CN104232309A - Tobacco flavor prepared from phyllanthus emblica, plum, broadleaf holly leaf and tobacco and application of tobacco flavor - Google Patents
Tobacco flavor prepared from phyllanthus emblica, plum, broadleaf holly leaf and tobacco and application of tobacco flavor Download PDFInfo
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Abstract
The invention discloses a tobacco flavor prepared from phyllanthus emblica, plum, broadleaf holly leaf and tobacco and application of the tobacco flavor. The preparation method of the tobacco flavor comprises the following steps: taking phyllanthus emblica, plum, broadleaf holly leaf and tobacco as raw materials, mixing the raw materials to prepare an extractive, adding compound amino acid, xylose, propylene glycol and water to form a reaction system, adjusting the pH value, and conducting Maillard reaction in a reaction kettle to prepare the tobacco flavor. The tobacco flavor is more obvious and comprehensive than the traditional extractive for improving the smoking quality of the cigarette, specifically for increasing the saliva secretion feeling and the sweet feeling; the tobacco flavor is rich and harmonious in fragrance; the whole smoking quality is obviously improved; meanwhile, the tobacco flavor can relieve the uncomfortable feeling in the throat.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, be specifically related to one with Yunnan olive, plum, Leaf of Chinese Holly and tobacco for main raw material, the tobacco aromatics using prepared after Maillard reaction.Meanwhile, the invention still further relates to the embody rule of this tobacco aromatics using in cigarette.
Background technology
Tobacco aromatics using is requisite material in production of cigarettes, is improving the mouthfeel of cigarette, and outstanding cigarette product style and features aspect has important effect.Along with people more and more pay attention to smoking and healthy problem, exploitation low tar Less harmful cigarette has become the long-term task of tobacco industry one.The insufficient fragrance on cigarette tobacco leaf formulation can be made up by the mode of flavoring and casing, assorted gas of forgoing, make the cigarette perfume (or spice) of cigarette product more abundant, sufficient, thus at suction taste, smell on perfume (or spice) there is individual style, strengthen the characteristic of cigarette product.Meanwhile, under the theory of development Chinese-style cigarette instructs, the application of Chinese medicinal materials in cigarette receives increasing concern.Chinese medicine is the carrier of China's traditional medicine, Chinese medicinal materials is introduced the common report of cigarette Application Areas, material containing Chinese medicinal materials composition is added in cigarette, stand differing temps heating in cigarette, effective constituent is through distillation, gasification and distillation, act on respiratory system, or enter blood through lung suction, reduce the discomfort caused because of smoking.At present, the main application mode of Chinese medicinal materials in cigarette comprises following a few class: 1) Chinese medicinal materials is made extract, add in cigarette in the mode of flavoring and casing; 2) Chinese medicinal materials is made pipe tobacco form, mix with pipe tobacco or directly substitute pipe tobacco and make health cigarette; 3) Chinese medicinal materials is laminated be applied to Cigarette processing again; 4) join in the auxiliary materials such as cigarette filter tip in the mode of particle or extract.But these application modes above all also exist the problems such as inharmonious with this perfume (or spice) of tobacco, effect aspect is comparatively single, this is also the problem of restriction Chinese medicinal materials broadened application in cigarette.
Maillard reaction is also known as " non enzymatic browning reacton ", and being that french chemist L.C.Maillard proposed in 1912, is the reaction between carbonyl compound and aminocompound, also known as carbonyl ammonia react.The fields such as food, medicine and tobacco are widely used in, in multiple links such as the modulation of Chinese medicinal materials prescription and tobacco modulation at present.Maillard reaction in various degree can produce multiple fragrance composition.In recent years, along with the development of tobacco aromatics using industry, application Maillard reaction prepares tobacco aromatics using has become a field received much attention, but relevant report is raw material mainly with single non-tobacco class plant, or is only that raw material prepares tobacco aromatics using through Maillard reaction with tobacco.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide one with Yunnan olive, plum, Leaf of Chinese Holly and tobacco for main raw material, then the tobacco aromatics using prepared after Maillard reaction.While lifting cigarette smoking quality, reduce throat's discomfort that smoking brings.
