CN107216947B - Preparation method of catechu extract for cigarettes - Google Patents
Preparation method of catechu extract for cigarettes Download PDFInfo
- Publication number
- CN107216947B CN107216947B CN201710615298.0A CN201710615298A CN107216947B CN 107216947 B CN107216947 B CN 107216947B CN 201710615298 A CN201710615298 A CN 201710615298A CN 107216947 B CN107216947 B CN 107216947B
- Authority
- CN
- China
- Prior art keywords
- catechu
- weight
- raw material
- parts
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 title claims abstract description 79
- 235000006226 Areca catechu Nutrition 0.000 title claims abstract description 79
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 244000080767 Areca catechu Species 0.000 title claims abstract 17
- 244000235603 Acacia catechu Species 0.000 claims abstract description 62
- 239000002994 raw material Substances 0.000 claims abstract description 35
- 239000000706 filtrate Substances 0.000 claims abstract description 18
- 238000002791 soaking Methods 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 235000021552 granulated sugar Nutrition 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 13
- 239000000052 vinegar Substances 0.000 claims abstract description 10
- 235000021419 vinegar Nutrition 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 9
- 239000008399 tap water Substances 0.000 claims abstract description 9
- 235000020679 tap water Nutrition 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 238000010298 pulverizing process Methods 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 24
- 239000000779 smoke Substances 0.000 abstract description 18
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 6
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 abstract description 6
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 abstract description 6
- 235000013599 spices Nutrition 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 5
- 238000006243 chemical reaction Methods 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 4
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 abstract description 3
- 229930091371 Fructose Natural products 0.000 abstract description 3
- 239000005715 Fructose Substances 0.000 abstract description 3
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 abstract description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract description 3
- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 abstract description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 3
- 229930006000 Sucrose Natural products 0.000 abstract description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 abstract description 3
- 150000001746 carotenes Chemical class 0.000 abstract description 3
- 235000005473 carotenes Nutrition 0.000 abstract description 3
- 239000008103 glucose Substances 0.000 abstract description 3
- 229910052742 iron Inorganic materials 0.000 abstract description 3
- 235000013379 molasses Nutrition 0.000 abstract description 3
- 229960003512 nicotinic acid Drugs 0.000 abstract description 3
- 235000001968 nicotinic acid Nutrition 0.000 abstract description 3
- 239000011664 nicotinic acid Substances 0.000 abstract description 3
- 238000012545 processing Methods 0.000 abstract description 3
- 235000019192 riboflavin Nutrition 0.000 abstract description 3
- 239000002151 riboflavin Substances 0.000 abstract description 3
- 229960002477 riboflavin Drugs 0.000 abstract description 3
- 239000005720 sucrose Substances 0.000 abstract description 3
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 abstract description 3
- 239000012530 fluid Substances 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract 2
- 244000061176 Nicotiana tabacum Species 0.000 abstract 1
- 238000002137 ultrasound extraction Methods 0.000 abstract 1
- 241000208125 Nicotiana Species 0.000 description 23
- 239000003205 fragrance Substances 0.000 description 16
- 210000001124 body fluid Anatomy 0.000 description 9
- 239000010839 body fluid Substances 0.000 description 9
- 230000000391 smoking effect Effects 0.000 description 7
- 235000009508 confectionery Nutrition 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 241000411851 herbal medicine Species 0.000 description 5
- 239000008213 purified water Substances 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 210000000214 mouth Anatomy 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000000523 sample Substances 0.000 description 3
- 235000000346 sugar Nutrition 0.000 description 3
- CXQWRCVTCMQVQX-LSDHHAIUSA-N (+)-taxifolin Chemical compound C1([C@@H]2[C@H](C(C3=C(O)C=C(O)C=C3O2)=O)O)=CC=C(O)C(O)=C1 CXQWRCVTCMQVQX-LSDHHAIUSA-N 0.000 description 2
