CN105011356A - Preparation method of flavoring and moisturizing agent using glucoside of red dates - Google Patents
Preparation method of flavoring and moisturizing agent using glucoside of red dates Download PDFInfo
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- CN105011356A CN105011356A CN201510346898.2A CN201510346898A CN105011356A CN 105011356 A CN105011356 A CN 105011356A CN 201510346898 A CN201510346898 A CN 201510346898A CN 105011356 A CN105011356 A CN 105011356A
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- Prior art keywords
- red date
- glucoside
- flavoring
- red dates
- extract
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- 229930182478 glucoside Natural products 0.000 title claims abstract description 43
- 150000008131 glucosides Chemical class 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 230000003020 moisturizing effect Effects 0.000 title abstract 7
- 239000000284 extract Substances 0.000 claims abstract description 32
- 238000004108 freeze drying Methods 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 12
- 238000000199 molecular distillation Methods 0.000 claims abstract description 8
- 239000003906 humectant Substances 0.000 claims description 20
- 239000012141 concentrate Substances 0.000 claims description 11
- 235000013399 edible fruits Nutrition 0.000 claims description 10
- 239000006228 supernatant Substances 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 230000001476 alcoholic effect Effects 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 239000002244 precipitate Substances 0.000 claims description 5
- 238000000746 purification Methods 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 235000019504 cigarettes Nutrition 0.000 abstract description 41
- 230000000694 effects Effects 0.000 abstract description 8
- 239000000796 flavoring agent Substances 0.000 abstract description 8
- 235000019634 flavors Nutrition 0.000 abstract description 8
- 238000000605 extraction Methods 0.000 abstract description 7
- 239000000779 smoke Substances 0.000 abstract description 6
- 239000002994 raw material Substances 0.000 abstract description 5
- 150000001875 compounds Chemical class 0.000 abstract description 4
- 239000003795 chemical substances by application Substances 0.000 abstract 5
- 238000009833 condensation Methods 0.000 abstract 2
- 230000005494 condensation Effects 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 238000003808 methanol extraction Methods 0.000 abstract 1
- 230000035699 permeability Effects 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- -1 glucoside compounds Chemical class 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 239000002304 perfume Substances 0.000 description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 230000008542 thermal sensitivity Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- VGGSULWDCMWZPO-ODEMIOGVSA-N spinosin Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1C1=C(O)C=2C(=O)C=C(OC=2C=C1OC)C=1C=CC(O)=CC=1)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VGGSULWDCMWZPO-ODEMIOGVSA-N 0.000 description 2
- 150000003505 terpenes Chemical class 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241000219100 Rhamnaceae Species 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- VGGSULWDCMWZPO-UHFFFAOYSA-N flavoayamenin Natural products COC1=CC=2OC(C=3C=CC(O)=CC=3)=CC(=O)C=2C(O)=C1C1OC(CO)C(O)C(O)C1OC1OC(CO)C(O)C(O)C1O VGGSULWDCMWZPO-UHFFFAOYSA-N 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 125000003147 glycosyl group Chemical group 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000010148 water-pollination Effects 0.000 description 1
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- Confectionery (AREA)
Abstract
The invention discloses a preparation method of a flavoring and moisturizing agent using glucoside of red dates.The preparation method comprises following steps: preparing red date extracts by using red dates as raw material; and carrying out operation including freeze drying, alcohol precipitation, condensation, molecular distillation and the like to red date extracts in order to obtain the flavoring and moisturizing agent using glucoside of red dates. The preparation method of the flavoring and moisturizing agent using glucoside of red dates has following beneficial effects: a high-quality flavoring and moisturizing agent using glucoside of red dates by utilizing red dates as raw material, employing glucoside-containing compounds of red dates extracted by ultrasonic waves, using manners such as freeze drying, low-temperature condensation and molecular distillation with the purpose of preventing glucoside-containing compounds from being decomposed during an extraction process; the flavoring and moisturizing agent using glucoside of red dates is applied to cigarettes and have effects of enriching cigarette flavors, improving permeability of cigarette flavor, tendering smoke, reducing irritation feelings and comforting the throat and helps increase moisture content of cigarette smoke in a range of 5% to 30%; and by replacing a conventional methanol extraction method, the method can be applied to cigarettes and offers a new approach to flavoring and moisturizing research of cigarettes.
Description
Technical field
The present invention relates to cigarette additive field, be specifically related to a kind ofly can promote flavor quality of cigarette and there is the preparation method of the red date glucosides flavouring humectant of flavouring humectation effect.
Background technology
Flavouring humectation technology be promote Chinese-style cigarette quality, increase perfume quantity, carry raise note, set off nature cigarette fragrant, reduce flue gas drying sense, strengthen flue gas and to promote the production of body fluid the key technology of sense, raising cigarette comfort level.Research cigarette flavouring humectation technology is conducive to improving cigarette product design, processing comprehensive technical level comprehensively, is conducive to outstanding Chinese-style cigarette style characteristic, strengthens Chinese-style cigarette competitiveness.
Red date is Rhamnaceae plant, all has cultivation all over China, is a kind of abundant plant resources.Meanwhile, red date is also a kind of integration of drinking and medicinal herbs food, has this abundant nutritive value, have the good reputation of " nutrition and health care ball " and " woody grain ".A large amount of glucoside compounds is rich in red date, such as ethyl-D-furanone glucosides and derivative thereof, brass-bis--glucoside A, different spinosin, Quercetin-4-O-a-L-rhamnopyranosyl-3-O-a-L-rhamnopyranosyl-β-D-glucopyranoside etc., the existence of these glucoside compounds makes to be that perfume material prepared by raw material has higher using value in cigarette with red date.Be that the cigarette perfume material of raw material mainly contains red date extract, red date medicinal extract, red date absolute oil and red date Maillard reaction thing on the market with red date, these extracts have larger using value in cigarette, but do not see the product of red date glucosides flavouring humectant.
Glucosides class is the derivative of sugar, it is the prerequisite of the aroma substance of many natural plants, itself does not have fragrance, its release fragrance component can be impelled by the method such as enzyme process, heating, be also referred to as latent aroma compounds, be added into using this compounds as cigarette additive in cigarette, be conducive to the slowly-releasing of cigarette flavor, and in glucosides class, glycosyl hydrophily is better, also has certain humectation effect.Glucosides class has thermal sensitivity, runs into high temperature and very easily decomposes, and therefore, the lower boiling solvent of the many employings of glucosides class extracts, and generally selects methyl alcohol to extract, but methyl alcohol extracts products obtained therefrom does not meet cigarette additive requirement.
Ultrasonic wave extracts the extraction low with its Extracting temperature, recovery rate is high, extraction time is short unique advantage is applied to natural plants effective content, and it effectively can solve a difficult problem for glucoside compound pyrolytic, is progressively applied in the extraction of glucoside compound.
Freeze drying is chilled to by water-containing materials below freezing, makes water change ice into, then under high vacuum, change ice into steam and the drying means removed.Freeze drying operates under vacuum and low temperature, and material dewatering is thorough, rehydration is fast.Dried material can keep original chemical composition and physical property.Heat-sensitive substance is particularly suitable for, after the dry materials of thermal sensitivity can be made, retains heat-sensitive ingredients.
Molecular distillation technique can be purified to glucosides class chemicals, get rid of red date slightly extract in terpene, thus eliminate these Small molecular terpenes and bring irritating negative effect to cigarette.
Summary of the invention
The object of this invention is to provide a kind of preparation method of red date glucosides flavouring humectant, the technology such as, molecular clock concentrated in conjunction with ultrasonic wave extraction, freeze drying, low temperature, develop a kind of novel red date glucosides flavouring humectant.
The invention provides a kind of preparation method of red date glucosides flavouring humectant, it is characterized in that, comprise the following steps:
(1) in red date fruit, add the water of corresponding red date fruit weight 4 ~ 6 times, be utilize ultrasonic wave to extract under the condition of 50 ~ 70 DEG C 2 ~ 6 hours in temperature, cooled and filtered, obtained red date extract;
(2) utilize Freeze Drying Technique to carry out concentration gained red date extract, wherein feed liquid thickness is 1 ~ 2 centimetre, and vacuum is 10Pa, and drying time is 6 ~ 12 hours;
(3) in the red date extract after gained freeze drying, add the alcoholic solution of 80 ~ 95% of 3 times of red date extract weight, precipitate after 24 hours and filter, obtain red date supernatant;
(4) be 0.1Mpa by gained red date supernatant at pressure, temperature is that to be concentrated into relative density under the condition of 45 DEG C be 1.20g/cm
3, obtain red date concentrate;
(5) molecular distillation technique is utilized to carry out separation and purification treatment gained red date concentrate, wherein molecular clock pressure is 5 ~ 50Pa, vapo(u)rizing temperature is 50 ~ 80 DEG C, inlet amount is 20 ~ 100ml/h, blade applicator rotating speed is 100 ~ 300r/min, and gained weight molecule component thing is red date glucosides flavouring humectant.
Due to it, ultrasonic wave extracts has that Extracting temperature is low, recovery rate is high and the advantage such as extraction time is short, rapidly and efficiently can extract the glucoside compound in natural plants, and can also ensure that glucosides class can not be decomposed.Freeze drying operates under vacuum and low temperature due to it, have and make the advantages such as material dewatering is thorough, rehydration is fast, and dried material can keep original chemical composition and physical property, retains heat-sensitive ingredients after can also making the glucoside compound drying of thermal sensitivity.
The present invention take red date as raw material, utilize the glucoside compound in ultrasonic wave extraction red date, and utilize the modes such as freeze drying and low temperature concentrate, prevent glucoside compound not to be decomposed in leaching process, obtain a kind of colory red date glucosides flavouring humectant.This red date glucosides flavouring humectant is applied in cigarette, have enrich cigarette perfume (or spice), increase cigarette flavor thoroughly the property sent out, soft fine and smooth flue gas, reduce excitant, improve the effects such as throat's comfortableness, and cigarette smoke moisture content can be made to improve 5% ~ 30%.Meanwhile, the method instead of traditional methyl alcohol and extracts, and it can be applied in cigarette, provides a new way to cigarette flavouring humectation research.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1:
The preparation method of a kind of red date glucosides flavouring humectant disclosed by the invention, comprises the following steps:
(1) in red date fruit, add the water of corresponding red date fruit weight 4 times, be utilize ultrasonic wave to extract 2 hours, cooled and filtered under the condition of 50 DEG C in temperature, obtained red date extract.
(2) utilize Freeze Drying Technique to carry out concentration gained red date extract, wherein feed liquid thickness is 2 centimetres, and vacuum is 10Pa, and drying time is 6 hours.
(3) in the red date extract after gained freeze drying, add the alcoholic solution of 95% of 3 times of red date extract weight, precipitate after 24 hours and filter, obtain red date supernatant.
(4) be 0.1Mpa by gained red date supernatant at pressure, temperature is that to be concentrated into relative density under the condition of 45 DEG C be 1.20g/cm
3, obtain red date concentrate.
(5) molecular distillation technique is utilized to carry out separation and purification treatment gained red date concentrate, wherein molecular clock pressure is 50Pa, and vapo(u)rizing temperature is 80 DEG C, and inlet amount is 100ml/h, blade applicator rotating speed is 300r/min, and gained weight molecule component thing is red date glucosides flavouring humectant.
This red date glucosides flavouring humectant is applied in cigarette, have enrich cigarette perfume (or spice), increase cigarette flavor thoroughly the property sent out, soft fine and smooth flue gas, reduce excitant, improve the effects such as throat's comfortableness, and cigarette smoke moisture content can be made to improve 6.25%.
Embodiment 2:
The preparation method of a kind of red date glucosides flavouring humectant disclosed by the invention, comprises the following steps:
(1) in red date fruit, add the water of corresponding red date fruit weight 5 times, be utilize ultrasonic wave to extract 4 hours, cooled and filtered under the condition of 60 DEG C in temperature, obtained red date extract.
(2) utilized by red date extract Freeze Drying Technique to carry out concentration, wherein feed liquid thickness is 1 centimetre, and vacuum is 10Pa, and drying time is 9 hours.
(3) in the red date extract after gained freeze drying, add the alcoholic solution of 95% of 3 times of red date extract weight, precipitate after 24 hours and filter, obtain red date supernatant.
(4) be 0.1Mpa by gained red date supernatant at pressure, temperature is that to be concentrated into relative density under the condition of 45 DEG C be 1.20g/cm
3, obtain red date concentrate.
(5) molecular distillation technique is utilized to carry out separation and purification treatment gained red date concentrate, wherein molecular clock pressure is 20Pa, and vapo(u)rizing temperature is 80 DEG C, and inlet amount is 60ml/h, blade applicator rotating speed is 200r/min, and gained weight molecule component thing is red date glucosides flavouring humectant.
This red date glucosides flavouring humectant is applied in cigarette, have enrich cigarette perfume (or spice), increase cigarette flavor thoroughly the property sent out, soft fine and smooth flue gas, reduce excitant, improve the effects such as throat's comfortableness, and cigarette smoke moisture content can be made to improve 8.32%.
Embodiment 3:
The preparation method of a kind of red date glucosides flavouring humectant disclosed by the invention, comprises the following steps:
(1) in red date fruit, add the water of corresponding red date fruit weight 6 times, be utilize ultrasonic wave to extract 6 hours, cooled and filtered under the condition of 70 DEG C in temperature, obtained red date extract.
(2) utilize Freeze Drying Technique to carry out concentration gained red date extract, wherein feed liquid thickness is 2 centimetres, and vacuum is 10Pa, and drying time is 6 hours.
(3) in the red date extract after gained freeze drying, add the alcoholic solution of 80% of 3 times of red date extract weight, precipitate after 24 hours and filter, obtain red date supernatant.
(4) be 0.1Mpa by gained red date supernatant at pressure, temperature is that to be concentrated into relative density under the condition of 45 DEG C be 1.20g/cm
3, obtain red date concentrate.
(5) molecular distillation technique is utilized to carry out separation and purification treatment gained red date concentrate, wherein molecular clock pressure is 5Pa, and vapo(u)rizing temperature is 80 DEG C, and inlet amount is 20ml/h, blade applicator rotating speed is 300r/min, and gained weight molecule component thing is red date glucosides flavouring humectant.
This red date glucosides flavouring humectant is applied in cigarette, have enrich cigarette perfume (or spice), increase cigarette flavor thoroughly the property sent out, soft fine and smooth flue gas, reduce excitant, improve the effects such as throat's comfortableness, and cigarette smoke moisture content can be made to improve 19.38%.
Above-mentioned unspecified part is prior art.
Claims (1)
1. a preparation method for red date glucosides flavouring humectant, is characterized in that, comprise the following steps:
(1) in red date fruit, add the water of corresponding red date fruit weight 4 ~ 6 times, be utilize ultrasonic wave to extract under the condition of 50 ~ 70 DEG C 2 ~ 6 hours in temperature, cooled and filtered, obtained red date extract;
(2) utilize Freeze Drying Technique to carry out concentration gained red date extract, wherein feed liquid thickness is 1 ~ 2 centimetre, and vacuum is 10Pa, and drying time is 6 ~ 12 hours;
(3) in the red date extract after gained freeze drying, add the alcoholic solution of 80 ~ 95% of 3 times of red date extract weight, precipitate after 24 hours and filter, obtain red date supernatant;
(4) be 0.1Mpa by gained red date supernatant at pressure, temperature is that to be concentrated into relative density under the condition of 45 DEG C be 1.20g/cm
3, obtain red date concentrate;
(5) molecular distillation technique is utilized to carry out separation and purification treatment gained red date concentrate, wherein molecular clock pressure is 5 ~ 50Pa, vapo(u)rizing temperature is 50 ~ 80 DEG C, inlet amount is 20 ~ 100ml/h, blade applicator rotating speed is 100 ~ 300r/min, and gained weight molecule component thing is red date glucosides flavouring humectant.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510346898.2A CN105011356A (en) | 2015-06-19 | 2015-06-19 | Preparation method of flavoring and moisturizing agent using glucoside of red dates |
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| CN201510346898.2A CN105011356A (en) | 2015-06-19 | 2015-06-19 | Preparation method of flavoring and moisturizing agent using glucoside of red dates |
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| CN201510346898.2A Pending CN105011356A (en) | 2015-06-19 | 2015-06-19 | Preparation method of flavoring and moisturizing agent using glucoside of red dates |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107011992A (en) * | 2017-06-06 | 2017-08-04 | 武汉黄鹤楼香精香料有限公司 | A kind of method of molecular clock Fructus Fici extract |
| CN115005493A (en) * | 2022-06-08 | 2022-09-06 | 吉林烟草工业有限责任公司 | Bean-flavor characteristic extract, preparation method thereof and cigarette |
| CN115067533A (en) * | 2022-06-14 | 2022-09-20 | 上海龙殷生物科技有限公司 | Fragrance synergist, additive and application |
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| US5513663A (en) * | 1991-12-17 | 1996-05-07 | Van Leuven; Dirk-Hector | Tobacco substitutes |
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| CN103585782A (en) * | 2013-11-26 | 2014-02-19 | 浙江安赛生物科技有限公司 | Method for preparing red date extract by utilizing ultrasonic cavitation technology |
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| CN104479879A (en) * | 2014-12-03 | 2015-04-01 | 湖北中烟工业有限责任公司 | Preparation method of cherry aroma-enhancing and moisture-preserving agent for cigarettes |
| CN104585651A (en) * | 2014-12-06 | 2015-05-06 | 西北大学 | Standardized red jujube extract and preparation method and analysis method thereof |
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2015
- 2015-06-19 CN CN201510346898.2A patent/CN105011356A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US5513663A (en) * | 1991-12-17 | 1996-05-07 | Van Leuven; Dirk-Hector | Tobacco substitutes |
| CN101942361A (en) * | 2010-09-28 | 2011-01-12 | 河南省新郑金叶香料有限公司 | Jujube flavor base, and preparation method and application thereof |
| CN103585782A (en) * | 2013-11-26 | 2014-02-19 | 浙江安赛生物科技有限公司 | Method for preparing red date extract by utilizing ultrasonic cavitation technology |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107011992A (en) * | 2017-06-06 | 2017-08-04 | 武汉黄鹤楼香精香料有限公司 | A kind of method of molecular clock Fructus Fici extract |
| CN115005493A (en) * | 2022-06-08 | 2022-09-06 | 吉林烟草工业有限责任公司 | Bean-flavor characteristic extract, preparation method thereof and cigarette |
| CN115067533A (en) * | 2022-06-14 | 2022-09-20 | 上海龙殷生物科技有限公司 | Fragrance synergist, additive and application |
| CN115067533B (en) * | 2022-06-14 | 2023-12-01 | 上海龙殷生物科技有限公司 | Fragrance synergist, additive and application |
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Application publication date: 20151104 |