CN105779125A - Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes - Google Patents
Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes Download PDFInfo
- Publication number
- CN105779125A CN105779125A CN201610154709.6A CN201610154709A CN105779125A CN 105779125 A CN105779125 A CN 105779125A CN 201610154709 A CN201610154709 A CN 201610154709A CN 105779125 A CN105779125 A CN 105779125A
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- China
- Prior art keywords
- extract
- hook
- serving
- glycerol triacetate
- extracting agent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a Luculia pinceana Hook.extract with glycerol triacetate serving as an extracting agent and application of the Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent to cigarettes. The Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent is prepared from ground and sieved dried flower of Luculia pinceana Hook.with the glycerol triacetate serving as the extracting agent through heating reflux extraction and then ultrasonic extraction. The Luculia pinceana Hook.extract is prepared into a 0.03-0.06% solution with the glycerol triacetate serving as a solvent, the solution is uniformly sprayed to filter stick tows according to a proportion accounting for 7-8% of the weight of cellulose acetate tows to obtain filter sticks of the cigarettes, and then a conventional cigarette tipping process is conducted so as to obtain the cigarettes with the filter sticks containing Luculia pinceana Hook. The Luculia pinceana Hook.extract can enrich the aroma of the cigarettes and enhance volatility of smoke and is clean in aftertaste so as to improve smoking comfort obviously. The Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent and application of the Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent to the cigarettes have the advantages of high operability and standardability, easy availability to raw materials, low cost, simple production technology, capability of achieving industrial production easily and promising application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of Dian clove triacetyl glycerine and extract
Thing.Meanwhile, the invention still further relates to the application in cigarette of the described Dian clove triacetyl glycerine extract.
Background technology
Dian clove (Luculia pinciana Hook.) is Rubiaceae Dian clove platymiscium, is distributed in Himalaya
Mountain to Yunnan Province of China and Guangxi, has higher gardens, medical value.Owing to Dian clove plant type is graceful,
With luxuriant foliage and spreading branches in leafy profusion, emerald green light, the florescence is long, and titbit is intensive and in great numbers, and pattern is gorgeous and fragrant, leads at present
Will be as ornamencal flower and tree.But it also has a long history as Chinese medicine among the people.According to records: cloves
Leaf, its bitter, pungent, slightly warm in nature；Fragrance enters lung, only band blood on lung cold cough or hemoptysis or phlegm.
About the medical value of Dian clove platymiscium, " Xinhua's book on Chinese herbal medicine outline " of Wu Zheng manganese chief editor is documented:
Root has promoting blood circulation for regulating menstruation, anti-inflammatory analgetic, buck functionality.Can be used for irregular menstruation, rheumatalgia pain, fall to beat and damage
Wound, antimigraine, nervous etc.；Flowers and fruits have relieving cough and reducing sputum function, can be used for pertussis, chronic bronchitis,
Pulmonary tuberculosis；Leaf has detumescence function.
Along with smoking increasingly receives publicity with healthy problem, the tar content of Chinese-style cigarette progressively obtains
Reduce.But cigarette tar content reduction also brings along cigarette satisfaction and natural cigarette perfume (or spice) has damaged
Losing, therefore, each tobacco productive corporation gradually will promote cigarette satisfaction and tobacco nature fragrance as research
Developing focus task.Cigarette smoking quality can be effectively improved by cigarette tobacco leaf formulation flavoring and casing,
But this mode finally needs that carrying out burns brings more complicated product, R&D worker is by filter stick
Some extracts with the effect such as flavouring, benefit perfume of middle addition will become a kind of simple and feasible application side
Formula.R&D worker has carried out some correlative studys work, and obtains certain achievement.Such as a kind of
The filtering material of cigarette filter rod and cigarette filter rod (200810219901.4), a kind of duck wheat with burnt odor
The application in cigarette filter rod of cigarette filter rod (201410372333.7), moringa seeds extract and cigarette filter thereof
Rod (201310159094.2) etc., but the filter stick additive described in above-mentioned patent mainly first passes through extraction
Or allotment additive dissolves in triacetyl glycerine and adds in cigarette, maybe by interpolation particle by increasing
Attach operation to be applied directly in cigarette filter rod.On the one hand, there is preparation work in this interpolation application mode
Skill is complicated, triacetyl glycerine is limited to the solvability of additive, much has flavouring, benefit to cigarette
The extract of Xiang Gong effect is difficult to be dissolved in triacetyl glycerine, limits such extract at cigarette filter rod
In application.On the other hand, if being not that carrier carries out filter stick perfuming by triacetyl glycerine, but
Additive is applied directly in cigarette filter rod, can produce to filter stick and bring bigger difficulty, dramatically increase life
Produce cost, be unfavorable for large-scale popularization and application.For meeting tobacco business in terms of cigarette flavouring, benefit perfume
Demand, how to use suitable technology, preparation is suitable for the additive of cigarette filter stick of Production requirement will
Become this field and need the technical barrier of solution badly.
