CN111418892A - Cigarette filter stick additive and application thereof - Google Patents
Cigarette filter stick additive and application thereof Download PDFInfo
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- CN111418892A CN111418892A CN202010429802.XA CN202010429802A CN111418892A CN 111418892 A CN111418892 A CN 111418892A CN 202010429802 A CN202010429802 A CN 202010429802A CN 111418892 A CN111418892 A CN 111418892A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Engineering & Computer Science (AREA)
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- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to the technical field of cigarette production, and particularly discloses a cigarette filter stick additive and application thereof, wherein the cigarette filter stick additive comprises a flavoring agent, a cooling agent and glyceryl triacetate, and the mass ratio of the flavoring agent to the cooling agent is 1: 0.5-1: 4, the sum of the mass of the flavoring agent and the cooling agent is 0.1-3% of the mass of the glyceryl triacetate, wherein the flavoring agent is an extract obtained by mixing one or more of the Yunnan wild mint and the dry sweet osmanthus, the hop, the broad bean flower or the dry fragrant leaves, the selected flavoring agent has simple and easily obtained sources, the selected raw materials have medicinal characteristics and are wide-spectrum medicinal, the effective components can be distilled, gasified, volatilized and sublimated to form a particle phase and a gas phase component, the substances can capture free radicals in smoke, reduce or block the generation of harmful substances, and simultaneously act on a respiratory system, smoke particles with different particle sizes are deposited on the respiratory tract or absorbed into human blood by alveoli, so that the medicinal effect of the flavoring agent is exerted.
Description
Technical Field
The invention relates to the technical field of cigarette production, in particular to a cigarette filter stick additive and application thereof.
Background
With the gradual progress of tar reduction and harm reduction at home and abroad in recent years, the contradiction between tar reduction and flavor retention is more prominent, and the problem that how to ensure the flavor quality of cigarette products while reducing tar and harm is one of the problems which are urgently needed to be solved in the tobacco industry. The cigarette perfuming can increase the smoke concentration and improve the taste, and the common perfuming modes endow the cigarette with unique fragrance style characteristics mainly comprise tobacco shred perfuming, filter stick perfuming, cigarette paper perfuming, packaging material perfuming and the like. Compared with the traditional tobacco shred flavoring, the flavoring of the filter stick can reduce the interception of the tobacco shred to the spice and bring a novel smoking feeling to consumers. The fragrant thread filter stick wraps the fragrant thread dipped with essence in the filter stick tow through a special device, thereby achieving the purpose of perfuming the filter stick.
In the prior art, although a lot of filter additives exist, such as a preparation method and an application of a filter additive CN201710197440.4 capable of improving the smoking comfort of cigarettes, the existing flavor sources and flavor substances extracted by an extraction method have great differences in components, have different influences on mainstream smoke in cigarettes, have different tastes for consumers, and cannot meet the individual requirements of different people. In addition, in the prior art, CN201910267797.4 cigarette filter stick plasticizer, a preparation method thereof and a cigarette filter stick are provided, the spice is prepared from rose, jasmine flower and the like and a cooling agent menthol solution, the menthol can selectively stimulate a human skin or mucous membrane cold sensor to generate cold reflex and cold sense, a hot or stabbing feeling can be brought to a human product, the smoking taste is greatly influenced, and the problems that the prior art for perfuming the cigarette filter stick has low utilization rate of the spice, most of spice components for perfuming the spice lines are left in the filter tip, the residual rate is high, the wanted fragrance effect is achieved, and the cost is increased are solved.
Disclosure of Invention
The invention mainly aims to provide a novel cigarette filter stick additive to solve the problem that the existing additive cannot meet individual requirements of different crowds.
