CN105349264B - A kind of preparation method of Maillard reaction fragrance and its application in cigarette - Google Patents
A kind of preparation method of Maillard reaction fragrance and its application in cigarette Download PDFInfo
- Publication number
- CN105349264B CN105349264B CN201510872153.XA CN201510872153A CN105349264B CN 105349264 B CN105349264 B CN 105349264B CN 201510872153 A CN201510872153 A CN 201510872153A CN 105349264 B CN105349264 B CN 105349264B
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- Prior art keywords
- fragrance
- maillard reaction
- cigarette
- tobacco
- fragrant
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
The invention discloses a kind of preparation method and applications of Maillard reaction fragrance, it is after dissolving sodium carbonate in water, material L- glycine is added, L-threonine and L-PROLINE, after material dissolution, sequentially add material propylene glycol, inverted sugar and cocoa power, then it is warming up to 90~98 DEG C after mixing evenly, 24 hours are stood after being cooled to room temperature, upper liquid is filtered after discarding insoluble matter, after Maillard reaction fragrance prepared by the present invention is used for flue-cured tobacco flavor types cigarette, the vanilla style and features fragrance of cocoa can be covered, it is fragrant to remain baking, nut is fragrant, burnt fragrant and sweet feature, spray the cigarette of Maillard reaction production of flavor prepared by the present invention, through smokeing panel test, do not add the tobacco of the fragrance relatively, fragrance is more plentiful, miscellaneous gas is reduced, irritation reduces, comfort is promoted, sugariness improves.Preparation process is simple, high income, production process is pollution-free, easy to operate, can utilize tobacco productive corporation existing equipment and raw material to greatest extent, it is only necessary to which buying a small amount of reaction raw materials can go into operation.
Description
Technical field
The present invention relates to the applications in flavouring essence for tobacco preparation process and its cigarette.
Background technique
Maillard reaction is the reaction occurred between amino-compound and reduced sugar, is to form tobacco characteristic chicken flavor main
One of source.Tobacco is during modulation, ageing, processing and burning and sucking, all along with different degrees of non enzymatic browning reacton.
Due to containing a large amount of fragrance matter, and most of and cigarette perfume harmony in maillard reaction product, low-grade cigarette can effectively improve
The quality of grass reduces wooden miscellaneous gas, increases cigarette perfume, thus becomes a kind of good tobacco aromaticss.
Tropical industrial crops important in the world can be can be, due to its peculiar flavour with strong fragrance and important battalion
Value is supported, is become one of the world today upper three greatly hobby property beverage (tea, coffee), it is lasting.Cocoa band beans are fragrant, baking is fragrant,
The features such as nut is fragrant, coke is fragrant and sweet, are widely used in food and Cigarette processing industry, and treated, and cocoa can be used for flavouring essence for tobacco,
For being generally used in the flavoring and casing of blended type cigarette.
Since cocoa has significant vanilla style fragrance, generally it is not used in Virginian-type cigarette production, and by
Have in cocoa and increase irritation and remaining characteristic, affects its use value in tobacco.
Summary of the invention
Object of the present invention is to insufficient according to prior art, provide a kind of Maillard reaction fragrance preparation method and its
Application in cigarette is used for Virginian-type cigarette using the maillard reaction thing of this method preparation, fragrant with the vanilla for covering cocoa
Gas feature, retains that baking is fragrant, nut is fragrant, Jiao Tianxiang feature, and with overcome can bring stimulation and persistence characteristic.
Purpose to realize the present invention, the preparation method of this Maillard reaction fragrance is it is characterized in that it includes following step
It is rapid:
A. after sodium carbonate being dissolved in water, material L- glycine, L-threonine and L-PROLINE are sequentially added, then
80~95 DEG C are warming up in stirring；
B. after above-mentioned material dissolution, material propylene glycol, inverted sugar and cocoa power is sequentially added, is then stirred evenly
After heat up；
C. 120~130 minutes are kept the temperature after being warming up to 90~98 DEG C, then naturally cools to after room temperature that stand at least 24 small
When, insoluble matter is then discarded, reaction product Maillard reaction fragrance is made after filtering upper liquid；
The sodium carbonate, water and each weight of material portion rate are as follows: water: sodium carbonate: L- glycine: L-threonine: L- dried meat
Propylhomoserin: propylene glycol: inverted sugar: cocoa power=20~30:2~3:10~15:1~2:1~2:35~50:15~30:2~10.
Application of the Maillard reaction fragrance in cigarette, it is characterised in that by Maillard reaction fragrance obtained above
After being diluted with the softened water that 10~100 volumes are measured again, uniformly it is sprayed on pipe tobacco.
The Maillard reaction fragrance being sprayed on pipe tobacco accounts for the 0.1%~0.5% of tobacco quality.
The technological progress achieved by the present invention:
Using the Maillard reaction fragrance of present invention process preparation for the fragrant pod of cocoa can be covered after flue-cured tobacco flavor types cigarette
Blue style and features fragrance remains baking perfume, nut perfume, Jiao Tianxiang feature, sprays Maillard reaction fragrance prepared by the present invention
The cigarette of production, smokes panel test through professional, and relative to the tobacco for not adding the fragrance, fragrance is more plentiful, and miscellaneous gas is reduced, irritation
It reduces, comfort is promoted, and sugariness improves.Preparation process of the present invention have simple process, high income, production process is pollution-free, behaviour
Make the features such as facilitating, tobacco productive corporation existing equipment and raw material can be utilized to greatest extent, it is only necessary to buy a small amount of reaction raw materials i.e.
It can put into production, application easy to spread.
Specific embodiment
The invention will be further described with reference to embodiments.
Embodiment 1:
A. after 6Kg sodium carbonate being dissolved in 60Kg water in a kettle, in order successively by 30Kg L- glycine, 3Kg L-
Reaction kettle is added in threonine and 3KgL- proline, stirs and is warming up to 80~95 DEG C；
B. after the above-mentioned material of about 10~20min is completely dissolved, then in order successively by 72Kg propylene glycol, 48Kg inverted sugar
Reaction kettle is added with 14Kg cocoa power, stirs evenly, and heat up after recording material gross weight；
C. it is stirred when being warming up to 95 DEG C and keeps the temperature 120 minutes, during which every the primary lost moisture of 30 minutes supplements, so
Supplement loss moisture, stands 24 hours after mixing evenly when naturally cooling to room temperature again afterwards, discards insoluble matter, and filtering upper liquid obtains
To reaction product Maillard reaction fragrance 230Kg, yield 97.5%.
By Maillard reaction fragrance obtained above with 0.1%(weight ratio) on ratio uniform is sprayed at and cuts filler, through special
Industry personnel smoke panel test, which significantly improves not spiced tobacco, flue gas concentration, and miscellaneous gas is reduced, and irritation reduces, sweet tea
Degree improves.
Embodiment 2:
A. after 6Kg sodium carbonate being dissolved in 60Kg water in order in a kettle, in order successively by the sweet ammonia of 24Kg L-
Acid, 4Kg L-threonine, 2Kg L-PROLINE are added in reaction kettle, stir and are warming up to 80~95 DEG C；
B. after the above-mentioned material of about 10~20min is completely dissolved, then in order successively by 90Kg propylene glycol, 40Kg inverted sugar
It is added in reaction kettle, stirs evenly, and heated up after recording material gross weight with 10kg cocoa power；
C. it is stirred when being warming up to 95 DEG C and keeps the temperature 120 minutes, during which every the primary lost moisture of 30 minutes supplements, so
Supplement loss moisture, then stands 24 hours after mixing evenly when naturally cooling to room temperature again afterwards, discards insoluble matter, filters upper layer
Reaction product Maillard reaction fragrance 231Kg, yield 97.9% is made in liquid.
By Maillard reaction fragrance made from the present embodiment with 0.15 %(weight ratio) ratio uniform is sprayed at and cuts filler
On, it smokes panel test through professional, the spice phase is for not spiced tobacco, and flue gas concentration significantly improves, soft exquisiteness, and miscellaneous gas subtracts
Few, pleasant impression improves, and sugariness improves.
Embodiment 3:
A. after 5Kg sodium carbonate being dissolved in 50Kg water in a kettle, in order successively by 25Kg L- glycine, 4Kg L-
Reaction kettle is added in threonine and 2KgL- proline, stirs and is warming up to 80~95 DEG C；
B. after the above-mentioned material of about 10~20min is completely dissolved, then in order successively by 85Kg propylene glycol, 50Kg inverted sugar
Reaction kettle is added with 12Kg cocoa power, stirs evenly, and heat up after recording material gross weight；
C. it is stirred when being warming up to 95 DEG C and keeps the temperature 120 minutes, during which every the primary lost moisture of 30 minutes supplements, so
Supplement loss moisture, stands 24 hours after mixing evenly when naturally cooling to room temperature again afterwards, discards insoluble matter, and filtering upper liquid obtains
To reaction product Maillard reaction fragrance 227Kg, yield 97.4%.
By Maillard reaction fragrance made from the present embodiment with 0.2%(weight ratio) on ratio uniform is sprayed at and cuts filler,
It smokes panel test through professional, which improves not spiced tobacco, flue gas concentration, and miscellaneous gas is reduced, and irritation reduces, remaining
Taste improves, sugariness improves.
The present invention is not limited to the above embodiments, and those skilled in the art's enlightenment according to the present invention does not depart from model of the present invention
The improvement that farmland is made all should be within protection scope of the present invention.
Claims (3)
1. a kind of preparation method of Maillard reaction fragrance, it is characterised in that it the following steps are included:
A. after sodium carbonate being dissolved in water, material L- glycine, L-threonine and L-PROLINE is sequentially added, is then being stirred
80~95 DEG C are warming up in mixing；
B. after above-mentioned material dissolution, material propylene glycol, inverted sugar and cocoa power is sequentially added, is then risen after mixing evenly
Temperature；
C. 120~130 minutes are kept the temperature after being warming up to 90~98 DEG C, then stands at least 24 hours after naturally cooling to room temperature, so
After discard insoluble matter, reaction product Maillard reaction fragrance is made after filtering upper liquid；
The sodium carbonate, water and each weight of material portion rate are as follows: water: sodium carbonate: L- glycine: L-threonine: L-PROLINE:
Propylene glycol: inverted sugar: cocoa power=20~30:2~3:10~15:1~2:1~2:35~50:20~30:2~10.
2. a kind of application of Maillard reaction fragrance as described in claim 1 in cigarette, it is characterised in that be made above-mentioned
The softened water dilution measured again with 10~100 volumes of Maillard reaction fragrance after, be uniformly sprayed on pipe tobacco.
3. application of the Maillard reaction fragrance according to claim 2 in cigarette, it is characterised in that be sprayed on pipe tobacco
Maillard reaction fragrance account for the 0.1%~0.5% of tobacco quality.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510872153.XA CN105349264B (en) | 2015-12-03 | 2015-12-03 | A kind of preparation method of Maillard reaction fragrance and its application in cigarette |
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| CN201510872153.XA CN105349264B (en) | 2015-12-03 | 2015-12-03 | A kind of preparation method of Maillard reaction fragrance and its application in cigarette |
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| Publication Number | Publication Date |
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| CN105349264A CN105349264A (en) | 2016-02-24 |
| CN105349264B true CN105349264B (en) | 2019-05-07 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106343510A (en) * | 2016-08-31 | 2017-01-25 | 王婧婧 | Preparation method of natural preserved plum flavored essence |
| CN106108105B (en) * | 2016-09-21 | 2017-11-03 | 宝可科技（上海）有限公司 | A kind of method that stems of tobacco leaves prepares strong nut note essence |
| CN106820253B (en) * | 2017-01-17 | 2018-02-13 | 浙江中烟工业有限责任公司 | Method that cysteine trace method aqueous phase prepares tobacco aromaticss precursor and products thereof and application |
| CN109222201B (en) * | 2018-09-07 | 2021-09-14 | 云南中烟工业有限责任公司 | Method for preparing baked fragrant reconstituted tobacco through targeted extraction |
| CN114009733A (en) * | 2021-11-15 | 2022-02-08 | 广州百花香料股份有限公司 | Preparation method and application of temperature-resistant cocoa-flavor reactant |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101445766A (en) * | 2008-12-17 | 2009-06-03 | 华宝食用香精香料（上海）有限公司 | Preparation method of cacao flavor, products obtained thereby and usage thereof |
| CN101580757A (en) * | 2009-06-02 | 2009-11-18 | 上海英华香精香料有限公司 | Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method |
| CN104983056A (en) * | 2015-05-19 | 2015-10-21 | 湖北中烟工业有限责任公司 | Preparation method of cocoa black powder cigarette additive and application of cigarette additive in cigarettes made of reconstituted tobacco |
| CN105040518A (en) * | 2015-06-16 | 2015-11-11 | 湖北中烟工业有限责任公司 | Coating liquid for tobacco sheet cigarette paper |
-
2015
- 2015-12-03 CN CN201510872153.XA patent/CN105349264B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101445766A (en) * | 2008-12-17 | 2009-06-03 | 华宝食用香精香料（上海）有限公司 | Preparation method of cacao flavor, products obtained thereby and usage thereof |
| CN101580757A (en) * | 2009-06-02 | 2009-11-18 | 上海英华香精香料有限公司 | Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method |
| CN104983056A (en) * | 2015-05-19 | 2015-10-21 | 湖北中烟工业有限责任公司 | Preparation method of cocoa black powder cigarette additive and application of cigarette additive in cigarettes made of reconstituted tobacco |
| CN105040518A (en) * | 2015-06-16 | 2015-11-11 | 湖北中烟工业有限责任公司 | Coating liquid for tobacco sheet cigarette paper |
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| CN105349264A (en) | 2016-02-24 |
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