CN109953367B - Cistanche extracting solution and preparation method, composition and application thereof - Google Patents
Cistanche extracting solution and preparation method, composition and application thereof Download PDFInfo
- Publication number
- CN109953367B CN109953367B CN201910224107.7A CN201910224107A CN109953367B CN 109953367 B CN109953367 B CN 109953367B CN 201910224107 A CN201910224107 A CN 201910224107A CN 109953367 B CN109953367 B CN 109953367B
- Authority
- CN
- China
- Prior art keywords
- cistanche
- cigarette
- extracting solution
- cigarettes
- blasting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention provides a cistanche extracting solution, a preparation method, a composition and application thereof, wherein the preparation method of the cistanche extracting solution comprises the following steps: extracting dry herba cistanches to obtain herba cistanches extract, adding enzyme preparation into herba cistanches extract, and concentrating; the invention also provides a composition rich in the cistanche extracting solution and application thereof in improving the sensory quality of cigarettes. The cigarette containing the cistanche extracting solution blasting beads has higher sensory quality evaluation during smoking, improves the exquisite smoke sense, is soft and smooth in mouth, has unique sweet sauce fragrance, has clean aftertaste, reduces the content of physicochemical indexes of the smoke of the cigarette, and has the effect of reducing the smoking harm of the cigarette.
Description
Technical Field
The application relates to the technical field of cigarette production, in particular to a cistanche extracting solution, a preparation method thereof, a composition containing the cistanche extracting solution and application of the cistanche extracting solution in improving cigarette quality.
Background
With the increasing concern of people on the relation between smoking and health, the cigarette has the advantages of improving the internal quality and safety of the cigarette, and simultaneously assisting in increasing certain components with health care functions and reducing harmful components in cigarette smoke, and is a great trend of cigarette development. Through the continuous and deep research on smoking and health and the continuous innovation of the cigarette industry technology, the tar content of cigarettes in the world tends to be gradually reduced, and how to maintain the aroma quality of cigarette smoke in the process of continuously reducing the tar content of cigarettes is one of the focus problems of general attention of cigarette industry enterprises.
In the traditional cigarette production process, the spice liquid is usually added into tobacco shreds, the spice liquid added in the mode is usually lost in the cigarette combustion process, and meanwhile, as the reaction of a complex material system at high temperature is difficult to expect, part of the spice liquid can also generate some adverse sensory effects.
The bead blasting is used as a new material in cigarettes, and due to the special release mode of the content of the bead blasting, the bead blasting has more and more prominent functions in the aspects of supplementing, improving and coordinating the smoking quality of the cigarettes, improving, changing, cigarette product style and the like. Although a certain number of bead-exploded cigarettes exist in the market at present, the aroma in the bead-exploded cigarettes is relatively poor in coordination with smoke due to lack of targeted design, and the aroma characteristics of the cigarettes are greatly influenced, so that the smoking quality of the bead-exploded cigarettes is influenced.
Cistanche deserticola is a dry fleshy stem with scaly leaves of cistanche deserticola or cistanche tubulosa of Orobanchaceae, mainly produced in inner Mongolia, Gansu and other places of China, and is called desert ginseng. Cistanchis herba is sweet, salty and warm in nature and flavor, and enters kidney, has effects of invigorating kidney yang, replenishing essence and blood, and loosening bowel to relieve constipation, and can be used for treating kidney yang deficiency, essence and blood deficiency, constipation due to intestinal dryness, etc. The compendium of materia Medica records: shizhen is a leisurely number because it tonifies without drastic action. It is easy and gentle. The chemical components of cistanche deserticola which are identified at present mainly comprise phenylethanoid glycosides, polysaccharides, iridoids and the like; pharmacological action research shows that the cistanche has the effects of protecting nerves, regulating immunity, resisting fatigue, regulating hormone balance, resisting oxidation and the like.
At present, most of the researches on cistanche at home and abroad are chemical component determination of cistanche polysaccharide serving as an active ingredient and medical use in the fields of medicine and food, the extraction method is mainly ethanol extraction after soaking by using distilled water, and no method related to treatment of cistanche extract by using a complex enzyme preparation is available, or the cistanche extract is prepared into exploded beads after being subjected to appropriate flavor blending and then placed in a cigarette filter stick, or is applied to related reports in cigarette production.
Disclosure of Invention
The invention aims to provide the cistanche extract which is applied to tobacco and can obviously reduce the irritation, improve the aroma and the sensory quality of cigarettes and simultaneously reduce the contents of tar, nicotine and carbon monoxide in the mainstream smoke of the cigarettes.
In one aspect, the invention provides a preparation method of a cistanche extract, which comprises the steps of extracting dry substances of cistanche to obtain the cistanche extract, and adding an enzyme preparation into the cistanche extract.
Wherein, the amount of the enzyme preparation added into each gram of dry cistanche is 3-3 ten thousand U. The enzyme preparation is selected from one or more of cellulase, beta-glucosidase, ligninase and pectinase.
