CN106820244A - A kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality - Google Patents
A kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality Download PDFInfo
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- CN106820244A CN106820244A CN201710049114.9A CN201710049114A CN106820244A CN 106820244 A CN106820244 A CN 106820244A CN 201710049114 A CN201710049114 A CN 201710049114A CN 106820244 A CN106820244 A CN 106820244A
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- Prior art keywords
- extracting solution
- stem extracting
- reconstituted tobaccos
- suction quality
- papermaking
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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Abstract
The invention provides a kind of method that modified stem extracting solution is used to improve papermaking-method reconstituted tobaccos suction quality, comprise the following steps:Stem extracting solution is taken, sugar and amino acid is separately added into, the pH value of appropriate ammoniacal liquor regulation system is added, reaction promoter is added, after stirring and evenly mixing, after being heated to uniform temperature reaction 2 hours, cooled down stand-by;The mixed liquor for obtaining will be reacted to be used as substrate coating fluid, described reaction temperature is 114 DEG C.Present invention firstly provides the chemical composition that chemical modification stem extracting solution improves stem extracting solution, the method for improving papermaking-method reconstituted tobaccos suction quality;Reaction temperature of the invention is the key point of reaction, and the reactant species and ratio obtained when temperature is too low or too high are completely different, only selects the suitable reaction temperature could be so that product obstruct the suction quality of liquid modification liquid improvement thin slice.
Description
Technical field
The invention belongs to papermaking-method reconstituted tobaccos production technical field, improved more particularly to a kind of modified stem extracting solution
The method of papermaking-method reconstituted tobaccos suction quality.
Background technology
Offal is the accessory substance of flue-cured tobacco beating and double roasting, as fillings such as expanded cut stem, stalk piece, granule peduncles generally in cigarette
The raw material of material, it is main in papermaking-method reconstituted tobaccos production that fiber is provided.Offal is being taken out due to structure and chemical composition
Inhale in quality and there is certain defect so that reconstituted tobacco has that excitant is larger.
, it is necessary to be extracted to raw materials such as offal, offals with water in papermaking-method reconstituted tobaccos technique.Wherein offal extract solution
In subsequent handling, in the way of coating fluid, addition manufacture paper with pulp after reconstituted tobacco substrate in.But stem extracting solution is for again
When making tobacco leaf, because protein, pectin, organic acid and some other flavor component and tobacco leaf have difference in offal, its
Contained flavor component species is few, and content is low, produce reconstituted tobacco excitant it is larger the problems such as, cause offal process during
The a large amount of extract solution application effects for producing are not good, or even cannot use, and are rejected.In consideration of it, the present invention passes through chemical modification cigarette
Stalk extract solution improves the chemical composition of stem extracting solution, reduces xylon gas and the excitant of papermaking-method reconstituted tobaccos, to ensure to produce
The suction quality of product, and by recycling the production cost of stem extracting solution reduction papermaking-method reconstituted tobaccos, improve economic effect
Benefit.
The content of the invention
It is an object of the invention to provide a kind of chemical composition for improving stem extracting solution by chemical modification stem extracting solution,
The method for improving papermaking-method reconstituted tobaccos suction quality.
Technical scheme is as follows:
A kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality, comprises the following steps:
Stem extracting solution is taken, sugar and amino acid is separately added into, the pH value of appropriate ammoniacal liquor regulation system is added, reaction promoter is added,
After stirring and evenly mixing, after being heated to uniform temperature reaction 2 hours, cool down stand-by;The mixed liquor for obtaining will be reacted to be coated with as substrate
Liquid is used, and described reaction temperature is 114 DEG C.
Described sugar is selected from glucose, fructose or sucrose, and described amino acid is selected from arginine, glycine, glutamic acid, color
Propylhomoserin, proline, leucine or lysine.
Described sugar and the amount ratio of the material of amino acid are (4-6):4;, the quality of the sugar is stem extracting solution weight
5%-15%.
The pH value of described reaction system is 6~7.
Described reaction promoter is propane diols, 1,3-BDO, glycerine or polyethylene glycol.
Described reaction promoter is 3~3.5 with the volume ratio of offal liquid:1.
Beneficial effects of the present invention:Present invention firstly provides the change that chemical modification stem extracting solution improves stem extracting solution
Composition is learned, the method for improving papermaking-method reconstituted tobaccos suction quality;Reaction temperature of the invention is the key point of reaction, works as temperature
The reactant species and ratio obtained when too low or too high are completely different, only select suitable reaction temperature to cause instead
Product is answered to obstruct the suction quality that liquid modification liquid improves thin slice;Operation is simple for the inventive method, and raw material is extensive, low cost
It is honest and clean, the excitant of papermaking-method reconstituted tobaccos can be significantly reduced, the utilization rate of offal is improved, be conducive to improving the economic effect of enterprise
Benefit.
Specific embodiment
In the present invention, the preparation process of stem extracting solution is as follows, takes appropriate offal, with a certain proportion of warm water as medium
(water is 7 with the weight ratio of offal:1) Extracting temperature and time (60 degrees Celsius of temperature, more than 20 minutes time), are controlled, is passed through
Reflux type extracts the composition in offal, then by centrifugation DDGS and insoluble matter, makes finally by heating evaporation molten
Liquid is concentrated, and obtains stem extracting solution (concentration about 1.2g/ml).
Embodiment 1
In the three-necked bottle of 250ml, 20ml stem extracting solutions are added, be separately added into the glucose and 4.4mmol of 6.7mmol
Arginine, the pH value for adding appropriate ammoniacal liquor regulation system is 6, then adds the propane diols of 70ml, and 114 DEG C of stirring condensing refluxes are anti-
After answering 2 hours, cool down stand-by.
The offal modification liquid of gained and unmodified offal solution are coated on according to identical spreading rate paper-making method reconstructed
In tobacco leaf substrate, aesthetic quality comparative evaluation is carried out.Find to apply modified offal after being aspirated through professional tobacco sense organ judging panel
The excitant of papermaking-method reconstituted tobaccos and xylon gas etc. are decreased obviously after extract solution, and total quality compares balance.
The stem extracting solution of table 1 before modified after papermaking-method reconstituted tobaccos sense organ evaluating meter
Embodiment 2
In the three-necked bottle of 250ml, 20ml stem extracting solutions are added, be separately added into the glucose and 8mmol of 10mmol
Tryptophan, the pH value for adding appropriate ammoniacal liquor regulation system is 6, then adds the propane diols of 60ml, 114 DEG C of stirring condensing reflux reactions
After 2 hours, cool down stand-by.
The offal modification liquid of gained and unmodified offal solution are coated on according to identical spreading rate paper-making method reconstructed
In tobacco leaf substrate, aesthetic quality comparative evaluation is carried out.Find to apply modified offal after being aspirated through professional tobacco sense organ judging panel
The excitant of papermaking-method reconstituted tobaccos and xylon gas etc. are decreased obviously after extract solution, and total quality compares balance.
The stem extracting solution of table 2 before modified after papermaking-method reconstituted tobaccos sense organ evaluating meter
Embodiment 3
In the three-necked bottle of 250ml, 20ml stem extracting solutions are added, be separately added into the glucose and 20mmol of 20mmol
Lysine, the pH value for adding appropriate ammoniacal liquor regulation system is 7, then adds the propane diols of 60ml, 114 DEG C of stirring condensing reflux reactions
After 2 hours, cool down stand-by.
The offal modification liquid of gained and unmodified offal solution are coated on according to identical spreading rate paper-making method reconstructed
In tobacco leaf substrate, aesthetic quality comparative evaluation is carried out.Find to apply modified offal after being aspirated through professional tobacco sense organ judging panel
The excitant of papermaking-method reconstituted tobaccos and xylon gas etc. are decreased obviously after extract solution, and total quality compares balance.
