CN105040518B - Coating liquid for tobacco sheet cigarette paper - Google Patents
Coating liquid for tobacco sheet cigarette paper Download PDFInfo
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- CN105040518B CN105040518B CN201510332704.3A CN201510332704A CN105040518B CN 105040518 B CN105040518 B CN 105040518B CN 201510332704 A CN201510332704 A CN 201510332704A CN 105040518 B CN105040518 B CN 105040518B
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- 239000011248 coating agent Substances 0.000 title claims abstract description 47
- 238000000576 coating method Methods 0.000 title claims abstract description 47
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 46
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 38
- 241000208125 Nicotiana Species 0.000 title claims abstract description 34
- 239000007788 liquid Substances 0.000 title claims abstract description 29
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 57
- 238000006243 chemical reaction Methods 0.000 claims abstract description 30
- 235000013599 spices Nutrition 0.000 claims abstract description 24
- 238000002485 combustion reaction Methods 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000000855 fermentation Methods 0.000 claims abstract description 20
- 230000004151 fermentation Effects 0.000 claims abstract description 20
- 150000001413 amino acids Chemical class 0.000 claims abstract description 19
- 108091005804 Peptidases Proteins 0.000 claims abstract description 10
- 239000004365 Protease Substances 0.000 claims abstract description 10
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims abstract description 10
- 239000002699 waste material Substances 0.000 claims abstract description 10
- 239000006228 supernatant Substances 0.000 claims abstract description 9
- 239000012530 fluid Substances 0.000 claims description 39
- 239000002671 adjuvant Substances 0.000 claims description 22
- 235000001014 amino acid Nutrition 0.000 claims description 18
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 238000009835 boiling Methods 0.000 claims description 9
- 239000000376 reactant Substances 0.000 claims description 9
- 230000004044 response Effects 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 8
- 229940119429 cocoa extract Drugs 0.000 claims description 7
- IMKHDCBNRDRUEB-UHFFFAOYSA-N Dihydroactinidiolide Natural products C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 claims description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 5
- IMKHDCBNRDRUEB-LLVKDONJSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)O[C@@]21C IMKHDCBNRDRUEB-LLVKDONJSA-N 0.000 claims description 5
- 150000002596 lactones Chemical class 0.000 claims description 4
- 239000001508 potassium citrate Substances 0.000 claims description 4
- 229960002635 potassium citrate Drugs 0.000 claims description 4
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 4
- 235000011082 potassium citrates Nutrition 0.000 claims description 4
- 239000001509 sodium citrate Substances 0.000 claims description 4
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 4
- 241000894006 Bacteria Species 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 4
- 239000002023 wood Substances 0.000 abstract description 2
- 241000235342 Saccharomycetes Species 0.000 abstract 1
- 239000012295 chemical reaction liquid Substances 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 239000000049 pigment Substances 0.000 abstract 1
- 239000000779 smoke Substances 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 10
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 description 8
- 229940089401 xylon Drugs 0.000 description 8
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 7
- 239000003546 flue gas Substances 0.000 description 7
- 235000019506 cigar Nutrition 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 4
- 244000061176 Nicotiana tabacum Species 0.000 description 4
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 4
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 229930091371 Fructose Natural products 0.000 description 2
- 239000005715 Fructose Substances 0.000 description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 239000004471 Glycine Substances 0.000 description 2
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 description 2
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 description 2
- 239000004472 Lysine Substances 0.000 description 2
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 2
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 description 2
- 235000004279 alanine Nutrition 0.000 description 2
- 230000004075 alteration Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 229930182830 galactose Natural products 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- 235000009470 Theobroma cacao Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000576 food coloring agent Substances 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000002772 monosaccharides Chemical class 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000005215 recombination Methods 0.000 description 1
- 230000006798 recombination Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Landscapes
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Abstract
The invention discloses a coating liquid for tobacco sheet cigarette paper. The coating liquid is prepared from a toner, a combustion improver and a spice, wherein the toner is prepared by the following steps: (1) adding water to tobacco leaf waste, decocting, extracting, adding saccharomycetes and protease to an extracted liquid for fermentation, concentrating the fermented liquid, adding ethanol, standing, taking a supernatant liquid, recovering the ethanol and carrying out vacuum concentration to form clear paste; and (2) adding hot water, revertose and amino acid to the clear paste, carrying out maillard reaction, ending the reaction, and concentrating a reaction liquid, so as to obtain the coating liquid. According to the coating liquid disclosed by the invention, the wood gas, the offensive odor and the oral irritation of the tobacco sheet cigarette paper can be reduced; the fragrance of the tobacco sheet cigarette paper can be increased; the smoke panel test result is improved; and meanwhile, the cigarette paper can also be dyed by the coating liquid instead of a natural pigment.