In order to solve the above problems, the present invention provides the following technical solutions:
the additive for the cigarette filter stick is characterized by comprising a flavoring agent, a cooling agent and glyceryl triacetate, wherein the mass ratio of the flavoring agent to the cooling agent is 1: 0.5-1: 4, the sum of the mass of the flavoring agent and the cooling agent is 0.1-3% of the mass of the glyceryl triacetate, wherein the flavoring agent is an extract obtained by mixing yunnan wild mint with at least one of dried sweet osmanthus, hops, broad bean flowers or dried leaves.
The plant natural medicine refers to a part or whole plant of medicinal plant, including root, stem, leaf, flower, fruit and seed, generally contains chemical components capable of preventing and treating diseases, and plants with certain curative effect can be called plant natural medicine. The plant natural medicines are the main body of Chinese traditional medicine, more than 3000 kinds are carried by ancient books, and 8000 kinds are reached by modern arrangement. When the cigarette containing the Chinese herbal medicine additive is smoked, the effective components of the Chinese herbal medicine or the extract thereof can be distilled, gasified, volatilized and sublimated by heating at different temperature gradients in the cigarette to form particulate phase and gaseous phase components, the substances can capture free radicals in smoke, reduce or block the generation of harmful substances, and simultaneously act on a respiratory system, smoke particles with different particle sizes are deposited on a respiratory tract or absorbed into human blood by alveoli, so that the effect of the Chinese herbal medicine is exerted.
The main components of the mint comprise monoterpene, phenols, esters, alcohols and ketones, the composition and accumulation of the volatile oil in the plant body are greatly influenced by the environment, according to GC-MS comparison analysis (facial Yonggang and the like) of the volatile oil in wild and cultivated mint produced in Yunnan, the wild mint has specificity, mainly comprises alkene, alcohol and ketone, 3 components contribute more than 90 percent to the total amount of the volatile oil, mainly comprises alkene and alcohol, the limonene keeps higher amount, namely 12.21 percent, the odor type change is larger, and the wild mint mainly comprises D-limonene, eucalyptol, β -phellandrene (12.21 percent, 46.70 percent and 20.19 percent).
Sweet osmanthus flower, flower fragrance, aromatic oil extraction, sweet osmanthus flower extract preparation, food and cosmetics preparation, cake preparation, candy preparation and wine brewing. Also an ornamental plant. Osmanthus fragrans flower is pungent in flavor and can be used as a medicine.
The hop chemical components are as follows: contains resin including humulone, isohumulone, lupulone, etc., and volatile oil including myrcene, humulene, linalool, lupulol, etc. In addition, there are tannin, flavone compounds, choline, fructose, sucrose, glucose, and the like. The lupulone contained in the composition has inhibitory effect on Bacillus tuberculosis, Staphylococcus aureus, Bacillus subtilis, etc., and can be used for treating experimental atheromatosis change of rabbit, and slightly lowering blood pressure. The extractive solution has sedative and hypnotic effects on central nervous system.
Broad bean flower, dried flower, black brown, wrinkled, about 2 cm long; the crown tube is stuck with a tightly pasted calyx, the front end is 5 pieces, and the head is damaged by drying and breaking; the flag valve of the flower is outside and wraps the petal and the keel valve, and the petal and the keel valve are not easy to distinguish due to crimpling. Slightly fragrant smell and bland taste. Preferably, the flowers are dry, intact and purple-black. It has hemostatic effect, and can be used for treating hemoptysis, hematemesis, leucorrhea with red and white discharge, and hypertension.
The bay leaves, namely the leaves of the cinnamon tree, are gray green, have no mildew spot, have strong fragrance and are superior in taste, have the effects of increasing fragrance, removing peculiar smell and promoting appetite, and can be used for treating rheumatism and hernia according to records in Guangxi Chinese materia medica.
Preferably, the cooling agent is WS-3, WS-23 or menthol.