Preferably, the volume ratio of the enzyme preparation to the cistanche extraction liquid is 1-2:100, preferably 1.1-1.8:100, more preferably 1.3-1.7: 100.
In one embodiment, the dry cistanche material can be dried fresh cistanche, or dried and crushed cistanche block or powder.
Further, the enzyme preparation is a complex enzyme at least comprising cellulase, beta-glucosidase, ligninase and pectinase, and the enzyme activity ratio of the cellulase, the beta-glucosidase, the ligninase and the pectinase is (2-5): 1-7): 3-6): 1-9, preferably 4:1:3: 5.
Preferably, the concentration of the enzyme preparation is 10-20 ten thousand U/ml; preferably, each gram of dry matter of the cistanche deserticola is added with 5000U of cellulase, 7000U of beta-glucosidase, 6000U of ligninase 3000 and 9000U of pectinase 1000; wherein, the conditions of the enzymolysis step are that the temperature is 20-25 ℃, and the enzymolysis time is 120-150 min.
Preferably, the enzyme preparation is derived from animal, plant and/or microbial extracts, more preferably from microbial extracts, such as bacteria, fungi, protists, etc. The complex enzyme can fully decompose cellulose, lignin, glucose and pectin in the cistanche extraction liquid to obtain the cistanche extraction liquid containing micromolecule effective components.
Further, the method specifically comprises the following steps:
carrying out water bath hot reflux or oscillation extraction on dry cistanche substances by using 60% ethanol at the temperature of 80-100 ℃ or under the condition of ultrasonic waves or microwaves for 1-12 hours to obtain cistanche extract, cooling, adding 1-2ml of an enzyme preparation into each 100ml of the cistanche extract, wherein the enzyme preparation is a complex enzyme containing cellulase, beta-glucosidase, ligninase and pectinase with the enzyme activity ratio of (2-5) to (1-7) to (3-6) to (1-9), and concentrating until the concentration of dry substances in the volume of a concentrated solution is 8-25% to obtain the cistanche extract.
In a preferred embodiment, the extraction is carried out by hot reflux or shaking in a water bath for 1 to 10 hours, preferably 2 to 8 hours, more preferably 4 to 7 hours; the feed-liquid ratio of the cistanche powder to the ethanol is 1g:7-10ml, preferably 1g:7ml, 1g:8ml, 1g:9ml and 1g:10 ml; the enzyme preparation preferably contains a complex enzyme of cellulase, beta-glucosidase, ligninase and pectinase with the enzyme activity ratio of 4:1:3: 5; cooling the Cistanchis herba extract to 15-25 deg.C, preferably 15 deg.C, 20 deg.C, 22 deg.C, and 25 deg.C before adding enzyme preparation; preferably, after concentration, the biological enzyme is inactivated at 100 ℃ for 5 minutes, and thus the added biological enzyme can be inactivated.
Furthermore, the method also comprises a step of pretreating the cistanche, and specifically comprises the following steps:
washing herba cistanches, removing impurities, air drying, oven drying at 30-60 deg.C, and pulverizing directly or pulverizing in liquid nitrogen to 40-100 mesh.
In one embodiment, the above pre-treatment step can be adopted to dry fresh cistanche or cistanche to obtain cistanche powder of 40-100 meshes, and then the cistanche powder is extracted; in another embodiment, the cistanche blocks, granules or particles are purchased directly and then crushed until the particle size is 40-100 mesh.
On the other hand, the invention also provides a cistanche extracting solution which is prepared by the method.
On the other hand, the invention also provides a composition which comprises the cistanche extracting solution prepared by the method, wherein the mass ratio of the cistanche extracting solution in the composition is 16-98%, preferably 50-80%, and more preferably 55-75%.
Further, the composition also comprises any one or more of the following components: glyceryl caprylate/caprate, glyceryl triacetate, maltol, menthyl acetate, vanillin, ethyl caprylate, D-limonene, gamma-terpinene, beta-pinene, alpha-pinene, D-pyroglutamic acid ethyl ester, 5-hydroxy maltol, nerol and geraniol.
In one embodiment, the composition preferably comprises the following components in percentage by mass: 16 to 98 percent of cistanche extracting solution, 15 to 30 percent of caprylic/capric glyceride, 1 to 2 percent of glyceryl triacetate, 0.3 to 2.5 percent of maltol, 0.1 to 2.3 percent of menthyl acetate, 0.2 to 1.8 percent of vanillin, 1 to 3 percent of ethyl vanillin, 0.7 to 1.4 percent of ethyl caprylate, 0.1 to 1.2 percent of D-limonene, 0.1 to 1.1 percent of gamma-terpinene, 0.2 to 1.5 percent of beta-pinene, 0.2 to 1.8 percent of alpha-pinene, 0.1 to 2.0 percent of D-pyroglutamic acid ethyl ester, 0.1 to 2.1 percent of 5-hydroxy maltol, 0.3 to 3.0 percent of nerol and 0.3 to 1.4 percent of geraniol.
