CN111000278A - Method for improving quality of paper-making reconstituted tobacco products - Google Patents
Method for improving quality of paper-making reconstituted tobacco products Download PDFInfo
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- CN111000278A CN111000278A CN201911403652.9A CN201911403652A CN111000278A CN 111000278 A CN111000278 A CN 111000278A CN 201911403652 A CN201911403652 A CN 201911403652A CN 111000278 A CN111000278 A CN 111000278A
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- tobacco
- powder
- reconstituted tobacco
- reconstituted
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention aims to provide a method for improving the quality of paper-making reconstituted tobacco products, which comprises the following steps: (1) grinding a tobacco raw material into powder by using a grinding machine, wherein the particle size distribution is 200-400 meshes, and the tobacco raw material is selected from sheet tobacco, cut tobacco, tobacco powder and tobacco stems; (2) taking 1-10 parts by weight of amino acid, 10 parts by weight of aldose and 5-40 parts by weight of tobacco powder obtained in the step 1), dissolving propylene glycol and water in a weight part ratio of 1: 1-10 to obtain a solution, adjusting the pH value to 7-8, pouring the solution into a Maillard reaction bottle, carrying out Maillard reaction at 60-130 ℃ for 6-10 hours, and standing for later use; (3) adding the Maillard reactant into the reconstituted tobacco coating liquid; the weight proportion of the added Maillard reactants is 5-20%; (4) and (4) coating the coating liquid in the step (3) on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, and finally slicing to prepare a reconstituted tobacco finished product.
Description
Technical Field
The invention relates to the field of paper-making reconstituted tobacco, in particular to a method for improving the quality of paper-making reconstituted tobacco products by adopting tobacco raw materials as Maillard reactant carriers.
Background
The reconstituted tobacco is a sheet or filiform regenerated product prepared from waste tobacco materials such as tobacco powder, tobacco stems, tobacco shreds and the like in the cigarette making process as raw materials and used as cigarette filler. The reconstituted tobacco originated in the 50 th of the 20 th century, and the development of the reconstituted tobacco goes through 3 stages of a rolling method, a thick pulp method and a paper making method. Compared with the tobacco leaves reproduced by the roller pressing method and the thick paste method which are produced at present, the tobacco leaves reproduced by the paper-making method have unique advantages, including small density and high filling value; the mechanical processing resistance is good, and the filament forming rate is high; the combustion speed is high, and the tar release amount is low; good product plasticity and the like. At present, the processes adopted by various production enterprises are slightly different, and basically, a typical two-step method is slightly improved, stems and powder are extracted by water, the extracted tobacco powder and the tobacco stems are mixed and pulped, the pulp is sent to a paper machine for making and forming, two kinds of extraction liquid are prepared, mixed and coated on a sheet base after being treated by means of concentration and the like. The main procedures comprise raw material pretreatment, extraction, concentration, pulping, papermaking, coating, post-treatment and the like.
Although the proper amount of reconstituted tobacco is added into the cigarette, the raw materials of the tobacco leaves can be saved to the maximum extent, and the cost of the cigarette is effectively reduced; on the other hand, the physical properties and chemical components of the cigarette can be adjusted and improved to a certain extent according to the will or requirements of people, thereby being beneficial to improving the internal quality of the cigarette. However, compared with the traditional cut tobacco, the taste still has certain problems, the most obvious expression is that the wood gas is obvious, the irritation is difficult to cover, and therefore, the adding proportion is not high generally. Compared with the paper-making process and quality at home and abroad (tobacco science and technology, 2002), Chenzhuanggang and the like find that the imported sheets have lighter wood gas, certain tobacco original fragrance, smaller irritation and slightly paper flavor, and are relatively poor in domestic production; the content of important aroma components in the imported slices is obviously higher than that of the domestic slices. The results of the research on the release amount of main harmful substances in the smoke of the domestic and international paper-making tobacco sheets and the evaluation on the harmfulness of the smoke (modern scientific instruments 2010) show that the domestic paper-making tobacco sheets have a high CO/tar ratio and relatively low release amounts of phenol, ammonia and NNK, and the imported products show that the release amounts of benzo [ a ] pyrene and CO are low. It can be said that the domestic reconstituted tobacco leaves are not much different from foreign tobacco leaves in the tar and harm reducing technology, but have a certain difference from foreign tobacco leaves in the internal smoking quality.