- 201000007100 Pharyngitis Diseases 0.000 description 2
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 208000002399 aphthous stomatitis Diseases 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- XHEFDIBZLJXQHF-UHFFFAOYSA-N fisetin Chemical compound C=1C(O)=CC=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 XHEFDIBZLJXQHF-UHFFFAOYSA-N 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- IYRMWMYZSQPJKC-UHFFFAOYSA-N kaempferol Chemical compound C1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 IYRMWMYZSQPJKC-UHFFFAOYSA-N 0.000 description 2
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002674 ointment Substances 0.000 description 2
- 239000008194 pharmaceutical composition Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- PADQINQHPQKXNL-LSDHHAIUSA-N (+)-dihydrokaempferol Chemical compound C1([C@@H]2[C@H](C(C3=C(O)C=C(O)C=C3O2)=O)O)=CC=C(O)C=C1 PADQINQHPQKXNL-LSDHHAIUSA-N 0.000 description 1
- BSYNFGPFPYSTTM-UHFFFAOYSA-N 2-hydroxypropanoic acid;hydrate Chemical compound O.CC(O)C(O)=O BSYNFGPFPYSTTM-UHFFFAOYSA-N 0.000 description 1
- 235000011438 Albizia odoratissima Nutrition 0.000 description 1
- 240000005482 Albizia procera Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000220485 Fabaceae Species 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- GQODBWLKUWYOFX-UHFFFAOYSA-N Isorhamnetin Natural products C1=C(O)C(C)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 GQODBWLKUWYOFX-UHFFFAOYSA-N 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 206010053615 Thermal burn Diseases 0.000 description 1
- 206010053476 Traumatic haemorrhage Diseases 0.000 description 1
- 208000025865 Ulcer Diseases 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001765 catechin Chemical class 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- RAYJUFCFJUVJBB-UHFFFAOYSA-N dihydrokaempferol Natural products OC1Oc2c(O)cc(O)cc2C(=O)C1c3ccc(O)cc3 RAYJUFCFJUVJBB-UHFFFAOYSA-N 0.000 description 1
- KQNGHARGJDXHKF-UHFFFAOYSA-N dihydrotamarixetin Natural products C1=C(O)C(OC)=CC=C1C1C(O)C(=O)C2=C(O)C=C(O)C=C2O1 KQNGHARGJDXHKF-UHFFFAOYSA-N 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000012734 epicatechin Nutrition 0.000 description 1
- -1 etc. Chemical compound 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000011990 fisetin Nutrition 0.000 description 1
- HVQAJTFOCKOKIN-UHFFFAOYSA-N flavonol Natural products O1C2=CC=CC=C2C(=O)C(O)=C1C1=CC=CC=C1 HVQAJTFOCKOKIN-UHFFFAOYSA-N 0.000 description 1
- 150000002216 flavonol derivatives Chemical class 0.000 description 1
- 235000011957 flavonols Nutrition 0.000 description 1
- 210000000232 gallbladder Anatomy 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 235000008800 isorhamnetin Nutrition 0.000 description 1
- IZQSVPBOUDKVDZ-UHFFFAOYSA-N isorhamnetin Chemical compound C1=C(O)C(OC)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 IZQSVPBOUDKVDZ-UHFFFAOYSA-N 0.000 description 1
- 235000008777 kaempferol Nutrition 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 229920002414 procyanidin Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- 239000013074 reference sample Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Abstract
The invention provides a preparation method of a catechu extract for cigarettes, which comprises the steps of crushing a catechu raw material, soaking the crushed catechu raw material in old vinegar in a Shanxi water tower, baking the catechu raw material, adding 300 parts by weight of baked catechu and 5-30 parts by weight of brown granulated sugar into 3000 parts by weight of tap water in 300-3000 parts by weight, soaking the mixture for 2-8 hours, carrying out ultrasonic extraction for 2 times at room temperature, wherein each time lasts for 0.5-1 hour, cooling and filtering the mixture, and respectively reserving two filtrates; mixing filtrates, and concentrating under reduced pressure at 40-54 deg.C to 2-6 times of Catechu raw material weight to obtain the required Catechu extract for cigarette. The invention refers to the technical method of processing Chinese traditional medicine, the catechu raw material is processed by vinegar, the components in the catechu raw material are easier to dissolve after full reaction, the prepared spice can also moisten smoke after being added into the tobacco leaf formula by utilizing the advantage that the brown granulated sugar is rich in sucrose, glucose, molasses, fructose, iron, riboflavin, carotene, nicotinic acid and other components, and the mouth and throat fluid production feeling is increased.
Description
Technical Field
The invention relates to a tobacco flavor and a preparation method thereof, in particular to a preparation method of a catechu extract for cigarettes.