In another aspect, the invention also provides a blasting bead, which contains the composition; preferably, the beadlets comprise 10-30 microliters of the composition; more preferably, the diameter of the blasting beads is 2-4mm, the weight is 10-25 mg/granule, the roundness is less than 0.15mm, and the crushing pressure value is 1-1.5 kgf.
In a preferred embodiment, the content of the composition in the above-mentioned blasting beads is 10 to 25 ul/pellet; the diameter of the blasting beads is 2.5-3.5mm, more preferably 2.5mm, 2.6mm, 3.0mm, 3.45mm, 3.5mm, the weight is preferably 10.5-24.2 mg/granule, and the crushing pressure value is preferably 1.3 kgf. In actual production operation, specific parameters such as the shape, size, specification, crushing pressure value and the like of the exploded bead can be adjusted according to the specification and the size of the cigarette filter stick to which the exploded bead is added, and the exploded bead can also be prepared by using tools, equipment or machines for producing corresponding specifications and the like.
On the other hand, the invention also provides application of the cistanche extract, and/or the cistanche extract prepared by the method, and/or the composition, and/or the exploded bead in improving the sensory quality of cigarettes.
The sensory quality of the cigarette is referred to GB 5606.4-2005 cigarette part 4: the cigarette sensory quality judgment standard in the sensory technical requirements comprises the following steps: gloss, aroma, harmony, miscellaneous gases, irritation, and aftertaste.
In one embodiment, the cistanche extract and/or the composition prepared by the method can be directly added into tobacco shreds, filter sticks, cigarette paper, forming paper and/or tipping glue; in another embodiment, the cistanche salsa extract and/or the composition can also be injected into a bead blasting and then added into a filter stick of a cigarette.
In one embodiment, the blasting beads may be added to regular cigarettes, binary composite cigarettes and/or ternary composite cigarettes; the position of the popping beads in the cigarette filter stick is not limited, and the popping beads are preferably 12-16mm away from the lip end, and more preferably 15 mm; one or more blasting beads can be added to each cigarette.
On the other hand, the invention also provides a cigarette which contains the cistanche extracting solution prepared by the method, and/or contains the composition, and/or contains at least one bead. Preferably, the cigarette has no limitation on the specification, and can be a fine cigarette, a medium cigarette or a conventional cigarette, and can also be a common cigarette, a binary composite cigarette and/or a ternary composite cigarette, wherein the circumference of the cigarette is preferably 15-30mm, more preferably 16mm, 17mm, 20mm, 22mm, 24mm, 24.1mm and 27 mm.
The following beneficial effects can be brought through the application:
1. according to the preparation method of the cistanche extracting solution, the cistanche extracting solution suitable for cigarettes can be obtained by carrying out enzymolysis on the cistanche extracting solution by using the compound enzyme preparation with a proper proportion, and the cistanche extracting solution can be applied to the cigarettes to improve the fragrance, reduce the irritation and obviously improve the sensory quality of the cigarettes, has a health-care effect and is particularly suitable for high-quality cigarettes.
2. The composition rich in the cistanche extract can be prepared into exploded beads to be applied to cigarettes, so that the cigarettes have sauce sweet aroma and thick aroma during smoking; the results of the smoke panel test show that: after the cigarette is smoked by the aid of the cigarette blasting beads rich in the cistanche extract provided by the invention, richness of aroma in smoke can be obviously improved, full feeling and joyful feeling of the smoke are enhanced, coordination of the aroma and sensory quality of products is further improved, interestingness of cigarette smoking is increased, contents of total particulate matters, tar, smoke nicotine, carbon monoxide and the like in physicochemical indexes of mainstream smoke of the cigarette can be reduced, and harm to human health is reduced.
3. The cigarette containing the bead blasting composition provided by the invention has better sensory quality evaluation during smoking, and is mainly characterized in that the richness, fineness and thickness of smoke are obviously improved, the smoke fragrance is more intense, permeable and better in fusion degree, the baking fragrance, the scorching sweetness and the spicy fragrance are improved, the cigarette fragrance is enriched, the smoke fragrance quality, the fullness and the smoking interestingness are obviously improved, the sensory irritation of the smoke is reduced, the fineness is improved, the taste is smooth and soft, the sweet feeling after taste is obviously enhanced, the aftertaste is clear, the physicochemical index content of the smoke of the cigarette is reduced, and the cigarette smoking harm is reduced to a certain degree.
Detailed Description
In order to more clearly explain the overall concept of the present application, the following detailed description is given by way of example. In the following description, numerous specific details are set forth in order to provide a more thorough understanding of the present application. It will be apparent, however, to one skilled in the art, that the present application may be practiced without one or more of these specific details. In other instances, well-known features of the art have not been described in order to avoid obscuring the present application.
In the following embodiments, cistanche salsa is purchased from Qinghai Sanshen cattle commercial Co., Ltd, and the components except the extract of cistanche salsa in the following compositions are commercially available; cellulase, pectinase, ligninase and beta-glucosidase in the enzyme preparation are all purchased from Novoxin (China) biotechnology limited; preparing a bead blasting pill by adopting a capsule pill dropping machine for cigarettes, which is provided by Shanghai Huabao biological science and technology limited company and has the model of MSM-06; placing the puffed beads into a cigarette filter stick by adopting a flavor capsule feeding device with the model number of JK-S1 provided by Korea Zhengguang Kogyo corporation; preparing cigarettes by adopting a cigarette making and tipping machine with the model ZJ17 provided by Hende tobacco machinery Limited liability company; and (4) a smoke detection test is carried out by adopting a full-automatic smoking machine.
In a preferred embodiment, the method for preparing the cistanche salsa extract specifically comprises the following steps:
s1, washing herba cistanches, removing impurities, air drying, oven drying at 30-60 deg.C, and pulverizing directly or pulverizing in liquid nitrogen to 40-100 mesh to obtain herba cistanches powder;
s2, performing water bath hot reflux or oscillation extraction on the cistanche powder by using 60% ethanol for 1-12 hours at 80-100 ℃ or under the condition of ultrasonic waves or microwaves, wherein the material-liquid ratio of the cistanche powder to the ethanol solution is as follows: cistanche powder: ethanol =1g:7-10 ml;
s3, after the extract liquid is cooled to 15-25 ℃, adding a complex enzyme preparation containing cellulase, beta-glucosidase, ligninase and pectinase, and carrying out enzymolysis at 20-25 ℃ for 120-150 min;
s4, concentrating the extract added with the various enzyme preparations until the dry matter concentration of the volume of the concentrated solution is 8-25%, and inactivating at 100 ℃ for 5 minutes after concentration to obtain the cistanche extract.
In the following embodiments, the cigarette blasting bead is preferably prepared by a split-liquid midpoint dropping method, which includes a step of cutting off a gel column by using a shearing force of cooling oil offset, and may specifically be: the cooling oil with different incident angles is utilized to form shearing force in the solenoid, the wall material and the core liquid in the dropping process are cut off, and are condensed into balls in the cooling oil under the action of surface tension, and then the balls are subjected to procedures of deoiling, drying, screening and the like to prepare the finished product of the blasting balls.
Example 1
A cistanche salsa extract is prepared by the following method:
washing herba Cistanchis, removing impurities, air drying, oven drying at 60 deg.C, and pulverizing in liquid nitrogen to 100 mesh to obtain herba Cistanchis powder; performing oscillation extraction for 10 hours at 100 ℃ according to a material-liquid ratio of cistanche powder to ethanol =1g to 10ml, cooling to 25 ℃, adding 1.7ml of complex enzyme with the concentration of 10 ten thousand U/ml into each 100ml of cistanche extract, namely adding 1.7 ten thousand U of enzyme preparation into each gram of cistanche dry matter, wherein the complex enzyme consists of cellulase, beta-glucosidase, ligninase and pectinase according to the enzyme activity ratio of 2:6:5:4, namely adding 2000U of cellulase, 6000U of beta-glucosidase, 5000U of ligninase and 4000U of pectinase into each gram of cistanche dry matter; after enzymolysis, the mixture is decompressed and concentrated under 70kPa until the concentration of the dry matter in the volume of the concentrated solution is 20 percent, and the concentrated solution is inactivated at 100 ℃ for 5 minutes to obtain the cistanche extracting solution.
A composition containing the cistanche extracting solution comprises the following components in parts by mass: 55% of cistanche extracting solution, 25% of caprylic-capric glyceride, 2% of glyceryl triacetate, 2.1% of maltol, 1.5% of menthyl acetate, 1.8% of vanillin, 1% of ethyl vanillin, 1.2% of ethyl caprylate, 0.9% of D-limonene, 0.8% of gamma-terpinene, 1.4% of beta-pinene, 1.5% of alpha-pinene, 1.5% of D-pyroglutamic acid ethyl ester, 1.1% of 5-hydroxy maltol, 2.2% of nerol and 1% of geraniol.
An explosive bead containing the composition is prepared by the flow-liquid mid-drop method. Wherein the content of the composition in the blasting beads is 24.2 μ l/granule, the diameter of the blasting beads is 3.4mm, the weight is 24.2 mg/granule, the roundness is less than 0.15mm, and the crushing pressure value is 1.3 kgf.
A cigarette containing the above puffed beads is prepared according to the existing cigarette production process. The cigarette is a common cigarette with the circumference of 24.1mm, an exploding bead is placed in a cigarette filter stick, and the exploding bead is placed in the middle section of the cigarette filter stick and is specifically 15.0mm away from the lip end.
The smoke test results and the smoking evaluation scores of the cigarettes of this example are shown in tables 2 and 3.
According to the feedback of the smoking evaluation result, the cigarette obtained in the embodiment has the advantages that after the popping beads rich in the cistanche extracting solution are added, the richness of the smoke of a cigarette sample is improved to a certain extent, the aroma of baking aroma and sauce aroma is prominent, no stimulation and foreign gas exist, the fine and smooth smoke is improved, the sweet return feeling is obviously enhanced, and the aftertaste is comfortable.