Description
Technical field
The invention belongs to reconstituted tobacoo manufacture field, and in particular to a kind of tobacco sheet cigarette paper coating fluid.
Background technology
Reconstituted tobacoo is also called recombination tobacco leaf, reconstituted tobacco etc., is Nicotiana tabacum L. to be harvested in redrying and cigarette making process to produce
Raw cabo, offal and secondary Nicotiana tabacum L. etc., according to the product that physical method or chemical method carry out recombinating, can be used as Nicotiana tabacum L.
Product raw material substitution cigar.When Medicated cigarette is prepared with reconstituted tobacoo, in order that the outward appearance of Medicated cigarette is closer to cigar, it is right to need
Cigarette paper carries out dyeing process, but common stain can usually affect the suction taste of Medicated cigarette, increases the zest of flue gas.
CN102972857A discloses a kind of method for adopting Maillard reaction and colouring for tobacco sheet cigarette paper, it be by
Tobacco leaf fragment or cabo are extracted with water, and residue is made and make again after tobacco pulp cigarette paper, and extract is added into reducing sugar, amino
Coating fluid is made after acid, spice, Maillard reaction is finally coated on cigarette paper and carry out.But, said method is in coating
Maillard reaction is carried out on cigarette paper afterwards, it is suffered from the drawback that：1) due to being reacted on cigarette paper, therefore react
Time can not be oversize, and the extent of reaction is insufficient, and responseless aminoacid is easily separated out in cigarette paper baking process, so as to affect
Color；2) because Maillard reaction is affected larger by factors such as environment, equipment, the extent of reaction on cigarette paper cannot
Precise control, causes reaction color uneven, and larger per the aberration criticized, Color is unstable.3) the cigarette paper wood after dyeing
Matter gas is heavier, and miscellaneous QI is more, and zest is big.
The content of the invention
The purpose of the present invention is to be directed to drawbacks described above, there is provided a kind of tobacco sheet cigarette paper coating fluid, the coating fluid is not only
The colourity of tobacco sheet cigarette paper can be made closer to cigar, while the fragrance of cigarette paper can also be increased, xylon gas, miscellaneous are reduced
Gas and reduction zest.
Above-mentioned purpose is achieved through the following technical solutions：
A kind of tobacco sheet cigarette paper coating fluid, it is made up of toner, combustion adjuvant and spice, and the combustion adjuvant accounts for coating
The 1.5%-4% of liquid weight, the spice accounts for the 0.15%-0.3% of coating fluid weight, and the toner is to make by the following method
Standby：
1) add 5-15 times of water boiling and extraction 1-5h by weight in tobacco waste, filter, add by weight in extracting solution
Enter 0.1-2% yeast and 2-8% protease, in 26-32 DEG C of ferment at constant temperature 2-5 days, filter, fermentation liquid is concentrated into relatively close
Spend for 1.06-1.15, then add 2-5 times of 60-90% ethanol by weight in the fermentation liquid after concentration, stand 6-12 hours, take
Ethanol is reclaimed in the supernatant and concentrating under reduced pressure is into clear paste；
2) hot water of 20-50 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, adjust pH
For 9-11, Maillard reaction is carried out under the conditions of 80-100 DEG C, the response time is 4-8 hours, after reaction terminates, reactant liquor is dense
Relative density is reduced to for 1.15-1.2, as toner,
The clear paste, reducing sugar, the weight ratio of aminoacid are followed successively by 1: (5-20): (5-20).