The Maillard reaction has various species and different fragrance, and is widely applied to tobacco products as a flavoring agent. Usually, it can be obtained by selecting an appropriate reaction substrate, and controlling the reaction conditions, reaction time and reaction environment. The tar content is not obviously increased after the reactants are added, and adverse effects on the taste and other qualities are not brought. The tobacco powder as the leftover material of common cigarette enterprises has the characteristic of more sufficient aroma compared with tobacco stems, and the morphological particles can be ground into powder, so the tobacco powder is a good tobacco natural aroma substance carrier. Based on the characteristics, how to improve the use efficiency of the tobacco powder so as to improve the sensory quality of the reconstituted tobacco is very important. Therefore, the invention firstly considers that the tobacco raw material is ground into powder, then the tobacco powder and the reaction raw materials such as amino acid, sugar and the like are subjected to Maillard reaction, and finally the tobacco powder suspension loaded with Maillard reaction products is coated on the reconstituted tobacco substrate. The method for improving the quality of the paper-making reconstituted tobacco products by adopting the tobacco raw materials as the Maillard reactant carrier provides reference for domestic research and development of reconstituted tobacco and improvement of sensory quality.
Disclosure of Invention
The invention aims to provide a method for improving the quality of paper-making reconstituted tobacco products by adopting a tobacco raw material as a Maillard reactant carrier, which is used for improving the sensory quality of reconstituted tobacco in the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides a method for improving the quality of paper-making reconstituted tobacco products, which comprises the following steps:
(1) grinding a tobacco raw material into powder by using a grinding machine, wherein the particle size distribution is 200-400 meshes, and the tobacco raw material is selected from at least one of sheet tobacco, cut tobacco, tobacco powder and tobacco stems;
the mesh number of the screen is 200 meshes and 400 meshes;
the tobacco powder is powder which passes through a 200-mesh screen and does not pass through a 400-mesh screen, the particle size distribution range is 200-400 meshes, the particle size is too large, the tobacco powder is not uniform in coating, and the smoking taste is influenced; the particle size is too small, and the particles are easy to permeate the substrate and cause loss during coating.
(2) Taking 1-10 parts by weight of amino acid, 10 parts by weight of aldose and 5-40 parts by weight of tobacco powder obtained in the step (1), dissolving propylene glycol and water in a weight part ratio of 1: 1-10 to obtain a solution, adjusting the pH value to 7-8, pouring the solution into a Maillard reaction bottle, carrying out Maillard reaction at 60-130 ℃ for 6-10 hours, and standing for later use;
(3) adding the Maillard reactant in the step (2) into a reconstituted tobacco coating liquid; the weight proportion of the added Maillard reactants is 5-20%;
(4) and (4) coating the coating liquid in the step (3) on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, and finally slicing to prepare a reconstituted tobacco finished product.
Preferably, the tobacco raw material is ground into powder by a grinding machine, and the powder is completely sieved by a 200-mesh sieve, and the particle size distribution is 200-400 meshes.
Further preferably, the amino acid is at least one selected from lysine, phenylalanine, cysteine, valine and glycine; the aldose is fructose and/or glucose.
In some embodiments of the present invention, the reconstituted tobacco coating liquid is prepared by the following steps: (a) respectively adding water into the tobacco raw materials for extraction; the tobacco raw material is at least one of tobacco stems, tobacco powder, broken tobacco leaves and tobacco ash; (b) respectively carrying out solid-liquid separation on the extracted slurry in the step (a) through a double-screw pulp extruder, a 600 high-concentration disc mill and a single-screw squeezer, feeding the solid-phase slurry into a 750 high-concentration disc mill, feeding the solid-phase slurry into a slurry tank, and finally carrying out pulp making through a pulp flowing box to obtain a reconstituted tobacco substrate; c) and (c) removing impurities and concentrating the collected liquid phase extract after extraction in the step (a) and carrying out alcoholization feeding to prepare the reconstituted tobacco coating liquid.
Compared with the traditional coating liquid, the coating liquid prepared by adding a certain mesh of tobacco powder in the Maillard reaction has the most intuitive effect of improving the smoking taste of the reconstituted tobacco. Especially when the ratio of the tobacco powder to the Maillard reactant is the above-mentioned preferred addition amount, the sensory quality of the reconstituted tobacco is greatly improved.
The method has simple treatment process, can well meet the requirements of the reconstituted tobacco production process, can directly carry out amplification batch production, and has good industrial application prospect.
Detailed Description
The present invention is further described in detail by the following examples, which are not intended to limit the present invention.
Example 0
(1) Respectively adding water into the tobacco raw materials for extraction;
the tobacco raw materials comprise tobacco stems, tobacco powder, broken tobacco leaves, tobacco ash and the like.