Example 2
A cistanche salsa extract is prepared by the following method:
washing herba Cistanchis, removing impurities, air drying, oven drying at 50 deg.C, and directly pulverizing to 80 mesh to obtain herba Cistanchis powder; under the condition of ultrasonic waves, carrying out water bath hot reflux extraction for 8 hours by using a material-liquid ratio of cistanche powder to ethanol =1g:8ml, cooling to 20 ℃, adding 1.5ml of complex enzyme with the concentration of 10 ten thousand U/ml into each 100ml of cistanche extraction liquid, namely adding 1.2 ten thousand U of enzyme preparation into each gram of cistanche dry matter, wherein the complex enzyme consists of cellulase, beta-glucosidase, ligninase and pectinase according to the enzyme activity ratio of 3:2:4:6, namely adding 3 thousand U of cellulase, 2 thousand U of beta-glucosidase, 4 thousand U of ligninase and 6 thousand U of pectinase into each gram of cistanche dry matter; after enzymolysis, the mixture is decompressed and concentrated under 50kPa until the concentration of the dry matter in the volume of the concentrated solution is 25 percent, and the concentrated solution is inactivated at 100 ℃ for 5 minutes to obtain the cistanche extracting solution.
A composition containing the cistanche extracting solution comprises the following components in parts by mass: 65% of cistanche extracting solution, 20% of caprylic-capric glyceride, 1.4% of glyceryl triacetate, 1.6% of maltol, 0.8% of menthyl acetate, 1.2% of vanillin, 1.5% of ethyl vanillin, 1% of ethyl caprylate, 0.9% of D-limonene, 0.8% of gamma-terpinene, 1.0% of beta-pinene, 0.9% of alpha-pinene, 1.0% of D-pyroglutamic acid ethyl ester, 0.9% of 5-hydroxy maltol, 1.2% of nerol and 0.8% of geraniol.
An explosive bead containing the composition is prepared by the flow-liquid mid-drop method. Wherein the content of the composition in the blasting beads is 14.0 μ l/granule, the diameter of the blasting beads is 3.0mm, the weight is 14.0 mg/granule, the roundness is less than 0.15mm, and the crushing pressure value is 1.3 kgf.
A cigarette containing the above puffed beads is prepared according to the existing cigarette production process. The cigarette is a binary composite cigarette with the circumference of 22.0mm, a popping bead is placed in the cigarette filter stick, and the popping bead is placed in the middle section of the cigarette filter stick, specifically 15.0mm away from the lip end.
The smoke test results and the smoking evaluation scores of the cigarettes of this example are shown in tables 2 and 3.
According to the embodiment, after the bead blasting method is used, the smoke richness of the cigarette sample is improved to a certain extent, the original tobacco fragrance and the sweet sauce fragrance are outstanding in fragrance, the harmony is good, the fine smoke sense is improved, the smoke fragrance is more transparent, the sweet return sense is obviously enhanced, and the aftertaste is clean.
Example 3
A cistanche salsa extract is prepared by the following method:
washing herba Cistanchis, removing impurities, air drying, oven drying at 40 deg.C, and pulverizing in liquid nitrogen to 90 mesh to obtain herba Cistanchis powder; under the microwave condition, carrying out water bath hot reflux extraction for 6 hours by using a material-liquid ratio of cistanche powder to ethanol =1g to 10ml, cooling to 15 ℃, adding 1.3ml of complex enzyme with the concentration of 10 ten thousand U/ml into each 100ml of cistanche extract, namely adding 1.3 ten thousand U of enzyme preparation into each gram of cistanche dry matter, wherein the complex enzyme consists of cellulase, beta-glucosidase, ligninase and pectinase according to the enzyme activity ratio of 4:1:3:5, namely adding 4 thousand U of cellulase, 1 thousand U of beta-glucosidase, 3 thousand U of ligninase and 5 thousand U of pectinase into each gram of cistanche dry matter; after enzymolysis, the mixture is decompressed and concentrated under 60kPa until the concentration of the dry matter in the volume of the concentrated solution is 15 percent, and the concentrated solution is inactivated at 100 ℃ for 5 minutes to obtain the cistanche extracting solution.
A composition containing the cistanche extracting solution comprises the following components in parts by mass: 75% of cistanche extracting solution, 16% of caprylic-capric glyceride, 1% of glyceryl triacetate, 0.5% of maltol, 0.4% of menthyl acetate, 0.4% of vanillin, 1.2% of ethyl vanillin, 0.8% of ethyl caprylate, 0.7% of D-limonene, 0.3% of gamma-terpinene, 0.75% of beta-pinene, 0.25% of alpha-pinene, 0.35% of D-pyroglutamic acid ethyl ester, 0.75% of 5-hydroxy maltol, 0.95% of nerol and 0.65% of geraniol.