Preferably, the toner is prepared as follows and forms：
1) 10 times of water boiling and extractions 3h are added by weight in tobacco waste, is filtered, added by weight in extracting solution
0.5% yeast and 5% protease, in 30 DEG C of ferment at constant temperature 3 days, filter, and fermentation liquid is concentrated into into relative density for 1.12, then
Add 4 times of 75% ethanol by weight in the fermentation liquid after concentration, stand 8 hours, take the supernatant and reclaim ethanol and reduce pressure dense
Shorten clear paste into；
2) hot water of 30 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, adjusting pH is
10, Maillard reaction is carried out under the conditions of 100 DEG C, the response time is 5 hours, after reaction terminates, reactant liquor is concentrated into relatively
Density is 1.16, as toner.
It is further preferred that the combustion adjuvant is one or more in potassium citrate, sodium citrate, Calcium Carbonate.
It is further preferred that the spice be fenugreck lactone, dihydroactinidiolide, cocoa extract in one kind or
It is various.
The invention has the beneficial effects as follows：
1) present invention with the addition of special toner in tobacco sheet cigarette paper coating fluid, and it is first to carry out enzyme to raw material
Hydrolysis and fermentation so as to have the fragrance component of peculiar flavour, while the macromolecular compounds such as protein therein are degraded to little
Molecule aminoacid and monosaccharide, improve next step Maillard reaction substrate content.More thickness is further produced using Maillard reaction
The distinctive flavor matter of grass, while the brown of Mei Lade products is close with cigar color, its as the natural stain of cigarette paper,
The use of food coloring can be reduced or be substituted, makes product quality safer stable.
2) coating fluid of the invention can be produced in batches, and directly cigarette paper dyeed when using, and method does not receive ring
The impact of the factors such as border, equipment, quality controllable, Color is stable, per the aberration very little criticized.
3) fully, residue is few for Maillard reaction, and Color is uniform, color closely cigar.
4) coating fluid prepared by the present invention can also reduce xylon gas, miscellaneous QI and the oral stimulation of cigarette paper, can increase
The fragrance of reconstituted tobacoo Medicated cigarette, improves effect of smokeing panel test.
Description of the drawings
Fig. 1 is Color figure of the toner of present invention preparation to cigarette paper.
Fig. 2 is Color figure of the common toner to cigarette paper.
Specific embodiment
In order to preferably explain the present invention, below in conjunction with specific embodiment, the present invention is described in further detail, but
They are not construed as limiting to protection scope of the present invention.
Embodiment 1
A kind of tobacco sheet cigarette paper coating fluid, is made up of toner, combustion adjuvant and spice, and the combustion adjuvant accounts for coating fluid
The 2.5% of weight, the spice accounts for the 0.2% of coating fluid weight, and the toner accounts for the 97.3% of coating fluid weight.The tune
Toner is prepared as follows and forms：
1) 10 times of water boiling and extractions 3h are added by weight in tobacco waste, is filtered, added by weight in extracting solution
0.5% yeast and 5% protease, in 30 DEG C of ferment at constant temperature 3 days, filter, and fermentation liquid is concentrated into into relative density for 1.12, then
Add 4 times of 75% ethanol by weight in the fermentation liquid after concentration, stand 8 hours, take the supernatant and reclaim ethanol and reduce pressure dense
Shorten clear paste into；
2) hot water of 30 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, adjusting pH is
10, Maillard reaction is carried out under the conditions of 100 DEG C, the response time is 5 hours, after reaction terminates, reactant liquor is concentrated into relatively
Density is 1.16, as toner.
The reducing sugar be xylose, the aminoacid be glycine, the clear paste, xylose, glycine weight ratio successively
For 1: 7.5: 8.
The combustion adjuvant is potassium citrate.
The spice is fenugreck lactone, dihydroactinidiolide, the mixture of cocoa extract, and its weight ratio is followed successively by
0.5∶0.8∶2。
The cocoa extract is the pressed powder that will be obtained after cocoa powder solvent (such as water or ethanol) extraction, can be passed through
Various commercial sources are obtained.
The preparation method of the tobacco sheet cigarette paper coating fluid is：Combustion adjuvant, spice are added in toner, are stirred
Mix homogeneously.
