CN109852476A - A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application - Google Patents
A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application Download PDFInfo
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Abstract
The present invention provides a kind of not to burn the essence of smoking article, preparation method and application suitable for low temperature, is related to low temperature and does not burn smoking article technical field.The essence includes having relieving cough and reducing sputum functional component, described to have relieving cough and reducing sputum functional component at least one of Blumea oil, daurian rhododendron oil, oil of negundo chastetree, α-asarone, Mang ox ketone, cymol, orthocoll, acetylcysteine, isofraxidin, aesculetin, Ligustilide, stachydrine, ligustrazine, Imperatorin, Isomperatorin, praeruptorin A, Praeruptorin B, Praeruptorin C, hygrine, Cuscohygrine.Relieving cough and reducing sputum functional component therein is active skull cap components, it can volatilize under atomization temperature is transferred in smoke's total particulate matter, while abundant flue gas, enhancing mouthfeel, part is absorbed by the body, so that low temperature does not burn, smoking article has the function of a degree of adjusting respiratory system function.
Description
Technical field
It does not burn smoking article technical field the present invention relates to low temperature, more particularly to a kind of is suitable for low temperature not burning fuming
The essence of product, preparation method and application.
Background technique
As the problem of smoking and health is increasingly subject to extensive concern, research and development can be effectively reduced the release of tobacco harmful components
The new tobacco products of amount has become industry research emphasis.Wherein, most representational new tobacco products have electronic cigarette and
Heat the smoking article that do not burn.
Heating the smoking article that do not burn is to be heated by heating source to cigarette core material, is wherein contained after cigarette core material is heated
Some smoke agents and volatile component evaporation generate gas to meet consumer demand.Heat the principle for the smoking article that do not burn
It is heating evaporation, is on-fuel state, does not generate tar, therefore the harmful components that traditional cigarette high-temp combustion generates are heating
It does not burn and is greatly reduced in smoking article, significantly reduce harm of the product to consumer health.
Obtain the favor of consumer with the low temperature smoking article that do not burn, major tobacco enterprise domestic in recent years also one after another plus
Greatly to the R&D intensity for heating the smoking article that do not burn.However, current low temperature does not burn, smoking article is mostly concern consumer
Mouthfeel demand and suction organoleptic quality, and cannot be considered in terms of reduces damage to consumer's health.Therefore, it needs a kind of low
Temperature does not burn smoking article to meet the mouthfeel demand of consumer, suction experience, meanwhile, tobacco product is reduced to consumer's throat
Stimulation.
Summary of the invention
The technical problems to be solved by the present invention are: low temperature how to be made not burn smoking article in the premise for guaranteeing mouthfeel
Under be provided simultaneously with adjust human respiratory function the effect of.
In order to solve the above-mentioned technical problem, the present invention proposes following technical scheme:
In a first aspect, the present invention proposes a kind of essence of smoking article that do not burn suitable for low temperature, including with cough-relieving
Phlegm functional component, it is described to have relieving cough and reducing sputum functional component for Blumea oil, daurian rhododendron oil, oil of negundo chastetree, α-asarone, Mang ox
Ketone, cymol, orthocoll, acetylcysteine, isofraxidin, aesculetin, Ligustilide, stachydrine,
Ligustrazine, Imperatorin, Isomperatorin, praeruptorin A, Praeruptorin B, Praeruptorin C, hygrine, red Gu
At least one of beans alkali.
Further technical solution is for it, includes following components: 1-70 parts of smoke agent, tobacco extract 0- based on 100 parts
50 parts, 0.1-5 parts of flavouring essence for tobacco, with relieving cough and reducing sputum functional component 0.00001-30 parts, have anti-inflammation and sterilization functional component
0.00001-30 parts, surplus is water.
Further technical solution is for it, described to have antiphlogistic antibacterial functional component for Herba Houttuyniae oil, wintergreen, cortex cinnamomi
Aldehyde, Thymol, eugenol, borneol, 1,8- Cineole, certain herbaceous plants with big flowers acyl acetaldehyde, Paeonol, Bronyl acetate, Hinokitiol, frutus cnidii
At least one of element, erythricine, allicin, dephnetin, dendrobine.
Further technical solution is for it, and the boiling point with relieving cough and reducing sputum functional component is described to have less than 500 DEG C
The boiling point of antiphlogistic antibacterial functional component is less than 500 DEG C.
Further technical solution is for it, the smoke agent be propylene glycol, glycerol, antierythrite, in D-sorbite extremely
Few one kind.