The present invention also aims to provide the embody rule of described tobacco aromatics using in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
Technical scheme of the present invention is mainly based on following understanding: by introducing tobacco extract and Maillard reaction, solves and applies merely the problem of Chinese medicinal materials extraction existing for tobacco aromatics using in the past.The Chinese medicinal materials used screens through repetition test, while coordinating with this perfume of tobacco, have health-care effect concurrently.Wherein, Yunnan olive and phyllanthus emblica, be the fruit of euphorbia plant phyllanthus emblica (Phyllanthus emblica L.), have relieving sore-throat by clearing away heat, promote the production of body fluid to quench thirst, the effect such as moistening the lung and resolving the phlegm; The fruit of plum and rose department plant plum (Armeniaca mume Sieb.), have promote the production of body fluid to quench thirst, effect of relieving restlessness; Leaf of Chinese Holly is the tealeaves that the branches and leaves of holly plant Cortex Ilicis Rotundae (Iiex latifolia Thunb.) are made, among the people as refrigerant solution hot drink.
With a tobacco aromatics using prepared by Yunnan olive, plum, Leaf of Chinese Holly and tobacco, prepared by following method:
(1) fresh Yunnan olive, fresh plum, Leaf of Chinese Holly and tobacco are pressed the mass ratio mixing of 4:4:1:3, add the water of 5 times of volumes, circumfluence distillation 2 hours, extracting liquid filtering, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, then uses 95% ethanol back dissolving of 4 times of volumes, suction filtration, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, obtains mixed extract;
(2) get gained mixed extract, add the aminoacids complex of 5 ~ 10%, the wood sugar of 5 ~ 10%, the propylene glycol of 40 ~ 60% and 20 ~ 30% water, then regulate pH value to 6 ± 0.5 of mixture with NaOH; Described aminoacids complex is mixed by glycine, L-Ala and the aspartic acid mass ratio by 3:1:1;
(3) mixture regulating pH value is placed in reactor, temperature of reaction 100 ~ 120 DEG C, mixing speed 500 ~ 800 revs/min, 3 ~ 5 hours reaction times; Take out reaction solution, filter and remove insolubles, gained filtrate is required tobacco aromatics using.
The tobacco cut produced in the preferred production of cigarettes process of described tobacco or offal.
The application of described tobacco aromatics using in production of cigarettes, is specially: after gained tobacco aromatics using dilute with water 10 times, with feed way, adds by 0.2% ~ 1% mass ratio, then rolls into cigarette in the usual way.
Compared with prior art, the present invention has the following advantages:
1, the fragrance of Yunnan olive, plum and Leaf of Chinese Holly and the fragrant Harmony of cigarette good, the fragrance can currently available products being avoided preferably to exist after being aided with tobacco material is inharmonious, act on the counter productives such as single, prepared tobacco aromatics using apply in cigarette after abundanter, the alcohol of cigarette flavor and;
2, selected Chinese medicinal materials has the effect such as the Hui Tian that promotes the production of body fluid, relieve sore throat heat-clearing, for symptoms such as throat's discomforts that smoker is common, has good mitigation;
3, the present invention with herbal mixture material and tobacco extract for raw material carries out Maillard reaction jointly, the application of its reactant in cigarette promotes more obvious to cigarette smoking quality, main manifestations is: sweet sense and sense of promoting the production of body fluid obviously increase, abundant, the coordination of fragrance, alleviate smoker throat malaise symptoms simultaneously;
4, with the tobacco cut produced in tobacco leaf production process and offal for raw material, improve the comprehensive utilization ratio of discarded smoking material, reduce production cost.
5, in the present invention on the basis of the existing carbohydrate of extract, increase wood sugar as sugared source, increase furans aroma component in reaction product, add the rich of fragrance.
6, present invention process is simple, is convenient to realize suitability for industrialized production, has good development prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, the protection domain be not intended to limit the present invention.
