CN104983056B - The preparation method of a kind of cocoa black powder cigarette additive and the application in recombination tobacco leaf Medicated cigarette thereof - Google Patents
The preparation method of a kind of cocoa black powder cigarette additive and the application in recombination tobacco leaf Medicated cigarette thereof Download PDFInfo
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- CN104983056B CN104983056B CN201510257588.3A CN201510257588A CN104983056B CN 104983056 B CN104983056 B CN 104983056B CN 201510257588 A CN201510257588 A CN 201510257588A CN 104983056 B CN104983056 B CN 104983056B
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- cocoa
- black powder
- tobacco leaf
- enzyme
- recombination tobacco
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 82
- 244000299461 Theobroma cacao Species 0.000 title claims abstract description 76
- 235000009470 Theobroma cacao Nutrition 0.000 title claims abstract description 76
- 239000000843 powder Substances 0.000 title claims abstract description 71
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 58
- 230000006798 recombination Effects 0.000 title claims abstract description 49
- 238000005215 recombination Methods 0.000 title claims abstract description 49
- 239000000654 additive Substances 0.000 title claims abstract description 45
- 230000000996 additive effect Effects 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 244000061176 Nicotiana tabacum Species 0.000 title claims description 6
- 241000208125 Nicotiana Species 0.000 claims abstract description 52
- 238000000855 fermentation Methods 0.000 claims abstract description 15
- 230000004151 fermentation Effects 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 13
- 150000001875 compounds Chemical class 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 6
- 102000004190 Enzymes Human genes 0.000 claims description 38
- 108090000790 Enzymes Proteins 0.000 claims description 38
- 239000003513 alkali Substances 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 14
- 108091005658 Basic proteases Proteins 0.000 claims description 12
- 229920002678 cellulose Polymers 0.000 claims description 12
- 239000001913 cellulose Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 229920002472 Starch Polymers 0.000 claims description 7
- 238000011534 incubation Methods 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 239000000376 reactant Substances 0.000 claims description 7
- 238000010992 reflux Methods 0.000 claims description 7
- 239000008107 starch Substances 0.000 claims description 7
- 235000019698 starch Nutrition 0.000 claims description 7
- 239000006228 supernatant Substances 0.000 claims description 7
- 239000013049 sediment Substances 0.000 claims description 5
- 239000003205 fragrance Substances 0.000 abstract description 6
- 238000004043 dyeing Methods 0.000 abstract description 3
- 239000004615 ingredient Substances 0.000 abstract description 2
- 235000019506 cigar Nutrition 0.000 description 13
- 230000000694 effects Effects 0.000 description 5
- 239000007789 gas Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 229940089401 xylon Drugs 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000002864 food coloring agent Nutrition 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000000199 molecular distillation Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
- A24B15/307—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation using microorganisms or enzymes as catalysts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses the preparation method of a kind of cocoa black powder cigarette additive, it is first to carry out biofermentation process with compound bio-enzyme powder black to natural cocoa, then using fermentation liquid as natural N source, maillard flavouring reaction is carried out with Mel, obtain that fragrance is more abundant, the higher cocoa of odourant ingredients content black powder cigarette additive, cocoa black powder cigarette additive prepared by the present invention can be used for perfumery and the dyeing of recombination tobacco leaf Medicated cigarette, can be not only used in recombination tobacco leaf it can also be used in cigarette paper.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of cocoa black powder cigarette additive
Preparation method, and cocoa black powder cigarette additive prepared by the method is in recombination tobacco leaf Medicated cigarette
Application.
Background technology
Recombination tobacco leaf is also known as reconstituted tobacco or homogenizing Nicotiana tabacum L., mainly by offal, fragment, cabo or low order
Nicotiana tabacum L. adds the compositions such as adhesive and other additives.Recombination tobacco leaf exist miscellaneous QI weight, zest big and
The suction taste defects such as mouthfeel is uncomfortable, have impact on recombination tobacco leaf using effect in cigarette product and addition.
Domestic common practice is that the way using additive is improved, and applies more additive at present
Being Nicotiana tabacum L., natural plant kind extract, these extracts are typically by water, alcohol extraction or molecular distillation
Obtain, improvement limitation to cigarette quality after interpolation, the most irritant big, the defect such as miscellaneous QI is many.