Further technical solution is for it, the tobacco extract, which is tobacco leaf and extracting solution, to be extracted in soak at room temperature, filtering,
After concentration, concentrate is refined through molecular distillation again and is obtained.
Further technical solution is for it, the flavouring essence for tobacco be perillaldehyde, perillartine, linalool, lactic acid, malic acid,
Alpha-Methyl irisone, linalyl cinnamate, geraniol, at least two in citronellal.
Second aspect, the present invention propose that a kind of low temperature that is suitable for as described in relation to the first aspect does not burn the essence of smoking article
Preparation method: each component is mixed in proportion, is sufficiently dissolved, the filtering of 80-120 mesh obtains and described is suitable for low temperature not
The essence of burning fuming product.
The third aspect, the present invention propose that a kind of low temperature that is suitable for as described in relation to the first aspect does not burn the essence of smoking article
Application, do not burnt in the cigarette core material of smoking article applied to low temperature, preparation process is as follows:
The essence of the smoking article that do not burn suitable for low temperature is added to perfume base carrier, is laminated, solid
Particle or pellet are to get cigarette core material.
Further technical solution is for it, and the perfume base carrier is thin slice, bennet, porous material particle, silica gel, macropore tree
At least one of rouge, C18 reversed material, ceramic particle, microcrystalline cellulose, starch, dextrin, CMC, CMC-Na.
The present invention compared with the prior art, has the advantages that
(1) it is added in the essence that low temperature does not burn smoking article with relieving cough and reducing sputum functional component, can be used for adjusting
There is relieving cough and reducing sputum functional component can be volatized into flue gas, play under conventional atomization temperature for human respiratory function
Flavouring, the effect for promoting mouthfeel improve suction comfort and pleasant feeling；It is with relieving cough and reducing sputum effect simultaneously, into flue gas
In be absorbed by the body, human respiratory function can be adjusted to a certain extent；
(2) low temperature proposed by the present invention do not burn the essence of smoking article preparation method it is simple, it is easy to accomplish it is extensive
Industrialized production has very strong practicability；
(3) present invention adds low temperature in cigarette core material and does not burn the essence of smoking article, and the heating produced is non-ignitable
Smoking article is burnt, the mouthfeel and suction organoleptic quality of consumer had both been met, while there is relieving cough and reducing sputum effect, in certain journey
Human respiratory function can be adjusted on degree.
Specific embodiment
To explain the technical content, the achieved purpose and the effect of the present invention in detail, it is explained in detail below in conjunction with embodiment.
The embodiment of the present invention proposes a kind of essence of smoking article that do not burn suitable for low temperature, including with relieving cough and reducing sputum function
Imitate ingredient, described to have relieving cough and reducing sputum functional component be Blumea oil, daurian rhododendron oil, oil of negundo chastetree, α-asarone, Mang ox ketone, p-
P-cymene, orthocoll, acetylcysteine, isofraxidin, aesculetin, Ligustilide, stachydrine, Rhizoma Chuanxiong
Piperazine, Imperatorin, Isomperatorin, praeruptorin A, Praeruptorin B, Praeruptorin C, hygrine, Cuscohygrine
At least one of.Wherein: Blumea oil used has effects that cough-relieving apophlegmatic, is mainly used for bronchial asthma, chronic bronchial
Scorching and cough phlegm treatment.Its characteristic component includes: 1,8- Cineole, 4- terpinenol, borneol, camphor, firpene, down alkene, pine
Oleyl alcohol, β-carypohyllene, absinthol etc..Oil of negundo chastetree used equally has effects that eliminating the phlegm, cough-relieving, relievings asthma, and it is slow to be mainly used for treatment
Property bronchitis.Its characteristic component includes: β-cloves alkene, beta-elemene etc..Daurian rhododendron oil used equally have cough-relieving, eliminating the phlegm it
Effect.It is usually used in acute and chronic bronchitis treatment.Its characteristic component includes: Mang ox ketone, Bronyl acetate, β-carypohyllene
Deng.
The present embodiment is added to relieving cough and reducing sputum functional component in the essence that low temperature does not burn smoking article, can be used for
Human respiratory function is adjusted, under conventional atomization temperature, there is relieving cough and reducing sputum functional component can be volatized into flue gas,
Play the role of flavouring, promote mouthfeel, improves suction comfort and pleasant feeling；It enters with relieving cough and reducing sputum effect simultaneously
It is absorbed by the body in flue gas, human respiratory function can be adjusted to a certain extent.