(2) And (3) respectively carrying out solid-liquid separation on the pulp extracted in the step (1) by a double-screw pulp extruder, a 600 high-concentration disc mill, a single-screw squeezer and the like, feeding the solid-phase pulp into a 750 high-concentration disc mill, then feeding the solid-phase pulp into a pulp tank, and finally carrying out pulp making by a pulp flowing box and the like to obtain the reconstituted tobacco substrate.
(3) And (3) removing impurities and concentrating the liquid phase extract collected in the step (1) after extraction, adding materials by alcoholization and the like to prepare the reconstituted tobacco coating liquid.
(4) Coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is better, the fragrance amount is more sufficient, the smoke fragrance is more permeable, the smoke amount is sufficient, the irritation is good, and the offensive odor is slightly obvious.
Example 1
(1) Grinding the tobacco raw material into powder by using a grinding machine, completely sieving the powder by using a 200-mesh sieve, and distributing the particle size of the powder in 200-400 meshes for later use;
(2) 2g of cysteine, 6g of fructose and 40g of tobacco powder were taken, and 40g of propylene glycol and 200g of water were added to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 80 ℃ to perform Maillard reaction for 8 hours, and standing the solution for later use after the reaction is finished;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 5 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke has good uniformity, sufficient fragrance, good fragrance quality, more smoke fragrance, sufficient smoke amount and good harmony.
Example 2
(1) Grinding the tobacco raw material into powder by a grinding machine, completely sieving the powder by a 200-mesh sieve, and distributing the particle size of the powder in 200-mesh and 400-mesh sieve for later use;
(2) a solution was prepared by adding 40g of propylene glycol and 200g of water to 2g of phenylalanine, 6g of glucose and 30g of tobacco powder. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 100 ℃ to perform Maillard reaction for 10 hours, and standing the solution for later use after the reaction is finished;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 10 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is relatively permeable, the smoke amount is sufficient, and the harmony is good.
Example 3
(1) Grinding the tobacco raw material into powder by using a grinding machine, completely sieving the powder by using a 200-mesh sieve, and distributing the particle size of the powder in 200-400 meshes for later use;
(2) 2g of lysine, 8g of fructose and 30g of tobacco powder were taken, and 40g of propylene glycol and 200g of water were added to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 110 ℃ to perform Maillard reaction for 8 hours, and standing the solution for later use after the reaction is finished;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 15 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is relatively permeable, the smoke amount is sufficient, and the harmony is good.
Example 4
(1) Grinding the tobacco raw material into powder by using a grinding machine, completely sieving the powder by using a 200-mesh sieve, and distributing the particle size of the powder in 200-400 meshes for later use;
(2) 2g of proline, 10g of glucose and 20g of tobacco powder were added with 40g of propylene glycol and 200g of water to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 120 ℃ to perform Maillard reaction for 6 hours, and standing the solution for later use after the reaction is finished;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 20 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is thoroughly emitted, the smoke amount is sufficient, and the harmony is good.
Example 5
(1) Grinding the tobacco raw material into powder by using a grinding machine, completely sieving the powder by using a 200-mesh sieve, and distributing the particle size of the powder in 200-400 meshes for later use;
(2) 2g of glycine, 8g of fructose and 30g of tobacco powder were taken, and 40g of propylene glycol and 200g of water were added to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 130 ℃ to perform Maillard reaction for 8 hours, and standing the solution for later use after the reaction is finished;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 10 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) The sensory evaluation result table shows that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is relatively permeable, the smoke amount is sufficient, and the harmony is good.
Example 6
(1) Grinding the tobacco raw material into powder by using a grinding machine, completely sieving the powder by using a 200-mesh sieve, and distributing the particle size of the powder in 200-400 meshes for later use;
(2) 2g of valine, 6g of glucose and 40g of tobacco powder were added to 40g of propylene glycol and 200g of water to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 100 ℃ to generate Maillard reaction for 10 hours, and standing the solution for later use;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 5 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is thoroughly emitted, the smoke amount is sufficient, and the harmony is good.
Example 7
(1) Grinding the tobacco raw material into powder by a grinding machine, and completely sieving the powder by a 600-mesh sieve for later use;
(2) 2g of valine, 6g of glucose and 40g of tobacco powder were added to 40g of propylene glycol and 200g of water to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 100 ℃ to generate Maillard reaction for 10 hours, and standing the solution for later use;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 5 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is thoroughly emitted, the smoke amount is sufficient, and the harmony is good.
