CN109758785A - A kind of preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor and the application in cigarette - Google Patents
A kind of preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor and the application in cigarette Download PDFInfo
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Abstract
The invention discloses a kind of preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor and the applications in cigarette, the preparation method includes: that (1) takes pretreated cigar tobacco leaf and distilled water to be sequentially placed into PE bags high pressure resistant, ultra high pressure treatment is carried out after stirring, cigar ultra high pressure extraction liquid is filtered by vacuum to obtain in treatment fluid；(2) cigar ultra high pressure extraction liquid is taken to be added in Maillard reactor, fructose, glycine and reaction dissolvent is added, reaction solution pH, 85 DEG C ~ 120 DEG C reaction h of 2 h ~ 12 are adjusted, obtain cigar ultra high pressure extraction liquid Maillard reaction flavor after sealing natural cooling, this fragrance is used for perfuming cigarette link, play the role of significantly augmenting cigarette perfume and strength, cigarette product flavouring essence quality can be obviously improved, increases perfume quantity, miscellaneous gas is covered, irritation and dry sensation are reduced.
Description
Technical field
The present invention relates to a kind of preparation methods of essence spice for cigarette, and in particular to a kind of cigar ultra high pressure extraction liquid
The preparation method of Maillard reaction flavor and the application in cigarette.
Background technique
The full name of super-pressure is " superelevation isostatic cool pressing ", and basic principle is under normal temperature conditions, 100 is applied to material liquid~
The hydrostatic pressure of 1 000 MPa, rapid removal pressure, solvent may penetrate into solid under super-pressure effect after a certain period of time for pressure maintaining
It inside body raw material, is dissolved in the effective component in raw material in Extraction solvent, keeps the regular hour under a predetermined, make to have
Effect ingredient reaches rapid release after dissolution equilibrium, and in the cell under the action of exosmosis pressure, effective component can rapidly diffuse into group
It knits in the extracting solution of surrounding.Superhigh pressure technique has many unique advantages, super-pressure compared with other traditional extractive techniques
Extraction is carried out under conditions of one completely enclosed, compared with other methods, can significantly reduce the consumption of solvent.Superelevation
Pressure extract can be carried out under conditions of close to room temperature, will not because of the structure change of small-molecule substance caused by fuel factor, extracting solution
The more conventional extracting method of stability significantly improves, and the more conventional refluxing extraction of the dissolution of impurity component obviously drops in extracting solution
It is low, conducive to extracting solution preservation and subsequent isolate and purify.
The cigar tobacco of high-quality mainly originates in those torrid areas for having active volcano in the world, and such as Latin America adds
Strangle Sumatra and the Java etc. than sea and Indonesia.The plantation of China's cigar tobacco be concentrated mainly on the Yangtze river basin and its with
The area in south, such as ShenFang,SiChuan, Zhejiang Tongxiang, Hainan.China's cigar tobacco leaf mostly uses greatly solarization preparation method, and minority uses the system of drying in the air
Method, cigar tobacco are the important components for drying cigarette.The aesthetic quality of cigar tobacco shows as that strength is big, and flue gas concentration is big,
Fragrance is mellow plentiful, and mouth feel omits sweet tea.This is because cigar total reducing sugar, content of reducing sugar are very low compared with flue-cured tobacco, deficiency is roasting
/ 10th of tobacco and sugar content, the total nitrogen and nicotine content of cigar are relatively high.The study found that different sunning cigarettes, total
The content difference of sugared content, nicotine, total nitrogen and potassium etc. is larger, and in domestic and international 8 cigar kind sample of extraction, cigar is total
Nitrogen content is distributed in 4.85% ~ 6.99%, and nicotine is 1.10% ~ 2.29%.The cigar sample for three kinds that cigarette district is introduced a fine variety in Shifang
In, it is 3.16% ~ 4.10% that cigar total nitrogen content, which is distributed in, and nicotine is about 1.13% ~ 5.09%.