The embodiment of the present invention also proposes a kind of essence of smoking article that do not burn suitable for low temperature, based on 100 parts, comprising with
Lower component: 1-70 parts of smoke agent, 0.1-5 parts of flavouring essence for tobacco, has relieving cough and reducing sputum functional component at 0-50 parts of tobacco extract
0.00001-30 parts, have 0.00001-30 parts of anti-inflammation and sterilization functional component, surplus is water.
In specific implementation, it is described have antiphlogistic antibacterial functional component be Herba Houttuyniae oil, wintergreen, cinnamic acid, Thymol,
Eugenol, borneol, 1,8- Cineole, certain herbaceous plants with big flowers acyl acetaldehyde, Paeonol, Bronyl acetate, Hinokitiol, Osthole, erythricine, garlic
At least one of element, dephnetin, dendrobine.Wherein: certain herbaceous plants with big flowers acyl acetaldehyde, Paeonol, Bronyl acetate, Hinokitiol, Osthole,
What erythricine, allicin, dephnetin, the effective component that dendrobine is some drugs and lot of documents were reported has antiphlogistic antibacterial raw
The active ingredient of object.Certain herbaceous plants with big flowers acyl acetaldehyde is Herba Houttuyniae volatile oil effective component, has effects that clearing heat, detoxicating, dispelling dampness.For lung abscess,
Phlegm-heat cough, leukorrhea, urinary tract infections etc..Paeonol has the effects that calmness, antibacterial, anti-inflammatory, anti-oxidant, blood pressure lowering, in daily use chemicals
Aspect, Paeonol can inhibit intracellular O2- free radical to generate, can make skin brightening, fossil pigments Reduction fading in skin disappears
Siltization spot；There is preferable treatment and health-care effect to color spot, courbature, pruitus, psoriasis, zona, eczema.This
Outside, there is preferable effect in toothpaste, gargle, tooth powder, toothache drops.Other several ingredients also have a large amount of document report to have
Preferable antiphlogistic antibacterial activity.The natural activity monomeric small molecule ingredient for having effects that antiphlogistic antibacterial can be commodity monomers chemical combination
Object or natural volatile oil and extract containing the monomeric compound, as Herba Houttuyniae volatile oil contains certain herbaceous plants with big flowers acyl acetaldehyde.
The present embodiment is added to antiphlogistic antibacterial functional component in the essence that low temperature does not burn smoking article, can be used for
Human respiratory function is adjusted, under conventional atomization temperature, there is antiphlogistic antibacterial functional component can be volatized into flue gas,
Play the role of flavouring, promote mouthfeel, improves suction comfort and pleasant feeling；It has effects that antiphlogistic antibacterial simultaneously, enters
It is absorbed by the body in flue gas, human respiratory function can be adjusted to a certain extent.
In specific implementation, the boiling point with relieving cough and reducing sputum functional component is described to have antiphlogistic antibacterial function less than 500 DEG C
The boiling point of ingredient is imitated less than 500 DEG C.It can be volatized into flue gas under conventional atomization temperature, to be sucked by consumer.
In specific implementation, the smoke agent is at least one of propylene glycol, glycerol, antierythrite, D-sorbite.
In another embodiment, the smoke agent propylene glycol and/or glycerol.
In other embodiments, tobacco extract obtains in the following manner: taking tobacco leaf, it is powdered to be crushed to 50-100 mesh
Extracting solution is added in solid, is 1:5-10 extraction by solid-to-liquid ratio, and soak at room temperature extracts 6-12 hours, and filtrate, 50-70 are collected in filtering
Concentration and recovery solvent is to state anhydrous and without ethyl alcohol at a temperature of DEG C.It is enterprising in molecular distillation equipment by above-mentioned gained concentrate
Row isolates and purifies purification, collects 300 DEG C of fractions below, obtains tobacco extract.
For example, in one embodiment, tobacco extract obtains in the following manner: taking tobacco leaf, it is powdered to be crushed to 100 mesh
Extracting solution is added in solid, is 1:10 extraction by solid-to-liquid ratio, and soak at room temperature extracts 12 hours, and filtrate, 50 DEG C of temperature are collected in filtering
Lower concentration and recovery solvent is to state anhydrous and without ethyl alcohol.By above-mentioned gained concentrate, separated on molecular distillation equipment
Purifying purification, collects 300 DEG C of fractions below, obtains tobacco extract.
In another embodiment, tobacco extract obtains in the following manner: taking tobacco leaf, it is powdered solid to be crushed to 50 mesh
Extracting solution is added in body, is 1:5 extraction by solid-to-liquid ratio, and soak at room temperature extracts 6 hours, filtering, collection filtrate, dense at a temperature of 70 DEG C
Contracting recycling design is to state anhydrous and without ethyl alcohol.By above-mentioned gained concentrate, isolated and purified on molecular distillation equipment
Purification collects 300 DEG C of fractions below, obtains tobacco extract.
