CN107216947A - A kind of preparation method of cigarette Catechu extract - Google Patents
A kind of preparation method of cigarette Catechu extract Download PDFInfo
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- CN107216947A CN107216947A CN201710615298.0A CN201710615298A CN107216947A CN 107216947 A CN107216947 A CN 107216947A CN 201710615298 A CN201710615298 A CN 201710615298A CN 107216947 A CN107216947 A CN 107216947A
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- catechu
- weight
- cigarette
- parts
- raw material
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- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 title claims abstract description 75
- 235000006226 Areca catechu Nutrition 0.000 title claims abstract description 74
- 244000235603 Acacia catechu Species 0.000 title claims abstract description 62
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 46
- 239000000284 extract Substances 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000706 filtrate Substances 0.000 claims abstract description 14
- 235000021552 granulated sugar Nutrition 0.000 claims abstract description 13
- 238000007654 immersion Methods 0.000 claims abstract description 11
- 239000000052 vinegar Substances 0.000 claims abstract description 10
- 235000021419 vinegar Nutrition 0.000 claims abstract description 10
- 238000002137 ultrasound extraction Methods 0.000 claims abstract description 9
- 244000080767 Areca catechu Species 0.000 claims abstract 12
- 239000007788 liquid Substances 0.000 claims description 4
- 241000208125 Nicotiana Species 0.000 abstract description 23
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 16
- 239000003546 flue gas Substances 0.000 abstract description 16
- 238000004519 manufacturing process Methods 0.000 abstract description 13
- 210000001124 body fluid Anatomy 0.000 abstract description 11
- 239000010839 body fluid Substances 0.000 abstract description 11
- 235000009508 confectionery Nutrition 0.000 abstract description 10
- 239000000203 mixture Substances 0.000 abstract description 9
- 238000000034 method Methods 0.000 abstract description 8
- 230000001737 promoting effect Effects 0.000 abstract description 8
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 abstract description 6
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 abstract description 6
- 239000003814 drug Substances 0.000 abstract description 6
- -1 irony Chemical compound 0.000 abstract description 5
- 235000013599 spices Nutrition 0.000 abstract description 5
- 210000000214 mouth Anatomy 0.000 abstract description 4
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 abstract description 3
- 229930091371 Fructose Natural products 0.000 abstract description 3
- 239000005715 Fructose Substances 0.000 abstract description 3
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 abstract description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 3
- 229930006000 Sucrose Natural products 0.000 abstract description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 abstract description 3
- 238000006243 chemical reaction Methods 0.000 abstract description 3
- 238000004090 dissolution Methods 0.000 abstract description 3
- 239000008103 glucose Substances 0.000 abstract description 3
- 235000013379 molasses Nutrition 0.000 abstract description 3
- 229960003512 nicotinic acid Drugs 0.000 abstract description 3
- 235000001968 nicotinic acid Nutrition 0.000 abstract description 3
- 239000011664 nicotinic acid Substances 0.000 abstract description 3
- 235000019192 riboflavin Nutrition 0.000 abstract description 3
- 239000002151 riboflavin Substances 0.000 abstract description 3
- 229960002477 riboflavin Drugs 0.000 abstract description 3
- 239000005720 sucrose Substances 0.000 abstract description 3
- 238000009472 formulation Methods 0.000 abstract description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 21
- 239000002304 perfume Substances 0.000 description 10
- 238000012360 testing method Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 5
- 239000003205 fragrance Substances 0.000 description 5
- 238000001035 drying Methods 0.000 description 4
- 241000411851 herbal medicine Species 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000008213 purified water Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000000523 sample Substances 0.000 description 3
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- RSYUFYQTACJFML-DZGCQCFKSA-N afzelechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C=C1 RSYUFYQTACJFML-DZGCQCFKSA-N 0.000 description 2
- 208000002399 aphthous stomatitis Diseases 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000013068 control sample Substances 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- XHEFDIBZLJXQHF-UHFFFAOYSA-N fisetin Chemical compound C=1C(O)=CC=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 XHEFDIBZLJXQHF-UHFFFAOYSA-N 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- IYRMWMYZSQPJKC-UHFFFAOYSA-N kaempferol Chemical compound C1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 IYRMWMYZSQPJKC-UHFFFAOYSA-N 0.000 description 2
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000006340 racemization Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- PADQINQHPQKXNL-LSDHHAIUSA-N (+)-dihydrokaempferol Chemical compound C1([C@@H]2[C@H](C(C3=C(O)C=C(O)C=C3O2)=O)O)=CC=C(O)C=C1 PADQINQHPQKXNL-LSDHHAIUSA-N 0.000 description 1
- PFTAWBLQPZVEMU-ZFWWWQNUSA-N (+)-epicatechin Natural products C1([C@@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-ZFWWWQNUSA-N 0.000 description 1
- PFTAWBLQPZVEMU-UKRRQHHQSA-N (-)-epicatechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-UKRRQHHQSA-N 0.000 description 1
- 241000220433 Albizia Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- RSYUFYQTACJFML-UKRRQHHQSA-N Epiafzelechin Natural products C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@H]2O)=CC=C(O)C=C1 RSYUFYQTACJFML-UKRRQHHQSA-N 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- GQODBWLKUWYOFX-UHFFFAOYSA-N Isorhamnetin Natural products C1=C(O)C(C)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 GQODBWLKUWYOFX-UHFFFAOYSA-N 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 206010053615 Thermal burn Diseases 0.000 description 1
- 208000025865 Ulcer Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 206010000269 abscess Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 230000002279 cholagogic effect Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- RAYJUFCFJUVJBB-UHFFFAOYSA-N dihydrokaempferol Natural products OC1Oc2c(O)cc(O)cc2C(=O)C1c3ccc(O)cc3 RAYJUFCFJUVJBB-UHFFFAOYSA-N 0.000 description 1
- LPTRNLNOHUVQMS-UHFFFAOYSA-N epicatechin Natural products Cc1cc(O)cc2OC(C(O)Cc12)c1ccc(O)c(O)c1 LPTRNLNOHUVQMS-UHFFFAOYSA-N 0.000 description 1
- 235000012734 epicatechin Nutrition 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000011990 fisetin Nutrition 0.000 description 1
- HVQAJTFOCKOKIN-UHFFFAOYSA-N flavonol Natural products O1C2=CC=CC=C2C(=O)C(O)=C1C1=CC=CC=C1 HVQAJTFOCKOKIN-UHFFFAOYSA-N 0.000 description 1
- 150000002216 flavonol derivatives Chemical class 0.000 description 1
- 235000011957 flavonols Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000002440 hepatic effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 235000008800 isorhamnetin Nutrition 0.000 description 1
- IZQSVPBOUDKVDZ-UHFFFAOYSA-N isorhamnetin Chemical compound C1=C(O)C(OC)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 IZQSVPBOUDKVDZ-UHFFFAOYSA-N 0.000 description 1
- 235000008777 kaempferol Nutrition 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 1
- 231100000862 numbness Toxicity 0.000 description 1
- 239000008194 pharmaceutical composition Substances 0.000 description 1
- 229920002414 procyanidin Polymers 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 244000089265 zong er cha Species 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Abstract
The invention provides a kind of preparation method of cigarette Catechu extract, this method is with the immersion of Shanxi water tower mature vinegar after catechu raw material is smashed, toast again, take the parts by weight of catechu 100 300 after baking, the parts by weight of brown granulated sugar 5 30, in the running water for being added to 300 3000 parts by weight, soak after 2 8h, at room temperature ultrasonic extraction 2 times, 0.5 1 hours every time, cooled and filtered, leaves and takes filtrate twice respectively；Merging filtrate, is concentrated under reduced pressure into 26 times of catechu raw-material weight at a temperature of 40 54 DEG C, produces required cigarette Catechu extract.The present invention uses for reference the process of Chinese medicine preparation, by catechu raw material vinegar system, fully the composition in catechu raw material is caused to be more easy to dissolution after reaction, recycle advantage of the brown granulated sugar rich in compositions such as sucrose, glucose, molasses, fructose, irony, riboflavin, carrotene and nicotinic acid, the spices being made is added to after tobacco tobacco leaf formulation can also sweet flue gas, the sense of promoting the production of body fluid of increase oral cavity and throat.
Description
Technical field
The present invention relates to a kind of tobacco aromaticss and preparation method thereof, specifically a kind of cigarette Catechu extract preparation side
Method.
Background technology
With the raising of people's level of consumption, the demand of high-quality cigarette is continuously increased, but limited first-class raw material limit
The production of high-quality cigarette has been made, and tobacco flavor is strengthened by flavoring and casing, has improved quality of tobacco, improves the use of tobacco leaf
Rate, is an important measures for solving this contradiction.In cigarette products, the fragrance and suction taste of cigarette are very important, are added
Perfuming is the key link in cigarette industry, be also improve product style and improve cigarette flavor quality effective means it
One, some fragrance can be provided to consumer and the cigarette products of taste satisfaction are inhaled.
China is the native place of Chinese herbal medicine, and application of the Chinese herb feed additive in Chinese-style cigarette is the peculiar excellent of Chinese Tobacco Industry
Gesture.There is abundant Chinese herbal medicine resource in China, and many kinds are similar to tobacco structure on chemical analysis, but different properties, they
The deficiency of tobacco can be made up in some aspects.As application of the Chinese herbal medicine class additive in cigarette is increasingly consumers in general
Received, existing increasing tobacco researcher finds essence spice for cigarette from natural Chinese medicinal herb, and natural perfume material exists
Application in cigarette is more and more extensive.
Catechu is a kind of conventional Chinese medicine, and alias catechu, ramulus acaciae, gambier are pulse family albizzia plant catechu tree
Remove the peel branch, dry drying soft extracts.South of Yunnan area is distributed in, there is cultivation in Hainan Island.Winter harvesting branch, dry, removing crust, cut
Into bulk, add water to cook, concentrate, drying is made.《Book on Chinese herbal medicine is just》Recording it has, and " fall fire is promoted the production of body fluid, clear sputum cough, controls aphtha larynx
The effect of numbness ".Clinically it is used for unhealing ulcer, eczema, aphtha, abscess of throat, the pain of injury caused by falling and tumbling, traumatism and bleeding.Modern pharmacology is real
Testing display, it has hepatic cholagogic, the effect of strengthen immunity and anti-inflammation.The chemical composition of catechu is mainly catechutannic acid,
Left-handed and racemization cachou extract, left-handed and racemization epicatechin, tannic red tannin, and fisetin, Quercetin, quercetagetin etc.
Flavonols and Kaempferol, Dihydrokaempferol, texifolin, Isorhamnetin, dextrorotation afzelechin etc..The exploitation profit of present catechu
With pharmaceuticals industry is used for, such as Publication No. CN03111902 Chinese invention patents disclose a kind for the treatment of throat disease containing catechu
Pharmaceutical composition and preparation method thereof of disease, Publication No. CN00102965.7 Chinese invention patents disclose a kind of containing catechu
Treat medicine of burn and scald and preparation method thereof.CN102978002A discloses a kind of cigarette Catechu extract preparation method, it
It is that obtained extract is added in cigarette can be rich by catechu 30-95% ethanol or the extraction of 0.1-1% lactic acid aqueous solutions
Rich cigarette perfume, soft fine and smooth flue gas, increase throat comfort.But the extract is added in cigarette, the sweet sense of flue gas is not obvious,
And sense of not promoted the production of body fluid when aspirating.
The content of the invention
It is an object of the invention to provide a kind of preparation method of cigarette Catechu extract, this method technique is simple, and cost is low
Honest and clean, raw material sources are stable, and use for reference the process of Chinese medicine preparation, by catechu raw material vinegar system, fully cause catechu former after reaction
Composition in material is more easy to dissolution, recycles brown granulated sugar to be rich in sucrose, glucose, molasses, fructose, irony, riboflavin, carrotene
With the advantage of the composition such as nicotinic acid, add in solvent and extract, not only fragrance is obvious for the spices being made, moreover it is possible to sweet flue gas, increase mouth
Chamber and the sense of promoting the production of body fluid of throat.
The technical scheme that the present invention is provided：A kind of preparation method of cigarette Catechu extract, comprises the following steps：
(1) catechu raw material is crushed, sieved with 100 eye mesh screens；
(2) the catechu raw material after crushing is pressed 1:1 weight ratio is soaked 8-24 hours with Shanxi water tower mature vinegar.
(3) the catechu raw material after immersion is toasted 2 hours under 200 DEG C of high temperature.
(4) the catechu 100-300 parts by weight after baking are taken, brown granulated sugar 5-30 parts by weight are added to 300-3000 parts by weight
Running water in, immersion 2-8h after, ultrasonic extraction 2 times at room temperature, each 0.5-1 hours, cooled and filtered leaves and takes two respectively
Secondary filtrate；
(5) filtrate in combining step (4), is concentrated under reduced pressure into 2-6 times of catechu raw-material weight at a temperature of 40-54 DEG C,
Produce required cigarette Catechu extract.
Further, the step (4) is：The parts by weight of catechu 200 after baking are taken, the parts by weight of brown granulated sugar 10 are added to
In the running water of 1000 parts by weight, after immersion 4h, ultrasonic extraction 2 times at room temperature, 0.5 hour every time, cooled and filtered, respectively
Leave and take filtrate twice；Merge filtrate twice, 5 times of catechu raw-material weight is concentrated under reduced pressure at a temperature of 40 DEG C, needed for producing
Cigarette Catechu extract.
The beneficial effects of the present invention are：
1st, the present invention uses for reference the process of Chinese medicine preparation, by catechu raw material vinegar system, fully causes catechu raw material after reaction
In composition be more easy to dissolution, recycle brown granulated sugar rich in sucrose, glucose, molasses, fructose, irony, riboflavin, carrotene and
The advantage of the compositions such as nicotinic acid, is added in solvent and extracts, and not only fragrance substantially, with tobacco this perfume coordination, is added to the spices being made
Can also sweet flue gas, the sense of promoting the production of body fluid of increase oral cavity and throat after tobacco tobacco leaf formulation.
2nd, raw material sources of the present invention are easy to get, and preparation technology is simple, and cost is low, are converted beneficial to production.
Embodiment
A part of embodiment is set forth below to be described in further detail the relevant technical problem of the present invention, it is necessary to
This points out that specific examples below is simply further illustrated to the present invention, does not represent limiting the scope of the invention.Its
Some nonessential modifications and adjustment that other people make according to the present invention, still fall within protection scope of the present invention.
Embodiment 1
1) catechu raw material is crushed, sieved with 100 eye mesh screens；
2) the catechu raw material after crushing is pressed 1:1 weight ratio is soaked 8-24 hours with Shanxi water tower mature vinegar；
3) the catechu raw material after immersion is toasted 2 hours under 200 DEG C of high temperature；
4) take in the parts by weight of catechu 200 after crushing, the parts by weight of brown granulated sugar 10, the running water for being added to 1000 parts by weight,
Soak after 4h, ultrasonic extraction 2 times at room temperature, 0.5 hour every time, cooled and filtered left and took 2 filtrates respectively；Merge 2 filters
Liquid, is concentrated under reduced pressure into 5 times of catechu raw-material weight at a temperature of 40 DEG C, produces required cigarette Catechu extract.
5) Catechu extract obtained above is taken, the addition of pipe tobacco dry weight 0.1% is accounted for by extract, according to Conventional feed introduction
Charging technology program, with being uniformly sprayed on after dissolved in purified water in blank pipe tobacco, by shredded tobacco baking to water under the conditions of 65 DEG C
Divide content 16%, cigarette is made.
Embodiment 2
1) catechu raw material is crushed, sieved with 100 eye mesh screens；
2) the catechu raw material after crushing is pressed 1:1 weight ratio is soaked 8-24 hours with Shanxi water tower mature vinegar；
3) the catechu raw material after immersion is toasted 2 hours under 200 DEG C of high temperature；
4) take in the parts by weight of catechu 100 after crushing, the parts by weight of brown granulated sugar 15, the running water for being added to 1500 parts by weight,
Soak after 2h, ultrasonic extraction 2 times at room temperature, 1 hour every time, cooled and filtered left and took 2 filtrates respectively；Merging is filtered twice
Liquid, is concentrated under reduced pressure into 2 times of catechu raw-material weight at a temperature of 54 DEG C, produces required cigarette Catechu extract.
5) Catechu extract obtained above is taken, the addition of pipe tobacco dry weight 0.01% is accounted for by extract, is added according to conventional
The charging technology program of material, with being uniformly sprayed on after dissolved in purified water in blank pipe tobacco, under the conditions of 55 DEG C by shredded tobacco baking extremely
Moisture 12%, is made cigarette.
Embodiment 3
1) catechu raw material is crushed, sieved with 100 eye mesh screens；
2) the catechu raw material after crushing is pressed 1:1 weight ratio is soaked 8-24 hours with Shanxi water tower mature vinegar；
3) the catechu raw material after immersion is toasted 2 hours under 200 DEG C of high temperature；
4) take in the parts by weight of catechu 150 after crushing, the parts by weight of brown granulated sugar 5, the running water for being added to 2000 parts by weight, leaching
Steep after 3h, ultrasonic extraction 2 times at room temperature, 45 minutes every time, cooled and filtered left and took 2 filtrates respectively；Merge 2 filtrates,
4 times of catechu raw-material weight is concentrated under reduced pressure at a temperature of 45 DEG C, required cigarette Catechu extract is produced.
5) Catechu extract obtained above is taken, the addition of pipe tobacco dry weight 0.05% is accounted for by extract, is added according to conventional
The charging technology program of material, with being uniformly sprayed on after dissolved in purified water in blank pipe tobacco, under the conditions of 65 DEG C by shredded tobacco baking extremely
Moisture 14%, is made cigarette.
Embodiment 4
1) catechu raw material is crushed, sieved with 100 eye mesh screens；
2) the catechu raw material after crushing is pressed 1:1 weight ratio is soaked 8-24 hours with Shanxi water tower mature vinegar；
3) the catechu raw material after immersion is toasted 2 hours under 200 DEG C of high temperature；
4) take in the parts by weight of catechu 300 after crushing, the parts by weight of brown granulated sugar 20, the running water for being added to 2500 parts by weight,
Soak after 6h, ultrasonic extraction 2 times at room temperature, 0.5 hour every time, cooled and filtered left and took 2 filtrates respectively；Merge 2 filters
Liquid, is concentrated under reduced pressure into 6 times of catechu raw-material weight at a temperature of 50 DEG C, produces required cigarette Catechu extract.
5) Catechu extract obtained above is taken, the addition of pipe tobacco dry weight 0.1% is accounted for by extract, is added according to conventional
Expect process, with being uniformly sprayed on after dissolved in purified water in blank pipe tobacco, contain shredded tobacco baking to moisture under the conditions of 70 DEG C
Amount 16%, is made cigarette.
Effect of smokeing panel test and detection：
Using CN102978002A as control sample, brown granulated sugar is not added, other steps are identical with the present invention, extract obtained catechu
Extract (not sugared sample preparation) is contrast, adopts and cigarette is made in a like fashion, smoked panel test by the cigarette standard of smokeing panel test, smoking result
It see the table below 1：
The cigarette of table 1 is smoked panel test effect
| Sample | Evaluation effect |
| Control sample | Cigarette perfume is enriched, the soft exquisiteness of flue gas. |
| Not sugared sample preparation | Cigarette perfume is enriched, and gas drying sense substantially, is slightly stimulated. |
| Embodiment 1 | Cigarette perfume is enriched, and the soft exquisiteness of flue gas, flue gas is sweet, there is sense of promoting the production of body fluid. |
| Embodiment 2 | Cigarette perfume is enriched, and the soft exquisiteness of flue gas, flue gas is sweet, there is sense of promoting the production of body fluid. |
| Embodiment 3 | Cigarette perfume is enriched, and the soft exquisiteness of flue gas, flue gas is sweet, there is sense of promoting the production of body fluid. |
| Embodiment 4 | Cigarette perfume is enriched, and the soft exquisiteness of flue gas, flue gas is sweet, there is sense of promoting the production of body fluid. |
Perfumer is smoked panel test, test result indicates that, compared with CN102978002A, embodiment 1-4 cigarette perfumes are more enriched,
The sense of flue gas sweet tea, sense of promoting the production of body fluid are stronger.Compared with the extract without sugar system processing, the extract gas drying sense without sugar system processing
Substantially, slightly stimulate.Not only fragrance is obvious for the spices that the present invention is made, moreover it is possible to sweet flue gas, and increase oral cavity and throat promote the production of body fluid
Sense.
The detailed description of specific embodiments of the present invention is the foregoing is only, the present invention is not limited with this, it is all at this
Any modifications, equivalent substitutions and improvements made in the mentality of designing of invention etc., should be included in protection scope of the present invention it
It is interior.
Claims (2)
1. a kind of preparation method of cigarette Catechu extract, it is characterised in that comprise the following steps：
(1) catechu raw material is crushed, sieved with 100 eye mesh screens；
(2) the catechu raw material after crushing is pressed 1:1 weight ratio is soaked 8-24 hours with Shanxi water tower mature vinegar；
(3) the catechu raw material after immersion is toasted 2 hours under 200 DEG C of high temperature；
(4) take baking after catechu 100-300 parts by weight, brown granulated sugar 5-30 parts by weight, be added to 300-3000 parts by weight from
In water, after immersion 2-8h, ultrasonic extraction 2 times at room temperature, each 0.5-1 hours, cooled and filtered is left and taken filter twice respectively
Liquid；
(5) filtrate in combining step (4), 2-6 times of catechu raw-material weight is concentrated under reduced pressure at a temperature of 40-54 DEG C, is produced
Required cigarette Catechu extract.
2. the preparation method of cigarette Catechu extract according to claim 1, it is characterised in that：The step (4) is：Take
In the parts by weight of catechu 200 after baking, the parts by weight of brown granulated sugar 10, the running water for being added to 1000 parts by weight, after immersion 4h, in room
The lower ultrasonic extraction of temperature 2 times, 0.5 hour every time, cooled and filtered left and took filtrate twice respectively；Merge filtrate twice, in 40 DEG C of temperature
5 times of catechu raw-material weight is concentrated under reduced pressure under degree, required cigarette Catechu extract is produced.
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| CN109259293A (en) * | 2018-09-13 | 2019-01-25 | 云南中烟工业有限责任公司 | A kind of tealeaves toasts fragrant reconstituted tobacco and its preparation method and application |
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| CN107216947B (en) | 2020-09-08 |
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