An explosive bead containing the composition is prepared by the flow-liquid mid-drop method. Wherein the content of the composition in the blasting beads is 10.5 mu l/particle, the diameter of the blasting beads is 2.60mm, the weight of the blasting beads is 10.5 mg/particle, the roundness is less than 0.15mm, and the crushing pressure value is 1.3 kgf.
A cigarette containing the above puffed beads is prepared according to the existing cigarette production process. The cigarette is a ternary composite cigarette, the circumference of the cigarette is 17.0mm, a popping bead is placed in a cigarette filter stick, and the popping bead is placed in the middle section of the cigarette filter stick, specifically 15.0mm away from the lip end.
The smoke test results and the smoking evaluation scores of the cigarettes of this example are shown in tables 2 and 3.
According to the feedback of the smoking evaluation result, the embodiment has the advantages that after the blasting beads rich in the cistanche extracting solution are added, the cigarette sample has more intense tobacco fragrance, the fragrance of the herbal medicine and the fragrance of the sweet sauce are outstanding, the blending degree of the tobacco fragrance is better, the thick smoke feeling is better, the mouth is smooth, and the aftertaste is sweet.
Example 4 physical and chemical Properties examination and sensory quality evaluation
Comparative example 1: the blank cigarette bead burst (i.e. not containing any content) prepared by the shunting-liquid mid-point dropping method is placed at the middle position of the filter stick of the ordinary cigarette with the same specification and components as those of the example 1, and specifically, the distance from the lip end is 15.0 mm.
Comparative example 2: the preparation method of the cistanche extracting solution is the same as that of the embodiment 1, and is characterized in that the cistanche extracting solution is directly concentrated after extraction, and an enzyme preparation is not added. The obtained cistanche extract was directly injected into 24.2. mu.l/pellet of the same size blasting beads as in example 1, and then placed in the same size cigarette as in example 1.
Comparative example 3: the preparation method of the cistanche extracting solution is the same as that of the embodiment 1, and the difference is that after extraction, 2.5ml of complex enzyme is added into each 100ml of cistanche extracting solution, wherein the enzyme activity ratio of cellulase, beta-glucosidase, ligninase and pectinase is 4:1:3: 5. The obtained cistanche extract was directly injected into 10.50. mu.l/pellet of the same size blasting beads as in example 3, and then placed into the same size cigarette as in example 3.
The conventional specification parameter tests were carried out on the popped beads and the cigarettes obtained in examples 1 to 3 and comparative examples 1 to 3, respectively, and the results are shown in table 1.
According to the detection method in GB/T19609-2004 cigarette total particulate matter and tar determination by a smoking machine for routine analysis, the physical and chemical properties of the cigarettes obtained in the above examples are detected to determine the contents of the total particulate matter, tar, nicotine in smoke and carbon monoxide in the main stream smoke of the cigarettes in the examples before and after bead breaking by pinching, and the obtained results are shown in Table 2.
As can be seen from the data in Table 2, the cigarettes of examples 1-3 exhibited decreasing amounts of total particulate matter, tar content, smoke nicotine content, and carbon monoxide in the mainstream smoke before and after bead blasting. The decrease of the main stream smoke index of each example is different because of different content of the cistanche extraction liquid, but is higher than that of the cistanche extraction liquid (comparative example 2) which is not treated by the enzyme preparation before and after bead blasting of the cigarette. Therefore, compared with the method in the prior art, the cistanche extracting solution treated by the complex enzyme preparation can effectively reduce the content of harmful substances in the cigarettes. In example 3, the total particulate matter content after bead blasting and breaking is 6.01 mg/count, the tar content is 4.9 mg/count, the nicotine content of smoke is 0.50 mg/count, the carbon monoxide content is 4.8 mg/count, and the index of mainstream smoke is reduced most remarkably.
Meanwhile, in the example 3 after bead blasting by pinching, compared with the comparative example 3, the total particulate matter amount, the tar amount, the nicotine amount and the carbon monoxide amount in the mainstream smoke are all remarkably reduced, so that the effect of the cistanche extract treated by a proper amount of the complex enzyme preparation on improving the cigarette quality is better.
The conclusion shows that the cigarette containing the composition taking the cistanche extract provided by the invention as the main component can effectively reduce the total particulate matter content, the tar content, the smoke nicotine content and the carbon monoxide content of the mainstream smoke of tobacco combustion during smoking, improve the cigarette quality and reduce the harm to human health.
33 professional sensory evaluators were randomly selected and the cigarettes obtained in each example were evaluated for sensory quality. The sensory quality of the cigarette is referred to GB 5606.4-2005 cigarette part 4: the cigarette sensory quality judgment standard in the sensory technical requirements comprises the following steps: gloss, aroma, harmony, offensive odor, irritation and aftertaste, the specific criteria are shown in table 3.
According to the cigarette sensory quality evaluation criteria in table 3, professional sensory evaluators score the sensory quality of each example cigarette, and then take the average value as the final score, and the obtained sensory quality evaluation scoring results of each example cigarette are shown in table 4.