In above embodiments, extracting solution is ethyl alcohol: propylene glycol: water (4:3:3) is obtained by mixing, and the tobacco leaf is Yunnan tobacco
Pipe tobacco, Zimbabwe's tobacco leaf pipe tobacco or Brazilian tobacco leaf pipe tobacco.
In specific implementation, the flavouring essence for tobacco is perillaldehyde, perillartine, linalool, lactic acid, malic acid, Alpha-Methyl purple sieve
Blue ketone, linalyl cinnamate, geraniol, at least two in citronellal.
The embodiment of the present invention also proposes a kind of application of the essence of smoking article that do not burn suitable for low temperature, and described is applicable in
In low temperature do not burn smoking article flavor application in the cigarette core material that low temperature does not burn smoking article, the preparation of cigarette core material
Process is as follows:
The essence of the smoking article that do not burn suitable for low temperature is added to perfume base carrier, routinely paper process or
Rolling process is laminated, solid particle or pellet are to get cigarette core material.Cigarette core material is rolled into tobacco rod, is placed in low temperature
Not in burning heater, i.e., for consumer's suction.
In specific implementation, the perfume base carrier is thin slice, bennet, porous material particle, silica gel, macroreticular resin, C18 reverse phase
At least one of material, ceramic particle, microcrystalline cellulose, starch, dextrin, CMC, CMC-Na.
Several the following are the production of different embodiments specific are not burnt the essence of smoking article suitable for low temperature.
Embodiment 1
One kind being suitable for low temperature and not burning smoking article essence, including following component (in terms of 100 parts):
40 parts of propylene glycol, 10 parts of glycerol, 10 parts of tobacco extract, 1 part of flavouring essence for tobacco, 0.04 part of α-asarone, oil of negundo chastetree
0.5 part, 0.5 part of daurian rhododendron oil, 1 part of Herba Houttuyniae oil, 0.1 part of borneol, surplus is water.Wherein, flavouring essence for tobacco be 1 part of perillaldehyde,
1.5 parts of perillartine, 0.5 part of linalool, 2 parts of lactic acid, 2 parts of malic acid, 0.5 part of Alpha-Methyl irisone, linalyl cinnamate 2
Part, 0.5 part of geraniol, 1 part of citronellal mixture.
Mentioned component is mixed in proportion, sufficiently dissolves, after 100 mesh filter-cloth filterings, obtains suitable for low temperature not
Burning fuming product essence.
Above-mentioned essence is added in perfume base carrier, prepares reconstituted tobacoo, or system according to conventional paper process or rolling process
At solid particle and pellet to get cigarette core material, then tobacco rod is rolled into, is placed in low temperature and is not taken out in burning heater
It inhales.
Embodiment 2
One kind being suitable for low temperature and not burning smoking article essence, including following component (in terms of 100 parts):
30 parts of propylene glycol, 20 parts of glycerol, 20 parts of tobacco extract, 1 part of flavouring essence for tobacco, 0.5 part of Blumea oil, oil of negundo chastetree 0.5
Part, 0.5 part of daurian rhododendron oil, 1 part of Herba Houttuyniae oil, 0.1 part of Paeonol, 0.1 part of 1, 8-Cineole, 0.1 part of Bronyl acetate, rough gentian
0.1 part of alkali, surplus is water.Wherein, flavouring essence for tobacco is 2 parts of perillaldehyde, 2 parts of perillartine, 1 part of linalool, 2 parts of malic acid, cortex cinnamomi
Sour 2 parts of virtue camphor tree ester, 1 part of geraniol of mixture.
The components in certain proportion mixed dissolution is obtained into the hair that do not burn suitable for low temperature after 80 mesh filter-cloth filterings
Tobacco product essence.
It is to prepare reconstituted tobacoo according to conventional paper process or rolling process in thin slice that above-mentioned essence, which is added to perfume base carrier,
Or solid particle and pellet is made to get cigarette core material, then roll into tobacco rod, low temperature is placed in not in burning heater
It is aspirated.