Summary of the invention
Present invention aims to the deficiencies in the prior art, it is provided that a kind of using triacetyl glycerine as
Dian clove extract prepared by extractant, this extract can be directly appended to be applied in triacetyl glycerine
Cigarette filter tip shaping, can be effectively increased that cigarette flavor is rich, the flue gas property sent out thoroughly, alleviate flue gas stimulate and
Residual, covers cigarette foreign gas, hence it is evident that promote cigarette sensory quality.
The Dian clove triacetyl glycerine extract that the present invention also aims to provide described is raw at cigarette
Concrete application in product.
The purpose of the present invention is achieved by following technical proposals.
The most except as otherwise noted, the percentage employed in the present invention is mass percent.
A kind of Dian clove triacetyl glycerine extract, is prepared by the method for following steps:
(1) taking fresh Dian clove flower to dry or dry, size-reduced machine is pulverized, and crosses 20～40 mesh sieves
Obtain Dian clove powder, standby；
(2) weigh 300～500g Dian clove powder to be placed in round-bottomed flask, by solid-liquid ratio 1:6～10
Ratio add glycerol triacetate for tobacco as extractant, soaking at room temperature 2～after 4 hours, 60～
Refluxing extraction is carried out under the conditions of 90 DEG C, extraction time 4～6 hours, standby after being cooled to room temperature；
(3) step (2) gains are placed in ultrasonic extractor, 400～600W, 40kHZ
Under the conditions of, extracting 30～60 minutes, the settled solution obtained after being filtered to remove filter residue is required Yunnan
Cloves triacetyl glycerine extract.
The application in cigarette of the described Dian clove triacetyl glycerine extract, it is characterised in that: with three
Acetoglyceride is solvent, described Dian clove triacetyl glycerine extract is configured to concentration and is
0.03～the solution of 0.06%, it is sprayed onto on tow by the ratio uniform of acetate silk weight 7～8%,
Make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the invention have the advantages that
1. the present invention uses triacetyl glycerine to be that extractant extracts Dian clove, it is possible to be dissolved in Dian clove
The effective efficiency composition of triacetyl glycerine fully extracts, it is to avoid use other solvent to extract
Redissolve again to the loss of effective efficiency composition during triacetyl glycerine；Simultaneously will not be to the safety of production of cigarettes
Property has a negative impact.
2. gained Dian clove triacetyl glycerine extract can enrich cigarette flavor, is effectively increased cigarette flower
Note is adjusted, and improves cigarette pleasant impression, improves effect of suction quality.
3. the Dian clove triacetyl glycerine extract prepared by and triacetyl glycerine ratio of dissolving each other is wider,
Extract is evenly distributed in filter stick tow, solves quality that cigarette brings because of spices inequality unstable
Problem.
Operability the most of the present invention and normative strong, raw material is easy to get, with low cost, and production technology is simple,
Facilitate implementation industrialized production, have a good application prospect.
Material the most used herein is food-grade, has higher safety in utilization.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment,
The present invention is described in further detail.Should be appreciated that specific embodiment described herein is only in order to solve
Release the present invention, be not limited to the technical solution.
Embodiment 1
Taking fresh Dian clove flower to dry, size-reduced machine is pulverized, and gained powder is crossed 20 mesh sieves, weighed 300g
Dian clove powder is placed in round-bottomed flask, adds glycerol triacetate for tobacco in the ratio of solid-liquid ratio 1:6,
After soaking at room temperature 2 hours, carrying out refluxing extraction under the conditions of 70 DEG C, extraction time is 4 hours, from
So it is cooled to room temperature, the Dian clove after described refluxing extraction and triacetyl glycerine is placed in ultrasonic wave and extracts
In equipment (400W, 40kHZ), extract 30 minutes, obtain settled solution after being filtered to remove filter residue, i.e.
For required Dian clove triacetyl glycerine extract.
With triacetyl glycerine as solvent, Dian clove triacetyl glycerine extract is configured to concentration is
The solution of 0.03%, is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, makes
Cigarette filter rod, makes the cigarette containing Dian clove active ingredient filter stick by conventional cigarette tipping program.
Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds the volume of above-mentioned Dian clove triacetyl glycerine extract
The cigarette fragrance property sent out thoroughly is good, and fragrance is rich be increased, and pleasant impression is more clean, and comfortableness is improved.
Embodiment 2
Taking fresh Dian clove flower to dry, size-reduced machine is pulverized, and gained powder is crossed 40 mesh sieves, weighed 400g
Dian clove powder is placed in round-bottomed flask, adds glycerol triacetate for tobacco in the ratio of solid-liquid ratio 1:8 and makees
For extractant, soaking at room temperature, after 3 hours, carries out refluxing extraction under the conditions of 80 DEG C, and extraction time is 5
Hour, naturally cool to room temperature, the Dian clove after described refluxing extraction and triacetyl glycerine are placed in super
In sound wave extraction equipment (500W, 40kHZ), extract 40 minutes, clarified after being filtered to remove filter residue
Solution, i.e. available required Dian clove triacetyl glycerine extract.
With triacetyl glycerine as solvent, Dian clove triacetyl glycerine extract is configured to concentration is
The solution of 0.04%, is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, system
Become cigarette filter rod, make the volume containing Dian clove active ingredient filter stick by conventional cigarette tipping program
Cigarette.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds above-mentioned Dian clove triacetyl glycerine extract
The rich obvious increase of cigarette flavor, flue gas concentration increase, miscellaneous gas is less, and flue gas excitant substantially drops
Low, pleasant impression is clean, clear.
Embodiment 3
Taking fresh Dian clove flower to dry, size-reduced machine is pulverized, and gained powder is crossed 30 mesh sieves, weighed 500g
Dian clove powder is placed in round-bottomed flask, adds glycerol triacetate for tobacco in the ratio of solid-liquid ratio 1:10 and makees
For extractant, soaking at room temperature, after 4 hours, carries out refluxing extraction under the conditions of 90 DEG C, and extraction time is
6 hours, naturally cool to room temperature, the Dian clove after described refluxing extraction and triacetyl glycerine are placed in
In ultrasonic wave extraction equipment (600W, 40kHZ), extract 50 minutes, obtain clear after being filtered to remove filter residue
Clear solution, i.e. available required Dian clove triacetyl glycerine extract.
With triacetyl glycerine as solvent, Dian clove triacetyl glycerine extract is configured to concentration is
The solution of 0.05%, is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8% and makes volume
Cigarette filter, makes the cigarette containing Dian clove active ingredient filter stick by conventional cigarette tipping program.Sense
Official's evaluation result shows: compared with the control, adds the cigarette of above-mentioned Dian clove triacetyl glycerine extract
The submissive harmony of flue gas, rich preferably, pleasant impression is clean, and excitant has alleviated.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all the present invention's
Any amendment, equivalent and the improvement etc. made within spirit and principle, should be included in the present invention's
Within protection domain.
Claims (2)
1. a Dian clove triacetyl glycerine extract, is prepared by the method for following steps:
(1) taking fresh Dian clove flower to dry or dry, size-reduced machine is pulverized, and crosses 20～40 mesh sieves
Obtain Dian clove powder, standby；
(2) weigh 300～500g Dian clove powder to be placed in round-bottomed flask, by solid-liquid ratio 1:6～10
Ratio add glycerol triacetate for tobacco as extractant, soaking at room temperature 2～after 4 hours, 60～
Refluxing extraction is carried out under the conditions of 90 DEG C, extraction time 4～6 hours, standby after being cooled to room temperature；
(3) step (2) gains are placed in ultrasonic extractor, 400～600W, 40kHZ
Under the conditions of, extracting 30～60 minutes, the settled solution obtained after being filtered to remove filter residue is required Yunnan
Cloves triacetyl glycerine extract.
2. the application in cigarette of the Dian clove triacetyl glycerine extract described in claim 1, its
It is characterised by: with triacetyl glycerine as solvent, described Dian clove triacetyl glycerine extract is joined
Make the solution that concentration is 0.03～0.06%, by acetate silk weight 7～the ratio uniform spray of 8%
It is spread across on tow, makes cigarette filter rod, and this filter stick is applied to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610154709.6A CN105779125A (en) | 2016-03-18 | 2016-03-18 | Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610154709.6A CN105779125A (en) | 2016-03-18 | 2016-03-18 | Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105779125A true CN105779125A (en) | 2016-07-20 |
Family
ID=56392899
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610154709.6A Pending CN105779125A (en) | 2016-03-18 | 2016-03-18 | Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105779125A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108179062A (en) * | 2017-12-27 | 2018-06-19 | 广东中烟工业有限责任公司 | A kind of composition containing natural extracts and its application in functionalization filter stick plasticizer is prepared |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1142338A (en) * | 1996-07-05 | 1997-02-12 | 荆树汉 | Paeonol health cigarette and production thereof |
| CN105132162A (en) * | 2015-06-17 | 2015-12-09 | 云南中烟工业有限责任公司 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
-
2016
- 2016-03-18 CN CN201610154709.6A patent/CN105779125A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1142338A (en) * | 1996-07-05 | 1997-02-12 | 荆树汉 | Paeonol health cigarette and production thereof |
| CN105132162A (en) * | 2015-06-17 | 2015-12-09 | 云南中烟工业有限责任公司 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108179062A (en) * | 2017-12-27 | 2018-06-19 | 广东中烟工业有限责任公司 | A kind of composition containing natural extracts and its application in functionalization filter stick plasticizer is prepared |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160720 |