CN107006888B - The method that reconstituted tobacco product filler retention is improved using compounded mix - Google Patents
The method that reconstituted tobacco product filler retention is improved using compounded mix Download PDFInfo
- Publication number
- CN107006888B CN107006888B CN201710202751.5A CN201710202751A CN107006888B CN 107006888 B CN107006888 B CN 107006888B CN 201710202751 A CN201710202751 A CN 201710202751A CN 107006888 B CN107006888 B CN 107006888B
- Authority
- CN
- China
- Prior art keywords
- slurry
- offal
- solid
- calcium carbonate
- reconstituted tobacco
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Landscapes
- Paper (AREA)
Abstract
The present invention provides a kind of methods improving papermaking-method reconstituted tobaccos product filler retention using diatomite and Calcium Carbonate Composite Fillers, including：(1) water is added to extract respectively tobacco material；(2) material after extracting is separated by solid-liquid separation respectively, and solid-phase material handles through beating process and solid phase slurry is made, and diatomite and Calcium Carbonate Composite Fillers are added after merging in each solid phase slurry, most manufacture paper with pulp afterwards through head box and are prepared into reconstituted tobacco substrate；Each water phase material concentrates by removal of impurities after merging and is prepared into coating fluid；(3) by coating solution on reconstituted tobacco substrate, through oven drying, drying cylinder flavoring, finally slice is prepared into reconstituted tobacco finished product.Retention of the filler in reconstituted tobacco can be improved in this method, and then improve reconstituted tobacco physical property, absorbent and appearance property etc., and improve the suction quality of substrate.
Description
Technical field
The present invention relates to papermaking-method reconstituted tobaccos fields, and diatomite and Calcium Carbonate Composite Fillers are used more particularly, to a kind of
The method for improving papermaking-method reconstituted tobaccos product filler retention.
Background technology
Papermaking-method reconstituted tobaccos (Paper-process reconstituted tobacco) are also known as reconstituted tobacoo, are
Using modern extraction and separation process and the paper technology after improvement, one kind " people that tobacco byproduct and dead meal are process
Make tobacco leaf ", also referred to as papermaking-method reconstituted tobaccos, cigarette made of the waste material in mainly being processed with tobaccos such as offal, broken cigarette and offals
Straw pulp and a certain amount of wood pulp and filler etc., which are mixed, manufactures paper with pulp into substrate through paper machine and is made again through dip coated.
Reconstituted tobacco originates from the 1950s, its development experience roll-in method-thick slurry method-stage of paper process 3.It makes
Paper method reconstituted tobacco with the roll-in method produced at present, have the advantages that uniqueness compared with thick slurry method reconstituted tobacco, including density it is small, fill out
Supplement height with money；Mechanical resistant processability can be good, high at silk rate；Burning velocity is fast, releasing content of coke tar is low；Product plasticity is good etc..
The technique that each manufacturing enterprise uses at present is slightly different, and substantially slightly improves typical two-step method, stalk, end
It is extracted with water, the offal offal after extraction is sent on paper machine forming of manufacturing paper with pulp, two kinds of extractions after being mixed with beating processing, by slurry
It takes liquid after the processing of the means such as concentration, prepares mixing and be coated in thin slice chip base.Its master operation includes that raw material is located in advance
Reason, concentration, slurrying, manufactures paper with pulp, is coated with, post-processing at extraction.
In order to improve reconstituted tobacco content of ashes, a certain proportion of filler is usually added in production, and then improve again
Tobacco leaf physical property, absorbent and appearance property etc. are made, and improves the suction quality of substrate.In addition in reconstituted tobacco substrate
Addition filler can also reduce enterprise's production cost during manufacturing paper with pulp, while the reduction of fibre fractionation can also reduce flue gas accordingly and have
The release of evil ingredient.Calcium carbonate is the most conventional filler of papermaking-method reconstituted tobaccos, and producer manufactures paper with pulp process in slurrying both at home and abroad at present
In all use calcium carbonate as filler substantially.But domestic reconstituted tobacco entirety filler retention level is deposited compared with foreign countries
It is exactly that filler retention is comparatively much lower in a major issue.Therefore filler use and retention raising at
For research emphasis, how filler retention is improved, seems non-so as to improve cigarette burning state and reduction Harmful ingredient content
It is often important.