Maillard reaction be occur between amino-compound (such as amino acid) and carbonyls (such as reduced sugar) it is non-
The browning reaction of enzymatic, generation, condensation product degradation including flavor precursors object generate various small molecules and polymerization
Generate the reaction such as melanoid macromolecule product.Maillard reaction can generate a large amount of aroma component and tobacco characteristic chicken flavor
The important reaction formed.Maillard reaction product is highly-safe as natural perfume material, has been put into the identification of internal authority mechanism
Fragrance register in, it can cover the acerbity of tobacco, bitter taste, tart flavour, play the role of Titian drop thorn, can also improve color and
Glossiness.In smoking and health problem the today for causing most attention in global range, retain very while reducing tar and reducing harm
It is problem in the urgent need to address to cigarette flavor quality is improved.Maillard reaction product helps to delay for perfuming cigarette
Solve the contradiction between tar reduction and lasting.In Maillard reaction, the reactivity of reduced sugar normally behaves as pentose > six carbon
Sugar > disaccharide, aldose > ketose, fructose are that pentose is aldose again, are reduction sugar source with fructose, Maillard reaction rate is fast, instead
Answer degree height.
In current art, it is anti-that Maillard is not prepared using cigar ultra high pressure extraction liquid as amino acid source combination fructose
Answer the report of object.
Summary of the invention
The present invention extracts cigar tobacco leaf effective component using superhigh pressure technique and prepares Maillard fragrance, extraction time
Short, extraction efficiency is high, and reaction condition is of less demanding, easy to industrialized production, using cigar ultra high pressure extraction liquid as amino acid source,
Joint glycine prepares Maillard reacting substance perfume as built amino-acid, and with fructose, with other amino acid and its collocation
It compares, is used for perfuming cigarette link, plays the role of significantly augmenting cigarette perfume and strength, cigarette product fragrance product can be obviously improved
Matter increases perfume quantity, covers miscellaneous gas, reduces irritation and dry sensation.
In order to achieve the above-mentioned object of the invention, the present invention provides following technical schemes:
The present invention provides a kind of preparation methods of cigar ultra high pressure extraction liquid Maillard reaction flavor, including following step
It is rapid:
(1) it takes pretreated cigar tobacco leaf and distilled water to be sequentially placed into PE bags high pressure resistant, is carried out at super-pressure after stirring
Cigar ultra high pressure extraction liquid is filtered by vacuum to obtain in reason, treatment fluid；
(2) it takes cigar ultra high pressure extraction liquid to be added in Maillard reactor, fructose, glycine and reaction dissolvent is added, adjust
Reacting liquid pH value is saved to 8.5 ~ 10.5, starts timing when temperature is ramped up 85 DEG C ~ 120 DEG C under magnetic stirring when reaction solution,
The h of 2 h ~ 12 is reacted, obtains cigar ultra high pressure extraction liquid Maillard reaction flavor after sealing natural cooling.
As the preferred embodiment of the invention, in the step (1), the preprocess method of cigar tobacco leaf are as follows: will avenge
Eggplant cigarette tobacco leaf goes stalk rear blade chopping, and it is dry 20 min ~ 60 in 40 DEG C ~ 60 DEG C electric drying oven with forced convections that cut tobacco, which is placed in temperature,
Min is sealed spare.
As the preferred embodiment of the invention, in the step (1), cigar tobacco leaf and distilled water mass volume ratio
It (g:mL) is 1:2 ~ 1:20, ultra high pressure treatment pressure is the MPa of 100 MPa ~ 700, and the dwell time is the min of 5 min ~ 30, is unloaded
The pressure time is 5 s ~ 15s.
As the preferred embodiment of the invention, in the step (2), fructose, glycine and cigar ultra high pressure treatment
The mass volume ratio (g:g:mL) of liquid is 1:0.4 ~ 0.6:3 ~ 7, and the volume ratio of cigar ultra high pressure treatment liquid and reaction dissolvent is 3
~13:1。
As the preferred embodiment of the invention, in the step (2), the mass ratio of fructose and glycine is 1:0.5.
As the preferred embodiment of the invention, in the step (2), reaction dissolvent is the compounding of propylene glycol and grain wine
Solution, compound proportion are 5:1 ~ 1:5 (v/v).
As the preferred embodiment of the invention, the grain wine is selected from one of corn wine, rice wine and liquor made from sorghum.
As the preferred embodiment of the invention, in the step (2), pH value adjusts the NaOH that liquid is ammonium hydroxide or 5% ~ 15%
Solution.
The present invention also provides a kind of cigar ultra high pressure extraction liquid Maillard of preparation of the method according to the present invention
Application of the reaction flavor in cigarette.