Example 8
(1) Grinding the tobacco raw material into powder by a grinding machine, and completely sieving the powder by a 100-mesh sieve for later use;
(2) 2g of valine, 6g of glucose and 40g of tobacco powder were added to 40g of propylene glycol and 200g of water to form a solution. Adjusting the pH value of the solution to 7.4, pouring the solution into a Maillard reaction bottle, heating the solution at 100 ℃ to generate Maillard reaction for 10 hours, and standing the solution for later use;
(3) adding the Maillard reactant into the reconstituted tobacco coating liquid according to the proportion of 5 percent;
(4) coating 38% (calculated on the absolute dry slurry) of the coating liquid on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, finally slicing and the like to prepare a finished reconstituted tobacco product.
(5) Sensory evaluation results show that the smoke uniformity is good, the fragrance amount is sufficient, the smoke fragrance is thoroughly emitted, the smoke amount is sufficient, and the harmony is good.
The sensory evaluation results (each value is the average of the evaluation results of 24 qualified smokers) of example 0 and examples 1-8 of the present invention are shown in table 1 below:
TABLE 1
In conclusion, the method effectively overcomes the sensory quality defect of the reconstituted tobacco in the prior art and has industrial application prospect. The examples are not only the ratios mentioned herein for amino acids, aldoses and tobacco powders, but also apply to any ratio formulation between the three.
The above description of the method for improving the quality of the paper-process reconstituted tobacco product by using the tobacco raw material as the maillard reactant carrier is provided to help understanding the present invention, but the implementation manner of the present invention is not limited by the above examples, and any changes, modifications, substitutions, combinations and simplifications which do not depart from the principle of the present invention shall be equivalent replacement manners, and shall be included in the protection scope of the present invention.
Claims (5)
1. The method for improving the quality of the paper-making reconstituted tobacco product is characterized by comprising the following steps:
(1) grinding a tobacco raw material into powder by using a grinding machine, wherein the particle size distribution is 200-400 meshes, and the tobacco raw material is selected from at least one of sheet tobacco, cut tobacco, tobacco powder and tobacco stems;
(2) taking 1-10 parts by weight of amino acid, 10 parts by weight of aldose and 5-40 parts by weight of tobacco powder obtained in the step (1), dissolving propylene glycol and water in a weight part ratio of 1: 1-10 to obtain a solution, adjusting the pH value to 7-8, pouring the solution into a Maillard reaction bottle, carrying out Maillard reaction at 60-130 ℃ for 6-10 hours, and standing for later use;
(3) adding the Maillard reactant in the step (2) into a reconstituted tobacco coating liquid; the weight proportion of the added Maillard reactants is 5-20%;
(4) and (4) coating the coating liquid in the step (3) on a reconstituted tobacco substrate, drying by an oven, perfuming by a drying cylinder, and finally slicing to prepare a reconstituted tobacco finished product.
2. The method of claim 1, wherein the tobacco material is ground in a mill and completely passed through a 200 mesh sieve with a particle size distribution of 200 to 400 mesh.
3. The method according to claim 1, wherein in the step (2), the amino acid is at least one selected from the group consisting of lysine, phenylalanine, cysteine, valine and glycine; the aldose is fructose and/or glucose.
4. The method of claim 1, wherein the reconstituted tobacco coating solution is prepared by the steps of:
(a) respectively adding water into the tobacco raw materials for extraction; the tobacco raw material is at least one of tobacco stems, tobacco powder, broken tobacco leaves and tobacco ash;
(b) respectively carrying out solid-liquid separation on the extracted slurry in the step (a) through a double-screw pulp extruder, a 600 high-concentration disc mill and a single-screw squeezer, feeding the solid-phase slurry into a 750 high-concentration disc mill, feeding the solid-phase slurry into a slurry tank, and finally carrying out pulp making through a pulp flowing box to obtain a reconstituted tobacco substrate;
(c) and (c) removing impurities and concentrating the collected liquid phase extract after extraction in the step (a) and carrying out alcoholization feeding to prepare the reconstituted tobacco coating liquid.
5. A reconstituted tobacco product obtained by the method of any one of claims 1 to 4.
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| CN112220099A (en) * | 2020-09-23 | 2021-01-15 | 云南中烟工业有限责任公司 | Method for preparing spice with nut fragrance and hay fragrance, spice and application thereof |
| CN113925191A (en) * | 2020-06-29 | 2022-01-14 | 上海烟草集团有限责任公司 | Tea-containing buccal cigarette and preparation method thereof |
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