Background
With the improvement of the consumption level of people, the demand of high-quality cigarettes is continuously increased, but the production of the high-quality cigarettes is limited by limited first-class raw materials, and the important measures for solving the contradiction are to enhance the fragrance of the tobacco, improve the quality of the tobacco leaves and improve the utilization rate of the tobacco leaves by adding fragrance and charging materials. In the cigarette products, the aroma and the smoking taste of cigarettes are very important, the addition of spices is a key link in the cigarette industry, and is also one of effective means for improving the product style and the cigarette aroma quality, and certain cigarette products with satisfactory aroma and smoking taste can be provided for consumers.
China is a hometown of Chinese herbal medicines, and the application of the Chinese herbal medicine additive in Chinese cigarettes is a special advantage of the Chinese tobacco industry. China has rich Chinese herbal medicine resources, and a plurality of varieties have similar chemical components with tobacco structures, but have different performances, and can make up for the deficiencies of the tobacco in some aspects. With the application of Chinese herbal medicine additives in cigarettes being increasingly accepted by consumers, more and more tobacco researchers have found tobacco flavors and fragrances from natural Chinese herbal medicines, and the natural fragrances are more and more widely applied to cigarettes.
Catechu is a commonly used Chinese medicine, also known as Catechu ointment, Catechu, and is dried decoction ointment of peeled branch and dried stem of Catechu of Albizia of Leguminosae. Distributed in south Yunnan region, Hainan island is cultivated. Collecting branches and trunks in winter, removing the outer skin, cutting into large blocks, adding water, decocting, concentrating, and drying. It is recorded in Ben Cao Zheng (materia medica decoction) that it has the actions of purging fire and promoting the production of body fluid, clearing phlegm and cough, and treating aphtha and pharyngitis. It is used clinically in treating unhealed ulcer, eczema, aphtha, sore throat, traumatic injury, traumatic hemorrhage. Modern pharmacological experiments show that the medicine has the functions of protecting liver, benefiting gallbladder, enhancing immunity, resisting bacteria and diminishing inflammation. The chemical components of catechu mainly include catechu tannic acid, levo-and racemic catechins, levo-and racemic epicatechins, tannin, and flavonols such as fisetin, quercetin, quercetagetin, etc., kaempferol, dihydrokaempferol, taxifolin, isorhamnetin, dextro-afzelechin, etc. The development and utilization of the catechu are mainly used in the pharmaceutical industry at present, for example, the chinese patent with application number CN03111902 discloses a pharmaceutical composition containing the catechu for treating throat diseases and a preparation method thereof, and the chinese patent with application number CN00102965.7 discloses a pharmaceutical composition containing the catechu for treating burns and scalds and a preparation method thereof. CN102978002A discloses a method for preparing a catechu extract for cigarettes, which is to extract the catechu by using 30-95% ethanol or 0.1-1% lactic acid water solution, and the prepared extract is added into the cigarettes to enrich the cigarette fragrance, soften and smooth the smoke and increase the comfort of the throat. However, when the extract is added into cigarettes, the sweet feeling of smoke is not obvious, and the body fluid is not generated during smoking.
Disclosure of Invention
The invention aims to provide a preparation method of a catechu extract for cigarettes, which has the advantages of simple process, low cost and stable raw material source, and the catechu raw material is processed with vinegar by referring to a process method for processing traditional Chinese medicines, so that components in the catechu raw material are easier to dissolve after full reaction, and the prepared spice has obvious fragrance and can also sweeten smoke and increase the body fluid production feeling of the oral cavity and the throat by adding a solvent for extraction by utilizing the advantage that brown granulated sugar is rich in sucrose, glucose, molasses, fructose, iron, riboflavin, carotene, nicotinic acid and other components.
The technical scheme provided by the invention is as follows: a preparation method of a catechu extract for cigarettes comprises the following steps:
(1) pulverizing Catechu, and sieving with 100 mesh sieve;
(2) soaking the pulverized Catechu raw materials in mature vinegar of Shanxi water tower at a weight ratio of 1:1 for 8-24 hr.
(3) Baking the soaked catechu raw material at 200 deg.C for 2 hr.
(4) Adding 300 parts by weight of baked catechu 100-containing materials and 5-30 parts by weight of brown granulated sugar into 3000 parts by weight of tap water 300-containing materials, soaking for 2-8h, ultrasonically extracting for 2 times at room temperature, each time for 0.5-1 h, cooling, filtering, and respectively reserving two filtrates;
(5) and (4) combining the filtrates in the step (4), and concentrating under reduced pressure at 40-54 ℃ until the weight of the catechu raw material is 2-6 times that of the catechu raw material, so as to obtain the required catechu extract for cigarettes.
Further, the step (4) is: adding 200 parts by weight of baked catechu and 10 parts by weight of brown granulated sugar into 1000 parts by weight of tap water, soaking for 4 hours, ultrasonically extracting for 2 times at room temperature, each time for 0.5 hour, cooling, filtering, and respectively reserving two filtrates; mixing the filtrates, and concentrating under reduced pressure at 40 deg.C to 5 times of the weight of Catechu raw material to obtain the required Catechu extract for cigarette.
The invention has the beneficial effects that:
1. the invention refers to the technical method of processing Chinese traditional medicine, the catechu raw material is processed by vinegar, the ingredients in the catechu raw material are easier to dissolve out after full reaction, the advantage that the brown granulated sugar is rich in sucrose, glucose, molasses, fructose, iron, riboflavin, carotene, nicotinic acid and other ingredients is utilized, the solvent is added for extraction, the prepared spice has obvious fragrance and is coordinated with the fragrance of the tobacco leaves, the spice can also moisten the smoke after being added into the tobacco leaf group formula, and the fluid production feeling of the oral cavity and the throat is increased.
2. The raw materials adopted by the invention are easily available, the preparation process is simple, the cost is low, and the production conversion is facilitated.
Detailed Description
The following examples are included to further illustrate the technical problems associated with the present invention, and it should be noted that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. Other insubstantial modifications and adaptations of the present invention can be made without departing from the scope of the present invention.
Example 1
1) Pulverizing Catechu, and sieving with 100 mesh sieve;
2) soaking the pulverized catechu raw material in aged vinegar of a water tower in Shanxi at a weight ratio of 1:1 for 8-24 hours;
3) baking the soaked catechu raw material for 2 hours at a high temperature of 200 ℃;
4) adding 200 parts by weight of baked catechu and 10 parts by weight of brown granulated sugar into 1000 parts by weight of tap water, soaking for 4 hours, ultrasonically extracting for 2 times at room temperature, each time for 0.5 hour, cooling, filtering, and respectively reserving 2 times of filtrate; mixing the filtrates, and concentrating under reduced pressure at 40 deg.C to 5 times of the weight of Catechu raw material to obtain the required Catechu extract for cigarette.
5) Taking the catechu extract obtained above, according to the addition amount of the extract accounting for 0.1% of the dry weight of the cut tobacco, according to the conventional feeding process, dissolving with purified water, uniformly spraying into blank cut tobacco, drying the cut tobacco at 65 ℃ until the water content is 16%, and making into cigarette.
Example 2
1) Pulverizing Catechu, and sieving with 100 mesh sieve;
2) soaking the pulverized catechu raw material in aged vinegar of a water tower in Shanxi at a weight ratio of 1:1 for 8-24 hours;
3) baking the soaked catechu raw material for 2 hours at a high temperature of 200 ℃;
4) adding baked catechu 100 weight parts and brown granulated sugar 15 weight parts into 1500 weight parts of tap water, soaking for 2h, ultrasonically extracting at room temperature for 2 times, each time for 1 h, cooling, filtering, and respectively collecting 2 filtrates; mixing the filtrates, and concentrating under reduced pressure at 54 deg.C until the weight of Catechu is 2 times of that of the raw material to obtain the required Catechu extract for cigarette.
5) Taking the catechu extract obtained above, according to the addition amount of the extract accounting for 0.01% of the dry weight of the cut tobacco, according to the conventional feeding process, dissolving with purified water, uniformly spraying into blank cut tobacco, drying the cut tobacco at 55 ℃ until the water content is 12%, and making into cigarette.
Example 3
1) Pulverizing Catechu, and sieving with 100 mesh sieve;
2) soaking the pulverized catechu raw material in aged vinegar of a water tower in Shanxi at a weight ratio of 1:1 for 8-24 hours;
3) baking the soaked catechu raw material for 2 hours at a high temperature of 200 ℃;
4) adding 150 parts by weight of roasted catechu and 5 parts by weight of brown granulated sugar into 2000 parts by weight of tap water, soaking for 3 hours, ultrasonically extracting for 2 times at room temperature, each time for 45 minutes, cooling, filtering, and respectively reserving 2 times of filtrate; mixing the filtrates, and concentrating under reduced pressure at 45 deg.C until the weight of Catechu is 4 times of that of the raw material to obtain the required Catechu extract for cigarette.