Diatomaceous chemical composition is mainly SiO2, contain a small amount of Al2O3、Fe2O3, CaO, MgO etc. and organic matter, in electricity
It is observed that special porous construction under sub- microscope, there is excellent extensibility, higher impact strength, tensile strength,
Tearing strength, light soft interior mill property is good, good etc. high-quality effect of doing Compressive Strength.In paper-making industry office paper, industrial paper etc.
Various paper, diatomite addition can make paper smooth, and light-weight, intensity is good, and reduction causes to stretch because humidity changes, in cigarette
Without any toxic side effects filtrate clarity can be improved, and filtering velocity is made to accelerate in adjustable combustion rate in paper in filter paper.
Invention content
The present invention is intended to provide a kind of improving papermaking-method reconstituted tobaccos product using diatomite, calcium carbonate binary compounded mix
The method of filler retention, for solving the problems, such as that filler retention is too low in the prior art.
A method of papermaking-method reconstituted tobaccos product filler retention is improved using diatomite and Calcium Carbonate Composite Fillers,
Include the following steps：
(1) water is added to extract respectively tobacco material；
The tobacco material includes at least one of offal, offal, crumbled tobacco and cigarette ash；
(2) material after the completion of extracting is separated by solid-liquid separation respectively, and solid-phase material is handled through beating process is made solid phase slurry
Material, each solid phase slurry are added diatomite and Calcium Carbonate Composite Fillers after merging, finally manufacture paper with pulp and be prepared into reconstituted tobacco substrate；Each water
Phase materials concentrate by removal of impurities after merging and are prepared into coating fluid；
(3) by coating solution on reconstituted tobacco substrate, by drying, flavoring, finally slice is prepared into reconstituted tobacco
Finished product.
The present invention is by seeking a kind of filler of high retention rate, optimization filler adding technology and ratio etc., to improve filler
Retention in reconstituted tobacco product, and then improve reconstituted tobacco physical property, absorbent and appearance property etc., and change
The suction quality of kind substrate.In addition the retention for improving filler can reduce fibre fractionation, can not only reduce enterprise's production cost, also
Cigarette burning state can be improved accordingly and reduce the release of harmful ingredients in flue gas.
Preferably, the tobacco material is by mass percentage, including following component：Offal 40~60%, offal,
30~40% crumbled tobaccos 10~20%, cigarette ash 0~10%.
In step (1), tobacco material is 1 with water quality ratio：2~8, pH4~6 are extracted, extraction temperature is 50~70 DEG C, extraction
It is 2~3h to take the time.
Preferably, in step (1), after offal, crumbled tobacco and cigarette ash are mixed plus water extracts, and mixing end is obtained after extraction
Material；Offal individually adds water to extract, and offal material is obtained after extraction.Since nicotine content is high in offal, crumbled tobacco and cigarette ash, and
Ingredient of the offal containing some the generation irritations and peculiar smell such as a large amount of pectin itself, therefore the extract liquor mouthfeel of offal can be poor,
Separately extraction is conducive to flexibly add the ratio of the two according to mouthfeel demand.
Further preferably, it in step (2), mixes last material and is separated by solid-liquid separation, the solid-phase material after separation is roughly ground
The last slurry of mixing is made；Offal material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal is made
Slurry.
Further preferably, the beating degree of the last slurry of mixing is 15~250SR, fiber arithmetic average length is 0.35~
0.45mm, fiber width are 80~90 μm, and fiber roll curvature is 15~20%.
Further preferably, the beating degree of the offal slurry is 15~250SR or so, fiber arithmetic average length 0.45~
0.55mm, fiber width are 70~80 μm, and fiber roll curvature is 15~20%.
Preferably, merge the last slurry of mixing and offal slurry to obtain mixing solid phase slurry, mixing solid phase slurry pass through into
Enter highly concentrated slurry-stablizing case after one step fine grinding, diatomite and Calcium Carbonate Composite Fillers are added.