Embodiment 3
A kind of essence for the smoking article that do not burn suitable for low temperature, including following component (in terms of 100 parts):
30 parts of propylene glycol, 10 parts of glycerol, 30 parts of tobacco extract, 1 part of flavouring essence for tobacco, 0.5 part of Blumea oil, oil of negundo chastetree 0.5
Part, 0.5 part of daurian rhododendron oil, 1 part of Herba Houttuyniae oil, 0.1 part of Paeonol, 0.1 part of 1, 8-Cineole, 0.1 part of Bronyl acetate, rough gentian
0.1 part of alkali, 1 part of borneol, 0.2 part of α-asarone, surplus is water.Wherein flavouring essence for tobacco is 1 part of perillaldehyde, 2 parts of perillartine, fragrant camphor tree
1 part of alcohol, 2 parts of malic acid, 3 parts of linalyl cinnamate, 1 part of geraniol mixture.
The components in certain proportion mixed dissolution is obtained into the hair that do not burn suitable for low temperature after 120 mesh filter-cloth filterings
Tobacco product essence.
Above-mentioned essence is added in bennet, prepares reconstituted tobacoo according to conventional paper process or rolling process, or is made solid
Body particle and pellet are to get cigarette core material, then roll into tobacco rod, are placed in low temperature and are not aspirated in burning heater.
Embodiment 4
A kind of essence for the smoking article that do not burn suitable for low temperature, including following component (in terms of 100 parts):
30 parts of propylene glycol, 10 parts of glycerol, 20 parts of antierythrite, 10 parts of tobacco extract, 2 parts of flavouring essence for tobacco, Blumea oil 0.5
Part, 0.5 part of oil of negundo chastetree, 0.5 part of daurian rhododendron oil, 1 part of Herba Houttuyniae oil, 0.1 part of Paeonol, 0.1 part of 1, 8-Cineole, acetic acid borneol
0.1 part of ester, 0.1 part of erythricine, 1 part of borneol, 0.2 part of α-asarone, surplus is water.Wherein flavouring essence for tobacco is 1 part of perillaldehyde, purple
The mixing of 1 part of Su Ting, 1 part of linalool, 2 parts of malic acid, 3 parts of linalyl cinnamate, 1 part of geraniol, 1 part of Alpha-Methyl irisone
Object.
The components in certain proportion mixed dissolution is obtained into the hair that do not burn suitable for low temperature after 100 mesh filter-cloth filterings
Tobacco product essence.
It is to prepare cigarette according to conventional paper process or rolling process in C18 reversed material that above-mentioned essence, which is added to perfume base carrier,
Careless thin slice, or solid particle and pellet is made to get cigarette core material, then roll into tobacco rod, be placed in low temperature do not burn plus
It is aspirated in thermal.
Embodiment 5
A kind of essence for the smoking article that do not burn suitable for low temperature, including following component (in terms of 100 parts):
30 parts of smoke agent, 4 parts of flavouring essence for tobacco, has 0.1 part of relieving cough and reducing sputum functional component, has 40 parts of tobacco extract
0.001 part of anti-inflammation and sterilization functional component, surplus is water.
Wherein, smoke agent is obtained by mixing by propylene glycol, glycerol and D-sorbite by 2:1:1；Flavouring essence for tobacco by perillaldehyde,
Perillartine, linalool, lactic acid, malic acid, Alpha-Methyl irisone, linalyl cinnamate are obtained by mixing by 1:1:1:1:1:1:1；
It is that Herba Houttuyniae oil, wintergreen, cinnamic acid, Thymol, eugenol, borneol mix in any proportion with antiphlogistic antibacterial functional component
It closes and obtains；It is Blumea oil, daurian rhododendron oil, oil of negundo chastetree, α-asarone, Mang ox ketone, p- poly- umbrella with relieving cough and reducing sputum functional component
Florigen is obtained by mixing in any proportion.
By mentioned component, mixed dissolution obtains the hair that do not burn suitable for low temperature after 100 mesh filter-cloth filterings in proportion
Tobacco product essence.
It is to prepare cigarette according to conventional paper process or rolling process in C18 reversed material that above-mentioned essence, which is added to perfume base carrier,
Careless thin slice, or solid particle and pellet is made to get cigarette core material, then roll into tobacco rod, be placed in low temperature do not burn plus
It is aspirated in thermal.
Embodiment 6
A kind of essence for the smoking article that do not burn suitable for low temperature, including following component (in terms of 100 parts):
10 parts of smoke agent, 5 parts of tobacco extract, 5 parts of flavouring essence for tobacco, with 15 parts of relieving cough and reducing sputum functional component, have disappear
8 parts of scorching biocidal efficacies ingredient, surplus is water.