Embodiment 1
1. the preparation of Yunnan olive, plum, Leaf of Chinese Holly and tobacco mixed extract: Yunnan olive (fresh), plum (fresh), Leaf of Chinese Holly (dry product) and tobacco (tobacco cut produced in production of cigarettes process, offal) are mixed in 4:4:1:3 ratio, add the water of 5 times of volumes, circumfluence distillation 2 hours, extracting liquid filtering, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, use 95% ethanol back dissolving of 4 times of volumes again, suction filtration, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, namely obtains mixed extract.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid mixture, blending ratio is 3:1:1) of 10%, the wood sugar of 10%, the propylene glycol of 60% and 30% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 120 DEG C, and mixing speed is 800 revs/min, reaction times: 5 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 0.2% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 2
1. the preparation of Yunnan olive, plum, Leaf of Chinese Holly and tobacco mixed extract: with embodiment 1.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid mixture, blending ratio is 3:1:1) of 8%, the wood sugar of 10%, the propylene glycol of 50% and 30% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 110 DEG C, and mixing speed is 700 revs/min, reaction times: 4 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 0.5% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 3
1. the preparation of Yunnan olive, plum, Leaf of Chinese Holly and tobacco mixed extract: with embodiment 1.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid mixture, blending ratio is 3:1:1) of 5%, the wood sugar of 5%, the propylene glycol of 40% and 20% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 100 DEG C, and mixing speed is 500 revs/min, reaction times: 3 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 1% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
Embodiment 4
1. the preparation of Yunnan olive, plum, Leaf of Chinese Holly and tobacco mixed extract: with embodiment 1.
2. the structure of Maillard reaction system: get a certain amount of above-mentioned mixed extract, add the aminoacids complex (glycine, L-Ala, aspartic acid mixture, blending ratio is 3:1:1) of 10%, the wood sugar of 5%, the propylene glycol of 40% and 30% water; With NaOH adjust ph to 6 ± 0.5.
3. the carrying out of Maillard reaction: above-mentioned reaction system is joined in reactor, temperature of reaction is 110 DEG C, and mixing speed is 600 revs/min, reaction times: 5 hours, reaction takes out reaction solution after stopping, and filter and remove insolubles, gained filtrate is tobacco aromatics using of the present invention.
4. the interpolation in cigarette and evaluation: after gained tobacco aromatics using is diluted 10 times with water, in reinforced mode, ratio according to 0.8% makes an addition to cloud and mist (purple) Ye Zuzhong, obtain treatment samples, and with the leaf group sample in contrast do not added, roll into cigarette and carry out sensory evaluating smoking, smoking result is as shown in the table:
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1., with a tobacco aromatics using prepared by Yunnan olive, plum, Leaf of Chinese Holly and tobacco, prepared by following method:
(1) fresh Yunnan olive, fresh plum, Leaf of Chinese Holly and tobacco are pressed the mass ratio mixing of 4:4:1:3, add the water of 5 times of volumes, circumfluence distillation 2 hours, extracting liquid filtering, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, then uses 95% ethanol back dissolving of 4 times of volumes, suction filtration, it is 1.10 ± 0.10 that filtrate is concentrated into relative density, obtains mixed extract;
(2) get gained mixed extract, add the aminoacids complex of 5 ~ 10%, the wood sugar of 5 ~ 10%, the propylene glycol of 40 ~ 60% and 20 ~ 30% water, then regulate pH value to 6 ± 0.5 of mixture with NaOH; Described aminoacids complex is mixed by the mass ratio of 3:1:1 by glycine, L-Ala, aspartic acid;
(3) mixture regulating pH value is placed in reactor, temperature of reaction 100 ~ 120 DEG C, mixing speed 500 ~ 800 revs/min, 3 ~ 5 hours reaction times; Take out reaction solution, filter and remove insolubles, gained filtrate is required tobacco aromatics using.
2. the application of tobacco aromatics using according to claim 1 in production of cigarettes, is specially: after gained tobacco aromatics using dilute with water 10 times, adds, then roll into cigarette in the usual way with feed way, mass ratio by 0.2% ~ 1%.
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| CN105029697A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Fructus phyllanthi glycerol triacetate extracts and application of fructus phyllanthi glycerol triacetate extracts on cigarettes |
| CN105713845A (en) * | 2016-04-18 | 2016-06-29 | 云南中烟工业有限责任公司 | Method for fermentation preparation of fructus phyllanthi perfume for cigarettes with Trichoderma aureoviride |
| CN105768203A (en) * | 2016-03-25 | 2016-07-20 | 广东省金叶科技开发有限公司 | Preparation method of tobacco particles improved by endogenous scent substances |
| CN105852193A (en) * | 2016-06-27 | 2016-08-17 | 云南中烟工业有限责任公司 | Fructus phyllanthi flavored bagged oral cigarette and preparation method thereof |
| CN105852192A (en) * | 2016-06-27 | 2016-08-17 | 云南中烟工业有限责任公司 | Fructus phyllanthi flavored chewing tobacco and preparation method thereof |
| CN106418669A (en) * | 2016-11-11 | 2017-02-22 | 湖北中烟工业有限责任公司 | High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice |
| CN108991596A (en) * | 2018-10-11 | 2018-12-14 | 玉溪开元金蓝生物科技有限责任公司 | Compound Yunnan olive additive, preparation method and its application on cigarette filter rod |
| CN109758785A (en) * | 2019-03-28 | 2019-05-17 | 江西中烟工业有限责任公司 | A kind of preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor and the application in cigarette |
| CN111772227A (en) * | 2020-08-10 | 2020-10-16 | 四川中烟工业有限责任公司 | Phyllanthus emblica targeted refined substance, preparation method and application thereof in cigarettes |
| CN113604283A (en) * | 2021-08-27 | 2021-11-05 | 珠海市广龙香料发展有限公司 | Tobacco essence capable of reducing smoke irritation and preparation method thereof |
| CN114703021A (en) * | 2022-03-21 | 2022-07-05 | 云南巴菰生物科技股份有限公司 | Emblic leafflower fruit extract and its preparing method and use |
| CN115413811A (en) * | 2022-09-23 | 2022-12-02 | 南通烟滤嘴有限责任公司 | Preparation method and application of burnt sweet tea flavored heating cigarette |
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| CN105029697A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Fructus phyllanthi glycerol triacetate extracts and application of fructus phyllanthi glycerol triacetate extracts on cigarettes |
| CN105768203A (en) * | 2016-03-25 | 2016-07-20 | 广东省金叶科技开发有限公司 | Preparation method of tobacco particles improved by endogenous scent substances |
| CN105713845A (en) * | 2016-04-18 | 2016-06-29 | 云南中烟工业有限责任公司 | Method for fermentation preparation of fructus phyllanthi perfume for cigarettes with Trichoderma aureoviride |
| CN105713845B (en) * | 2016-04-18 | 2019-04-05 | 云南中烟工业有限责任公司 | A method of cigarette Yunnan olive fragrance is prepared using trichoderma aureoviride fermentation |
| CN105852192A (en) * | 2016-06-27 | 2016-08-17 | 云南中烟工业有限责任公司 | Fructus phyllanthi flavored chewing tobacco and preparation method thereof |
| CN105852193A (en) * | 2016-06-27 | 2016-08-17 | 云南中烟工业有限责任公司 | Fructus phyllanthi flavored bagged oral cigarette and preparation method thereof |
| CN106418669A (en) * | 2016-11-11 | 2017-02-22 | 湖北中烟工业有限责任公司 | High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice |
| CN106418669B (en) * | 2016-11-11 | 2018-06-01 | 湖北中烟工业有限责任公司 | A kind of high time sweet tea sense tobacco aromaticss and its preparation method and application |
| CN108991596A (en) * | 2018-10-11 | 2018-12-14 | 玉溪开元金蓝生物科技有限责任公司 | Compound Yunnan olive additive, preparation method and its application on cigarette filter rod |
| CN108991596B (en) * | 2018-10-11 | 2020-07-28 | 玉溪开元金蓝生物科技有限责任公司 | Compound fructus phyllanthi additive, preparation method and application thereof in cigarette filter tip rod |
| CN109758785A (en) * | 2019-03-28 | 2019-05-17 | 江西中烟工业有限责任公司 | A kind of preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor and the application in cigarette |
| CN111772227A (en) * | 2020-08-10 | 2020-10-16 | 四川中烟工业有限责任公司 | Phyllanthus emblica targeted refined substance, preparation method and application thereof in cigarettes |
| CN113604283A (en) * | 2021-08-27 | 2021-11-05 | 珠海市广龙香料发展有限公司 | Tobacco essence capable of reducing smoke irritation and preparation method thereof |
| CN113604283B (en) * | 2021-08-27 | 2023-11-21 | 珠海市广龙香料发展有限公司 | Tobacco essence capable of reducing smoke irritation and preparation method thereof |
| CN114703021A (en) * | 2022-03-21 | 2022-07-05 | 云南巴菰生物科技股份有限公司 | Emblic leafflower fruit extract and its preparing method and use |
| CN115413811A (en) * | 2022-09-23 | 2022-12-02 | 南通烟滤嘴有限责任公司 | Preparation method and application of burnt sweet tea flavored heating cigarette |
| CN115413811B (en) * | 2022-09-23 | 2023-11-14 | 南通烟滤嘴有限责任公司 | Preparation method and application of burnt sweet tea flavored heating cigarette |
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Application publication date: 20141224 |