Recombination tobacco leaf can be used for replacing natural cigar binder, the most extensively as tobacco product raw material
As raw material of cigarette.The advantage that the cigar type Medicated cigarette that recombination tobacco leaf makes has merged cigar and flue-cured tobacco is special
Levy, formed and have the strong plentiful and pure comfortable special favor of flue-cured tobacco of cigar concurrently, construct and be different from
The Chinese style cigar category of cigar type and fire-cured tobacco type.
In order to make the style of cigar type Medicated cigarette that recombination tobacco leaf makes closer to cigar, generally also need to
Recombination tobacco leaf or cigarette paper are carried out dyeing process, and the recombination tobacco leaf that prior art produces or cigarette paper,
Not only tone and cigar there is also the biggest gap, and cigarette paper there is also in combustion process and produces relatively
Many xylon gas, sting peppery sense and affect the problems such as the pure abnormal smells from the patient of cigarette smoke.
The black powder of cocoa is the alkalization dark cocoa powder extracting from natural cocoa, refining, pure
Cocoa fragrance, fragrant and sweet, fatty, multiple micro-containing rich in protein, several amino acids, high heat
Secondary element, multivitamin and multiple bioactive alkaloid, the wherein protein containing about 20%,
And the suction taste of Medicated cigarette can be had a negative impact by the combustion product of protein.
Summary of the invention
It is an object of the invention to provide the preparation method of a kind of cocoa black powder cigarette additive, the party's legal system
Standby cocoa black powder cigarette additive can be not only used for the coordination flavouring of recombination tobacco leaf Medicated cigarette, can be used for again weight
The dyeing of group Nicotiana tabacum L. Medicated cigarette.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of preparation method of cocoa black powder cigarette additive, it comprises the following steps:
1) in the black powder of natural cocoa, add the compound bio-enzyme of 0.1～0.5% by weight, at pH be
8～11, stirring incubation 4～24 hours during temperature is the water of 40～60 DEG C, 8000～10000rpm are centrifuged,
Take supernatant, for cocoa black powder enzyme fermentation liquid；
2) adding Mel in cocoa black powder enzyme fermentation liquid, the addition of described Mel is that natural cocoa is black
The 0.5～5% of grain weight amount, mixing, stirring, regulation pH is 9～11, is heated to reflux carrying out maillard anti-
Answer 3～8 hours, after reaction terminates, reactant liquor be concentrated into the black extractum that relative density is 1.1～1.2,
Obtain cocoa black powder cigarette additive,
Described compound bio-enzyme is that alkaline protease, alkali cellulose enzyme, alkaline pectase and alkalescence are formed sediment
Powder enzyme, described alkaline protease, alkali cellulose enzyme, alkaline pectase and the weight of alkali starch enzyme
Than for=1: 0.5～2: 0.5～2:0.5～2；
Preferably, the preparation method of described cocoa black powder cigarette additive comprises the following steps:
1) in the black powder of natural cocoa, add the compound bio-enzyme of 0.3% by weight, pH be 10, temperature
Degree is to stir incubation 8 hours in the water of 50 DEG C, and 9000rpm is centrifuged, and takes supernatant, for the black powder of cocoa
Enzyme fermentation liquid；
2) adding Mel in cocoa black powder enzyme fermentation liquid, the addition of described Mel is that natural cocoa is black
The 2% of grain weight amount, mixing, stirring, regulation pH is 10, is heated to reflux carrying out mailland reaction 5 little
Time, after reaction terminates, reactant liquor is concentrated into the black extractum that relative density is 1.15, obtains cocoa
Black powder cigarette additive.
Preferably, step 1) in, the weight of water is 8～20 times of natural cocoa black grain weight amount.
Preferably, described alkaline protease, alkali cellulose enzyme, alkaline pectase and alkali starch enzyme
Weight ratio be=1: 1: 0.5: 1.
Cocoa black powder cigarette additive prepared by the said method application in recombination tobacco leaf Medicated cigarette, should
With being that black for described cocoa powder cigarette additive is joined restructuring cigarette by the 0.1～0.3% of recombination tobacco leaf weight
Add by the 0.1～1% of recombination tobacco leaf cigarette paper weight in leaf and/or by black for described cocoa powder cigarette additive
Enter in recombination tobacco leaf cigarette paper.
The invention has the beneficial effects as follows:
1) the cocoa black powder cigarette additive that prepared by the present invention can be used for perfumery and the dye of recombination tobacco leaf Medicated cigarette
Color, can be not only used in recombination tobacco leaf it can also be used in cigarette paper.When recombination tobacco leaf, can coordinate
Flue gas, makes aroma quality promote, and fragrance is more rich and with obvious cocoa characteristic perfume, the most also has
There is reduction to stimulate, reduce the effect of miscellaneous QI；When cigarette paper, the quality of cigarette paper can be promoted, make
It presents the dark brown of elegant and tone is naturally uniform, outward appearance closely cigar, also simultaneously
Solve current process use food colour brought affect the problems such as suction quality, can cover well
The produced xylon gas of lid cigarette paper burning, sting peppery sense.
2) using cocoa black powder cigarette additive prepared by the present invention, odourant ingredients content is high, and product is received
Rate is high, and raw material with short production cycle and used has the advantages such as natural environmental-protective is harmless, has bigger
Commercial Application converts prospect.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1
A kind of preparation method of cocoa black powder cigarette additive, its step is as follows:
1) in the 1Kg black powder of natural cocoa, add 3g compound bio-enzyme, 15Kg pH be 10, temperature
Degree is to stir incubation 8 hours in the water of 50 DEG C, and 9000rpm is centrifuged, and takes supernatant, for the black powder of cocoa
Enzyme fermentation liquid；
2) in cocoa black powder enzyme fermentation liquid, 20g Mel is added, mixing, stirring, regulation pH is 10,
It is heated to reflux carrying out mailland reaction 5 hours, after reaction terminates, reactant liquor is concentrated into relative density
It is the black extractum of 1.15, obtains cocoa black powder cigarette additive.
Described compound bio-enzyme is that alkaline protease, alkali cellulose enzyme, alkaline pectase and alkalescence are formed sediment
Powder enzyme, described alkaline protease, alkali cellulose enzyme, alkaline pectase and the weight of alkali starch enzyme
Than for=1: 1: 0.5: 1.
Embodiment 2
A kind of preparation method of cocoa black powder cigarette additive, its step is as follows:
1) in the 1Kg black powder of natural cocoa, add 5g compound bio-enzyme, 20Kg pH be 8, temperature
Degree is to stir incubation 4 hours in the water of 60 DEG C, and 10000rpm is centrifuged, and takes supernatant, for the black powder of cocoa
Enzyme fermentation liquid；
2) in cocoa black powder enzyme fermentation liquid, 50g Mel is added, mixing, stirring, regulation pH is 11,
It is heated to reflux carrying out mailland reaction 8 hours, after reaction terminates, reactant liquor is concentrated into relative density
It is the black extractum of 1.1, obtains cocoa black powder cigarette additive.
Described compound bio-enzyme is that alkaline protease, alkali cellulose enzyme, alkaline pectase and alkalescence are formed sediment
Powder enzyme, described alkaline protease, alkali cellulose enzyme, alkaline pectase and the weight of alkali starch enzyme
Than for=1: 2: 2: 2.
Embodiment 3
A kind of preparation method of cocoa black powder cigarette additive, its step is as follows:
1) in the 1Kg black powder of natural cocoa, add 1g compound bio-enzyme, 8Kg pH be 11, temperature
Degree is to stir incubation 24 hours in the water of 40 DEG C, and 8000rpm is centrifuged, and takes supernatant, for the black powder of cocoa
Enzyme fermentation liquid；
2) in cocoa black powder enzyme fermentation liquid, 50g Mel is added, mixing, stirring, regulation pH is 9,
It is heated to reflux carrying out mailland reaction 3 hours, after reaction terminates, reactant liquor is concentrated into relative density
It is the black extractum of 1.2, obtains cocoa black powder cigarette additive.
Described compound bio-enzyme is that alkaline protease, alkali cellulose enzyme, alkaline pectase and alkalescence are formed sediment
Powder enzyme, described alkaline protease, alkali cellulose enzyme, alkaline pectase and the weight of alkali starch enzyme
Than for=1: 0.5: 0.5: 0.5.
Test example 1: use cocoa black powder cigarette additive to the effect test of smokeing panel test after recombination tobacco leaf perfumery
Cocoa black powder cigarette additive embodiment 1-3 prepared is by 0.2% interpolation of recombination tobacco leaf weight
In recombination tobacco leaf (B class), then recombination tobacco leaf is loaded and seal bag, place 80 DEG C in an oven
Constant temperature 30min, suitable to recombination tobacco leaf moisture, roll into cigarette, put into climatic chamber (22
DEG C+1, relative humidity is 60%+2%) smooth 48h, asks the expert group of smokeing panel test to be smoked panel test.Comparison adds for spray
The Medicated cigarette that the recombination tobacco leaf (B class) of the equal amount black powder of unprocessed natural cocoa rolls.
Repeatedly smokeing panel test through the group of smokeing panel test, result shows: cocoa black powder cigarette additive prepared by the present invention,
Recombination tobacco leaf aroma quality can be made to promote, and fragrance is abundanter, increases the fragrant and sweet breath of cocoa, reduces cigarette
Gas stimulates, reduces the advantage of miscellaneous QI, and especially improving recombination tobacco leaf stimulates suction taste big, that mouthfeel is uncomfortable
Defect, can be added by the 0.1 of recombination tobacco leaf weight～0.3%.
Table 1. uses cocoa black powder cigarette additive to the effect of smokeing panel test after recombination tobacco leaf perfumery
Test example 2: the effect assessment after using cocoa black powder cigarette additive that recombination tobacco leaf cigarette paper is dyeed
It is 1.02-1.05 that cocoa black powder cigarette additive embodiment 1-3 prepared is diluted to relative density,
Add potassium salt again and make coating fluid, be applied on cigarette paper by the mode of coating, the wherein addition of potassium salt
For the 1% of body paper weight, addition is body paper weight the 0.5% of cocoa black powder cigarette additive.
Cigarette paper through coating is dried 0.3 hour under the temperature conditions of 100 DEG C, then carries out back
After tide, it is finished product recombination tobacco leaf cigarette paper and uses it for the cigar type Medicated cigarette that recombination tobacco leaf makes.
Recombination tobacco leaf cigar type cigarette smoke exquisiteness plentiful, soft, miscellaneous QI zest are less, especially
Not having xylon gas, sting peppery sense, outward appearance presents the dark brown of elegant and color is naturally uniform, very
Close to cigar, can add by the 0.1 of recombination tobacco leaf cigarette paper weight～1%.Wherein embodiment 1
Perfumery and Color are substantially better than embodiment 2 and 3.
Claims (6)
1. the preparation method of a cocoa black powder recombination tobacco leaf cigarette paper additive, it is characterised in that include
Following steps:
1) in the black powder of natural cocoa, add the compound bio-enzyme of 0.1～0.5% by weight, at pH be
8～11, stirring incubation 4～24 hours during temperature is the water of 40～60 DEG C, 8000～10000rpm are centrifuged,
Take supernatant, for cocoa black powder enzyme fermentation liquid；
2) adding Mel in cocoa black powder enzyme fermentation liquid, the addition of described Mel is that natural cocoa is black
The 0.5～5% of grain weight amount, mixing, stirring, regulation pH is 9～11, is heated to reflux carrying out maillard anti-
Answer 3～8 hours, after reaction terminates, reactant liquor be concentrated into the black extractum that relative density is 1.1～1.2,
Obtain cocoa black powder recombination tobacco leaf cigarette paper additive,
Described compound bio-enzyme is that alkaline protease, alkali cellulose enzyme, alkaline pectase and alkalescence are formed sediment
Powder enzyme, described alkaline protease, alkali cellulose enzyme, alkaline pectase and the weight of alkali starch enzyme
Than for=1: 0.5～2: 0.5～2:0.5～2.
2. the preparation method of cocoa black powder recombination tobacco leaf cigarette paper additive as claimed in claim 1,
It is characterized in that comprising the following steps:
1) in the black powder of natural cocoa, add the compound bio-enzyme of 0.3% by weight, pH be 10, temperature
Degree is to stir incubation 8 hours in the water of 50 DEG C, and 9000rpm is centrifuged, and takes supernatant, for the black powder of cocoa
Enzyme fermentation liquid；
2) adding Mel in cocoa black powder enzyme fermentation liquid, the addition of described Mel is that natural cocoa is black
The 2% of grain weight amount, mixing, stirring, regulation pH is 10, is heated to reflux carrying out mailland reaction 5 little
Time, after reaction terminates, reactant liquor is concentrated into the black extractum that relative density is 1.15, obtains cocoa
Black powder recombination tobacco leaf cigarette paper additive.
3. the preparation method of cocoa black powder recombination tobacco leaf cigarette paper additive as claimed in claim 1,
It is characterized in that: step 1) in, the weight of water is 8～20 times of natural cocoa black grain weight amount.
4. the preparation method of cocoa black powder recombination tobacco leaf cigarette paper additive as claimed in claim 1,
It is characterized in that: described alkaline protease, alkali cellulose enzyme, alkaline pectase and alkali starch enzyme
Weight ratio be=1: 1: 0.5: 1.
5. cocoa black powder recombination tobacco leaf cigarette paper additive application in recombination tobacco leaf cigarette paper, it is special
Levy and be: described cocoa black powder recombination tobacco leaf cigarette paper additive is according to Claims 1 to 4 any
Prepared by the method described in Xiang.
6. cocoa black powder recombination tobacco leaf cigarette paper additive as claimed in claim 5 is rolled up at recombination tobacco leaf
Application in cigarette paper, it is characterised in that: by black for described cocoa powder recombination tobacco leaf cigarette paper additive by weight
The 0.1～1% of group Nicotiana tabacum L. cigarette paper weight joins in recombination tobacco leaf cigarette paper.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510257588.3A CN104983056B (en) | 2015-05-19 | 2015-05-19 | The preparation method of a kind of cocoa black powder cigarette additive and the application in recombination tobacco leaf Medicated cigarette thereof |
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| CN201510257588.3A CN104983056B (en) | 2015-05-19 | 2015-05-19 | The preparation method of a kind of cocoa black powder cigarette additive and the application in recombination tobacco leaf Medicated cigarette thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105349264B (en) * | 2015-12-03 | 2019-05-07 | 河北中烟工业有限责任公司 | A kind of preparation method of Maillard reaction fragrance and its application in cigarette |
| CN106418663B (en) * | 2016-10-31 | 2017-12-05 | 湖北中烟工业有限责任公司 | A kind of biochemistry combined preparation process of rose extrait and its application |
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| US4289146A (en) * | 1979-10-05 | 1981-09-15 | International Flavors & Fragrances Inc. | Use of 2,4,6-trimethylcyclohexanemethanol and derivatives for augmenting or enhancing the aroma or taste of smoking tobacco and smoking tobacco articles |
| CN101445766A (en) * | 2008-12-17 | 2009-06-03 | 华宝食用香精香料（上海）有限公司 | Preparation method of cacao flavor, products obtained thereby and usage thereof |
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| CN102551009A (en) * | 2010-12-17 | 2012-07-11 | 上海爱普植物科技有限公司 | Method for preparing natural dried fruit essence by utilizing dried fruit raw materials |
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| CN102972857A (en) * | 2012-10-31 | 2013-03-20 | 湖北新业烟草薄片开发有限公司 | Method for tobacco slice cigarette paper coloring by adopting Millard reaction |
| CN103211297A (en) * | 2013-04-03 | 2013-07-24 | 红云红河烟草(集团)有限责任公司 | Preparation method of kiwi fruit extracts and application of kiwi fruit extracts in cigarettes |
| CN104187539A (en) * | 2014-09-17 | 2014-12-10 | 王婧婧 | Method for preparing chocolate essence from cocoa bean husk |
-
2015
- 2015-05-19 CN CN201510257588.3A patent/CN104983056B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4289146A (en) * | 1979-10-05 | 1981-09-15 | International Flavors & Fragrances Inc. | Use of 2,4,6-trimethylcyclohexanemethanol and derivatives for augmenting or enhancing the aroma or taste of smoking tobacco and smoking tobacco articles |
| CN101445766A (en) * | 2008-12-17 | 2009-06-03 | 华宝食用香精香料（上海）有限公司 | Preparation method of cacao flavor, products obtained thereby and usage thereof |
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| CN102551009A (en) * | 2010-12-17 | 2012-07-11 | 上海爱普植物科技有限公司 | Method for preparing natural dried fruit essence by utilizing dried fruit raw materials |
| CN102687838A (en) * | 2011-03-21 | 2012-09-26 | 广州市名花香料有限公司 | Cocoa extract preparation method |
| CN102972857A (en) * | 2012-10-31 | 2013-03-20 | 湖北新业烟草薄片开发有限公司 | Method for tobacco slice cigarette paper coloring by adopting Millard reaction |
| CN103211297A (en) * | 2013-04-03 | 2013-07-24 | 红云红河烟草(集团)有限责任公司 | Preparation method of kiwi fruit extracts and application of kiwi fruit extracts in cigarettes |
| CN104187539A (en) * | 2014-09-17 | 2014-12-10 | 王婧婧 | Method for preparing chocolate essence from cocoa bean husk |
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