Further, the preparation method of the flavoring agent comprises the following steps:
(1) mixing 75% of Yunnan wild mint and 25% of at least one spice of dry sweet osmanthus, hop, broad bean flower or dry fragrant leaf, and pulverizing into 20-30 mesh plant fine powder;
(2) dissolving 1g of plant fine powder in 10ml of solvent in ethyl acetate, glyceryl triacetate or MCT, extracting at 20-50 deg.C for 24 hr, extracting at 50-100 deg.C for 2-5 hr, filtering with qualitative filter paper to obtain extractive solution, distilling under reduced pressure, and concentrating to obtain flavoring agent with special fragrance.
Preferably, the flavoring agent comprises 75% of Yunnan wild mint, 10% of dry sweet osmanthus and 15% of hop by mass, the solvent is ethyl acetate, and the mass ratio of the flavoring agent to the cooling agent is 1: 0.5.
Preferably, the flavoring agent comprises 75% of Yunnan wild mint, 5% of dry sweet osmanthus, 5% of hops, 5% of broad bean flowers and 10% of dry fragrant leaves by mass, the solvent is glyceryl triacetate, and the mass ratio of the flavoring agent to the cooling agent is 1: 4.
Preferably, the flavoring agent comprises 75% of Yunnan wild mint, 5% of hop and 20% of dry fragrant leaves by mass, the solvent is MCT, and the mass ratio of the flavoring agent to the cooling agent is 1: 2.
Further, the invention provides a cigarette filter stick, which comprises any one of the cigarette filter stick additives prepared by the invention.
Furthermore, in the process of forming and curing the filter stick, the application amount of the filter stick additive is 6-8%, the temperature and humidity of the curing environment are 24 +/-2 ℃, 60 +/-5%, and the curing time is not less than 4.0 hours in combination with actual production.
The quality of a filter stick directly influences the quality of a cigarette in a rolling connection mode and a finished cigarette, the application amount of a plasticizer, the curing time and the temperature and humidity in the filter stick processing process are not specified and are not based at present, a 2016 (cigarette process specification) provides a wider guide range (4-12%) for the application amount of triacetin serving as the plasticizer, the curing time of the filter stick is determined according to the characteristics of the triacetin and is preferably more than 8 hours, the spice extract is added to the triacetin serving as the plasticizer, and in order that the hardness of the filter stick is not influenced and the corresponding production index of the filter stick is reached, the application amount of the filter stick additive is recommended to be added in the actual production and is 6-8%, the temperature and the humidity of the curing environment are 24 +/-2 ℃, 60 +/-5% and the curing time is more than or.
The invention has the following advantages:
1. the spice of the invention is prepared by mixing Yunnan wild mint and at least one spice of dry sweet osmanthus, hop, broad bean flower or dry fragrant leaf, after extraction, the fragrant substances are rich, and a plurality of choices are provided for consumers to select different tastes and fragrances.
2. The selected spice has simple and easily obtained sources, the selected raw materials have medicinal characteristics and broad-spectrum medicinal property, the effective components can be distilled, gasified, volatilized and sublimated to form granular phase and gaseous phase components, the substances can capture free radicals in smoke, reduce or block the generation of harmful substances, and simultaneously act on a respiratory system, smoke particles with different grain sizes are deposited on a respiratory tract or absorbed into human blood by alveoli, so that the medicinal effect of the spice is exerted.
3. The cooling agent used in the invention is a novel cooling agent W-3 or W-23, has extremely high cooling activity without burning, numbness, irritation and other side effects, and can generate more impact, fresh and lasting fragrance after being matched with the flavoring agent.
4. The final product cigarette filter stick additive can obtain obvious taste experience by adding a small amount of the product when in use, the utilization rate of the spice is high, and the rejection rate of the filter stick after smoking detection is greatly reduced by only 70%.
Detailed Description
In order to clearly understand the technical spirit and the advantages of the present invention, the applicant below describes in detail by way of example, but the description of the example is not intended to limit the technical scope of the present invention, and any equivalent changes made according to the present inventive concept, which are merely in form and not in material, should be considered as the technical scope of the present invention. The methods used in the examples below are conventional methods unless otherwise specified, the materials and reagents used therein are commercially available, and the equipment used in the experiments are well known to those skilled in the art without otherwise specified. In the following examples,% is by mass unless otherwise specified.
Example 1
Mixing and crushing 75% of Yunnan wild mint, 10% of dry sweet osmanthus and 15% of hop into 20-30 meshes of plant fine powder; dissolving 1g of plant fine powder in ethyl acetate per 10ml of solvent, leaching at 20-50 deg.C for 24 hr, standing at room temperature for 24 hr, extracting at 50 deg.C for 5 hr, filtering with qualitative filter paper to obtain extractive solution, distilling under reduced pressure, and concentrating to obtain flavoring agent A with special fragrance.
And mixing the flavoring agent A with a novel compound cooling agent WS-3 according to the mass ratio of 1:0.5 to obtain a mixture A1.
Dissolving A1 in a filter stick plasticizer glyceryl triacetate according to the proportion of 3.0% to obtain the final product filter stick additive, wherein the relative density is 1.1521, the refractive index is 1.4233, and the application amount of the prepared filter stick additive is 6%, the temperature and humidity of a curing environment are 24 +/-2 ℃, 60 +/-5% and the curing time is 4.0h, so that a molded product is obtained. The cigarette filter stick additive is placed on a Hongtashan classic 1956 (hard-shelled cigarette) cigarette for smoking evaluation, and the cigarette filter stick additive is full in fragrance, good in smoke conglobation, not obvious in stimulation, free of miscellaneous gas and free of residual taste.
According to the implementation method of example 1, the flavoring agent A and the cooling agent WS-3 are mixed according to the mass ratio of 1:0.5, 1:1, 1:2 and 1:4 to obtain mixtures A2, A3 and A4, and the mixtures A1, A2, A3 and A4 are directly injected into a cigarette of Hongtashan classic 1956 (hard-shell package) by a micro-injector to be evaluated, so that the evaluation table 1 is obtained.
As can be seen from table 1, the effect is the best in the proportion of a1, and it can be seen that when ethyl acetate is used as the extraction solvent, the flavor extract prepared by the present invention is added to the solidified filter stick, and the mixture of the flavor a and the cooling agent WS-3 is dissolved in triacetin as the filter stick plasticizer in the proportion of 1:0.5 by mass, so that the final filter stick additive of the present invention is obtained.
Example 2
Mixing Yunnan wild mint 75%, dry sweet osmanthus 5%, hop 5%, broad bean flower 5% and dry fragrant leaf 10%, and pulverizing into 20-30 mesh plant fine powder. Dissolving 1g plant fine powder in 10ml solvent in glyceryl triacetate, extracting at 20-50 deg.C for 24 hr, extracting at 100 deg.C for 2 hr, filtering with qualitative filter paper to obtain extractive solution, distilling under reduced pressure, and concentrating to obtain flavoring agent B with special fragrance.
And mixing the flavoring agent B with a novel compound cooling agent WS-3 according to the mass ratio of 1:4 to obtain a mixture B4.
Dissolving B4 in a filter stick plasticizer glyceryl triacetate at a ratio of 2.0% to obtain the final product filter stick additive, wherein the relative density is 1.1536, the refractive index is 1.4261, and the application amount of the prepared filter stick additive is 7%, the temperature and humidity of a curing environment are 24 +/-2 ℃, 60 +/-5% and the curing time is 4.0h, so that a molded product is obtained. The cigarette filter stick additive is placed on a Hongtashan classic 1956 (hard-shelled cigarette) cigarette for smoking detection, and the cigarette filter stick additive disclosed by the invention is soft, fine and mellow in fragrance, free of stimulation and obvious miscellaneous gas, and clean and comfortable in oral cavity.
According to the implementation method of example 2, the flavoring agent B and the cooling agent WS-3 are mixed according to the mass ratio of 1:0.5, 1:1, 1:2 and 1:4 to obtain mixtures B1, B2 and B3, and the mixtures B1, B2, B3 and B4 are directly injected into a traditional cigarette filter stick by a micro-injector for evaluation to obtain an evaluation table 2.
As can be seen from table 2, the effect is the best in the proportion of B4, and it can be seen that when triacetin is used as the extraction solvent, the flavor extract prepared by the present invention is added to the already solidified filter rod, and the fusion is better in the overall case, and the evaluation result is the best in the proportion of flavor B and cooling agent WS-3 in the mass ratio of 1:4, so that in the case of this solvent extraction, the mixture of flavor B and cooling agent WS-3 in this proportion is preferably selected to be dissolved in triacetin the filter rod plasticizer triacetin to obtain the final product filter rod additive of the present invention.
Example 3
Pulverizing Yunnan wild herba Menthae 75%, flos Lupuli 5%, and dry folium aucklandiae 20% into 20-30 mesh plant fine powder. Dissolving 1g plant fine powder in MCT solvent per 10ml solvent, extracting at 20-50 deg.C for 24 hr, extracting at 70 deg.C for 3 hr, filtering with qualitative filter paper to obtain extractive solution, distilling under reduced pressure, and concentrating to obtain flavoring agent C with special fragrance.
And mixing the flavoring agent C with a novel cooling agent WS-23 according to the mass ratio of 1:2 to obtain a mixture C3.
C3 is dissolved in a filter stick plasticizer MCT according to the proportion of 0.1% to obtain the final product filter stick additive, the relative density is 1.1498, the refractive index is 1.4341, the application amount of the prepared filter stick additive is 8%, the temperature and humidity of the curing environment are 24 +/-2 ℃, 60 +/-5% and the curing time is 4.0h, and then the formed product is obtained. The cigarette filter stick additive is placed on a Hongtashan classic 1956 (hard-shelled cigarette) cigarette for smoking detection, and has the advantages of full fragrance, good harmony, no miscellaneous gas and comfortable aftertaste.
According to the implementation method of example 3, the flavoring agent C and the cooling agent WS-23 are mixed according to the mass ratio of 1:0.5, 1:1, 1:2 and 1:4 to obtain mixtures C1, C2 and C4, and the mixtures C1, C2, C3 and C4 are directly injected into a traditional cigarette filter stick by a micro-injector for 10 microliter respectively to be evaluated to obtain an evaluation table 3.
As can be seen from table 2, the effect is the best in the C3 ratio, and it can be seen that when MCT is used as the extraction solvent, the flavor extract prepared by the present invention is added to the already solidified filter rod, the fusibility is better, and the evaluation result is the best in the ratio of flavor C to cooling agent WS-23 by mass of 1:2, so in the case of this solvent extraction, the mixture of flavor C and cooling agent WS-23 in this ratio is preferably selected to be dissolved in the filter rod plasticizer triacetin to obtain the final product filter rod additive of the present invention.
Example 4
Mixing Yunnan wild mint 75%, dry sweet osmanthus 5%, hop 5%, broad bean flower 5% and dry fragrant leaf 10%, and pulverizing into 20-30 mesh plant fine powder. Dissolving 1g plant fine powder in 10ml solvent in glyceryl triacetate, extracting at 20-50 deg.C for 24 hr, extracting at 100 deg.C for 2 hr, filtering with qualitative filter paper to obtain extractive solution, distilling under reduced pressure, and concentrating to obtain flavoring agent with special fragrance.
And mixing the flavoring agent and the menthol according to the mass ratio of 1:1 to obtain a mixture. And dissolving the mixture in a filter stick plasticizer glyceryl triacetate according to the proportion of 1.0% to obtain the final product filter stick additive, wherein the relative density is 1.1436, the refractive index is 1.4161, the application amount of the prepared filter stick additive is 7%, the temperature and humidity of the curing environment are 24 +/-2 ℃, 60 +/-5% and the curing time is 4.0h, and then the formed product is obtained. The cigarette filter stick additive is placed on a Hongtashan classic 1956 (hard-shelled cigarette) cigarette for smoking detection, and the cigarette filter stick additive disclosed by the invention is soft, fine and mellow in fragrance, free of stimulation, good in coordination, free of obvious miscellaneous gas and clean in aftertaste.
Claims (8)
1. The additive for the cigarette filter stick is characterized by comprising a flavoring agent, a cooling agent and glyceryl triacetate, wherein the mass ratio of the flavoring agent to the cooling agent is 1: 0.5-1: 4, the sum of the mass of the flavoring agent and the cooling agent is 0.1-3% of the mass of the glyceryl triacetate, wherein the flavoring agent is an extract obtained by mixing yunnan wild mint with one or more of dried sweet osmanthus, hop, broad bean flower or dried fragrant leaves.
2. The cigarette filter stick additive of claim 1, wherein the cooling agent is WS-3, WS-23 or menthol.
3. The cigarette filter stick additive according to claim 1, wherein the preparation method of the flavoring agent comprises the following steps:
(1) mixing 75% of Yunnan wild mint and 25% of at least one spice of dry sweet osmanthus, hop, broad bean flower or dry fragrant leaf, and pulverizing into 20-30 mesh plant fine powder;
(2) dissolving 1g of plant fine powder in 10ml of solvent in ethyl acetate, glyceryl triacetate or MCT, extracting at 20-50 deg.C for 24 hr, extracting at 50-100 deg.C for 2-5 hr, filtering with qualitative filter paper to obtain extractive solution, distilling under reduced pressure, and concentrating to obtain flavoring agent with special fragrance.
4. The additive for cigarette filter sticks according to claim 3, wherein the raw materials in the flavoring agent comprise 75% of Yunnan wild mint, 10% of dried sweet osmanthus and 15% of hops by mass, the solvent is ethyl acetate, and the mass ratio of the flavoring agent to the cooling agent is 1: 0.5.
5. The cigarette filter stick additive according to claim 3, wherein the raw materials of the flavoring agent comprise, by mass, 75% of Yunnan wild mint, 5% of dried sweet osmanthus, 5% of hops, 5% of broad bean flower and 10% of dried fragrant leaf, the solvent is glyceryl triacetate, and the mass ratio of the flavoring agent to the cooling agent is 1: 4.
6. The additive for cigarette filter sticks according to claim 3, wherein the raw materials in the flavoring agent comprise 75% of Yunnan wild mint, 5% of hop and 20% of dry fragrant leaves by mass, the solvent is MCT, and the mass ratio of the flavoring agent to the cooling agent is 1: 2.
7. A cigarette filter stick characterized by comprising the cigarette filter stick additive according to any one of claims 1 to 6.
8. The cigarette filter stick according to claim 7, wherein in the process of forming and curing the filter stick, in combination with actual production, the application amount of the filter stick additive is 6-8%, the temperature and humidity of the curing environment are 24 +/-2 ℃, 60 +/-5%, and the curing time is not less than 4.0 h.
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| CN202010429802.XA CN111418892A (en) | 2020-05-20 | 2020-05-20 | Cigarette filter stick additive and application thereof |
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| CN202010429802.XA CN111418892A (en) | 2020-05-20 | 2020-05-20 | Cigarette filter stick additive and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113817547A (en) * | 2021-11-03 | 2021-12-21 | 江苏大亚滤嘴材料有限公司 | Hawthorn essence for cigarettes and application of hawthorn essence to filter stick |
| CN114041626A (en) * | 2021-11-29 | 2022-02-15 | 江苏大亚滤嘴材料有限公司 | Granulation additive capable of improving suction comfort of plant-based granulated tobacco |
| CN114468354A (en) * | 2021-12-14 | 2022-05-13 | 江苏大亚滤嘴材料有限公司 | Preparation method of dust-free paper with cooling function and application of dust-free paper to composite filter stick |
| WO2023021292A1 (en) * | 2021-08-18 | 2023-02-23 | Essentra Filter Products Development Co Pte Ltd. | A cooling element |
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