5) Taking the catechu extract obtained above, according to the addition amount of the extract accounting for 0.05% of the dry weight of the cut tobacco, according to the conventional feeding process, dissolving with purified water, uniformly spraying into blank cut tobacco, drying the cut tobacco at 65 ℃ until the moisture content is 14%, and making into cigarette.
Example 4
1) Pulverizing Catechu, and sieving with 100 mesh sieve;
2) soaking the pulverized catechu raw material in aged vinegar of a water tower in Shanxi at a weight ratio of 1:1 for 8-24 hours;
3) baking the soaked catechu raw material for 2 hours at a high temperature of 200 ℃;
4) adding 300 parts by weight of roasted catechu and 20 parts by weight of brown granulated sugar into 2500 parts by weight of tap water, soaking for 6h, ultrasonically extracting at room temperature for 2 times, each time for 0.5 h, cooling, filtering, and respectively reserving 2 times of filtrate; mixing the filtrates, and concentrating under reduced pressure at 50 deg.C to 6 times of the weight of Catechu raw material to obtain the required Catechu extract for cigarette.
5) Taking the catechu extract obtained above, dissolving with purified water according to the addition amount of 0.1% of the extract in the dry weight of tobacco shreds, uniformly spraying into blank tobacco shreds according to conventional charging process, drying the tobacco shreds at 70 deg.C to water content of 16%, and making into cigarette.
And (3) evaluating and detecting:
CN102978002A is used as a reference sample, brown granulated sugar is not added, other steps are the same as the steps of the method, the catechu extract (non-sugar sample preparation) obtained by extraction is used as a comparison, the cigarette is prepared by adopting the same method, the smoking evaluation is carried out according to the cigarette smoking evaluation standard, and the smoking evaluation result is shown in the following table 1:
TABLE 1 cigarette evaluation effect
| Sample (I) | Evaluation of Effect |
| Control sample | The cigarette has rich fragrance and soft and delicate smoke. |
| Unsweetened sample | The cigarette has rich fragrance, obvious dry feeling of the smoke and slight stimulation. |
| Example 1 | The cigarette has rich fragrance, soft and delicate smoke, sweet smoke and body fluid generation feeling. |
| Example 2 | The cigarette has rich fragrance, soft and delicate smoke, sweet smoke and body fluid generation feeling. |
| Example 3 | The cigarette has rich fragrance, soft and delicate smoke, sweet smoke and body fluid generation feeling. |
| Example 4 | The cigarette has rich fragrance, soft and delicate smoke, sweet smoke and body fluid generation feeling. |
The cigarette blending engineer performs smoking evaluation, and the experimental result shows that compared with CN102978002A, the cigarette of the examples 1-4 is richer in fragrance, and stronger in sweet feeling and body fluid production feeling of the smoke. Compared with the extract without the sugar treatment, the extract without the sugar treatment has obvious smoke drying feeling and slight stimulation. The spice prepared by the invention has obvious fragrance, can also sweeten smoke and increase the body fluid production feeling of the oral cavity and the throat.
The above description is only a detailed description of specific embodiments of the present invention, and should not be taken as limiting the invention, and any modifications, equivalents, improvements, etc. made on the design concept of the present invention should be included in the protection scope of the present invention.
Claims (2)
1. A preparation method of a catechu extract for cigarettes is characterized by comprising the following steps:
(1) pulverizing Catechu, and sieving with 100 mesh sieve;
(2) soaking the pulverized catechu raw material in aged vinegar of a water tower in Shanxi at a weight ratio of 1:1 for 8-24 hours;
(3) baking the soaked catechu raw material for 2 hours at a high temperature of 200 ℃;
(4) adding 300 parts by weight of baked catechu 100-containing materials and 5-30 parts by weight of brown granulated sugar into 3000 parts by weight of tap water 300-containing materials, soaking for 2-8h, ultrasonically extracting for 2 times at room temperature, each time for 0.5-1 h, cooling, filtering, and respectively reserving two filtrates;
(5) and (4) combining the filtrates in the step (4), and concentrating under reduced pressure at 40-54 ℃ until the weight of the catechu raw material is 2-6 times that of the catechu raw material, so as to obtain the required catechu extract for cigarettes.
2. The method for preparing a catechu extract for cigarettes according to claim 1, which is characterized in that: the step (4) is as follows: adding 200 parts by weight of baked catechu and 10 parts by weight of brown granulated sugar into 1000 parts by weight of tap water, soaking for 4 hours, ultrasonically extracting for 2 times at room temperature, each time for 0.5 hour, cooling, filtering, and respectively reserving two filtrates; mixing the filtrates, and concentrating under reduced pressure at 40 deg.C to 5 times of the weight of Catechu raw material to obtain the required Catechu extract for cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710615298.0A CN107216947B (en) | 2017-07-26 | 2017-07-26 | Preparation method of catechu extract for cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710615298.0A CN107216947B (en) | 2017-07-26 | 2017-07-26 | Preparation method of catechu extract for cigarettes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107216947A CN107216947A (en) | 2017-09-29 |
| CN107216947B true CN107216947B (en) | 2020-09-08 |
Family
ID=59954038
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710615298.0A Active CN107216947B (en) | 2017-07-26 | 2017-07-26 | Preparation method of catechu extract for cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107216947B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107637859B (en) * | 2017-10-24 | 2023-03-21 | 湖北中烟工业有限责任公司 | Mixed acid for tobacco charging and preparation method and application thereof |
| CN109259293B (en) * | 2018-09-13 | 2021-03-23 | 云南中烟工业有限责任公司 | Tea baking aroma reconstituted tobacco and preparation method and application thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101744362B (en) * | 2008-12-04 | 2012-12-19 | 安徽中烟工业公司 | Processing material for improving quality of black coral tobacco |
| CN102978002A (en) * | 2012-11-13 | 2013-03-20 | 湖北中烟工业有限责任公司 | Cutch extracts preparation method for tobacco and application thereof |
| CN106148011A (en) * | 2016-07-20 | 2016-11-23 | 湖北中烟工业有限责任公司 | The preparation method of a kind of cigarette radix valerianae extract and the application in Medicated cigarette thereof |
-
2017
- 2017-07-26 CN CN201710615298.0A patent/CN107216947B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN107216947A (en) | 2017-09-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101768514B (en) | Alhagi sparsifolia extract and preparation method and application thereof | |
| CN101322579A (en) | Low-harm type cigarette capable of reducing cigarette harm and manufacture method thereof | |
| CN101704900A (en) | Extraction method of cactus polysaccharide and application thereof in cigarettes | |
| CN101912147A (en) | Functional tobacco sheet and preparation method thereof | |
| CN107216947B (en) | Preparation method of catechu extract for cigarettes | |
| CN103351950A (en) | Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same | |
| CN111528519A (en) | Preparation method and application of enzyme preparation treated tobacco emblic leafflower fruit enzymolysis extract | |
| CN102839051B (en) | Cigarette sensory flavoring humectant and preparation method and application thereof | |
| CN106539125A (en) | Sweetened humectant additive of a kind of cigarette shreds and preparation method thereof | |
| CN110150727B (en) | Preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes | |
| CN101878955B (en) | Manufacturing method of rich-fragrance reduced-harmfulness cigarette | |
| CN107802025B (en) | Preparation method of ginkgo leaf extract and application of ginkgo leaf extract in cigarettes | |
| CN107201274B (en) | Method for extracting tobacco flavor by taking tamarind as raw material and application | |
| CN110771944A (en) | Apocynum venetum health-care cigarette and preparation method thereof | |
| CN102978002A (en) | Cutch extracts preparation method for tobacco and application thereof | |
| CN105713924A (en) | Method for preparing fermented type tobacco spice from rosa sterilis | |
| CN106833897B (en) | Preparation method of crisp pear tobacco flavor | |
| CN102703216A (en) | Method for making momordica grosvenori tobacco flavor | |
| CN105011356A (en) | Preparation method of flavoring and moisturizing agent using glucoside of red dates | |
| KR101119883B1 (en) | Manufacturing Method of Conventional Soybean Paste Using Leaf, Stem and Root Bark of Mulberry Tree | |
| CN114532580A (en) | Preparation method of cigar tobacco leaves | |
| CN109007965B (en) | Liupu tea cigarette and making method thereof | |
| CN103540407A (en) | Kapok essential oil | |
| CN111466609A (en) | Preparation method of momordica grosvenori extract for treating cigarettes by using enzyme preparation | |
| CN105768200A (en) | Application of plumeria rubra and leaves in cigarette |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |