiple links such as the modulation of Chinese medicinal materials prescription and tobacco modulation at present.Maillard reaction in various degree can produce multiple fragrance composition.In recent years, along with the development of tobacco aromatics using industry, application Maillard reaction prepares tobacco aromatics using has become a field received much attention, but relevant report is raw material mainly with single non-tobacco class plant, or is only that raw material prepares tobacco aromatics using through Maillard reaction with tobacco.With fruit, spice berry and tobacco extract for raw material, prepare tobacco aromatics using by Maillard reaction, there is not been reported.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide one with black tomato, lavandula angustifolia and tobacco for main raw material, then the tobacco aromatics using prepared after Maillard reaction.Be applied to production of cigarettes to promote the suction quality of cigarette.
The present invention also aims to provide the embody rule of described tobacco aromatics using in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
Technical scheme of the present invention is mainly based on following understanding: by emerging fruits black tomato, spice berry lavandula angustifolia and tobacco three mixed extraction, reaction nitrogenous source is provided with aminoacids complex, carbohydrate kind is increased again with wood sugar, the Novel tobacco flavor obtained after Maillard reaction, tool is significantly increased sense of promoting the production of body fluid, sweet sense, fragrance is abundant, coordination, and solid sense increases, and stimulates, remains the effect reduced.Wherein, black tomato is the upstart in tomato family, has fruit aroma, and sugar degree is higher than Lycopersicon esculentum, with rich flavor, and it contains higher lycopene, anthocyanidin simultaneously, extremely easily absorbed by the body.Lavandula angustifolia is famous scented plants, there is distinctive refreshing aroma and banksia rose fragrance, main aroma component is L-phanteine, firpene, myrcene, ocimene, camphor, terpinol, L-phantol, lavandula angustifolia alcohol, Geraniol, ethanol lavandula angustifolia ester etc., is widely used in essence and flavoring agent, food, the aspect such as medicinal.
With a tobacco aromatics using prepared by black tomato, lavandula angustifolia and tobacco, prepared by following method:
(1) fresh black tomato, lavandula angustifolia inflorescence and tobacco are pressed the mass ratio mixing of 2:1:3, add the water of 5 times of volumes, circumfluence distillation 2 hours, extracting liquid filtering, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, then uses 95% ethanol back dissolving of 4 times of volumes, suction filtration, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, obtains mixed extract;
(2) get gained mixed extract, add the aminoacids complex of 5 ~ 10%, the wood sugar of 5 ~ 10%, the propylene glycol of 40 ~ 60% and 20 ~ 30% water, then regulate pH value to 6 ± 0.5 of mixture with NaOH; Described aminoacids complex is mixed by glycine, L-Ala and the aspartic acid mass ratio by 3:1:1;
(3) mixture regulating pH value is placed in reactor, temperature of reaction 100 ~ 120 DEG C, mixing speed 500 ~ 800 revs/min, 3 ~ 5 hours reaction times; Take out reaction solution, filter and remove insolubles, gained filtrate is required tobacco aromatics using.
The tobacco cut produced in the preferred production of cigarettes process of described tobacco or offal.
The application of described tobacco aromatics using in production of cigarettes, is specially: after gained tobacco aromatics using dilute with water 10 times, adds, then roll into cigarette in the usual way with feed way, mass ratio by 0.2% ~ 1%.
Compared with prior art, the present invention has the following advantages:
1, with black tomato, lavandula angustifolia for raw material, comparatively Lycopersicon esculentum is high because of materials such as carbohydrates contained by it for black tomato, is more suitable for carrying out Maillard reaction; Be aided with the spice berry lavandula angustifolia of the harmonizing of fragrance with it filtered out through repetition test, through technique for extracting mixed process, extract obtained have enrich cigarette perfume (or spice), reduce to stimulate, promote the effect of comfortableness;
2, on the basis of black tomato, lavandula angustifolia, being aided with tobacco extract is raw material, and prepared tobacco aromatics using fragrance is more coordinated, this perfume (or spice) of tobacco more alcohol and;
3, with the tobacco cut produced in tobacco leaf production process and offal for raw material, improve the comprehensive utilization ratio of discarded smoking material, reduce production cost.
4, in the present invention on the basis of the existing carbohydrate of extract, increase wood sugar as sugared source, increase furans aroma component in reaction product, add the rich of fragrance.
5, present invention process is simple, is convenient to realize suitability for industrialized production, has good development prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, the protection domain be not intended to limit the present invention.
Embodiment 1
1. the preparation of black tomato, lavandula angustifolia, tobacco mixed extract: black tomato is (fresh, cut fritter), lavandula angustifolia (fresh inflorescence, be cut into the section of long about 1cm), tobacco (tobacco cut produced in production of cigarettes process, offal) mixes in the ratio of 2:1:3, add the water of 5 times of volumes, circumfluence distillation 2 hours, extracting liquid filtering, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, use 95% ethanol back dissolving of 4 times of volumes again, suction filtration, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, namely obtains mixed extract.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid, blending ratio is 3:1:1) of 10%, the wood sugar of 10%, the propylene glycol of 60% and 30% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 120 DEG C, and mixing speed is 800 revs/min, reaction times: 5 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 0.2% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 2
1. the preparation of black tomato, lavandula angustifolia, tobacco mixed extract: with embodiment 1.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid, blending ratio is 3:1:1) of 8%, the wood sugar of 10%, the propylene glycol of 50% and 30% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 110 DEG C, and mixing speed is 700 revs/min, reaction times: 4 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 0.5% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 3
1. the preparation of black tomato, lavandula angustifolia, tobacco mixed extract: with embodiment 1.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid, blending ratio is 3:1:1) of 5%, the wood sugar of 5%, the propylene glycol of 40% and 20% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 100 DEG C, and mixing speed is 500 revs/min, reaction times: 3 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 1% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 4
1. the preparation of black tomato, lavandula angustifolia, tobacco mixed extract: with embodiment 1.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid, blending ratio is 3:1:1) of 10%, the wood sugar of 5%, the propylene glycol of 40% and 30% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 110 DEG C, and mixing speed is 600 revs/min, reaction times: 5 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 0.8% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1., with a tobacco aromatics using prepared by black tomato, lavandula angustifolia and tobacco, prepared by following method:
(1) fresh black tomato, lavandula angustifolia inflorescence and tobacco are pressed the mass ratio mixing of 2:1:3, add the water of 5 times of volumes, circumfluence distillation 2 hours, extracting liquid filtering, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, then uses 95% ethanol back dissolving of 4 times of volumes, suction filtration, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, obtains mixed extract;
(2) get gained mixed extract, add the aminoacids complex of 5 ~ 10%, the wood sugar of 5 ~ 10%, the propylene glycol of 40 ~ 60% and 20 ~ 30% water, then regulate pH value to 6 ± 0.5 of mixture with NaOH; Described aminoacids complex is mixed by glycine, L-Ala and the aspartic acid mass ratio by 3:1:1;
(3) mixture regulating pH value is placed in reactor, temperature of reaction 100 ~ 120 DEG C, mixing speed 500 ~ 800 revs/min, 3 ~ 5 hours reaction times; Take out reaction solution, filter and remove insolubles, gained filtrate is required tobacco aromatics using.
2. the application of tobacco aromatics using according to claim 1 in production of cigarettes, is specially: after gained tobacco aromatics using dilute with water 10 times, adds, then roll into cigarette in the usual way with feed way, mass ratio by 0.2% ~ 1%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410515952.7A CN104263517A (en) | 2014-09-30 | 2014-09-30 | Tobacco flavor prepared from black tomato, lavender and tobacco and application of tobacco flavor |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410515952.7A CN104263517A (en) | 2014-09-30 | 2014-09-30 | Tobacco flavor prepared from black tomato, lavender and tobacco and application of tobacco flavor |
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| CN104263517A true CN104263517A (en) | 2015-01-07 |
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| CN201410515952.7A Pending CN104263517A (en) | 2014-09-30 | 2014-09-30 | Tobacco flavor prepared from black tomato, lavender and tobacco and application of tobacco flavor |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104830534A (en) * | 2015-05-22 | 2015-08-12 | 云南中烟工业有限责任公司 | Preparation method of tomato extract and application of tomato extract in cigarette production |
| CN105542959A (en) * | 2015-12-17 | 2016-05-04 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette liquid flavor |
| CN105768203A (en) * | 2016-03-25 | 2016-07-20 | 广东省金叶科技开发有限公司 | Preparation method of tobacco particles improved by endogenous scent substances |
| CN109517663A (en) * | 2017-09-20 | 2019-03-26 | 湖南中烟工业有限责任公司 | A kind of grape flavor tobacco aromaticss and its preparation method and application |
-
2014
- 2014-09-30 CN CN201410515952.7A patent/CN104263517A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104830534A (en) * | 2015-05-22 | 2015-08-12 | 云南中烟工业有限责任公司 | Preparation method of tomato extract and application of tomato extract in cigarette production |
| CN104830534B (en) * | 2015-05-22 | 2018-05-01 | 云南中烟工业有限责任公司 | A kind of preparation method of tomato extract and its application in production of cigarettes |
| CN105542959A (en) * | 2015-12-17 | 2016-05-04 | 立场电子科技发展（上海）有限公司 | Method for preparing electronic cigarette liquid flavor |
| CN105768203A (en) * | 2016-03-25 | 2016-07-20 | 广东省金叶科技开发有限公司 | Preparation method of tobacco particles improved by endogenous scent substances |
| CN109517663A (en) * | 2017-09-20 | 2019-03-26 | 湖南中烟工业有限责任公司 | A kind of grape flavor tobacco aromaticss and its preparation method and application |
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Application publication date: 20150107 |