As can be seen from the data in Table 4, the sensory quality evaluation scores of the cigarettes obtained in examples 1 to 3 were all higher than those of comparative examples 1 to 3, indicating that the sensory quality of the cigarettes of the examples of the present invention was significantly improved. As can be seen from the detailed feedback descriptions of professional sensory evaluators, the sensory feelings of the cigarettes obtained in examples 1-3 during smoking are mainly reflected in: the smoke richness, the fine and smooth feeling and the thick feeling are remarkably improved, the tobacco fragrance is more rich and is full-blown, the blending degree is better, the charm of the baking fragrance, the herb fragrance and the sweet fragrance of the sauce is outstanding, no stimulation and impurity gas exist, the harmony is good, the smoke fineness is improved, the mouth is smooth, the sweet feeling is obviously enhanced, and the aftertaste is clean.
The conclusion shows that the cigarette containing the composition taking the cistanche extract provided by the invention as the main component can obviously improve the sensory quality, enhance the aroma, obviously improve the aftertaste and obviously reduce the irritation and the miscellaneous gas of the tobacco during smoking.
In conclusion, the preparation method of the cistanche extract provided by the invention has the advantages that the complex enzyme preparation with a proper proportion is used for enzymolysis, the aroma can be improved when the complex enzyme preparation is used in cigarettes, the complex enzyme preparation also has a health-care effect, and the complex enzyme preparation is particularly suitable for high-quality cigarettes.
The composition taking the cistanche extract as the main component shows strong and unique sweet sauce flavor and herbal flavor when being applied to cigarettes, which are not possessed by cigarettes containing other additives or cigarettes only containing cistanche, and can reduce the physical and chemical indexes of the total particulate matter content, tar content, nicotine content of smoke, carbon monoxide content and the like of the mainstream smoke of the cigarettes and reduce the harm to the human health.
The popping beads containing the composition provided by the invention can be suitable for cigarettes of different specifications and types, and the interestingness of the cigarettes during smoking is improved. The cigarette containing the popping beads is remarkably improved in both mainstream smoke indexes and sensory quality evaluation.
The formula of the blasting beads with specific fragrance is designed in a targeted manner, and after the blasting beads are applied to cigarettes, the smoking internal quality of the cigarettes can be obviously improved, and the smoking feeling is enriched and improved. Meanwhile, the cistanche has certain nourishing and health-care effects, so that the harm of cigarettes can be reduced to a certain extent. Therefore, the cistanche extracting solution, the composition thereof and the bead cracker provided by the application have certain popularization and application values in the tobacco industry.
The above description is only an example of the present application and is not intended to limit the present application. Various modifications and changes may occur to those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present application should be included in the scope of the claims of the present application.
Claims (1)
1. A cigarette containing cistanche extracting solution is characterized in that the preparation method of the cigarette comprises the following steps:
washing herba Cistanchis, removing impurities, air drying, oven drying at 40 deg.C, and pulverizing in liquid nitrogen to 90 mesh to obtain herba Cistanchis powder; under the microwave condition, carrying out water bath hot reflux extraction for 6 hours by using a material-liquid ratio of cistanche deserticola powder to ethanol of 1g to 10ml, cooling to 15 ℃, adding 1.3ml of complex enzyme with the concentration of 10 ten thousand U/ml into each 100ml of cistanche deserticola extract, namely adding 1.3 ten thousand U of enzyme preparation into each gram of cistanche deserticola dry matter, wherein the complex enzyme comprises cellulase, beta-glucosidase, ligninase and pectinase according to the enzyme activity ratio of 4:1:3:5, namely adding 4 thousand U of cellulase, 1 thousand U of beta-glucosidase, 3 thousand U of ligninase and 5 thousand U of pectinase into each gram of cistanche deserticola dry matter, the enzymolysis temperature is 20-25 ℃, and the enzymolysis time is 120-times 150 min; after enzymolysis, concentrating under reduced pressure at 60kPa until the dry matter content of the concentrated solution is 15%, and inactivating at 100 deg.C for 5 min to obtain Cistanchis herba extract;
preparing the cistanche extracting solution into a composition which comprises the following components in parts by mass: 75% of cistanche extracting solution, 16% of caprylic-capric glyceride, 1% of glyceryl triacetate, 0.5% of maltol, 0.4% of menthyl acetate, 0.4% of vanillin, 1.2% of ethyl vanillin, 0.8% of ethyl caprylate, 0.7% of D-limonene, 0.3% of gamma-terpinene, 0.75% of beta-pinene, 0.25% of alpha-pinene, 0.35% of D-pyroglutamic acid ethyl ester, 0.75% of 5-hydroxy maltol, 0.95% of nerol and 0.65% of geraniol;
