CN105581374A - Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes - Google Patents
Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes Download PDFInfo
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- CN105581374A CN105581374A CN201610154707.7A CN201610154707A CN105581374A CN 105581374 A CN105581374 A CN 105581374A CN 201610154707 A CN201610154707 A CN 201610154707A CN 105581374 A CN105581374 A CN 105581374A
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- pelargonium
- pelargonium graveolens
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a glycerol triacetate extract of pelargonium graveolens L'Herit. and application of the extract in cigarettes. A method comprises the steps that pelargonium graveolens L'Herit powder obtained by smashing and sieving dried flowers of pelargonium graveolens L'Herit serves as the raw material, glycerol triacetate serves as an extracting agent, extraction is conducted in a heating reflux mode, extraction is conducted through an ultrasonic wave, and the glycerol triacetate extract of pelargonium graveolens L'Herit. is prepared. A pelargonium graveolens L'Herit. extract is prepared into a solution with the concentration of 0.05%-0.20% by taking glycerol triacetate as solvent, the solution is evenly sprayed to filter stick tows according to the proportion of 7%-8% by weight of cellulose acetate tows, a cigarette filter stick is prepared, and a cigarette containing the filter stick with the effective ingredient of pelargonium graveolens L'Herit. is prepared through the conventional cigarette tipping procedure. The extract can increase richness of cigarette fragrance, enhance diffusiveness, eliminate aftertaste and obviously promote comfort of smoking. According to the glycerol triacetate extract of pelargonium graveolens L'Herit. and the application of the extract in the cigarettes, the operability and standardability are high, the raw materials are easy to obtain, the cost is low, the production technology is simple, industrial production is convenient to achieve, and a good application prospect is achieved.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of Pelargonium roseum triacetyl glycerineExtract. Meanwhile, the invention still further relates to described Pelargonium roseum triacetyl glycerine extract at cigaretteIn application.
Background technology
Pelargonium roseum has another name called Mozzie buster, is MangNiu Er seedling section Pelargonium perennial herb. Spiceleaf IndiaStem, leaf and the Huadu of certain herbaceous plants with big flowers, containing volatile aroma, can be used to refine essence or spices. Rose pelargonium essential oilFormed by more than 30 kinds of terpenoids and derivative thereof, its main component be geraniol, citronellol,Linalool, citronellyl formate, formic acid spiceleaf grass ester and menthones, above-mentioned flavor component can be given cigaretteThe notes such as delicate fragrance, fragrant and sweet, flue-cured tobacco is fragrant. For this reason, the essential oil Chang Zuowei tobacco aromatics using of Pelargonium roseum addsIn cigarette, there is the side such as exquisiteness and mildness that enriches cigarette cigarette perfume (or spice), lifting musical tone, promotes flue gasEffect of face.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette progressively obtainsReduce. But cigarette tar content reduction also can bring cigarette satisfaction and natural cigarette perfume (or spice) more or less to damage to some extentLose, therefore, each tobacco productive corporation will promote the natural fragrance of cigarette satisfaction and tobacco gradually as researchDeveloping focus task. Can effectively improve cigarette smoking quality by cigarette tobacco leaf formulation flavoring and casing,But this mode finally need to be burnt and be brought the product of more complicated, R&D worker passes through at filter stickIn add some to there is flavouring, the extract of mending the effect such as fragrant will become a kind of simple and feasible application sideFormula. R&D worker has carried out some correlative study work, and obtains certain achievement. For example a kind ofThe filtering material of cigarette filter rod and cigarette filter rod (200810219901.4), a kind of duck wheat with burnt odorApplication and the cigarette filter thereof in cigarette filter rod of cigarette filter rod (201410372333.7), moringa seeds extractRod (201310159094.2), a kind of Pelargonium roseum porous particle and the application in cigarette thereof(201310643496.X) filter stick additive etc., but described in above-mentioned patent be mainly first by extracting orAllotment additive dissolves and adds in cigarette again in triacetyl glycerine, maybe interpolation particle is passed through to increaseAdding operation is applied directly in cigarette filter rod. On the one hand, there is preparation technology in this interpolation application modeComplicated, triacetyl glycerine is limited to the solvability of additive, much to cigarette there is flavouring, mend fragrantThe extract of effect is difficult to be dissolved in triacetyl glycerine, has limited such extract in cigarette filter rodApplication. On the other hand, if be not or not carrier carries out filter stick perfuming by triacetyl glycerine, but willAdditive is applied directly in cigarette filter rod, can produce and bring larger difficulty, significantly increase production to filter stickCost, is unfavorable for applying on a large scale. For meet tobacco business at cigarette flavouring, mend aspect fragrantHow demand, adopt suitable technology, and the additive of cigarette filter stick that preparation is applicable to Production requirement will becomeFor needing the technical barrier of solution badly in this field.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide a kind of using triacetyl glycerine asPelargonium roseum extract prepared by extractant, this extract can directly add to should in triacetyl glycerineFor cigarette filter tip shaping, can effectively increase cigarette flavor rich, promote flue gas thoroughly the property sent out, promote sweetMoisture feeling, cover cigarette foreign gas, obviously promote cigarette organoleptic quality.
