CN101912147B - Functional tobacco sheet and preparation method thereof - Google Patents

Functional tobacco sheet and preparation method thereof Download PDF

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Publication number
CN101912147B
CN101912147B CN201010242200XA CN201010242200A CN101912147B CN 101912147 B CN101912147 B CN 101912147B CN 201010242200X A CN201010242200X A CN 201010242200XA CN 201010242200 A CN201010242200 A CN 201010242200A CN 101912147 B CN101912147 B CN 101912147B
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CN
China
Prior art keywords
glycyrrhiza residue
preparation
tobacco sheet
water
glycyrrhiza
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN201010242200XA
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Chinese (zh)
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CN101912147A (en
Inventor
赵谋明
田英姿
崔春
李军
徐俊
陈超
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South China University of Technology SCUT
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South China University of Technology SCUT
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Priority to CN201010242200XA priority Critical patent/CN101912147B/en
Priority to PCT/CN2010/078944 priority patent/WO2012012989A1/en
Publication of CN101912147A publication Critical patent/CN101912147A/en
Application granted granted Critical
Publication of CN101912147B publication Critical patent/CN101912147B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Paper (AREA)

Abstract

The invention relates to a functional tobacco sheet and a preparation method thereof. The preparation method comprises the steps of: washing raw materials of glycyrrhiza residue with water, grinding the glycyrrhiza residue into thick liquid, washing the thick liquid to remove water-soluble substances, condensing, making paper, then coating on the two faces of a glycyrrhiza residue sheet and drying. The invention has the advantages that firstly, the tobacco sheet prepared by the method is free from tar, secondly, the release amount of carbon monoxide is lower, and thirdly, the tobacco sheet can obviously increase fragrance and reduce the excitement of cigarette after being added in the cigarette.

Description

Functional tobacco sheet and preparation method thereof
Technical field
The invention belongs to the pulping and paper-making field, particularly functional tobacco sheet and preparation method thereof.
Technical background
Improving constantly of Along with people's living standard and quality of life; Cigarette consumption changes to brand consumption; Especially high-grade cigarette market; The consumer also proposes increasingly high requirement to health, the local flavor of cigarette, and the cigarette of producing high fragrance, low tar, low harm has become one of important directions of China and even the development of world's cigarette industry.At present, the main technology path that adopts has two: a kind of is " falling Jiao ", promptly through the burst size that reduces coke tar in cigarette harmful components is reduced simultaneously, and promptly concertedness reduces the cigarette smoke harmful components; Another kind is " harm reduction ", promptly adopts special technique, effectively reduces part harmful components in the cigarette smoke, and less to other composition effects, i.e. harmful components in the selectivity reducing cigarette fume.Yet this kind technology also causes the aroma-producing substance in the main flume to reduce synchronously when reducing tar, and great changes will take place to cause the local flavor of cigarette, and the consumer choice cigarette at first just needs good local flavor.
Radix Glycyrrhizae is a perennial herb, mainly is distributed in ground such as Xinjiang, Qinghai, Gansu.Radix Glycyrrhizae has beneficial gas bowl spares, relieving spasm to stop pain, moistens the lung and relieve the cough, the effect of purging intense heat and detonicating and coordinating the drug actions of a prescription, is widely used in medicine and food service industry.China Radix Glycyrrhizae is mainly used in and produces Radix Glycyrrhizae extract, glycyrrhizic acid and derivative thereof at present, and glycyrrhiza residue is the accessory substance of Radix Glycyrrhizae processing.Because the process technology means limited, China's glycyrrhiza residue also is not fully used at present, or is used for breeding feed, or the direct landfill of as fertilizer sources goes back to the soil.
Summary of the invention
The objective of the invention is to overcome the above-mentioned deficiency that prior art exists, a kind of functional tobacco sheet and preparation method thereof is provided.The reconstituted tobacoo that adopts the present invention to prepare does not have tar content, the carbon monoxide burst size is lower.This reconstituted tobacoo is added to the effect that has obvious flavouring and minimizing cigarette excitement in the cigarette.
For achieving the above object, the technical scheme that the present invention adopts is following:
A kind of preparation method of functional tobacco sheet is a raw material with the glycyrrhiza residue, and through the washing glycyrrhiza residue, defibrination is removed the water-soluble substances in the slurry, manufactures paper with pulp, and the coating plant extracts prepares.
Among the preparation method of above-mentioned functional tobacco sheet, may further comprise the steps:
(1) the glycyrrhiza residue raw material is mixed with 4-6 times of weight water, after stirring 20-50min under the mixture 80-100 ℃ condition, filter and remove moisture, must wash the back glycyrrhiza residue;
(2) will wash the back glycyrrhiza residue and mix with water, make mixed liquor solid quality content reach 5%-10% after, adding disc mill defibrination must the glycyrrhiza residue slurries;
(3) the glycyrrhiza residue slurries are mixed with 1-3 times of weight water, filter after stirring 0.5-3h under 20-30 ℃ the mixing back, gets the glycyrrhiza residue slurry;
(4) the glycyrrhiza residue slurry is carried out thin slice and manufacture paper with pulp, the glycyrrhiza residue thin slice both sides coating plant extracts obtaining gets functional tobacco sheet.
Among the preparation method of above-mentioned functional tobacco sheet, the grinding clearance of the said disc mill of step (2) is 0.05mm-0.5mm.
Among the preparation method of above-mentioned functional tobacco sheet, said plant extracts comprises more than one in emblic extract, Radix Glycyrrhizae leaf extract and the offal extract.
Among the preparation method of above-mentioned functional tobacco sheet; Said plant extracts is to be raw material with in emblic, Radix Glycyrrhizae leaf or the offal more than one; Add 4-5 times of weight ethanol water; The mass concentration of ethanol water is 60-80%, and under 40-70 ℃, extracts 1-3h, and being concentrated into the solid content weight content is that 35-60% makes.
The functional tobacco sheet that is made by above-mentioned preparation method does not have tar content, the carbon monoxide burst size is lower, can add to have obvious flavouring and the effect that reduces the cigarette excitement in the cigarette.
The present invention compared with prior art has following advantage:
(1) reconstituted tobacoo of the present invention's preparation is raw material with the glycyrrhiza residue, does not contain raw materials such as offal, offal, does not therefore have tar content.Add this reconstituted tobacoo to can significantly reduce cigarette in the production of cigarettes tar content with certain proportion.
(2) 10-50% (w/w) reconstituted tobacoo is added in the cigarette, can cigarette product carbon monoxide burst size can be reduced 10-25%, effluent cigarette carbon monoxide burst size can be reduced 20-45%.
(3) this reconstituted tobacoo adds the fragrance that can significantly improve cigarette product in the cigarette to, reduces the excitement of fragrance.
The specific embodiment
Below in conjunction with implementing enforcement of the present invention is described further, but enforcement of the present invention and protection domain are not limited thereto.
Embodiment 1
Emblic is mixed with 4 times of weight 70% (w/w) ethanol water, and behind 70 ℃ of extraction 1h, being concentrated into solid content is 40% (w/w), obtains emblic extract.
The glycyrrhiza residue raw material is mixed with 4 times of weight water, behind 90 ℃ of stirring 30min, filter and remove moisture, must wash the back glycyrrhiza residue; To wash the back glycyrrhiza residue and mix with water, make the mixed liquor solid content reach 6% (mass percent) after, the adding grinding clearance is the disc mill defibrination of 0.05mm, must the glycyrrhiza residue slurries; The glycyrrhiza residue slurries are mixed with 2 times of weight water, behind 30 ℃ of stirring 1h, filter, get the glycyrrhiza residue slurry; The Radix Glycyrrhizae slurry is carried out thin slice manufacture paper with pulp, and be coated with emblic extract, get functional tobacco sheet in glycyrrhiza residue thin slice both sides.
This functional tobacco sheet is added in the cigarette with 15% (w/w) reconstituted tobacoo; The fragrance of cigarette product obviously improves; The tar content of cigarette reduces by 17.5%, and its carbon monoxide burst size reduces by 12.3%, and its effluent cigarette carbon monoxide burst size can reduce by 20.4%.
Embodiment 2
With Radix Glycyrrhizae leaf and 4 times of weight 70% (w/w) ethanol water, 40 ℃ are extracted 3h, and being concentrated into solid content is 50% (w/w), obtains the Radix Glycyrrhizae leaf extract.
The glycyrrhiza residue raw material is mixed with 6 times of weight water, behind 80 ℃ of stirring 20min, filter and remove moisture, must wash the back glycyrrhiza residue; To wash the back glycyrrhiza residue and mix with water, make the mixed liquor solid content reach 10% after, the adding grinding clearance is the disc mill defibrination of 0.5mm, must the glycyrrhiza residue slurries; The glycyrrhiza residue slurries are mixed with 3 times of weight water, behind 20 ℃ of stirring 3h, filter, get the glycyrrhiza residue slurry; The Radix Glycyrrhizae slurry is carried out thin slice manufacture paper with pulp, and be coated with the Radix Glycyrrhizae leaf extract, carry out drying again, get functional tobacco sheet in glycyrrhiza residue thin slice both sides.
This functional tobacco sheet is added in the cigarette with 25% (w/w) reconstituted tobacoo; The fragrance of cigarette product significantly improves; The tar content of cigarette reduces by 19.5%, and its carbon monoxide burst size reduces by 16.6%, and its effluent cigarette carbon monoxide burst size can reduce by 31.6%.
Embodiment 3
With offal and 5 times of weight 80% (w/w) ethanol water, 60 ℃ are extracted 2h, and being concentrated into solid content is 60% (w/w), obtains the offal extract.
The glycyrrhiza residue raw material is mixed with 6 times of weight water, behind 80 ℃ of stirring 20min, filter and remove moisture, must wash the back glycyrrhiza residue; To wash the back glycyrrhiza residue and mix with water, make the mixed liquor solid content reach 10% after, the adding grinding clearance is the disc mill defibrination of 0.1mm, must the glycyrrhiza residue slurries; The glycyrrhiza residue slurries are mixed with 3 times of weight water, behind 20 ℃ of stirring 3h, filter, get the glycyrrhiza residue slurry; The Radix Glycyrrhizae slurry is carried out thin slice manufacture paper with pulp, and be coated with the offal extract, get functional tobacco sheet in glycyrrhiza residue thin slice both sides.
This functional tobacco sheet is added in the cigarette with 40% (w/w) reconstituted tobacoo; The fragrance of cigarette product significantly improves; The tar content of cigarette reduces by 36.9%, and its carbon monoxide burst size reduces by 18.6%, and its effluent cigarette carbon monoxide burst size can reduce by 42.4%.

Claims (5)

1. the preparation method of functional tobacco sheet is characterized in that with the glycyrrhiza residue being raw material, and through the washing glycyrrhiza residue, defibrination is removed the water-soluble substances in the slurry, manufactures paper with pulp, and the coating plant extracts prepares; Specifically may further comprise the steps:
(1) the glycyrrhiza residue raw material is mixed with 4-6 times of weight water, after stirring 20-50min under the 80-100 ℃ of condition, filter and remove moisture, must wash the back glycyrrhiza residue;
(2) will wash the back glycyrrhiza residue and mix with water, make mixed liquor solid quality content reach 5%-10% after, adding disc mill defibrination must the glycyrrhiza residue slurries;
(3) the glycyrrhiza residue slurries are mixed with 1-3 times of weight water, filter after stirring 0.5-3h under 20-30 ℃ the mixing back, gets the glycyrrhiza residue slurry;
(4) the glycyrrhiza residue slurry is carried out thin slice and manufacture paper with pulp, the glycyrrhiza residue thin slice both sides coating plant extracts obtaining gets functional tobacco sheet.
2. preparation method according to claim 1 is characterized in that the grinding clearance of the said disc mill of step (2) is 0.05mm-0.5mm.
3. preparation method according to claim 1 is characterized in that said plant extracts comprises more than one in emblic extract, Radix Glycyrrhizae leaf extract and the offal extract.
4. preparation method according to claim 1; It is characterized in that said plant extracts is is raw material with in emblic, Radix Glycyrrhizae leaf or the offal more than one; Add 4-5 times of weight ethanol water, and under 40-70 ℃, extract 1-3h, being concentrated into the solid content weight content is that 35-60% makes; The mass concentration of said ethanol water is 60-80%.
5. the functional tobacco sheet that makes by each said preparation method of claim 1~4.
CN201010242200XA 2010-07-30 2010-07-30 Functional tobacco sheet and preparation method thereof Expired - Fee Related CN101912147B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201010242200XA CN101912147B (en) 2010-07-30 2010-07-30 Functional tobacco sheet and preparation method thereof
PCT/CN2010/078944 WO2012012989A1 (en) 2010-07-30 2010-11-22 Functional tobacco sheet and preparation method thereof

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Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102068035A (en) * 2011-01-26 2011-05-25 河南卷烟工业烟草薄片有限公司 Method for processing tobacco pulp
CN102423124B (en) * 2011-11-01 2013-08-28 吉林烟草工业有限责任公司 Tobacco slice and preparation method thereof
CN102524941B (en) * 2012-01-17 2013-11-06 湖北中烟工业有限责任公司 Sheets capable of reducing tar content of cigarettes and manufacture method thereof
CN103110179B (en) * 2013-03-11 2014-10-22 华宝食用香精香料(上海)有限公司 Tobacco thin composite fiber plate manufacture method
CN103181613B (en) * 2013-04-10 2015-10-21 湖北中烟工业有限责任公司 A kind of preparation method of electric destructive distillation type reconstituted tobacoo
CN105077557B (en) * 2015-07-15 2017-03-08 河北中烟工业有限责任公司 A kind of preparation method and application of pake purpke odor type plant cigarette material
CN109171011A (en) * 2018-10-12 2019-01-11 武汉醉吟茶品茶业科技有限公司 One kind replacing cigarette sifting tea
CN111575113A (en) * 2020-05-21 2020-08-25 云南中烟再造烟叶有限责任公司 Cigarette containing emblic leafflower fruit extract and application thereof
CN112586795A (en) * 2021-01-08 2021-04-02 中烟施伟策(云南)再造烟叶有限公司 Plant scented chip for cigarette leaf group and preparation method thereof
CN115644488B (en) * 2022-11-07 2024-06-11 上海烟草集团有限责任公司 Preparation method of reconstituted tobacco

Citations (3)

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Publication number Priority date Publication date Assignee Title
CN1082365A (en) * 1993-05-25 1994-02-23 潘昆年 Nutrient health-protecting cigarette
CN1126262A (en) * 1994-12-26 1996-07-10 丁树乔 Licorice root paper pulp and its products
CN1274548A (en) * 2000-06-26 2000-11-29 华南理工大学 Tabacco sheet producing process by using the leftover of cigarette factory

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Publication number Priority date Publication date Assignee Title
CN100370927C (en) * 2003-06-13 2008-02-27 广东省金叶烟草薄片技术开发有限公司 Method for tobacco leaf reforger for making cigarette using paper making method
CN101536811B (en) * 2008-03-20 2011-12-07 湖北中烟工业有限责任公司 Method for applying non-tobacco raw-material lotus leaves to paper-making sheets

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1082365A (en) * 1993-05-25 1994-02-23 潘昆年 Nutrient health-protecting cigarette
CN1126262A (en) * 1994-12-26 1996-07-10 丁树乔 Licorice root paper pulp and its products
CN1274548A (en) * 2000-06-26 2000-11-29 华南理工大学 Tabacco sheet producing process by using the leftover of cigarette factory

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WO2012012989A1 (en) 2012-02-02

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