the composition is prepared into the blasting bead by using a shunting-liquid mid-point dropping method, and the method comprises the step of cutting off a gel column by utilizing the shearing force of the counter flushing of cooling oil and then dropping, and specifically comprises the following steps: utilizing two cooling oils with different incident angles to form shearing force in a solenoid, cutting off wall materials and core liquid in the dropping process, condensing into balls in the cooling oil under the action of surface tension, and preparing finished blasting balls after deoiling, drying and screening; wherein the content of the composition in the blasting beads is 10.5 mu l/particle, the diameter of the blasting beads is 2.60mm, the weight of the blasting beads is 10.5 mg/particle, the roundness is less than 0.15mm, and the crushing pressure value is 1.3 kgf;
and preparing the blasting beads into cigarettes according to the existing cigarette production process, wherein the cigarettes are ternary composite cigarettes, the circumference of each cigarette is 17.0mm, one blasting bead is placed in a cigarette filter stick, and the blasting beads are placed in the middle section of the cigarette filter stick and are specifically 15.0mm away from the lip end.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910224107.7A CN109953367B (en) | 2019-03-22 | 2019-03-22 | Cistanche extracting solution and preparation method, composition and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910224107.7A CN109953367B (en) | 2019-03-22 | 2019-03-22 | Cistanche extracting solution and preparation method, composition and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109953367A CN109953367A (en) | 2019-07-02 |
| CN109953367B true CN109953367B (en) | 2022-08-02 |
Family
ID=67024830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910224107.7A Active CN109953367B (en) | 2019-03-22 | 2019-03-22 | Cistanche extracting solution and preparation method, composition and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109953367B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113475752A (en) * | 2021-06-30 | 2021-10-08 | 河南中烟工业有限责任公司 | Noctilucent bead blasting wall material, noctilucent cigarette bead blasting and preparation method thereof, and bead blasting cigarette |
| CN115948202B (en) * | 2023-03-13 | 2023-06-09 | 内蒙古昆明卷烟有限责任公司 | Sesame oil and preparation method, composition and application thereof |
| CN116676138A (en) * | 2023-07-25 | 2023-09-01 | 内蒙古昆明卷烟有限责任公司 | Oncidium essential oil for cigarettes and preparation method and application thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101538260B (en) * | 2009-04-28 | 2011-07-20 | 云南烟草科学研究院 | Isoflavone compound and prepration method and application thereof |
| CN104770725B (en) * | 2015-04-28 | 2017-04-12 | 内蒙古中兴华冠生物工程股份有限公司 | Cistanche salsa biological fermentation ferment and manufacturing method thereof |
| CN107173738A (en) * | 2017-06-17 | 2017-09-19 | 柴华 | The preparation method of desert cistanche Snakegourd Fruit health-care powder |
| CN108913361A (en) * | 2018-07-26 | 2018-11-30 | 云南中烟新材料科技有限公司 | A kind of purification tea extract, quick-fried pearl and its preparation method and application |
-
2019
- 2019-03-22 CN CN201910224107.7A patent/CN109953367B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN109953367A (en) | 2019-07-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109953366B (en) | Cordyceps sinensis extracting solution and preparation method, composition and application thereof | |
| CN109953367B (en) | Cistanche extracting solution and preparation method, composition and application thereof | |
| CN101548797B (en) | Cigarette and preparation method thereof | |
| CN106987314B (en) | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes | |
| CN104983066A (en) | Folium ginkgo and aloe tobacco substitute product and preparing method thereof | |
| CN115948202B (en) | Sesame oil and preparation method, composition and application thereof | |
| CN115948197B (en) | Preparation method and application of sesame oil | |
| CN111418892A (en) | Cigarette filter stick additive and application thereof | |
| CN109953369A (en) | A kind of preparation method of agalloch eaglewood cigarette | |
| CN101569438A (en) | Method for preparing mulberry cigarette flavor | |
| CN106947597B (en) | Pine pollen essence for cigarette bead blasting and application of pine pollen essence in cigarettes | |
| CN107057856B (en) | Preparation method of liquorice sweetening and moisturizing essence for filter tip | |
| CN107022415B (en) | Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette | |
| CN106867667A (en) | The preparation and its application of a kind of essence spice for cigarette | |
| CN1986759A (en) | Petroleum extracted sophora flower extractum and its application in perfuming cigarette | |
| KR100274825B1 (en) | Smoking material having a prohibition function of smoking | |
| CN107874318A (en) | A kind of turf composite particles, preparation method and its application in cigarette | |
| CN104694254B (en) | Red ginseng extract and its preparation method and application | |
| CN109965340A (en) | A kind of preparation method and application of Herba Cistanches extracting solution | |
| CN115011410B (en) | Schisandra chinensis branch spice, preparation method thereof and cigarette | |
| KR20010030937A (en) | A cigarette of ginkgo leaves | |
| CN110122921A (en) | A kind of preparation method of the quick-fried pearl of black tea | |
| CN107216947A (en) | A kind of preparation method of cigarette Catechu extract | |
| CN109757759B (en) | Composition and application thereof in field of cigarettes/cartridges | |
| JPH1179982A (en) | Smoking material serving also for prohibition of smoking and its production |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |