CN105132167A - Plant particle capable of moisturizing and carrying fragrance, and preparation method and applications thereof - Google Patents
Plant particle capable of moisturizing and carrying fragrance, and preparation method and applications thereof Download PDFInfo
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- CN105132167A CN105132167A CN201510504506.0A CN201510504506A CN105132167A CN 105132167 A CN105132167 A CN 105132167A CN 201510504506 A CN201510504506 A CN 201510504506A CN 105132167 A CN105132167 A CN 105132167A
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- 239000002245 particle Substances 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000003205 fragrance Substances 0.000 title abstract 2
- 230000003020 moisturizing effect Effects 0.000 title abstract 2
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 60
- 239000000284 extract Substances 0.000 claims abstract description 26
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 25
- 235000009566 rice Nutrition 0.000 claims abstract description 25
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 244000178870 Lavandula angustifolia Species 0.000 claims abstract description 6
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims abstract description 6
- 241000220317 Rosa Species 0.000 claims abstract description 6
- 240000007594 Oryza sativa Species 0.000 claims abstract 6
- 244000269722 Thea sinensis Species 0.000 claims abstract 6
- 235000013311 vegetables Nutrition 0.000 claims description 37
- 238000010298 pulverizing process Methods 0.000 claims description 20
- 239000002904 solvent Substances 0.000 claims description 10
- 238000004821 distillation Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 241000132446 Inula Species 0.000 claims description 5
- 244000246386 Mentha pulegium Species 0.000 claims description 5
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 5
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 5
- 235000017276 Salvia Nutrition 0.000 claims description 5
- 244000272264 Saussurea lappa Species 0.000 claims description 5
- 235000006784 Saussurea lappa Nutrition 0.000 claims description 5
- 238000000641 cold extrusion Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 5
- 235000001050 hortel pimenta Nutrition 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 240000007164 Salvia officinalis Species 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 abstract description 15
- 241000382455 Angelica sinensis Species 0.000 abstract 1
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 1
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 1
- 244000182022 Salvia sclarea Species 0.000 abstract 1
- 235000002911 Salvia sclarea Nutrition 0.000 abstract 1
- 239000001102 lavandula vera Substances 0.000 abstract 1
- 235000018219 lavender Nutrition 0.000 abstract 1
- 241001122767 Theaceae Species 0.000 description 21
- 241000209094 Oryza Species 0.000 description 19
- 230000000391 smoking effect Effects 0.000 description 18
- 239000002304 perfume Substances 0.000 description 11
- 239000002131 composite material Substances 0.000 description 9
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 8
- 239000003546 flue gas Substances 0.000 description 8
- 239000011236 particulate material Substances 0.000 description 8
- 230000001953 sensory effect Effects 0.000 description 7
- 244000176261 Viburnum cassinoides Species 0.000 description 6
- 238000000465 moulding Methods 0.000 description 6
- 239000000779 smoke Substances 0.000 description 6
- 238000001179 sorption measurement Methods 0.000 description 5
- 241001072909 Salvia Species 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 230000033228 biological regulation Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000013068 control sample Substances 0.000 description 3
- 238000007306 functionalization reaction Methods 0.000 description 3
- 230000006798 recombination Effects 0.000 description 3
- 238000005215 recombination Methods 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 210000000697 sensory organ Anatomy 0.000 description 3
- 239000000470 constituent Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000005469 granulation Methods 0.000 description 2
- 230000003179 granulation Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229960000892 attapulgite Drugs 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000013335 mesoporous material Substances 0.000 description 1
- 229910052901 montmorillonite Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229910052625 palygorskite Inorganic materials 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a plant particle capable of moisturizing and carrying fragrance, and a preparation method and applications thereof, and belongs to the technical field of cigarette filter added material. The plant particle is prepared from, by weight, 10 to 25 parts of radix saussureae lappae, 10 to 25 parts of radix inulae racemosae, 5 to 15 parts of salvia sclarea L., 5 to 25 parts of rose, 5 to 25 parts of lavender, 10 to 25 parts of mint, 5 to 25 parts of angelica sinensis, and 15 to 35 parts of rice tea extract. According to the preparation method, Yunnan characteristic fragrant plants are taken as raw materials; superfine grinding is adopted, and groove-type material mixing is adopted for material mixing; self-made rice tea extract is added; and the plant particle is obtained via cold extruding using a pelletizer at room temperature. The plant particle is prepared from natural fragrant plant raw materials, is natural and safe, can be accepted by consumers easily, and possesses relatively high application value.
Description
Technical field
The present invention relates to a kind of profit that increases and carry fragrant vegetable particle and its preparation method and application, belong to cigarette mouth rod adding material technical field.
Background technology
The sucking quality of cigarette product and security determine that human consumer selects the main factor bought.Along with society is to smoking and health problem pay attention to day by day, reducing tar and reducing harm becomes one of focus of people's concern.While reduction harmful ingredients in flue gas, style and the sucking quality, particularly flue gas that must have influence on cigarette be dry, stimulate the problems such as increase, throat's comfortableness reduction.But at present report be applied to inorganic materials in filter tip as gac, montmorillonite, medical stone, attapulgite etc., the loss of cigarette flavor can be caused while reducing tar and reducing harm, many potential safety hazards can be brought simultaneously; The additive such as bio-extract, natural plant extracts, its biological activity has certain effect to reduction objectionable impurities, but its stability is bad; Some natural materialss such as tea dust, tea stalk and expanded cabo, play pore structure and mostly be airtight cell cavity, filtration efficiency is low.Therefore, develop a kind of can increase cigarette flavor, promote moisture feeling, do not affect the filter stick filtering material that cigarette sensory quality, high adsorption capacity have good processing characteristics simultaneously, become the technical problem that tobacco industry is to be solved.
Increasing a profit year fragrant Yunnan Special plant particle is with direct application mode, Special plant by Yunnan pulverizes rear granulation, add to after special functionalization again in filter stick, farthest can remain aroma component and the activeconstituents of plant, along with the change of cigarette smoking temperature, its effective constituent can be distilled, gasifies, volatilizees and distil, and reaches and enriches cigarette cigarette perfume, give cigarette characteristic perfume.Due to the porous performance of particulate material, have the effect of adsorbing and retaining concurrently, can the objectionable impurities such as tar in active adsorption cigarette smoke.Meanwhile, on particulate material, load homemade increasing profit material, gives the functional performance that particulate material increases profit, thus reaches the wetting property increasing flue gas, improve the object of cigarette smoking quality.
Summary of the invention
A kind of profit that increases is the object of the present invention is to provide to carry fragrant vegetable particle, prepared by following raw material, each raw material and parts by weight are: Saussurea lappa Clarke 10 ~ 25 weight part, Tibet inula root 10 ~ 25 weight part, Salvia Sclare L. 5 ~ 15 weight part, rose 5 ~ 25 weight part, lavandula angustifolia 5 ~ 25 weight part, peppermint 10 ~ 25 parts, Radix Angelicae Sinensis 5 ~ 25 weight part, rice tea extract 15 ~ 35 weight part; Above raw material is raw materials used except rice tea extract is dry product.
The preparation method of rice tea extract of the present invention specifically comprises the following steps: the preparation method of described rice tea extract specifically comprises the following steps: in mass ratio for polished rice is mixed rear pulverizing by the ratio of 4:1 ~ 10:1 with tealeaves, using the mixing solutions of second alcohol and water as extraction solvent, than the ratio for 1:20 ~ 1:60, the polished rice after pulverizing is mixed with tealeaves in raw material and solvent quality after pulverizing, then carry out microwave-assisted wet distillation and obtain a meter tea extract.
Preferably, the condition of microwave-assisted wet distillation of the present invention is microwave power 350 ~ 750W, radiated time 5 ~ 30min.
The described preparation method increasing profit year fragrant vegetable particle of the present invention, specifically comprises the following steps:
(1) at 50 ~ 70 DEG C by raw material pulverizing to >=90 object powder, adopt slot type mixer to mix material, then add a meter tea extract;
(2) mixture that step (1) obtains manufactures 20-40 order particle by the cold extrusion of tablets press room temperature, obtains increasing profit and carry fragrant vegetable particle after drying materials.
The profit that increases of the present invention is when carrying the filter tip of fragrant vegetable particle for the preparation of cigarette, and increasing profit, to carry the addition of fragrant vegetable particle in mouth rod be that 10mg ~ 30mg/ props up.
The present invention tests in conjunction with smoke chemistry, plant chemical ingredient, plant inhales taste allotment test, directly apply in the form of granules after screening Yunnan Special plant is carried out functionalization, Special plant by Yunnan pulverizes rear granulation, add to after special functionalization again in filter stick, farthest can remain aroma component and the activeconstituents of plant, along with the change of cigarette smoking temperature, its effective constituent can be distilled, gasification, volatilization and distillation, ensure that the release of its flavour ingredient also can reach with the harmony of cigarette style phase and enrich cigarette cigarette perfume, give cigarette characteristic perfume, increase flue gas moist feeling, reduce and stimulate, significantly improve throat's comfortableness, improve the object of cigarette smoking quality, meanwhile, this particulate material has porous performance, and have larger specific surface area, mean pore size is moderate, belongs to mesoporous material category, meets the feature requirement of filter stick sorbing material, and therefore, this particulate material has had the effect retaining absorption concurrently.
Relative to prior art, the present invention has the following advantages:
(1) increasing profit year fragrant vegetable particle of the present invention is natural, nontoxic, and source is sufficient, and technical process is simple, easy to make, with low cost, adds simply, does not change existing cigarette producing process.
(2) of the present inventionly increase the rice tea extract that profit carries fragrant vegetable particle load and can have humectation effect in various degree to kinds of cigarettes, can coordinate with cigarette smoke, flue gas moist feeling can be increased again, reduce and stimulate, significantly improve throat's comfortableness.
(3) increase profit to carry a fragrant plants particles material and be rich in the feature coordinated with cigarette and volatilize wet goods chemical composition, and effectively aroma component has the volatile feature of lower boiling, can guarantee its flavour ingredient release and can with the harmony of cigarette style phase, thus it is fragrant to enrich cigarette cigarette, make cigarette perfume (or spice) softer, fine and smooth, sweet sense well, without assorted gas, pleasant impression is clean, improves the object of cigarette smoking quality.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail, but protection scope of the present invention is not limited to described content.
embodiment 1
Increase profit described in the present embodiment and carry fragrant vegetable particle, prepared by following raw material, each raw material and parts by weight are: Saussurea lappa Clarke 10 weight part, Tibet inula root 20 weight part, Salvia Sclare L. 5 weight part, rose 25 weight part, lavandula angustifolia 5 weight part, peppermint 10 parts, Radix Angelicae Sinensis 5 weight part, rice tea extract 15 weight part.
Described in the present embodiment, the preparation method of rice tea extract specifically comprises the following steps: in mass ratio for polished rice is mixed rear pulverizing by the ratio of 4:1 with tealeaves, using the mixing solutions of second alcohol and water as extraction solvent, polished rice after pulverizing is mixed with tealeaves than the ratio for 1:20 in raw material and solvent quality after pulverizing, then carry out microwave-assisted wet distillation (microwave power 350, radiated time 30min) and obtain a meter tea extract.
Increase the preparation method that profit carries fragrant vegetable particle described in the present embodiment, specifically comprise the following steps:
(1) at 50 DEG C by raw material pulverizing to >=90 object powder, adopt slot type mixer to mix material, then add a meter tea extract;
(2) mixture that step (1) obtains manufactures 20-40 order particle by the cold extrusion of tablets press room temperature, and material obtains increasing profit and carries fragrant vegetable particle after drying in 70 DEG C.
Select specific standard tow, 20-40 object particle is carried out charge bar on KDF-2E forming machine roll, select specification tow to roll white rod on KDF-2E forming machine, charge bar carries out composite molding with white rod on composite molding machine, roll into binary compound filter candle, recombination length is 1:1; It is that 25mg/ props up that this increasing profit carries the addition of fragrant vegetable particle in mouth rod.
Then cigarette sensory evaluating smoking is carried out by the regulation of panel of experts by " technical requirements of GB5606.4-1996 cigarette sense organ " of smokeing panel test.Control sample is do not add to increase the normal cigarette that profit carries fragrant vegetable particle, and smoking result is in table 1; Smoking result in table 1 shows, this increasing profit carries fragrant vegetable particle can enrich cigarette cigarette perfume, and cigarette perfume (or spice) is softer, reduces and stimulates, and increases flue gas moist feeling, significantly improves throat's comfortableness.
Table 1 cigarette sensory evaluating smoking result
For analyzing this particulate material adsorption further, analyzing, the results are shown in Table 2 according to the main flume routine of relevant criterion to cigarette of GB5606.5-2005, result is the mean value after survey three times.Table 2 result shows, this increasing profit carries fragrant vegetable particle to cigarette smoke index without negative impact, and wherein tar content and CO content decrease.
Table 2 composite filter tip cigarette conventional index detects
embodiment 2
Increase profit described in the present embodiment and carry fragrant vegetable particle, prepared by following raw material, each raw material and parts by weight are: Saussurea lappa Clarke 20 weight part, Tibet inula root 10 weight part, Salvia Sclare L. 10 weight part, rose 15 weight part, lavandula angustifolia 15 weight part, peppermint 20 parts, Radix Angelicae Sinensis 18 weight part, rice tea extract 25 weight part.
Described in the present embodiment, the preparation method of rice tea extract specifically comprises the following steps: in mass ratio for polished rice is mixed rear pulverizing by the ratio of 6:1 with tealeaves, using the mixing solutions of second alcohol and water as extraction solvent, polished rice after pulverizing is mixed with tealeaves than the ratio for 1:40 in raw material and solvent quality after pulverizing, then carry out microwave-assisted wet distillation (microwave power 550W, radiated time 20min) and obtain a meter tea extract.
Increase the preparation method that profit carries fragrant vegetable particle described in the present embodiment, specifically comprise the following steps:
(1) at 60 DEG C by raw material pulverizing to >=90 object powder, adopt slot type mixer to mix material, then add a meter tea extract;
(2) mixture that step (1) obtains manufactures 20-40 order particle by the cold extrusion of tablets press room temperature, and material obtains increasing profit and carries fragrant vegetable particle after drying in 70 DEG C.
Select specific standard tow, 20-40 object particle is carried out charge bar on KDF-2E forming machine roll, select specification tow to roll white rod on KDF-2E forming machine, charge bar carries out composite molding with white rod on composite molding machine, roll into binary compound filter candle, recombination length is 1:1; It is that 10mg/ props up that this increasing profit carries the addition of fragrant vegetable particle in mouth rod.
Then cigarette sensory evaluating smoking is carried out by the regulation of panel of experts by " technical requirements of GB5606.4-1996 cigarette sense organ " of smokeing panel test.Control sample is do not add to increase the normal cigarette that profit carries fragrant vegetable particle, and smoking result is in table 3; Smoking result in table 3 shows, this increasing profit carries fragrant vegetable particle can enrich cigarette cigarette perfume, and cigarette perfume (or spice) is softer, reduces and stimulates, and increases flue gas moist feeling, significantly improves throat's comfortableness.
Table 3 cigarette sensory evaluating smoking result
For analyzing this particulate material adsorption further, analyzing, the results are shown in Table 4 according to the main flume routine of relevant criterion to cigarette of GB5606.5-2005, result is the mean value after survey three times.Table 4 result shows, this increasing profit carries fragrant vegetable particle to cigarette smoke index without negative impact, and wherein tar content and CO content decrease.
Table 4 composite filter tip cigarette conventional index detects
embodiment 3
Increase profit described in the present embodiment and carry fragrant vegetable particle, prepared by following raw material, each raw material and parts by weight are: Saussurea lappa Clarke 25 weight part, Tibet inula root 25 weight part, Salvia Sclare L. 15 weight part, rose 5 weight part, lavandula angustifolia 25 weight part, peppermint 25 parts, Radix Angelicae Sinensis 25 weight part, rice tea extract 35 weight part.
Described in the present embodiment, the preparation method of rice tea extract specifically comprises the following steps: in mass ratio for polished rice is mixed rear pulverizing by the ratio of 10:1 with tealeaves, using the mixing solutions of second alcohol and water as extraction solvent, polished rice after pulverizing is mixed with tealeaves than the ratio for 1:60 in raw material and solvent quality after pulverizing, then carry out microwave-assisted wet distillation (microwave power 750W, radiated time 5min) and obtain a meter tea extract.
Increase the preparation method that profit carries fragrant vegetable particle described in the present embodiment, specifically comprise the following steps:
(1) at 70 DEG C by raw material pulverizing to >=90 object powder, adopt slot type mixer to mix material, then add a meter tea extract;
(2) mixture that step (1) obtains manufactures 20-40 order particle by the cold extrusion of tablets press room temperature, and material obtains increasing profit and carries fragrant vegetable particle after drying in 70 DEG C.
Select specific standard tow, 20-40 object particle is carried out charge bar on KDF-2E forming machine roll, select specification tow to roll white rod on KDF-2E forming machine, charge bar carries out composite molding with white rod on composite molding machine, roll into binary compound filter candle, recombination length is 1:1; It is that 35mg/ props up that this increasing profit carries the addition of fragrant vegetable particle in mouth rod.
Then cigarette sensory evaluating smoking is carried out by the regulation of panel of experts by " technical requirements of GB5606.4-1996 cigarette sense organ " of smokeing panel test.Control sample is do not add to increase the normal cigarette that profit carries fragrant vegetable particle, and smoking result is in table 5; Smoking result in table 5 shows, this increasing profit carries fragrant vegetable particle can enrich cigarette cigarette perfume, and cigarette perfume (or spice) is softer, reduces and stimulates, and increases flue gas moist feeling, significantly improves throat's comfortableness.
Table 5 cigarette sensory evaluating smoking result
For analyzing this particulate material adsorption further, analyzing, the results are shown in Table 6 according to the main flume routine of relevant criterion to cigarette of GB5606.5-2005, result is the mean value after survey three times.Table 6 result shows, this increasing profit carries fragrant vegetable particle to cigarette smoke index without negative impact, and wherein tar content and CO content decrease.
Table 6 composite filter tip cigarette conventional index detects
Claims (5)
1. one kind increases profit year fragrant vegetable particle, it is characterized in that, prepared by following raw material, each raw material and parts by weight are: Saussurea lappa Clarke 10 ~ 25 weight part, Tibet inula root 10 ~ 25 weight part, Salvia Sclare L. 5 ~ 15 weight part, rose 5 ~ 25 weight part, lavandula angustifolia 5 ~ 25 weight part, peppermint 10 ~ 25 parts, Radix Angelicae Sinensis 5 ~ 25 weight part, rice tea extract 15 ~ 35 weight part.
2. increase profit according to claim 1 and carry fragrant vegetable particle, it is characterized in that: the preparation method of described rice tea extract specifically comprises the following steps: in mass ratio for polished rice is mixed rear pulverizing by the ratio of 4:1 ~ 10:1 with tealeaves, using the mixing solutions of second alcohol and water as extraction solvent, than the ratio for 1:20 ~ 1:60, the polished rice after pulverizing is mixed with tealeaves in raw material and solvent quality after pulverizing, then carry out microwave-assisted wet distillation and obtain a meter tea extract.
3. increase profit according to claim 2 and carry fragrant vegetable particle, it is characterized in that: the condition of described microwave-assisted wet distillation is microwave power 350 ~ 750W, radiated time 5 ~ 30min.
4. increase the preparation method that profit carries fragrant vegetable particle described in claim 1, it is characterized in that, specifically comprise the following steps:
(1) at 50 ~ 70 DEG C by raw material pulverizing to >=90 object powder, adopt slot type mixer to mix material, then add a meter tea extract;
(2) mixture that step (1) obtains manufactures 20-40 order particle by the cold extrusion of tablets press room temperature, obtains increasing profit and carry fragrant vegetable particle after drying materials.
5. increasing profit according to claim 1 carries fragrant vegetable particle for the preparation of the filter tip of cigarette, it is characterized in that: increasing the profit year addition of fragrant vegetable particle in filter tip is that 10mg ~ 30mg/ props up.
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Cited By (1)
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CN111418892A (en) * | 2020-05-20 | 2020-07-17 | 云南如茨生物科技有限公司 | Cigarette filter stick additive and application thereof |
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