As the preferred embodiment of the invention, the application is the cigar super-pressure for preparing the method for the invention
Extracting solution Maillard reaction flavor is sprayed on cigarette shreds with 1.0 ‰ ~ 4.0 ‰ mass ratio, and 24 h ~ 48 are placed in sealing
Cigarette is made in h.
To sum up, the device have the advantages that are as follows:
Cigar ultra high pressure extraction liquid Maillard reactant prepared by the present invention has pleasant tobacco book on Chinese herbal medicine fragrance special
Sign, and with light aroma fragrance.Using cigar ultra high pressure extraction liquid as amino acid source, joint glycine is as compounding amino
Acid, and prepare Maillard reacting substance perfume with fructose, compared with other amino acid and its collocation, have apparent supplement cigarette perfume and
The effect of strength can be obviously improved cigarette product flavouring essence quality, increase perfume quantity, cover miscellaneous gas, reduce irritation and dry sensation.
Specific embodiment
The present invention is described in further detail combined with specific embodiments below.But this should not be interpreted as in the present invention
The range for stating theme is only limitted to embodiment below, all that model of the invention is belonged to based on the technology that the content of present invention is realized
It encloses.In addition to specializing, technological means used in following embodiment and operating method are well known to those skilled in the art
Conventional means and method, institute using raw material is commercial goods.
Comparative example 1
(1) cigar tobacco leaf is subjected to stalk, to be placed on temperature be dry 30 min in 40 DEG C of electric drying oven with forced convections for chopping,
It seals spare.It weighs 100 g(and is accurate to 0.01 g) pretreated cigar pipe tobacco, 800mL95% ethyl alcohol, 80 DEG C of water are added
Bath reflux 2h, volatilizes solvent and obtains leaf tobacco extract；
(2) leaf tobacco extract 100g, fructose 100g, glycine 50g and propylene glycol 50mL, ethyl alcohol 50mL mixing are taken, ammonium hydroxide is adjusted
PH value of solution is placed in magnetic agitation oil bath pan, 95 DEG C of reaction 5h, natural cooling, obtains tobacco aromaticss at room temperature to 8.5.
Comparative example 2
(1) cigar tobacco leaf is subjected to stalk, to be placed on temperature be dry 40 min in 40 DEG C of electric drying oven with forced convections for chopping, close
It seals spare.By pretreated cigar tobacco 100g be added 800mL95% ethyl alcohol, 300W Microwave Extraction 10min, after letting cool, again
300W Microwave Extraction 10min, extracting solution filtering, obtains filtrate；
(2) filtrate 500mL, fructose 100g, glycine 50g and propylene glycol 50mL, corn wine 50mL mixing are taken, ammonium hydroxide adjusts solution
PH to 8.5 is placed in magnetic agitation oil bath pan, and 95 DEG C of reaction 5h, natural cooling, obtains tobacco aromaticss at room temperature.
Comparative example 3
(1) cigar tobacco leaf is subjected to stalk, to be placed on temperature be dry 30 min in 40 DEG C of electric drying oven with forced convections for chopping,
It seals spare.It weighs 100 g(and is accurate to 0.01 g) pretreated cigar pipe tobacco, 400 mL distilled water, be put into high pressure resistant
In PE bags, ultra high pressure treatment is carried out after stirring, pressure keeps 20 min after rising to 300 MPa, and reduction pressure time is 5s, will be surpassed
Cigar treatment fluid after HIGH PRESSURE TREATMENT, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(2) propylene glycol and corn wine base are prepared with the ratio of volume parts 1:1, is stirred evenly, it is anti-as Maillard
Answer solvent.100 g fructose, 550 mL cigar extracting solutions, 100 mL reaction dissolvents are sequentially added in round-bottomed flask, stirring is equal
Even, ammonium hydroxide adjusts pH value to 9.5, is placed in magnetic agitation oil bath pan, 3.5 h are reacted at 100 DEG C.Natural cooling at room temperature, system
Obtain tobacco aromaticss.