Further preferably, the beating degree of the mixing solid phase slurry in highly concentrated slurry-stablizing case is 29~320SR, fiber overall porosity
It is 61~69%.
Preferably, the diatomite and the additive amount of Calcium Carbonate Composite Fillers are the 4~15% of slurry oven-dry weight.
Include following components by mass percentage in the diatomite and Calcium Carbonate Composite Fillers：Diatomite 20~
80%, calcium carbonate 20~80%.
The diatomaceous grain size is 5~50 μm, and d50 is 20~30 μm, and surface area average grain diameter D (3,2) is 10~15 μ
m。
The grain size of the calcium carbonate is 1~40 μm, and d50 is 10~20 μm, and surface area average grain diameter D (3,2) is 1~5 μm.
Selected calcium carbonate grain size is small compared with diatomite, is added before highly concentrated slurry-stablizing case and first mixes diatomite and calcium carbonate according to the ratio
It is compounded, grain size small calcium carbonate in part can be adsorbed in diatomite macrovoid by when mixing, to improve the whole of filler
Body keeps ratio；Meanwhile the two can not only adjust cigarette burning state when being used in mixed way according to the ratio, but also cigarette can also be adjusted
Aspirate mouthfeel.
Mixing solid phase slurry in highly concentrated slurry-stablizing case is after defibrinations at different levels, and fiber surface morphology is changed, fiber
Weave in is distributed with different porosities, and the diatomite and Calcium Carbonate Composite Fillers of the particle size range can effectively be inhaled therewith
Attached combination.
It is mixed 2~5 minutes preferably, high-speed stirred after diatomite and Calcium Carbonate Composite Fillers is added, stir speed (S.S.) is
800~1500r/min, at this time the fiber in slurry due to refining process processing and form different porosities, with diatomite, carbonic acid
Calcium can wad a quilt with cotton and get together in water, and effective absorption combines.Diatomite mainly passes through sieving actoion, effect of depth and suction-operated
3 kinds of synergistic effects have the function that retention, to improve papermaking-method reconstituted tobaccos product filler retention.
Preferably, in step (3), the coating weight of the coating fluid is the 35~40% of slurry oven-dry weight.
Compared with prior art, the beneficial effects of the present invention are：
Filler provided by the present invention prepares papermaking-method reconstituted tobaccos, and the paper-making method reconstructed cigarette of calcium carbonate is only added with tradition
Leaf is compared, and what is most intuitively acted on improves filler in the retention of product, and improves every physical index of reconstituted tobacco,
It has some improvement simultaneously to the suction mouthfeel of reconstituted tobacco.Especially when the additive amount of filler refers to preferred additive amount to be above-mentioned
When, have to retention and remarkably promote effect, compared with calcium carbonate directly is used alone, is filled out using diatomite and calcium carbonate are compound
The retention of material can be improved 10.4~25.7%.
The method of the present invention is simple for process, can meet the requirement of reconstituted tobacco production technology well, and save the energy,
It can be directly amplified batch production, there is good industrial applications foreground.
Specific implementation mode
Further detailed description is done to the present invention by following embodiment, but the embodiment is not constituted to the present invention's
Limitation.
Comparative example
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, carbon is added
Sour calcium filler, the additive amount of pearl filler are the 4~15% of slurry oven-dry weight, and calcium carbonate grain size is 1.71~36.13 μm,
D50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and high-speed stirred mixes 2~3 minutes after calcium carbonate is added, and stirs
It is 1000r/min to mix rate, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco substrate.After water phase material after each separation merges
It is prepared into coating fluid by removal of impurities concentration.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Calcium carbonate retention rate the results are shown in Table 1 in reconstituted tobacco product.
Calcium carbonate retention rate in 1 reconstituted tobacco product of table
Embodiment 1
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 4% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 1：1, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 2 in reconstituted tobacco product.
Filler retention in 2 reconstituted tobacco product of table
Embodiment 2
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 6% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 1：1, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 3 in reconstituted tobacco product.
Filler retention in 3 reconstituted tobacco product of table
Embodiment 3
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 8% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 1：1, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 4 in reconstituted tobacco product.
