CN101912147B - Functional tobacco sheet and preparation method thereof - Google Patents
Functional tobacco sheet and preparation method thereof Download PDFInfo
- Publication number
- CN101912147B CN101912147B CN201010242200XA CN201010242200A CN101912147B CN 101912147 B CN101912147 B CN 101912147B CN 201010242200X A CN201010242200X A CN 201010242200XA CN 201010242200 A CN201010242200 A CN 201010242200A CN 101912147 B CN101912147 B CN 101912147B
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- China
- Prior art keywords
- glycyrrhiza residue
- preparation
- tobacco sheet
- water
- glycyrrhiza
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 23
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- LTINPJMVDKPJJI-UHFFFAOYSA-N iodinated glycerol Chemical group CC(I)C1OCC(CO)O1 LTINPJMVDKPJJI-UHFFFAOYSA-N 0.000 claims abstract description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 238000000227 grinding Methods 0.000 claims abstract description 6
- 239000011248 coating agent Substances 0.000 claims abstract description 5
- 238000000576 coating method Methods 0.000 claims abstract description 5
- 239000000126 substance Substances 0.000 claims abstract description 5
- 238000005406 washing Methods 0.000 claims abstract description 4
- 239000002002 slurry Substances 0.000 claims description 22
- 239000000284 extract Substances 0.000 claims description 15
- 239000007787 solid Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 239000000419 plant extract Substances 0.000 claims description 8
- 235000015489 Emblica officinalis Nutrition 0.000 claims description 7
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 244000119298 Emblica officinalis Species 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 2
- 235000019504 cigarettes Nutrition 0.000 abstract description 36
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 11
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract description 11
- 239000003205 fragrance Substances 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract 2
- 239000011269 tar Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 239000003814 drug Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 1
- VTAJIXDZFCRWBR-UHFFFAOYSA-N Licoricesaponin B2 Natural products C1C(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2)C(O)=O)C)(C)CC2)(C)C2C(C)(C)CC1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O VTAJIXDZFCRWBR-UHFFFAOYSA-N 0.000 description 1
- 240000009120 Phyllanthus emblica Species 0.000 description 1
- 208000005392 Spasm Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 description 1
- 239000001685 glycyrrhizic acid Substances 0.000 description 1
- 229960004949 glycyrrhizic acid Drugs 0.000 description 1
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 description 1
- 235000019410 glycyrrhizin Nutrition 0.000 description 1
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Paper (AREA)
Abstract
The invention relates to a functional tobacco sheet and a preparation method thereof. The preparation method comprises the steps of: washing raw materials of glycyrrhiza residue with water, grinding the glycyrrhiza residue into thick liquid, washing the thick liquid to remove water-soluble substances, condensing, making paper, then coating on the two faces of a glycyrrhiza residue sheet and drying. The invention has the advantages that firstly, the tobacco sheet prepared by the method is free from tar, secondly, the release amount of carbon monoxide is lower, and thirdly, the tobacco sheet can obviously increase fragrance and reduce the excitement of cigarette after being added in the cigarette.
Description
Technical field
The invention belongs to the pulping and paper-making field, particularly functional tobacco sheet and preparation method thereof.
Technical background
Improving constantly of Along with people's living standard and quality of life; Cigarette consumption changes to brand consumption; Especially high-grade cigarette market; The consumer also proposes increasingly high requirement to health, the local flavor of cigarette, and the cigarette of producing high fragrance, low tar, low harm has become one of important directions of China and even the development of world's cigarette industry.At present, the main technology path that adopts has two: a kind of is " falling Jiao ", promptly through the burst size that reduces coke tar in cigarette harmful components is reduced simultaneously, and promptly concertedness reduces the cigarette smoke harmful components; Another kind is " harm reduction ", promptly adopts special technique, effectively reduces part harmful components in the cigarette smoke, and less to other composition effects, i.e. harmful components in the selectivity reducing cigarette fume.Yet this kind technology also causes the aroma-producing substance in the main flume to reduce synchronously when reducing tar, and great changes will take place to cause the local flavor of cigarette, and the consumer choice cigarette at first just needs good local flavor.
Radix Glycyrrhizae is a perennial herb, mainly is distributed in ground such as Xinjiang, Qinghai, Gansu.Radix Glycyrrhizae has beneficial gas bowl spares, relieving spasm to stop pain, moistens the lung and relieve the cough, the effect of purging intense heat and detonicating and coordinating the drug actions of a prescription, is widely used in medicine and food service industry.China Radix Glycyrrhizae is mainly used in and produces Radix Glycyrrhizae extract, glycyrrhizic acid and derivative thereof at present, and glycyrrhiza residue is the accessory substance of Radix Glycyrrhizae processing.Because the process technology means limited, China's glycyrrhiza residue also is not fully used at present, or is used for breeding feed, or the direct landfill of as fertilizer sources goes back to the soil.
Summary of the invention
The objective of the invention is to overcome the above-mentioned deficiency that prior art exists, a kind of functional tobacco sheet and preparation method thereof is provided.The reconstituted tobacoo that adopts the present invention to prepare does not have tar content, the carbon monoxide burst size is lower.This reconstituted tobacoo is added to the effect that has obvious flavouring and minimizing cigarette excitement in the cigarette.
For achieving the above object, the technical scheme that the present invention adopts is following:
A kind of preparation method of functional tobacco sheet is a raw material with the glycyrrhiza residue, and through the washing glycyrrhiza residue, defibrination is removed the water-soluble substances in the slurry, manufactures paper with pulp, and the coating plant extracts prepares.
Among the preparation method of above-mentioned functional tobacco sheet, may further comprise the steps:
(1) the glycyrrhiza residue raw material is mixed with 4-6 times of weight water, after stirring 20-50min under the mixture 80-100 ℃ condition, filter and remove moisture, must wash the back glycyrrhiza residue;
(2) will wash the back glycyrrhiza residue and mix with water, make mixed liquor solid quality content reach 5%-10% after, adding disc mill defibrination must the glycyrrhiza residue slurries;
(3) the glycyrrhiza residue slurries are mixed with 1-3 times of weight water, filter after stirring 0.5-3h under 20-30 ℃ the mixing back, gets the glycyrrhiza residue slurry;
(4) the glycyrrhiza residue slurry is carried out thin slice and manufacture paper with pulp, the glycyrrhiza residue thin slice both sides coating plant extracts obtaining gets functional tobacco sheet.
Among the preparation method of above-mentioned functional tobacco sheet, the grinding clearance of the said disc mill of step (2) is 0.05mm-0.5mm.
Among the preparation method of above-mentioned functional tobacco sheet, said plant extracts comprises more than one in emblic extract, Radix Glycyrrhizae leaf extract and the offal extract.
Among the preparation method of above-mentioned functional tobacco sheet; Said plant extracts is to be raw material with in emblic, Radix Glycyrrhizae leaf or the offal more than one; Add 4-5 times of weight ethanol water; The mass concentration of ethanol water is 60-80%, and under 40-70 ℃, extracts 1-3h, and being concentrated into the solid content weight content is that 35-60% makes.
The functional tobacco sheet that is made by above-mentioned preparation method does not have tar content, the carbon monoxide burst size is lower, can add to have obvious flavouring and the effect that reduces the cigarette excitement in the cigarette.
The present invention compared with prior art has following advantage:
(1) reconstituted tobacoo of the present invention's preparation is raw material with the glycyrrhiza residue, does not contain raw materials such as offal, offal, does not therefore have tar content.Add this reconstituted tobacoo to can significantly reduce cigarette in the production of cigarettes tar content with certain proportion.
(2) 10-50% (w/w) reconstituted tobacoo is added in the cigarette, can cigarette product carbon monoxide burst size can be reduced 10-25%, effluent cigarette carbon monoxide burst size can be reduced 20-45%.
(3) this reconstituted tobacoo adds the fragrance that can significantly improve cigarette product in the cigarette to, reduces the excitement of fragrance.
The specific embodiment
Below in conjunction with implementing enforcement of the present invention is described further, but enforcement of the present invention and protection domain are not limited thereto.
Embodiment 1
Emblic is mixed with 4 times of weight 70% (w/w) ethanol water, and behind 70 ℃ of extraction 1h, being concentrated into solid content is 40% (w/w), obtains emblic extract.
The glycyrrhiza residue raw material is mixed with 4 times of weight water, behind 90 ℃ of stirring 30min, filter and remove moisture, must wash the back glycyrrhiza residue; To wash the back glycyrrhiza residue and mix with water, make the mixed liquor solid content reach 6% (mass percent) after, the adding grinding clearance is the disc mill defibrination of 0.05mm, must the glycyrrhiza residue slurries; The glycyrrhiza residue slurries are mixed with 2 times of weight water, behind 30 ℃ of stirring 1h, filter, get the glycyrrhiza residue slurry; The Radix Glycyrrhizae slurry is carried out thin slice manufacture paper with pulp, and be coated with emblic extract, get functional tobacco sheet in glycyrrhiza residue thin slice both sides.
This functional tobacco sheet is added in the cigarette with 15% (w/w) reconstituted tobacoo; The fragrance of cigarette product obviously improves; The tar content of cigarette reduces by 17.5%, and its carbon monoxide burst size reduces by 12.3%, and its effluent cigarette carbon monoxide burst size can reduce by 20.4%.
Embodiment 2
With Radix Glycyrrhizae leaf and 4 times of weight 70% (w/w) ethanol water, 40 ℃ are extracted 3h, and being concentrated into solid content is 50% (w/w), obtains the Radix Glycyrrhizae leaf extract.
The glycyrrhiza residue raw material is mixed with 6 times of weight water, behind 80 ℃ of stirring 20min, filter and remove moisture, must wash the back glycyrrhiza residue; To wash the back glycyrrhiza residue and mix with water, make the mixed liquor solid content reach 10% after, the adding grinding clearance is the disc mill defibrination of 0.5mm, must the glycyrrhiza residue slurries; The glycyrrhiza residue slurries are mixed with 3 times of weight water, behind 20 ℃ of stirring 3h, filter, get the glycyrrhiza residue slurry; The Radix Glycyrrhizae slurry is carried out thin slice manufacture paper with pulp, and be coated with the Radix Glycyrrhizae leaf extract, carry out drying again, get functional tobacco sheet in glycyrrhiza residue thin slice both sides.
This functional tobacco sheet is added in the cigarette with 25% (w/w) reconstituted tobacoo; The fragrance of cigarette product significantly improves; The tar content of cigarette reduces by 19.5%, and its carbon monoxide burst size reduces by 16.6%, and its effluent cigarette carbon monoxide burst size can reduce by 31.6%.
Embodiment 3
With offal and 5 times of weight 80% (w/w) ethanol water, 60 ℃ are extracted 2h, and being concentrated into solid content is 60% (w/w), obtains the offal extract.
The glycyrrhiza residue raw material is mixed with 6 times of weight water, behind 80 ℃ of stirring 20min, filter and remove moisture, must wash the back glycyrrhiza residue; To wash the back glycyrrhiza residue and mix with water, make the mixed liquor solid content reach 10% after, the adding grinding clearance is the disc mill defibrination of 0.1mm, must the glycyrrhiza residue slurries; The glycyrrhiza residue slurries are mixed with 3 times of weight water, behind 20 ℃ of stirring 3h, filter, get the glycyrrhiza residue slurry; The Radix Glycyrrhizae slurry is carried out thin slice manufacture paper with pulp, and be coated with the offal extract, get functional tobacco sheet in glycyrrhiza residue thin slice both sides.
This functional tobacco sheet is added in the cigarette with 40% (w/w) reconstituted tobacoo; The fragrance of cigarette product significantly improves; The tar content of cigarette reduces by 36.9%, and its carbon monoxide burst size reduces by 18.6%, and its effluent cigarette carbon monoxide burst size can reduce by 42.4%.
Claims (5)
1. the preparation method of functional tobacco sheet is characterized in that with the glycyrrhiza residue being raw material, and through the washing glycyrrhiza residue, defibrination is removed the water-soluble substances in the slurry, manufactures paper with pulp, and the coating plant extracts prepares; Specifically may further comprise the steps:
(1) the glycyrrhiza residue raw material is mixed with 4-6 times of weight water, after stirring 20-50min under the 80-100 ℃ of condition, filter and remove moisture, must wash the back glycyrrhiza residue;
(2) will wash the back glycyrrhiza residue and mix with water, make mixed liquor solid quality content reach 5%-10% after, adding disc mill defibrination must the glycyrrhiza residue slurries;
(3) the glycyrrhiza residue slurries are mixed with 1-3 times of weight water, filter after stirring 0.5-3h under 20-30 ℃ the mixing back, gets the glycyrrhiza residue slurry;
(4) the glycyrrhiza residue slurry is carried out thin slice and manufacture paper with pulp, the glycyrrhiza residue thin slice both sides coating plant extracts obtaining gets functional tobacco sheet.
2. preparation method according to claim 1 is characterized in that the grinding clearance of the said disc mill of step (2) is 0.05mm-0.5mm.
3. preparation method according to claim 1 is characterized in that said plant extracts comprises more than one in emblic extract, Radix Glycyrrhizae leaf extract and the offal extract.
4. preparation method according to claim 1; It is characterized in that said plant extracts is is raw material with in emblic, Radix Glycyrrhizae leaf or the offal more than one; Add 4-5 times of weight ethanol water, and under 40-70 ℃, extract 1-3h, being concentrated into the solid content weight content is that 35-60% makes; The mass concentration of said ethanol water is 60-80%.
5. the functional tobacco sheet that makes by each said preparation method of claim 1～4.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010242200XA CN101912147B (en) | 2010-07-30 | 2010-07-30 | Functional tobacco sheet and preparation method thereof |
| PCT/CN2010/078944 WO2012012989A1 (en) | 2010-07-30 | 2010-11-22 | Functional tobacco sheet and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010242200XA CN101912147B (en) | 2010-07-30 | 2010-07-30 | Functional tobacco sheet and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101912147A CN101912147A (en) | 2010-12-15 |
| CN101912147B true CN101912147B (en) | 2012-08-08 |
Family
ID=43319939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010242200XA Expired - Fee Related CN101912147B (en) | 2010-07-30 | 2010-07-30 | Functional tobacco sheet and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN101912147B (en) |
| WO (1) | WO2012012989A1 (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102068035A (en) * | 2011-01-26 | 2011-05-25 | 河南卷烟工业烟草薄片有限公司 | Method for processing tobacco pulp |
| CN102423124B (en) * | 2011-11-01 | 2013-08-28 | 吉林烟草工业有限责任公司 | Tobacco slice and preparation method thereof |
| CN102524941B (en) * | 2012-01-17 | 2013-11-06 | 湖北中烟工业有限责任公司 | Sheets capable of reducing tar content of cigarettes and manufacture method thereof |
| CN103110179B (en) * | 2013-03-11 | 2014-10-22 | 华宝食用香精香料（上海）有限公司 | Tobacco thin composite fiber plate manufacture method |
| CN103181613B (en) * | 2013-04-10 | 2015-10-21 | 湖北中烟工业有限责任公司 | A kind of preparation method of electric destructive distillation type reconstituted tobacoo |
| CN105077557B (en) * | 2015-07-15 | 2017-03-08 | 河北中烟工业有限责任公司 | A kind of preparation method and application of pake purpke odor type plant cigarette material |
| CN109171011A (en) * | 2018-10-12 | 2019-01-11 | 武汉醉吟茶品茶业科技有限公司 | One kind replacing cigarette sifting tea |
| CN111575113A (en) * | 2020-05-21 | 2020-08-25 | 云南中烟再造烟叶有限责任公司 | Cigarette containing emblic leafflower fruit extract and application thereof |
| CN112586795A (en) * | 2021-01-08 | 2021-04-02 | 中烟施伟策（云南）再造烟叶有限公司 | Plant scented chip for cigarette leaf group and preparation method thereof |
| CN115644488B (en) * | 2022-11-07 | 2024-06-11 | 上海烟草集团有限责任公司 | Preparation method of reconstituted tobacco |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1082365A (en) * | 1993-05-25 | 1994-02-23 | 潘昆年 | Nutrient health-protecting cigarette |
| CN1126262A (en) * | 1994-12-26 | 1996-07-10 | 丁树乔 | Licorice root paper pulp and its products |
| CN1274548A (en) * | 2000-06-26 | 2000-11-29 | 华南理工大学 | Tabacco sheet producing process by using the leftover of cigarette factory |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100370927C (en) * | 2003-06-13 | 2008-02-27 | 广东省金叶烟草薄片技术开发有限公司 | Method for tobacco leaf reforger for making cigarette using paper making method |
| CN101536811B (en) * | 2008-03-20 | 2011-12-07 | 湖北中烟工业有限责任公司 | Method for applying non-tobacco raw-material lotus leaves to paper-making sheets |
-
2010
- 2010-07-30 CN CN201010242200XA patent/CN101912147B/en not_active Expired - Fee Related
- 2010-11-22 WO PCT/CN2010/078944 patent/WO2012012989A1/en active Application Filing
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1082365A (en) * | 1993-05-25 | 1994-02-23 | 潘昆年 | Nutrient health-protecting cigarette |
| CN1126262A (en) * | 1994-12-26 | 1996-07-10 | 丁树乔 | Licorice root paper pulp and its products |
| CN1274548A (en) * | 2000-06-26 | 2000-11-29 | 华南理工大学 | Tabacco sheet producing process by using the leftover of cigarette factory |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101912147A (en) | 2010-12-15 |
| WO2012012989A1 (en) | 2012-02-02 |
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