The Pelargonium roseum triacetyl glycerine extract that the present invention also aims to provide described is at volumeConcrete application in cigarette production.
Object of the present invention is achieved by following technical proposals.
* the percentage adopting in the present invention except as otherwise noted, is mass percent.
A kind of Pelargonium roseum triacetyl glycerine extract, makes by the method for following steps:
(1) getting fresh Pelargonium roseum stem, leaf, flower is to dry under 55～60 DEG C of conditions in temperature, pointStem, leaf, flower are not pulverized through pulverizer, crossed 20～60 mesh sieves and obtain Pelargonium roseum powder, according toThe powder of stem: the powder of leaf: the weight ratio of the powder=30:60:10 of flower mixes, for subsequent use;
(2) take 300～500g Pelargonium roseum powder and be placed in extraction flask, by solid-liquid ratio 1:8～12Ratio add glycerol triacetate for tobacco as extractant, soaking at room temperature is after 3～5 hours, 80～Under 90 DEG C of conditions, carry out refluxing extraction, 5～7 hours extraction times, to be cooled to for subsequent use after room temperature;
(3) step (2) gains are placed in to ultrasonic extractor, at 400～600W, 40kHZUnder condition, extract 40～80 minutes, remove by filter the settled solution obtaining after filter residue and be required perfume (or spice)Leaf fish pelargonium triacetyl glycerine extract.
The application of described Pelargonium roseum triacetyl glycerine extract in cigarette, is characterized in that:Taking triacetyl glycerine as solvent, described Pelargonium roseum triacetyl glycerine extract is mixed with denseDegree is 0.05～0.20% solution, is evenly sprayed onto silk in the ratio of acetate silk weight 7～8%Shu Shang, makes cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
The present invention adopt triacetyl glycerine be extractant extract Pelargonium roseum, can be to spiceleaf IndiaThe effective efficiency composition that is dissolved in triacetyl glycerine in certain herbaceous plants with big flowers fully extracts, and has avoided adopting other solventExtract the loss of effective efficiency composition while redissolving again to triacetyl glycerine; Simultaneously can be not raw to cigaretteThe security of producing has a negative impact.
2. gained Pelargonium roseum triacetyl glycerine extract can enrich cigarette flavor, effectively promotes cigaretteGas is the property sent out thoroughly, increases sweet sense, covers cigarette foreign gas, improves effect of suction quality.
3. prepared Pelargonium roseum triacetyl glycerine extract and the triacetyl glycerine ratio of dissolving each otherWider, extract is evenly distributed in filter stick tow, has solved quality that cigarette brings because of spices inequality notStable problem.
4. operability of the present invention and normative strong, raw material is easy to get, with low cost, and production technology is simple,Be convenient to realize suitability for industrialized production, have a good application prospect.
5. material used herein is food stage, has higher safety in utilization.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment,The present invention is described in further detail. Should be appreciated that specific embodiment described herein is only in order to separateRelease the present invention, be not limited to the technical solution.
Embodiment 1
Getting fresh Pelargonium roseum stem, leaf, flower is to dry under 55～60 DEG C of conditions in temperature, respectively willStem, leaf, flower are pulverized through pulverizer, cross 20 mesh sieves and obtain Pelargonium roseum powder, the powder according to stem:The powder of leaf: the weight ratio of the powder=30:60:10 of flower mixes, and takes 300g Pelargonium roseumPowder is placed in extraction flask, adds glycerol triacetate for tobacco, soaking at room temperature in the ratio of solid-liquid ratio 1:8After 3 hours, under 80 DEG C of conditions, carry out refluxing extraction, extraction time is 5 hours, naturally cools toRoom temperature, is placed in ultrasonic wave extraction equipment by the Pelargonium roseum after described refluxing extraction and triacetyl glycerineIn (400W, 40kHZ), extract 40 minutes, obtain settled solution after removing by filter filter residue, be instituteNeed Pelargonium roseum triacetyl glycerine extract.
Taking triacetyl glycerine as solvent, Pelargonium roseum triacetyl glycerine extract is mixed with to concentrationBe 0.05% solution, be evenly sprayed onto on filter stick tow in the ratio of acetate silk weight 8%,Make cigarette filter rod, make and contain Pelargonium roseum active ingredient filter stick by conventional cigarette tipping programCigarette. Analyses Methods for Sensory Evaluation Results shows: compared with the control, add above-mentioned Pelargonium roseum three triacetinsThe cigarette flavor of the ester extract thoroughly property sent out is good, and fragrance is rich to be increased to some extent, covers assorted gas, and comfortableness hasImprove.
Embodiment 2
Getting fresh Pelargonium roseum stem, leaf, flower is to dry under 55～60 DEG C of conditions in temperature, respectively willStem, leaf, flower are pulverized through pulverizer, cross 40 mesh sieves and obtain Pelargonium roseum powder, the powder according to stem:The powder of leaf: the weight ratio of the powder=30:60:10 of flower mixes, and takes 400g Pelargonium roseumPowder is placed in extraction flask, adds glycerol triacetate for tobacco as extraction in the ratio of solid-liquid ratio 1:10Agent, soaking at room temperature, after 4 hours, is carried out refluxing extraction under 85 DEG C of conditions, and extraction time is 6 hours,Naturally cool to room temperature, the Pelargonium roseum after described refluxing extraction and triacetyl glycerine are placed in ultrasonicIn ripple extraction equipment (500W, 40kHZ), extract 60 minutes, remove by filter obtain clarifying after filter residue moltenLiquid, can obtain required Pelargonium roseum triacetyl glycerine extract.
Taking triacetyl glycerine as solvent, Pelargonium roseum triacetyl glycerine extract is mixed with to concentrationBe 0.10% solution, be evenly sprayed onto on filter stick tow in the ratio of acetate silk weight 7.5%,Make cigarette filter rod, make and contain Pelargonium roseum active ingredient filter stick by conventional cigarette tipping programCigarette. Analyses Methods for Sensory Evaluation Results shows: compared with the control, add above-mentioned Pelargonium roseum three triacetinsThe rich obvious increase of cigarette flavor of ester extract, flue gas concentration increases, and sweet sense increases, flue gas thornSharp property obviously reduces, and pleasant impression is clean, clear.
Embodiment 3
Getting fresh Pelargonium roseum stem, leaf, flower is to dry under 55～60 DEG C of conditions in temperature, respectively willStem, leaf, flower are pulverized through pulverizer, cross 60 mesh sieves and obtain Pelargonium roseum powder, the powder according to stem:The powder of leaf: the weight ratio of the powder=30:60:10 of flower mixes, and takes 500g Pelargonium roseumPowder is placed in extraction flask, adds glycerol triacetate for tobacco as extraction in the ratio of solid-liquid ratio 1:12Agent, soaking at room temperature, after 5 hours, is carried out refluxing extraction under 90 DEG C of conditions, and extraction time is 7 hours,Naturally cool to room temperature, the Pelargonium roseum after described refluxing extraction and triacetyl glycerine are placed in ultrasonicIn ripple extraction equipment (600W, 40kHZ), extract 80 minutes, remove by filter obtain clarifying after filter residue moltenLiquid, can obtain required Pelargonium roseum triacetyl glycerine extract.
Taking triacetyl glycerine as solvent, Pelargonium roseum triacetyl glycerine extract is mixed with to concentrationBe 0.15% solution, be evenly sprayed onto on filter stick tow and make in the ratio of acetate silk weight 8%Become cigarette filter rod, make and contain Pelargonium roseum active ingredient filter stick by conventional cigarette tipping programCigarette. Analyses Methods for Sensory Evaluation Results shows: compared with the control, add above-mentioned Pelargonium roseum triacetyl glycerineThe submissive harmony of cigarette smoke of extract, it is rich that better pleasant impression is clean, and excitant alleviates to some extent.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all of the present inventionAny amendment of doing within spirit and principle, be equal to replacement and improvement etc., all should be included in of the present inventionWithin protection domain.
Claims (2)
1. a Pelargonium roseum triacetyl glycerine extract, makes by the method for following steps:
(1) getting fresh Pelargonium roseum stem, leaf, flower is to dry under 55～60 DEG C of conditions in temperature, pointStem, leaf, flower are not pulverized through pulverizer, crossed 20～60 mesh sieves and obtain Pelargonium roseum powder, according to stemPowder: the powder of leaf: the weight ratio of powder=30:60:10 of flower mixes, for subsequent use;
(2) take 300～500g Pelargonium roseum powder and be placed in extraction flask, by solid-liquid ratio 1:8～12Ratio add glycerol triacetate for tobacco as extractant, soaking at room temperature is after 3～5 hours, 80～Under 90 DEG C of conditions, carry out refluxing extraction, 5～7 hours extraction times, to be cooled to for subsequent use after room temperature;
(3) step (2) gains are placed in to ultrasonic extractor, at 400～600W, 40kHZUnder condition, extract 40～80 minutes, remove by filter the settled solution obtaining after filter residue and be required perfume (or spice)Leaf fish pelargonium triacetyl glycerine extract.
2. the application of Pelargonium roseum triacetyl glycerine extract claimed in claim 1 in cigarette,It is characterized in that: taking triacetyl glycerine as solvent, described Pelargonium roseum triacetyl glycerine is carriedGetting thing, to be mixed with concentration be 0.05～0.20% solution, in the ratio of acetate silk weight 7～8%Evenly be sprayed onto on tow, make cigarette filter rod, and this filter stick is applied to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610154707.7A CN105581374A (en) | 2016-03-18 | 2016-03-18 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
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| CN201610154707.7A CN105581374A (en) | 2016-03-18 | 2016-03-18 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111418892A (en) * | 2020-05-20 | 2020-07-17 | 云南如茨生物科技有限公司 | Cigarette filter stick additive and application thereof |
| CN114052283A (en) * | 2021-11-25 | 2022-02-18 | 云南中烟新材料科技有限公司 | Abelmoschus manihot bead-blasting essence and preparation method and application thereof |
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| CN103146483A (en) * | 2013-03-21 | 2013-06-12 | 红云红河烟草(集团)有限责任公司 | Pelargonium roseum extract and application of extract in cigarette |
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| CN105029700A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Plant composite glycerol triacetate extract and application thereof in cigarettes |
| CN105146709A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing pelargonium graveolens |
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2016
- 2016-03-18 CN CN201610154707.7A patent/CN105581374A/en active Pending
Patent Citations (6)
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| CN103126054A (en) * | 2013-03-21 | 2013-06-05 | 红云红河烟草(集团)有限责任公司 | Preparation method of recreating tobacco with increasing aroma function |
| CN103146483A (en) * | 2013-03-21 | 2013-06-12 | 红云红河烟草(集团)有限责任公司 | Pelargonium roseum extract and application of extract in cigarette |
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| CN105146709A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing pelargonium graveolens |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111418892A (en) * | 2020-05-20 | 2020-07-17 | 云南如茨生物科技有限公司 | Cigarette filter stick additive and application thereof |
| CN114052283A (en) * | 2021-11-25 | 2022-02-18 | 云南中烟新材料科技有限公司 | Abelmoschus manihot bead-blasting essence and preparation method and application thereof |
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Application publication date: 20160518 |
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