Filler retention in 4 reconstituted tobacco product of table
Embodiment 4
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 10% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 1：1, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 5 in reconstituted tobacco product.
Filler retention in 5 reconstituted tobacco product of table
Embodiment 5
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 12% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 1：1, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 6 in reconstituted tobacco product.
Filler retention in 6 reconstituted tobacco product of table
Embodiment 6
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 15% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 1：1, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 7 in reconstituted tobacco product.
Filler retention in 7 reconstituted tobacco product of table
Embodiment 7
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 10% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 3：2, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 8 in reconstituted tobacco product.
Filler retention in 8 reconstituted tobacco product of table
Embodiment 8
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 10% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 7：3, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 9 in reconstituted tobacco product.
Filler retention in 9 reconstituted tobacco product of table
Embodiment 9
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
The mass ratio of the 10% addition diatomite and Calcium Carbonate Composite Fillers of oven-dry weight, diatomite and calcium carbonate is 2：3, diatomite grain size
Be 5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 10 in reconstituted tobacco product.
Filler retention in 10 reconstituted tobacco product of table
Embodiment 10
(1) tobacco material is pressed into offal：Offal：Crumbled tobacco presses 5：4：1 mass ratio samples, after offal and crumbled tobacco are mixed
Add water to extract, obtains mixing last material after extraction；Offal individually adds water to extract, and offal material is obtained after extraction.The technique of extraction
Condition is：Tobacco material is 1 with water proportioning：6, pH 4~6,50 DEG C of extraction temperature, 2~3h of extraction time.
(2) it mixes last material to be separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；Offal
Material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made.Will the last slurry of mixing and
Offal slurry merges to obtain mixing solid phase slurry, and mixing solid phase slurry enters highly concentrated slurry-stablizing case after further fine grinding, with slurry
Diatomite and Calcium Carbonate Composite Fillers, the mass ratio 3 of diatomite and calcium carbonate is added in the 10% of oven-dry weight：7, diatomite grain size is
5.02~46.43 μm, d50 be 23.44 μm, surface area average grain diameter D (3,2) be 11.97 μm, calcium carbonate grain size be 1.71~
36.13 μm, d50 is 11.34 μm, and surface area average grain diameter D (3,2) is 1.42 μm, and diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~3 minutes, stir speed (S.S.) 1000r/min afterwards, finally enters head box and manufactures paper with pulp to obtain reconstituted tobacco base
Piece.Water phase material after each separation concentrates by removal of impurities after merging and is prepared into coating fluid.
(3) by coating solution on reconstituted tobacco substrate, by oven drying, drying cylinder flavoring, finally slice is prepared into
Reconstituted tobacco finished product.
Diatomite and Calcium Carbonate Composite Fillers retention the results are shown in Table 11 in reconstituted tobacco product.
Filler retention in 11 reconstituted tobacco product of table
In conclusion the present invention effectively overcomes in the prior art using diatomite and Calcium Carbonate Composite Fillers as filler
The too low disadvantage of filler retention and have industrial applications foreground.
The method for improving papermaking-method reconstituted tobaccos product filler retention a kind of to the present invention is expounded above, is used for
Help understands the present invention, but embodiment of the present invention are not limited by the above embodiments, any without departing from the principle of the invention
Changes, modifications, substitutions, combinations, simplifications made by lower, should be equivalent substitute mode, be included in the protection model of the present invention
Within enclosing.
Claims (6)
1. the method for improving reconstituted tobacco product filler retention using compounded mix, which is characterized in that include the following steps：
(1) water is added to extract respectively tobacco material；
The tobacco material includes offal, offal, crumbled tobacco and cigarette ash；
In step (1), after offal, crumbled tobacco and cigarette ash are mixed plus water extracts, and obtains mixing last material after extraction；Offal is independent
Add water to extract, offal material is obtained after extraction；
(2) material after the completion of extracting is separated by solid-liquid separation respectively, and solid-phase material handles through beating process and solid phase slurry is made, respectively
Diatomite and Calcium Carbonate Composite Fillers are added after merging in solid phase slurry, finally manufacture paper with pulp and are prepared into reconstituted tobacco substrate；Each aqueous-phase material
Material concentrates by removal of impurities after merging and is prepared into coating fluid；
It in step (2), mixes last material and is separated by solid-liquid separation, the solid-phase material after separation carries out corase grinding and the last slurry of mixing is made；
Offal material is separated by solid-liquid separation after pre-grinding, and the solid-phase material after separation carries out corase grinding and offal slurry is made；
The last slurry of mixing and offal slurry are merged into obtain mixing solid phase slurry, mixing solid phase slurry enters after further fine grinding
Diatomite and Calcium Carbonate Composite Fillers are added in highly concentrated slurry-stablizing case；
The beating degree of mixing solid phase slurry in highly concentrated slurry-stablizing case is 29~32 ° of SR, and fiber overall porosity is 61~69%；
(3) by coating solution on reconstituted tobacco substrate, by drying, flavoring, finally slice is prepared into reconstituted tobacco finished product.
2. according to the method described in claim 1, it is characterized in that, the beating degree of the last slurry of the mixing is 15~25 ° of SR, fibre
Dimension arithmetic average length is 0.35~0.45mm, and fiber width is 80~90 μm, and fiber roll curvature is 15~20%.
3. according to the method described in claim 1, it is characterized in that, the beating degree of the offal slurry be 15~25 ° of SR, fiber
0.45~0.55mm of arithmetic average length, fiber width are 70~80 μm, and fiber roll curvature is 15~20%.
4. according to claims 1 to 3 any one of them method, which is characterized in that the diatomite and Calcium Carbonate Composite Fillers
Additive amount be slurry oven-dry weight 4~15%.
5. according to claims 1 to 3 any one of them method, which is characterized in that the diatomaceous grain size is 5~50 μm,
D50 is 20~30 μm, and surface area average grain diameter D (3,2) is 10~15 μm.
6. according to claims 1 to 3 any one of them method, which is characterized in that diatomite and Calcium Carbonate Composite Fillers are added
High-speed stirred mixes 2~5 minutes afterwards, and stir speed (S.S.) is 800~1500r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710202751.5A CN107006888B (en) | 2017-03-30 | 2017-03-30 | The method that reconstituted tobacco product filler retention is improved using compounded mix |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710202751.5A CN107006888B (en) | 2017-03-30 | 2017-03-30 | The method that reconstituted tobacco product filler retention is improved using compounded mix |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107006888A CN107006888A (en) | 2017-08-04 |
| CN107006888B true CN107006888B (en) | 2018-10-12 |
Family
ID=59445797
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710202751.5A Active CN107006888B (en) | 2017-03-30 | 2017-03-30 | The method that reconstituted tobacco product filler retention is improved using compounded mix |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107006888B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108783562B (en) * | 2018-07-02 | 2021-08-31 | 云南拓宝科技有限公司 | Preparation method of tobacco shreds suitable for novel cigarettes |
| CN110013047A (en) * | 2019-04-30 | 2019-07-16 | 云南中烟工业有限责任公司 | A kind of reconstituted tobacco comprising metallic particles and preparation method thereof and cigarette comprising it |
| CN111248486A (en) * | 2020-03-18 | 2020-06-09 | 浙江中烟工业有限责任公司 | Method for improving reconstituted tobacco quality by adopting filler as Maillard reactant carrier |