Embodiment 2
A kind of tobacco sheet cigarette paper coating fluid, is made up of toner, combustion adjuvant and spice, and the combustion adjuvant accounts for coating fluid
The 3% of weight, the spice accounts for the 0.25% of coating fluid weight, and the toner accounts for the 96.75% of coating fluid weight.The tune
Toner is prepared as follows and forms：
1) 5 times of water boiling and extractions 1h are added by weight in tobacco waste, is filtered, added by weight in extracting solution
0.1% yeast and 2% protease, in 26 DEG C of ferment at constant temperature 5 days, filter, and fermentation liquid is concentrated into into relative density for 1.06, then
Add 2 times of 90% ethanol by weight in the fermentation liquid after concentration, stand 6 hours, take the supernatant and reclaim ethanol and reduce pressure dense
Shorten clear paste into；
2) hot water of 20 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, it is 9 to adjust pH,
Maillard reaction is carried out under the conditions of 80 DEG C, the response time is 8 hours, after reaction terminates, reactant liquor is concentrated into into relative density
For 1.15, as toner.
The reducing sugar be xylose, the aminoacid be alanine, the clear paste, xylose, alanine weight ratio successively
For 1: 15: 15.
The combustion adjuvant is sodium citrate.
The spice is fenugreck lactone, the mixture of cocoa extract, and its weight ratio is 1: 2.
Embodiment 3
A kind of tobacco sheet cigarette paper coating fluid, is made up of toner, combustion adjuvant and spice, and the combustion adjuvant accounts for coating fluid
The 4% of weight, the spice accounts for the 0.3% of coating fluid weight, and the toner accounts for the 95.7% of coating fluid weight.The toning
Agent is prepared as follows and forms：
1) 15 times of water boiling and extractions 5h are added by weight in tobacco waste, is filtered, add 2% by weight in extracting solution
Yeast and 8% protease, in 32 DEG C of ferment at constant temperature 2 days, filter, and fermentation liquid is concentrated into into relative density for 1.15, then to dense
Add 5 times of 60% ethanol in fermentation liquid after contracting by weight, stand 12 hours, take the supernatant reclaim ethanol and concentrating under reduced pressure into
Clear paste；
2) hot water of 50 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, adjusting pH is
11, Maillard reaction is carried out under the conditions of 100 DEG C, the response time is 4 hours, after reaction terminates, reactant liquor is concentrated into relatively
Density is 1.2, as toner.
The reducing sugar be glucose, the aminoacid be serine, the clear paste, glucose, the weight ratio of serine
It is followed successively by 1: 10: 14.
The combustion adjuvant is Calcium Carbonate.
The spice is dihydroactinidiolide, the mixture of cocoa extract, and its weight ratio is 1: 1.
Embodiment 4
A kind of tobacco sheet cigarette paper coating fluid, is made up of toner, combustion adjuvant and spice, and the combustion adjuvant accounts for coating fluid
The 2% of weight, the spice accounts for the 0.2% of coating fluid weight, and the toner accounts for the 97.8% of coating fluid weight.The toning
Agent is prepared as follows and forms：
1) 8 times of water boiling and extractions 4h are added by weight in tobacco waste, is filtered, added by weight in extracting solution
1.5% yeast and 4% protease, in 28 DEG C of ferment at constant temperature 4 days, filter, and fermentation liquid is concentrated into into relative density for 1.08, then
Add 3 times of 85% ethanol by weight in the fermentation liquid after concentration, stand 10 hours, take the supernatant and reclaim ethanol and reduce pressure dense
Shorten clear paste into；
2) hot water of 40 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, adjusting pH is
10, Maillard reaction is carried out under the conditions of 95 DEG C, the response time is 7 hours, after reaction terminates, reactant liquor is concentrated into relatively close
Spend for 1.16, as toner.
The reducing sugar be Fructose, the aminoacid be Phenylalanine, the clear paste, Fructose, the weight of Phenylalanine ratio
It is followed successively by 1: 6: 7.
The combustion adjuvant is Calcium Carbonate and sodium citrate, and its weight ratio is 1: 2.
The spice is dihydroactinidiolide.