The stem extracting solution of table 3 before modified after papermaking-method reconstituted tobaccos sense organ evaluating meter
The above embodiment of the present invention is only intended to clearly illustrate example of the present invention, not to reality of the invention
Apply the restriction of mode.For those of ordinary skill in the field, other can also be made on the basis of the above description
The change or variation of multi-form.Here all of implementation method cannot be exhaustive.It is every to belong to technical side of the invention
Obvious change that case is extended out changes row still in protection scope of the present invention.
Claims (6)
1. a kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality, it is characterised in that including
Following steps:Stem extracting solution is taken, sugar and amino acid is separately added into, the pH value of appropriate ammoniacal liquor regulation system is added, added
Reaction promoter, after stirring and evenly mixing, after being heated to uniform temperature reaction 2 hours, cools down stand-by;To react the mixed liquor that obtains as
Substrate coating fluid is used, and described reaction temperature is 114 DEG C.
2. modified stem extracting solution according to claim 1 is used for the method for improving papermaking-method reconstituted tobaccos suction quality,
Characterized in that, described sugar is selected from glucose, fructose or sucrose, described amino acid is selected from arginine, glycine, paddy ammonia
Acid, tryptophan, proline, leucine or lysine.
3. modified stem extracting solution according to claim 1 is used for the method for improving papermaking-method reconstituted tobaccos suction quality,
Characterized in that, the amount ratio of the material of described sugar and amino acid is(4-6):4, the quality of the sugar is stem extracting solution weight
5%-15%.
4. modified stem extracting solution according to claim 1 is used for the method for improving papermaking-method reconstituted tobaccos suction quality,
Characterized in that, the pH value of described reaction system is 6 ~ 7.
5. modified stem extracting solution according to claim 1 is used for the method for improving papermaking-method reconstituted tobaccos suction quality,
Characterized in that, described reaction promoter is propane diols, 1,3-BDO, glycerine or polyethylene glycol.
6. modified stem extracting solution according to claim 1 is used for the method for improving papermaking-method reconstituted tobaccos suction quality,
Characterized in that, described reaction promoter is 3 ~ 3.5 with the volume ratio of offal liquid:1.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108113047A (en) * | 2017-12-20 | 2018-06-05 | 江苏中烟工业有限责任公司 | It is a kind of to be used to improve the method that the high pressure of thin section for tobacco quality is modified stem extracting solution |
CN108125272A (en) * | 2017-12-13 | 2018-06-08 | 江西中烟工业有限责任公司 | A kind of preparation method of papermaking-method reconstituted tobaccos |
CN108420104A (en) * | 2018-03-28 | 2018-08-21 | 江苏中烟工业有限责任公司 | A method of reducing crotonaldehyde and ammonia in cigarette mainstream flue gas using offal |
CN108477662A (en) * | 2018-04-11 | 2018-09-04 | 湖北中烟工业有限责任公司 | A kind of manufacturing process of burley tobaccos characteristic reconstituted tobacco |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN108125272A (en) * | 2017-12-13 | 2018-06-08 | 江西中烟工业有限责任公司 | A kind of preparation method of papermaking-method reconstituted tobaccos |
CN108125272B (en) * | 2017-12-13 | 2020-05-22 | 江西中烟工业有限责任公司 | Preparation method of paper-making reconstituted tobacco |
CN108113047A (en) * | 2017-12-20 | 2018-06-05 | 江苏中烟工业有限责任公司 | It is a kind of to be used to improve the method that the high pressure of thin section for tobacco quality is modified stem extracting solution |
CN108420104A (en) * | 2018-03-28 | 2018-08-21 | 江苏中烟工业有限责任公司 | A method of reducing crotonaldehyde and ammonia in cigarette mainstream flue gas using offal |
CN108477662A (en) * | 2018-04-11 | 2018-09-04 | 湖北中烟工业有限责任公司 | A kind of manufacturing process of burley tobaccos characteristic reconstituted tobacco |
CN108477662B (en) * | 2018-04-11 | 2020-07-24 | 湖北中烟工业有限责任公司 | Manufacturing process of reconstituted tobacco with burley tobacco characteristics |
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Application publication date: 20170613 |