| CN113243548A (en) * | 2021-05-18 | 2021-08-13 | 河南卷烟工业烟草薄片有限公司 | Preparation method of low-viscosity low-irritation reconstituted tobacco of heated cigarette |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB753965A (en) * | 1953-09-08 | 1956-08-01 | Gen Cigar Co | Improved process for the production of continuous tobacco sheet |
| CN103141928A (en) * | 2012-12-31 | 2013-06-12 | 杭州利群环保纸业有限公司 | Preparation method for paper-making process tobacco sheet and finished product of paper-making process tobacco sheet |
| CN103416839A (en) * | 2013-08-02 | 2013-12-04 | 上海烟草集团有限责任公司 | Method for improving paper-making reconstituted tobacco product performance |
| CN105614942A (en) * | 2016-04-08 | 2016-06-01 | 云南中烟工业有限责任公司 | Method for increasing retention rate of fillers on sheet bases of reconstituted tobaccos by paper-making process |
| CN106235374A (en) * | 2016-08-30 | 2016-12-21 | 河南卷烟工业烟草薄片有限公司 | A kind of papermaking-method reconstituted tobaccos applying filler method |
-
2017
- 2017-03-30 CN CN201710202751.5A patent/CN107006888B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB753965A (en) * | 1953-09-08 | 1956-08-01 | Gen Cigar Co | Improved process for the production of continuous tobacco sheet |
| CN103141928A (en) * | 2012-12-31 | 2013-06-12 | 杭州利群环保纸业有限公司 | Preparation method for paper-making process tobacco sheet and finished product of paper-making process tobacco sheet |
| CN103416839A (en) * | 2013-08-02 | 2013-12-04 | 上海烟草集团有限责任公司 | Method for improving paper-making reconstituted tobacco product performance |
| CN105614942A (en) * | 2016-04-08 | 2016-06-01 | 云南中烟工业有限责任公司 | Method for increasing retention rate of fillers on sheet bases of reconstituted tobaccos by paper-making process |
| CN106235374A (en) * | 2016-08-30 | 2016-12-21 | 河南卷烟工业烟草薄片有限公司 | A kind of papermaking-method reconstituted tobaccos applying filler method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107006888A (en) | 2017-08-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107006888B (en) | The method that reconstituted tobacco product filler retention is improved using compounded mix | |
| CN103141928B (en) | A kind of tobacco sheets by paper making method preparation method and manufactured goods thereof | |
| CN103005661B (en) | Mixed paper-making reconstituted tobacco as well as preparation method and application thereof | |
| CN101536811B (en) | Method for applying non-tobacco raw-material lotus leaves to paper-making sheets | |
| CN101912147B (en) | Functional tobacco sheet and preparation method thereof | |
| CN103892436B (en) | A kind of improve tobacco material method of service efficiency in reconstituted tobacco produces | |
| CN105286078B (en) | Method for papermaking method reconstituted tobacco by replacing wood pulp fibers through cotton stalk bark fibers | |
| CN104687236A (en) | Preparation method of tobacco fiber for cigarette paper | |
| CN102845828A (en) | Method for producing paper cigar cloth and cigar jacket for cigars and cigarettes | |
| CN101214089A (en) | Blend type cigarette filter tip and preparation thereof | |
| CN106858699B (en) | The method that reconstituted tobacco product filler retention is improved using diatomite | |
| CN104068463B (en) | A kind of cane shoots leaves prepares the method for reconstituted tobacoo | |
| CN102499464A (en) | Application method of ash bars in papermaking-method reconstituted tobaccos | |
| CN104473318A (en) | Harm-reducing and tar-lowering recombined tobacco and producing method thereof | |
| CN105077555B (en) | A kind of processing method of papermaking-method reconstituted tobaccos | |
| CN104005291B (en) | A kind of strong absorption reduces cork paper of flue gas and preparation method thereof | |
| CN102599633A (en) | Material adding method for dry reconstitution of tobacco | |
| CN106901398B (en) | The method that papermaking-method reconstituted tobaccos product filler retention is improved using titanium dioxide | |
| CN106901397B (en) | The method that tri compound filler improves papermaking-method reconstituted tobaccos product filler retention | |
| CN106880076B (en) | A method of improving papermaking-method reconstituted tobaccos product filler retention | |
| CN107242603A (en) | A kind of production method of reconstituted tobacoo | |
| CN107268095B (en) | A kind of selenium-rich fiber producing processes | |
| CN102726823A (en) | Method for reducing content of pectic substance of tobacco sheet extraction solution in papermaking method | |
| CN102499468A (en) | Method capable of remarkably increasing softness and absorptivity of papermaking-method reconstituted tobaccos | |
| CN109567254B (en) | Tobacco sheet, preparation method thereof, substrate of tobacco sheet and preparation method of coating liquid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |