CN108125272B - Preparation method of paper-making reconstituted tobacco - Google Patents
Preparation method of paper-making reconstituted tobacco Download PDFInfo
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- CN108125272B CN108125272B CN201711324768.4A CN201711324768A CN108125272B CN 108125272 B CN108125272 B CN 108125272B CN 201711324768 A CN201711324768 A CN 201711324768A CN 108125272 B CN108125272 B CN 108125272B
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- slurry
- reconstituted tobacco
- paper
- solid
- pectinase
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
Abstract
The invention provides a preparation method of paper-making reconstituted tobacco, which comprises the following steps: mixing and crushing tobacco stems, tea leaf residues and rhizoma atractylodis, soaking the mixture in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry to obtain slurry, adding glucose oxidase and pectinase into the slurry, fermenting for 12-72 hours, putting the slurry into a sheet-making machine to obtain a sheet base, adding propylene glycol and proline into the extracting solution, concentrating to obtain a coating liquid, coating the coating liquid on the sheet base, and drying to obtain the reconstituted tobacco leaves by a paper-making method.
Description
Technical Field
The invention belongs to the technical field of reconstituted tobacco, and particularly relates to a preparation method of reconstituted tobacco by a paper-making method.
Background
The reconstituted tobacco is also called recombined tobacco, tobacco sheets, homogenized tobacco and the like, and the reconstituted tobacco is prepared by recycling tobacco stems, tobacco levels, tobacco powder and the like serving as main raw materials. The paper-making reconstituted tobacco is one of important formulas in cigarette formulas, is used as an effective auxiliary material for reducing harm and tar of cigarettes, and is mixed in the cigarette formula in a use ratio of 15-30%.
The authorization number CN 105661621B discloses a preparation method of reconstituted tobacco by a full-stem paper-making method, the raw materials of the reconstituted tobacco completely adopt stems, the cost of the raw materials is reduced, but the cigarette prepared from the reconstituted tobacco has poor taste, and the content of harmful substances in smoke is high. Application number 201010524106.3 discloses a method for reducing the carbon monoxide release amount of paper-making reconstituted tobacco, which aims to reduce the carbon monoxide release amount by adding alkali metal inorganic salt, but the reduction range is small, and the problem of high carbon monoxide content in smoke cannot be solved. The No. CN103251125B discloses a manufacturing method of a high-quality functional paper-making reconstituted tobacco, which carries out biological enzyme treatment during preparation of reconstituted tobacco pulp so as to complete tobacco cellulose, simultaneously reduces the content of protein and pectin in the pulp, is beneficial to the production of sheets, and has higher content of harmful substances in the obtained cigarette smoke.
Disclosure of Invention
In order to overcome the defects in the prior art, the invention provides a preparation method of paper-making reconstituted tobacco.
The technical scheme adopted by the invention is as follows: a preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing tobacco stem, tea leaf residue and rhizoma Atractylodis, mincing, soaking in water, extracting to obtain solid and extractive solution, and grinding the solid into slurry to obtain slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 12-72 hours, and placing the slurry into a sheet making machine to obtain a sheet base;
(3) adding propylene glycol and proline into the extracting solution, and concentrating to obtain a coating liquid;
(4) coating the coating liquid on the base sheet, and drying to obtain the paper-making reconstituted tobacco.
Further, the mass ratio of the tobacco stems, the tea leaves and the rhizoma atractylodis in the step (1) is 10-20: 2-5.
Further, the grinding degree of the ground pulp in the step (1) is 25-30 DEG SR.
Further, the total mass of the glucose oxidase and the pectinase in the step (2) is 0.5-1% of the mass of the pulp, and the mass ratio of the glucose oxidase to the pectinase is 1: 3.
Further, the fermentation temperature in the step (2) is 30-60 ℃.
Further, in the step (3), the total mass of the propylene glycol and the proline is 10-20% of the extracting solution, and the mass ratio of the propylene glycol to the proline is 1: 1.
Compared with the prior art, the invention has the beneficial effects that:
(1) the tobacco stems, the tea leaves and the rhizoma atractylodis are selected as raw materials, so that the sensory quality of the prepared cigarette can be effectively improved, and harmful substances in smoke can be reduced;
(2) the glucose oxidase and the pectinase are added for fermentation before the base sheet is prepared, so that harmful substances in the smoke of the prepared cigarette can be greatly reduced;
(3) the sensory quality of the prepared cigarette can be further improved by the propylene glycol and the proline.
Detailed Description
The present invention will be described in further detail with reference to examples.
Example 1
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis in a mass ratio of 10:10:2, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 25 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 12 hours, wherein the total mass of the glucose oxidase and the pectinase is 0.5 percent of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 30 ℃, and after the fermentation is finished, placing the slurry into a sheet-making machine to obtain a sheet base;
(3) adding propylene glycol and proline into the extracting solution, wherein the total mass of the propylene glycol and the proline is 10% of the extracting solution, and the mass ratio is 1:1, and concentrating to obtain a coating liquid;
(4) coating the coating liquid on the base sheet, and drying to obtain the paper-making reconstituted tobacco.
Example 2
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis in a mass ratio of 20:20:5, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 30 DEG SR, and thus obtaining slurry;
steps (2), (3) and (4) were the same as in example 1.
Example 3
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
steps (2), (3) and (4) were the same as in example 1.
Comparative example 1
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) crushing tobacco stems, soaking the tobacco stems in water, extracting to obtain solid and extracting solution, polishing the solid into slurry with the polishing degree of 27 DEG SR to obtain slurry;
steps (2), (3) and (4) were the same as in example 1.
Comparative example 2
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems and tea leaves, wherein the mass ratio of the tobacco stems to the tea leaves is 18:13, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, and grinding the slurry to obtain slurry with the grinding degree of 27 DEG SR;
steps (2), (3) and (4) were the same as in example 1.
Example 4
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 72 hours, wherein the total mass of the glucose oxidase and the pectinase is 1% of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 60 ℃, and after fermentation, placing the slurry into a sheet making machine to obtain a sheet base;
steps (3) and (4) were the same as in example 1.
Example 5
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 58 hours, wherein the total mass of the glucose oxidase and the pectinase is 0.6 percent of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 55 ℃, and after the fermentation is finished, placing the slurry into a sheet-making machine to obtain a sheet base;
steps (3) and (4) were the same as in example 1.
Comparative example 3
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) putting the slurry into a sheet making machine to obtain a sheet base;
steps (3) and (4) were the same as in example 1.
Comparative example 4
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding pectinase into the pulp, fermenting for 58 hours, wherein the mass of the pectinase is 0.6 percent of the mass of the pulp, the fermentation temperature is 55 ℃, and after the fermentation is finished, placing the pulp into a sheet-making machine to obtain a sheet base;
steps (3) and (4) were the same as in example 1.
Example 6
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 58 hours, wherein the total mass of the glucose oxidase and the pectinase is 0.6 percent of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 55 ℃, and after the fermentation is finished, placing the slurry into a sheet-making machine to obtain a sheet base;
(3) adding propylene glycol and proline into the extracting solution, wherein the total mass of the propylene glycol and the proline is 20% of the extracting solution, and the mass ratio is 1:1, and concentrating to obtain a coating liquid;
step (4) was the same as in example 1.
Example 7
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 58 hours, wherein the total mass of the glucose oxidase and the pectinase is 0.6 percent of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 55 ℃, and after the fermentation is finished, placing the slurry into a sheet-making machine to obtain a sheet base;
(3) adding propylene glycol and proline into the extracting solution, wherein the total mass of the propylene glycol and the proline is 17% of the extracting solution, and the mass ratio is 1:1, and concentrating to obtain a coating liquid;
step (4) was the same as in example 1.
Comparative example 5
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 58 hours, wherein the total mass of the glucose oxidase and the pectinase is 0.6 percent of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 55 ℃, and after the fermentation is finished, placing the slurry into a sheet-making machine to obtain a sheet base;
(3) adding propylene glycol into the extracting solution, wherein the total mass of the propylene glycol accounts for 17% of the extracting solution, and concentrating to obtain a coating liquid;
step (4) was the same as in example 1.
Comparative example 6
A preparation method of paper-making reconstituted tobacco comprises the following steps:
(1) mixing and crushing tobacco stems, tea leaves and rhizoma atractylodis according to the mass ratio of 18:13:3, soaking in water, extracting to obtain a solid and an extracting solution, grinding the solid into slurry, wherein the grinding degree is 27 DEG SR, and thus obtaining slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 58 hours, wherein the total mass of the glucose oxidase and the pectinase is 0.6 percent of the mass of the slurry, the mass ratio is 1:3, the fermentation temperature is 55 ℃, and after the fermentation is finished, placing the slurry into a sheet-making machine to obtain a sheet base;
(3) adding ethanol into the extracting solution, wherein the total mass of the ethanol is 17% of the extracting solution, and concentrating to obtain a coating liquid;
step (4) was the same as in example 1.
The contents of tar, CO and nicotine were measured and the sensory qualities of the cigarettes produced from the reconstituted tobaccos obtained in the above examples and comparative examples were evaluated, and the results are shown in tables 1 and 2.
As shown in tables 1 and 2, the tobacco stems, the tea leaves and the rhizoma atractylodis are selected as raw materials, so that the sensory quality of the prepared cigarettes can be effectively improved, and harmful substances in smoke can be reduced; the glucose oxidase and the pectinase are added for fermentation before the base sheet is prepared, so that harmful substances in the smoke of the prepared cigarette can be greatly reduced; the sensory quality of the prepared cigarette can be further improved by the propylene glycol and the proline. The content of tar, CO and nicotine in the smoke of the example 7 is respectively reduced by 41.0%, 35.5% and 35.7% compared with the smoke of the comparative example 1, and is respectively reduced by 36.1%, 22.3% and 18.2% compared with the smoke of the comparative example 3.
TABLE 1
| Grouping | Sweet taste (0 to 5) | Sour taste (0 to 5) | Bitter taste (0 &)5) | Cool taste (0 to 5) |
| Comparative example 1 | 3.3 | 3.0 | 0 | 3.2 |
| Comparative example 3 | 2.6 | 2.2 | 0 | 2.9 |
| Example 7 | 3.9 | 3.6 | 0 | 3.7 |
TABLE 2
| Grouping | Tar (mg/count) | CO (mg/count) | Nicotine (mg/count) |
| Example 1 | 5.9 | 10.3 | 1.09 |
| Example 2 | 5.8 | 11.0 | 1.14 |
| Example 3 | 5.1 | 9.8 | 0.95 |
| Comparative example 1 | 7.8 | 13.5 | 1.26 |
| Comparative example 2 | 7.2 | 11.8 | 1.13 |
| Example 4 | 5.5 | 10.5 | 1.04 |
| Example 5 | 5.0 | 9.3 | 0.87 |
| Comparative example 3 | 7.2 | 11.2 | 0.99 |
| Comparative example 4 | 6.8 | 10.4 | 0.92 |
| Example 6 | 5.3 | 9.4 | 0.95 |
| Example 7 | 4.6 | 8.7 | 0.81 |
| Comparative example 5 | 5.8 | 9.4 | 0.92 |
| Comparative example 6 | 6.4 | 10.1 | 1.16 |
In light of the foregoing description of the preferred embodiment of the present invention, it is to be understood that various changes and modifications may be made by one skilled in the art without departing from the spirit and scope of the invention. The technical scope of the present invention is not limited to the content of the specification, and must be determined according to the scope of the claims.
Claims (3)
1. The preparation method of the paper-making reconstituted tobacco is characterized by comprising the following steps:
(1) mixing tobacco stem, tea leaf residue and rhizoma Atractylodis, mincing, soaking in water, extracting to obtain solid and extractive solution, and grinding the solid into slurry to obtain slurry;
(2) adding glucose oxidase and pectinase into the slurry, fermenting for 12-72 hours, and placing the slurry into a sheet making machine to obtain a sheet base;
(3) adding propylene glycol and proline into the extracting solution, and concentrating to obtain a coating liquid;
(4) coating the coating liquid on the film base, and drying to obtain the paper-making reconstituted tobacco;
the mass ratio of the tobacco stems, the tea leaves and the rhizoma atractylodis in the step (1) is 10-20: 2-5;
the total mass of the glucose oxidase and the pectinase in the step (2) is 0.5-1% of the mass of the pulp, and the mass ratio of the glucose oxidase to the pectinase is 1: 3;
in the step (3), the total mass of the propylene glycol and the proline is 10-20% of the extracting solution, and the mass ratio of the propylene glycol to the proline is 1: 1.
2. The method for preparing reconstituted tobacco through a papermaking method according to claim 1, wherein the grinding degree of the ground pulp in the step (1) is 25-30 ° SR.
3. The method for preparing reconstituted tobacco leaves through a papermaking method according to claim 1, wherein the fermentation temperature in the step (2) is 30-60 ℃.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711324768.4A CN108125272B (en) | 2017-12-13 | 2017-12-13 | Preparation method of paper-making reconstituted tobacco |
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| CN108125272B true CN108125272B (en) | 2020-05-22 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109430926A (en) * | 2018-10-12 | 2019-03-08 | 武汉醉吟茶品茶业科技有限公司 | A kind of preparation method for cigarette sifting tea |
| CN113080504A (en) * | 2021-03-30 | 2021-07-09 | 福建中烟工业有限责任公司 | Method for simultaneously carrying out enzymolysis and alcoholization on reconstituted tobacco, reconstituted tobacco and application thereof |
| CN113995157B (en) * | 2021-11-19 | 2023-04-18 | 贵州省烟草公司遵义市公司 | Method for preparing reconstituted tobacco by adopting paper-making method after fresh tobacco is smashed, pulped, oxygen-supplying and temperature-supplying fermentation |
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|---|---|---|---|---|
| US3513857A (en) * | 1967-12-26 | 1970-05-26 | Philip Morris Inc | Process for the treatment of tobacco stems |
| CN1957777A (en) * | 2006-11-22 | 2007-05-09 | 厦门卷烟厂 | Method for preparing slices reconstituted from tea, and application in tobacco product |
| CN101283837A (en) * | 2008-05-20 | 2008-10-15 | 云南瑞升烟草技术（集团）有限公司 | Cigarette flavouring process, flavouring reconstruction tobacco and preparation method thereof |
| CN105326086A (en) * | 2015-11-25 | 2016-02-17 | 红云红河烟草(集团)有限责任公司 | Method for increasing body and sweet fragrance of tobacco flake by utilizing complex enzyme preparation |
| CN106820244A (en) * | 2017-01-23 | 2017-06-13 | 江苏中烟工业有限责任公司 | A kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality |
-
2017
- 2017-12-13 CN CN201711324768.4A patent/CN108125272B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3513857A (en) * | 1967-12-26 | 1970-05-26 | Philip Morris Inc | Process for the treatment of tobacco stems |
| CN1957777A (en) * | 2006-11-22 | 2007-05-09 | 厦门卷烟厂 | Method for preparing slices reconstituted from tea, and application in tobacco product |
| CN101283837A (en) * | 2008-05-20 | 2008-10-15 | 云南瑞升烟草技术（集团）有限公司 | Cigarette flavouring process, flavouring reconstruction tobacco and preparation method thereof |
| CN105326086A (en) * | 2015-11-25 | 2016-02-17 | 红云红河烟草(集团)有限责任公司 | Method for increasing body and sweet fragrance of tobacco flake by utilizing complex enzyme preparation |
| CN106820244A (en) * | 2017-01-23 | 2017-06-13 | 江苏中烟工业有限责任公司 | A kind of modified stem extracting solution is used for the method for improving papermaking-method reconstituted tobaccos suction quality |
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