Comparative example 4
(1) cigar tobacco leaf is subjected to stalk, to be placed on temperature be dry 30 min in 40 DEG C of electric drying oven with forced convections for chopping,
It seals spare.It weighs 100 g(and is accurate to 0.01 g) pretreated cigar pipe tobacco, 400 mL distilled water, be put into high pressure resistant
In PE bags, ultra high pressure treatment is carried out after stirring, pressure keeps 20 min after rising to 300 MPa, and reduction pressure time is 5s, will be surpassed
Cigar treatment fluid after HIGH PRESSURE TREATMENT, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(2) propylene glycol and corn wine base are prepared with the ratio of volume parts 1:1, is stirred evenly, it is anti-as Maillard
Answer solvent.It is anti-that 100 g fructose, 50g phenylalanine, 550 mL cigar extracting solutions, 100 mL are sequentially added in round-bottomed flask
Solvent is answered, is stirred evenly, ammonium hydroxide adjusts pH value to 9.5, is placed in magnetic agitation oil bath pan, 3.5 h are reacted at 100 DEG C.Room temperature
Tobacco aromaticss are made in lower natural cooling.
Comparative example 5
(1) Maryland tobacco leaf is subjected to stalk, chopping is placed on temperature as in 40 DEG C of electric drying oven with forced convections dry 30
Min is sealed spare.It weighs 100 g(and is accurate to 0.01 g) pretreated Maryland pipe tobacco, 400 mL distilled water, be put into
In PE bags high pressure resistant, ultra high pressure treatment is carried out after stirring, pressure keeps 20 min after rising to 300 MPa, reduces pressure time and is
5s, by the Maryland treatment fluid after ultra high pressure treatment, through being filtered by vacuum, gained filtrate is Maryland ultra high pressure extraction
Liquid.
(2) propylene glycol and corn wine base are prepared with the ratio of volume parts 1:1, is stirred evenly, it is anti-as Maillard
Answer solvent.Fructose 100g, glycine 50g, 250 mL Maryland extracting solutions, 100 mL reaction are sequentially added in round-bottomed flask
Solvent stirs evenly, and ammonium hydroxide adjusts pH value to 9.5, is placed in magnetic agitation oil bath pan, 3.5 h are reacted at 100 DEG C.At room temperature
Tobacco aromaticss are made in natural cooling.
Embodiment 1
(1) going stalk, chopping to be placed on temperature cigar tobacco leaf is dry 40 min, sealing in 40 DEG C of electric drying oven with forced convections
It is spare.Weigh 200 g(be accurate to 0.01 g) pretreated cigar pipe tobacco, 500 mL distilled water be put into it is PE bags high pressure resistant
In, ultra high pressure treatment is carried out after stirring, pressure keeps 25 min after rising to 300 MPa, and the release time is 5 s.At super-pressure
Cigar treatment fluid after reason, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(2) propylene glycol and corn wine base are prepared with the ratio of volume parts 1:1, is stirred evenly, it is anti-as Maillard
Answer solvent.100 g fructose, 350 mL cigar extracting solutions, 60 g glycine, 100 mL reaction are sequentially added in round-bottomed flask
Solvent stirs evenly, and ammonium hydroxide adjusts pH value to 9.0, is placed in magnetic agitation oil bath pan, 4.5 h are reacted at 90 DEG C.At room temperature
Cigar ultra high pressure extraction liquid Maillard reactant A is made in natural cooling.
Embodiment 2
(1) going stalk, chopping to be placed on temperature cigar tobacco leaf is dry 30 min, sealing in 45 DEG C of electric drying oven with forced convections
It is spare.Weigh 200 g(be accurate to 0.01 g) pretreated cigar pipe tobacco, 700 mL distilled water be put into it is PE bags high pressure resistant
In, ultra high pressure treatment is carried out after stirring, pressure keeps 15 min after rising to 400 MPa, and the release time is 10 s.At super-pressure
Cigar treatment fluid after reason, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(2) propylene glycol and sorghum wine base are prepared with the ratio of volume parts 2:1, is stirred evenly, it is anti-as Maillard
Answer solvent.100 g fructose, 550 mL cigar extracting solutions, 60 g glycine, 50 mL reaction are sequentially added in round-bottomed flask
Solvent stirs evenly, and ammonium hydroxide adjusts pH value to 9.5, is placed in magnetic agitation oil bath pan, 4.0 h are reacted at 95 DEG C.At room temperature
Cigar ultra high pressure extraction liquid Maillard reactant B is made in natural cooling.