Embodiment 5
A kind of tobacco sheet cigarette paper coating fluid, is made up of toner, combustion adjuvant and spice, and the combustion adjuvant accounts for coating fluid
The 1.5% of weight, the spice accounts for the 0.15% of coating fluid weight, and the toner accounts for the 98.35% of coating fluid weight.It is described
Toner is prepared as follows and forms：
1) 12 times of water boiling and extractions 2h are added by weight in tobacco waste, is filtered, add 1% by weight in extracting solution
Yeast and 6% protease, in 30 DEG C of ferment at constant temperature 3 days, filter, and fermentation liquid is concentrated into into relative density for 1.1, then to concentration
Add 3 times of 65% ethanol in fermentation liquid afterwards by weight, stand 6 hours, take the supernatant and reclaim ethanol and concentrating under reduced pressure Cheng Qing
Cream；
2) hot water of 30 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, adjusting pH is
11, Maillard reaction is carried out under the conditions of 100 DEG C, the response time is 5 hours, after reaction terminates, reactant liquor is concentrated into relatively
Density is 1.18, as toner.
The reducing sugar be galactose, the aminoacid be lysine, the clear paste, galactose, the weight ratio of lysine
It is followed successively by 1: 5: 5.
The combustion adjuvant is Calcium Carbonate and potassium citrate, and its weight ratio is 2: 1.
The spice is cocoa extract.
Test example：Effect assessment is tested
The coating fluid prepared with embodiment 1-5 is coated to tobacco sheet cigarette paper, and coating fluid accounts for reconstituted tobacoo Medicated cigarette
The 0.5% of paper weight, after being dried, with identical tobacco shred Medicated cigarette is made.The cigarette paper for being prepared with common coating fluid simultaneously is control,
Effect of smokeing panel test is shown in Table 1.
The toner of the present invention of table 1. is smoked panel test the impact of effect to Medicated cigarette
| Feeding quantity | Sensory evaluating smoking's result |
| Embodiment 1 | Aroma quality is lifted, and flue gas harmony is good, and zest substantially reduces, without miscellaneous QI and xylon gas |
| Embodiment 2 | Aroma quality is lifted, and flue gas harmony is good, and zest decreases, without miscellaneous QI and xylon gas |
| Embodiment 3 | Aroma quality is lifted, and flue gas harmony is good, and zest decreases, without miscellaneous QI and xylon gas |
| Embodiment 4 | Aroma quality is lifted, and preferably, zest decreases flue gas harmony, miscellaneous QI and xylon gas are few |
| Embodiment 5 | Aroma quality is lifted, and preferably, zest decreases flue gas harmony, miscellaneous QI and xylon gas are few |
| Common coating fluid | Aroma quality is not lifted, flue gas inaccurate coordination, irritant, there is miscellaneous QI and xylon gas |
It can be seen from the results above that toner prepared by the present invention can be obviously improved the effect of smokeing panel test of Medicated cigarette, from Fig. 1 and
The color contrast of Fig. 2 can be seen that the toner of present invention preparation makes the color of cigarette paper more uniform, immaculate, and colourity is more
Close to cigar.
Claims (2)
1. a kind of tobacco sheet cigarette paper coating fluid, it is characterised in that be made up of toner, combustion adjuvant and spice, the combustion adjuvant
The 1.5%-4% of coating fluid weight is accounted for, the spice accounts for the 0.15%-0.3% of coating fluid weight, and the toner is by following
What method was prepared from：
1) add 5-15 times of water boiling and extraction 1-5h by weight in tobacco waste, filter, add by weight in extracting solution
0.1-2% yeast and 2-8% protease, in 26-32 DEG C of ferment at constant temperature 2-5 days, filter, and fermentation liquid is concentrated into into relative density
For 1.06-1.15, then add 2-5 times of 60-90% ethanol by weight in the fermentation liquid after concentration, stand 6-12 hours, take
Layer clear liquid reclaims ethanol and concentrating under reduced pressure is into clear paste；
2) hot water of 20-50 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, regulation pH is 9-
11, Maillard reaction is carried out under the conditions of 80-100 DEG C, the response time is 4-8 hours, after reaction terminates, reactant liquor is concentrated into
Relative density is 1.15-1.2, as toner,
The clear paste, reducing sugar, the weight ratio of aminoacid are followed successively by 1: (5-20): (5-20)；
The combustion adjuvant is one or more in potassium citrate, sodium citrate, Calcium Carbonate；
The spice is one or more in fenugreck lactone, dihydroactinidiolide, cocoa extract.
2. tobacco sheet cigarette paper coating fluid as claimed in claim 1, it is characterised in that：The toner is by the following method
It is prepared from：
1) 10 times of water boiling and extractions 3h are added by weight in tobacco waste, is filtered, add 0.5% ferment by weight in extracting solution
Female bacterium and 5% protease, in 30 DEG C of ferment at constant temperature 3 days, filter, and fermentation liquid is concentrated into into relative density for 1.12, then to concentration
Add 4 times of 75% ethanol in fermentation liquid afterwards by weight, stand 8 hours, take the supernatant and reclaim ethanol and concentrating under reduced pressure Cheng Qing
Cream；
2) hot water of 30 times of weight is added in clear paste, reducing sugar, aminoacid is added after stirring and dissolving, it is 10 to adjust pH,
Maillard reaction is carried out under the conditions of 100 DEG C, the response time is 5 hours, and after reaction terminates, reactant liquor is concentrated into into relative density is
1.16, as toner.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510332704.3A CN105040518B (en) | 2015-06-16 | 2015-06-16 | Coating liquid for tobacco sheet cigarette paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510332704.3A CN105040518B (en) | 2015-06-16 | 2015-06-16 | Coating liquid for tobacco sheet cigarette paper |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105040518A CN105040518A (en) | 2015-11-11 |
| CN105040518B true CN105040518B (en) | 2017-04-12 |
Family
ID=54447468
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510332704.3A Active CN105040518B (en) | 2015-06-16 | 2015-06-16 | Coating liquid for tobacco sheet cigarette paper |
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| Country | Link |
|---|---|
| CN (1) | CN105040518B (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105349264B (en) * | 2015-12-03 | 2019-05-07 | 河北中烟工业有限责任公司 | A kind of preparation method of Maillard reaction fragrance and its application in cigarette |
| CN106820244A (en) * | 2017-01-23 | 2017-06-13 | 江苏中烟工业有限责任公司 | A kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality |
| CN106962969A (en) * | 2017-05-18 | 2017-07-21 | 山东瑞博斯烟草有限公司 | It is a kind of that the method that tobacco waste prepares reconstruction stem backfill feed liquid is handled by zymotechnic |
| CN107476122A (en) * | 2017-09-22 | 2017-12-15 | 安徽顺彤包装材料有限公司 | A kind of coating fluid of osmanthus fragrance type cigarette lining paper |
| CN108968132B (en) * | 2018-10-09 | 2021-08-03 | 湖北中烟工业有限责任公司 | Preparation method of reconstituted tobacco coating liquid |
| CN112089088A (en) * | 2020-10-16 | 2020-12-18 | 河南中烟工业有限责任公司 | Additive for improving sensory quality of tobacco leaves with poor combustibility and application thereof |
| CN113512306A (en) * | 2021-07-12 | 2021-10-19 | 云南中烟工业有限责任公司 | Dye, preparation method and application thereof |
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| DE10112826C1 (en) * | 2001-03-16 | 2002-10-31 | Reemtsma H F & Ph | Smokable article with a two or more layers wrapping |
| CN102440432B (en) * | 2011-09-08 | 2014-03-19 | 上海烟草集团有限责任公司 | Two-step microorganism fermentation method for preparing tobacco leachate |
| CN102488317B (en) * | 2011-12-23 | 2014-04-09 | 华宝食用香精香料（上海）有限公司 | Biological spice for tobacco and preparation method and use thereof |
| CN102551194A (en) * | 2011-12-30 | 2012-07-11 | 广东中烟工业有限责任公司 | Method of improving fragrance component content of stem extracting solution |
| CN103564645A (en) * | 2012-07-18 | 2014-02-12 | 朱大恒 | Method and application for producing tobacco extracts through field tobacco waste |
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