Wherein, smoke agent is obtained by mixing by propylene glycol, glycerol, antierythrite and D-sorbite by 2:1:1:1；Cigarette is fragrant
Essence is obtained by mixing in any proportion by perillartine, linalool, lactic acid, malic acid, geraniol, citronellal；With antiphlogistic antibacterial function
Effect ingredient is certain herbaceous plants with big flowers acyl acetaldehyde, Paeonol, Bronyl acetate, Hinokitiol, Osthole, erythricine, allicin, dephnetin, dendrobium nobile
Alkali is obtained by mixing in any proportion；It is Blumea oil, daurian rhododendron oil, oil of negundo chastetree, α-asarone, Mang with relieving cough and reducing sputum functional component
Ox ketone, cymol, orthocoll, acetylcysteine, isofraxidin, aesculetin, Ligustilide, water
Soviet Union's alkali, is obtained by mixing ligustrazine in any proportion.
By mentioned component, mixed dissolution obtains the hair that do not burn suitable for low temperature after 100 mesh filter-cloth filterings in proportion
Tobacco product essence.
Above-mentioned essence is added in perfume base carrier, prepares reconstituted tobacoo, or system according to conventional paper process or rolling process
At solid particle and pellet to get cigarette core material, then tobacco rod is rolled into, is placed in low temperature and is not taken out in burning heater
It inhales.
Embodiment 7
A kind of essence for the smoking article that do not burn suitable for low temperature, including following component (in terms of 100 parts):
70 parts of smoke agent, 3 parts of flavouring essence for tobacco, has 0.0001 part of relieving cough and reducing sputum functional component, tool at 1 part of tobacco extract
There are 2 parts of anti-inflammation and sterilization functional component, surplus is water.
Wherein, smoke agent is obtained by mixing in any proportion by propylene glycol, glycerol；Flavouring essence for tobacco is by perillartine, linalool, apple
Tartaric acid, geraniol, citronellal are obtained by mixing in any proportion；It is certain herbaceous plants with big flowers acyl acetaldehyde, Paeonol, second with antiphlogistic antibacterial functional component
Sour borneol acetate is obtained by mixing in any proportion；It is Blumea oil, daurian rhododendron oil, oil of negundo chastetree by any with relieving cough and reducing sputum functional component
Ratio is obtained by mixing.
By mentioned component, mixed dissolution obtains the hair that do not burn suitable for low temperature after 100 mesh filter-cloth filterings in proportion
Tobacco product essence.
Above-mentioned essence is added in perfume base carrier, prepares reconstituted tobacoo, or system according to conventional paper process or rolling process
At solid particle and pellet to get cigarette core material, then tobacco rod is rolled into, is placed in low temperature and is not taken out in burning heater
It inhales.
Embodiment 8
A kind of essence for the smoking article that do not burn suitable for low temperature, including following component (in terms of 100 parts):
5 parts of smoke agent, 1 part of tobacco extract, 0.5 part of flavouring essence for tobacco, with 20 parts of relieving cough and reducing sputum functional component, have disappear
30 parts of scorching biocidal efficacies ingredient, surplus is water.
Wherein, smoke agent is obtained by mixing in any proportion by propylene glycol, glycerol；Flavouring essence for tobacco is by perillartine, linalool, apple
Tartaric acid, geraniol, citronellal are obtained by mixing in any proportion；It is certain herbaceous plants with big flowers acyl acetaldehyde, Paeonol, second with antiphlogistic antibacterial functional component
Sour borneol acetate is obtained by mixing in any proportion；It is Blumea oil, daurian rhododendron oil, oil of negundo chastetree by any with relieving cough and reducing sputum functional component
Ratio is obtained by mixing.
By mentioned component, mixed dissolution obtains the hair that do not burn suitable for low temperature after 100 mesh filter-cloth filterings in proportion
Tobacco product essence.
Above-mentioned essence is added in perfume base carrier, prepares reconstituted tobacoo, or system according to conventional paper process or rolling process
At solid particle and pellet to get cigarette core material, then tobacco rod is rolled into, is placed in low temperature and is not taken out in burning heater
It inhales.
Active constituent flue gas shift experiment:
Using Conventional cryogenic not combustion products smoking set, tobacco rod made from embodiment 1-3 is added thereto, is smoked in improvement
It is aspirated on machine, collects smoke's total particulate matter with cambridge filter, analyze its ingredient using GC-MS, the results are shown in Table 1.
1 active constituent flue gas shift experiment result of table
The results show that the embodiment of the present invention is not burnt the essence of smoking article suitable for low temperature using being made, what is contained is small
Molecular activity monomer (with relieving cough and reducing sputum functional component, having antiphlogistic antibacterial functional component) can be measured, explanation by GC-MS
These small molecule active monomers can be transferred in smoke's total particulate matter, i.e. these functional components energy under conventional atomization temperature
It is enough volatized into flue gas, and then is absorbed by the body.
Sensory quality assessment:
(1) it chooses low temperature prepared by the embodiment of the present invention 1,2,3 and does not burn smoking article as sample, have not add
Relieving cough and reducing sputum functional component, the composition with antiphlogistic antibacterial functional component prepare low temperature and do not burn smoking article as a comparison
Sample.
(2) sensory quality assessment standard:
6 assessment items of whole installation, comprising: aroma quality, perfume quantity, sweet sense, irritation, miscellaneous gas, pleasant impression.Each comment
The maximum scale of valence project is 9 points, and for each assessment item with 1 point for scoring unit, specific evaluation criterion is shown in Table 2.
2 electronic cigarette sensory quality assessment standard of table
| Score value | Aroma quality | Perfume quantity | Sweet sense | Irritation | Miscellaneous gas | Pleasant impression |
| 9 | Very well | It is sufficient | It is very light | Very little | It is very light | Very well |
| 8 | It is good | Foot | It is light | It is small | Gently | It is good |
| 7 | Preferably | It is relatively sufficient | It is thin | It is smaller | It is relatively light | Preferably |
| 6 | It is slightly good | It is slightly sufficient | It is slightly weaker | It is slightly smaller | It is slightly light | It is slightly good |
| 5 | In | In | In | In | In | In |
| 4 | It is slightly worse | Slightly | It is slightly dense | It is slightly larger | It is slightly heavy | It is slightly worse |
| 3 | It is poor | It is thin | It is denseer | It is larger | It is heavier | It is poor |
| 2 | Difference | It is light | It is dense | Greatly | Weight | Difference |
| 1 | It is very poor | It is very light | It is dense | It is very big | It is very heavy | It is very poor |
(3) evaluation method: to smokeing panel test, technical specialist provides sample and sensory quality assessment standard scale, by table requirement to each
Item index is smoked panel test.
(4) result counts: the smoking result of all technical specialists that smoke panel test is effective, and the individual event for the expert that respectively smokes panel test is smoked panel test knot
Fruit seeks arithmetic mean of instantaneous value, as a result retains to 1 decimal, and sums it up to the arithmetic mean of instantaneous value of each individual event, obtains total score, the results are shown in Table
3。
3 sensory quality assessment result of table
| Score value | Aroma quality | Perfume quantity | Sweet sense | Irritation | Miscellaneous gas | Pleasant impression | Total score |
| Embodiment 1 | 7.5 | 7.1 | 7.5 | 7.4 | 7.2 | 7.3 | 44.0 |
| Embodiment 2 | 7.6 | 7.4 | 7.2 | 7.4 | 7.4 | 7.4 | 44.4 |
| Embodiment 3 | 7.3 | 7.5 | 7.2 | 7.4 | 7.3 | 7.3 | 44.0 |
| Comparative example | 6.5 | 7.0 | 6.8 | 7.0 | 7.2 | 7.0 | 41.5 |
As shown in Table 3, the low temperature provided in an embodiment of the present invention low temperature made from the essence of smoking article that do not burn or not
Smoking article, and is not added with the low temperature that obtains with relieving cough and reducing sputum functional component, the essence with antiphlogistic antibacterial functional component not
Burning fuming product is compared, with mouthfeel is more comfortable, aroma quality is more pleasant, blandness, suction quality are with good consumption body
It tests.
The present invention is by adding some low boiling points and having relieving cough and reducing sputum active skull cap components small molecule, these small molecules
There is good fragrance and taste simultaneously, flavouring can be played and promote mouthfeel, then be aided with suitable fragrance taste, perfume (or spice) is made
Gas is abundant, comfortable taste, suction is pleasant, satisfaction is strong, while having a degree of relieving cough and reducing sputum function.Efficacy data is shown in Table
4。
4 efficacy data of table
| Smoker | Pathologic condition | Suction time | Effect situation |
| Zhao (male, 26 years old) | Abundant expectoration, cough | 3.5 all | It improves, improves |
| Temperature certain (male, 28 years old) | Abundant expectoration, cough | 3.5 all | It improves, improves |
| Mr. Wang (male, 30 years old) | Abundant expectoration, cough | 4 weeks | It improves, improves |
| Journey (male, 40 years old) | Abundant expectoration, cough | 3.5 all | It improves, improves |
| Hair certain (male, 25 years old) | Abundant expectoration, cough | 4 weeks | It improves, improves |
The present invention adds low temperature in cigarette core material and does not burn the essence of smoking article, and the heating produced is not burnt hair
Tobacco product, had both met the mouthfeel and suction organoleptic quality of consumer, while having relieving cough and reducing sputum effect, to a certain extent
Human respiratory function can be adjusted.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (10)
1. a kind of essence for the smoking article that do not burn suitable for low temperature, which is characterized in that including with relieving cough and reducing sputum functional component,
It is described to have relieving cough and reducing sputum functional component for Blumea oil, daurian rhododendron oil, oil of negundo chastetree, α-asarone, Mang ox ketone, p- poly- umbrella flower
Element, orthocoll, acetylcysteine, isofraxidin, aesculetin, Ligustilide, stachydrine, ligustrazine, Ou Qian
Hu Su, Isomperatorin, praeruptorin A, Praeruptorin B, Praeruptorin C, hygrine, in Cuscohygrine extremely
Few one kind.
2. not burning the essence of smoking article suitable for low temperature as described in claim 1, which is characterized in that based on 100 parts, packet
Containing following components: 1-70 parts of smoke agent, 0.1-5 parts of flavouring essence for tobacco, has relieving cough and reducing sputum functional component at 0-50 parts of tobacco extract
0.00001-30 parts, have 0.00001-30 parts of anti-inflammation and sterilization functional component, surplus is water.
3. not burning the essence of smoking article suitable for low temperature as described in claim 1, which is characterized in that described that there is anti-inflammatory
Antibiotic effect ingredient is Herba Houttuyniae oil, wintergreen, cinnamic acid, Thymol, eugenol, borneol, 1,8- Cineole, certain herbaceous plants with big flowers acyl second
At least one of aldehyde, Paeonol, Bronyl acetate, Hinokitiol, Osthole, erythricine, allicin, dephnetin, dendrobine.
4. not burning the essence of smoking article suitable for low temperature as claimed in claim 3, which is characterized in that described that there is cough-relieving
The boiling point of resolving sputum functional component is less than 500 DEG C, and the boiling point with antiphlogistic antibacterial functional component is less than 500 DEG C.
5. not burning the essence of smoking article suitable for low temperature as described in claim 1, which is characterized in that the smoke agent is
At least one of propylene glycol, glycerol, antierythrite, D-sorbite.
6. not burning the essence of smoking article suitable for low temperature as described in claim 1, which is characterized in that the tobacco is extracted
Object is tobacco leaf and extracting solution after soak at room temperature extracts, filters, is concentrated, and concentrate is refined through molecular distillation again and obtained.
7. not burning the essence of smoking article suitable for low temperature as described in claim 1, which is characterized in that the flavouring essence for tobacco
For perillaldehyde, perillartine, linalool, lactic acid, malic acid, Alpha-Methyl irisone, linalyl cinnamate, geraniol, citronellal
In at least two.
8. it is a kind of as claim 1-7 it is described in any item suitable for low temperature do not burn smoking article essence preparation method,
It is characterized in that, in proportion mix each component, sufficiently dissolve, the filtering of 80-120 mesh, obtains and described be suitable for low temperature not
The essence of burning fuming product.
9. it is a kind of as claim 1-7 it is described in any item suitable for low temperature do not burn smoking article essence application, it is special
Sign is that in the cigarette core material for the smoking article that do not burn applied to low temperature, preparation process is as follows:
The essence of the smoking article that do not burn suitable for low temperature is added to perfume base carrier, is laminated, solid particle
Or pellet is to get cigarette core material.
10. as claimed in claim 9 suitable for low temperature do not burn smoking article essence application, which is characterized in that it is described
Perfume base carrier is thin slice, bennet, porous material particle, silica gel, macroreticular resin, C18 reversed material, ceramic particle, microcrystalline cellulose
At least one of element, starch, dextrin, CMC, CMC-Na.
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| CN111165871A (en) * | 2020-01-17 | 2020-05-19 | 湖南中烟工业有限责任公司 | Low-harm cigarette subjected to cigarette enhancement treatment |
| CN113331463A (en) * | 2020-03-03 | 2021-09-03 | 常州丰源生物科技有限公司 | Carrier for aerosol products and method for producing same |
| CN114098141A (en) * | 2021-11-28 | 2022-03-01 | 深圳市真味生物科技有限公司 | Electronic atomized liquid containing borneol plant components and preparation method thereof |
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| CN114098141B (en) * | 2021-11-28 | 2023-02-10 | 深圳市真味生物科技有限公司 | Electronic atomized liquid containing borneol plant components and preparation method thereof |
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Application publication date: 20190607 |