Embodiment 3
(1) going stalk, chopping to be placed on temperature cigar tobacco leaf is dry 30 min, sealing in 45 DEG C of electric drying oven with forced convections
It is spare.Weigh 200 g(be accurate to 0.01 g) pretreated cigar pipe tobacco, 800 mL distilled water be put into it is PE bags high pressure resistant
In, ultra high pressure treatment is carried out after stirring, pressure keeps 10 min after rising to 500 MPa, and the release time is 15 s.At super-pressure
Cigar treatment fluid after reason, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(2) propylene glycol and sorghum wine base are prepared with the ratio of volume parts 2:1, is stirred evenly, it is anti-as Maillard
Answer solvent.100 g fructose, 550 mL cigar extracting solutions, 50 g glycine, 50 mL reaction are sequentially added in round-bottomed flask
Solvent stirs evenly, and ammonium hydroxide adjusts pH value to 9.0, is placed in magnetic agitation oil bath pan, 3.5 h are reacted at 100 DEG C.At room temperature
Cigar ultra high pressure extraction liquid Maillard reactant C is made in natural cooling.
Embodiment 4
(1) going stalk, chopping to be placed on temperature cigar tobacco leaf is dry 40 min, sealing in 40 DEG C of electric drying oven with forced convections
It is spare.Weigh 200 g(be accurate to 0.01 g) pre-process after cigar pipe tobacco, 600 mL distilled water be put into PE bags high pressure resistant,
Ultra high pressure treatment is carried out after stirring, pressure keeps 20 min after rising to 300 MPa, and the release time is 5 s.After ultra high pressure treatment
Cigar treatment fluid, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(2) propylene glycol and rice wine base are prepared with the ratio of volume parts 1:1, is stirred evenly, it is anti-as Maillard
Answer solvent.100 g fructose, 450 mL cigar extracting solutions, 45 g glycine, 50 mL reaction are sequentially added in round-bottomed flask
Solvent stirs evenly, and 10%NaOH solution adjusts pH value to 10.0, is placed in magnetic agitation oil bath pan, reacts 4.5 at 95 DEG C
h.Cigar ultra high pressure extraction liquid Maillard reactant D is made in natural cooling at room temperature.
Embodiment 5
(1) going stalk, chopping to be placed on temperature cigar tobacco leaf is dry 40 min, sealing in 40 DEG C of electric drying oven with forced convections
It is spare.Weigh 200 g(be accurate to 0.01 g) pretreated cigar pipe tobacco, 1000 mL distilled water be put into it is PE bags high pressure resistant
In, ultra high pressure treatment is carried out after stirring, pressure keeps 20 min after rising to 300 MPa, and the release time is 10 s.At super-pressure
Cigar treatment fluid after reason, through being filtered by vacuum, gained filtrate is cigar ultra high pressure extraction liquid.
(4) propylene glycol and corn wine base are prepared with the ratio of volume parts 2:1, is stirred evenly, it is anti-as Maillard
Answer solvent.100 g fructose, 650 mL cigar extracting solutions, 40 g glycine, 50 mL reaction are sequentially added in round-bottomed flask
Solvent stirs evenly, and ammonium hydroxide adjusts pH value to 9.5, is placed in magnetic agitation oil bath pan, 4.5 h are reacted at 95 DEG C.At room temperature
Cigar ultra high pressure extraction liquid Maillard reactant E is made in natural cooling.
Application Example 1
The above-mentioned fragrance for preparing comparative example and embodiment is sprayed on pipe tobacco by 2.0 ‰ mass ratio for accounting for tobacco quality,
48 h are placed in sealing, and cigarette is made.Cigarette sample (20 ± 1) DEG C, relative humidity (60 ± 3) % constant-temperature constant-humidity environment under put down
It weighs after 24 h, organizes 7 personnel foundation tobaccos of smokeing panel test in product sensory evaluation method (YC/T 415-2011) to addition embodiment
The cigarette sample and blank cigarette for preparing fragrance are smoked panel test, and using sense organ technical requirements (GB 5606.4-2005) to addition pair
The cigarette sample that ratio and embodiment prepare fragrance carries out sensory evaluation, and smoking result is as shown in Table 1 and Table 2.
Analyses Methods for Sensory Evaluation Results when 1 cigar ultra high pressure extraction liquid Maillard reactant adding proportion of table is 2.0 ‰
Through sensory evaluation, compared with blank control, after addition cigar ultra high pressure extraction liquid Maillard reactant A, B, C, volume
Cigarette flue gas flavouring essence quality gets a promotion, and flue gas concentration increases, and flue gas strength increases, the plumpness of flue gas and thoroughly good, the physiology of hair property
Satisfaction enhancing, can significantly cover miscellaneous gas, augment cigarette perfume, oral cavity time sweet tea sense is obvious, and pleasant impression is showed with respect to blank control sample
It is more comfortable.
Sensory evaluation scores when 2 comparative example of table and embodiment tobacco aromaticss adding proportion are 2.0 ‰
Through sensory evaluation, compared with the tobacco leaves such as Maryland tobacco leaf prepare Maillard reactant as one of amino acid source, with
And with other extraction processes extract cigar tobacco leaf ingredient compared with or cigar ingredient and fructose and phenylalanine etc. preparation perfume
Material is compared, and the present invention combines glycine as built amino-acid using cigar ultra high pressure extraction liquid as amino acid source, and and fructose
Maillard reacting substance perfume is prepared, compared with other amino acid and its collocation, plays the role of significantly augmenting cigarette perfume and strength,
It can be obviously improved cigarette product flavouring essence quality, increase perfume quantity, cover miscellaneous gas, reduce irritation and dry sensation.
The foregoing is merely the detailed descriptions of specific embodiments of the present invention, do not limit the present invention with this, all at this
Made any modifications, equivalent replacements, and improvements etc. in the mentality of designing of invention, should be included in protection scope of the present invention it
It is interior.
Claims (10)
1. a kind of preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor, the described method comprises the following steps:
(1) it takes pretreated cigar tobacco leaf and distilled water to be sequentially placed into PE bags high pressure resistant, is carried out at super-pressure after stirring
Cigar ultra high pressure extraction liquid is filtered by vacuum to obtain in reason, treatment fluid；
(2) it takes cigar ultra high pressure extraction liquid to be added in Maillard reactor, fructose, glycine and reaction dissolvent is added, adjust
Reacting liquid pH value is saved to 8.5 ~ 10.5, starts timing when temperature is ramped up 85 DEG C ~ 120 DEG C under magnetic stirring when reaction solution,
The h of 2 h ~ 12 is reacted, obtains cigar ultra high pressure extraction liquid Maillard reaction flavor after sealing natural cooling.
2. the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor according to claim 1, feature
It is in the step (1), the preprocess method of cigar tobacco leaf are as follows: cigar tobacco leaf is gone into stalk rear blade chopping, cut tobacco is set
It is the dry min of 20 min ~ 60 in 40 DEG C ~ 60 DEG C electric drying oven with forced convections in temperature, seals spare.
3. the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor according to claim 1, feature
It is in the step (1), cigar tobacco leaf and distilled water mass volume ratio (g:mL) are 1:2 ~ 1:20, ultra high pressure treatment pressure
For the MPa of 100 MPa ~ 700, the dwell time is the min of 5 min ~ 30, and the release time is 5 s ~ 15s.
4. the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor according to claim 1, feature
Be in the step (2), the mass volume ratio (g:g:mL) of fructose, glycine and cigar ultra high pressure treatment liquid be 1:0.4 ~
The volume ratio of 0.6:3 ~ 7, cigar ultra high pressure treatment liquid and reaction dissolvent is 3 ~ 13:1.
5. according to the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor described in claim 1, feature exists
In the step (2), the mass ratio of fructose and glycine is 1:0.5.
6. the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor according to claim 1, feature
It is in the step (2), reaction dissolvent is the combination solution of propylene glycol and grain wine, and compound proportion is 5:1 ~ 1:5 (v/v).
7. the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor according to claim 6, feature
It is that the grain wine is selected from one of corn wine, rice wine and liquor made from sorghum.
8. the preparation method of cigar ultra high pressure extraction liquid Maillard reaction flavor according to claim 1, feature
It is in the step (2), pH value adjusts the NaOH solution that liquid is ammonium hydroxide or 5% ~ 15%.
9. the cigar ultra high pressure extraction liquid Maillard reaction flavor of any one of claim 1 ~ 8 the method preparation is being rolled up
Application in cigarette.
10. application according to claim 9, it is characterised in that by the preparation of any one of claim 1 ~ 8 the method
Cigar ultra high pressure extraction liquid Maillard reaction flavor is sprayed on cigarette shreds with 1.0 ‰ ~ 4.0 ‰ mass ratio, sealing
The h of 24 h ~ 48 is placed, cigarette is made.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113667536A (en) * | 2021-07-19 | 2021-11-19 | 河南中烟工业有限责任公司 | Cigar-flavor essence and application thereof |
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Application publication date: 20190517 |