CN102920016B - Porcini extract and preparation method and application thereof - Google Patents
Porcini extract and preparation method and application thereof Download PDFInfo
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- CN102920016B CN102920016B CN201210444734.XA CN201210444734A CN102920016B CN 102920016 B CN102920016 B CN 102920016B CN 201210444734 A CN201210444734 A CN 201210444734A CN 102920016 B CN102920016 B CN 102920016B
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Abstract
The invention discloses a porcini extract. The porcini extract is prepared according to the following method: commercially available porcini is smashed and filtered by a 40-mesh sieve to obtain dry powder, then the powder and a solvent are added in an extraction pot according to mass ratio of 1:10, heated and extracted through reflux or ultrasonic wave to obtain a crude extract, the crude extract is filtered through a 150-200-mesh sieve to obtain filtrate, and then the filtrate is decompressed and concentrated through a film falling concentrator to obtain the porcini extract. In the film falling concentration process, vacuum degree is from -0.07 to -0.088 MPa, holding temperature is 60-80 DEG C, and concentration multiple is 5-10 times. The porcini extract is applied to cigarettes creatively, can increase fragrance strength of the cigarettes and brightness degree of the cigarettes, improves taste of the cigarettes, and provides a novel raw material for cigarette flavor.
Description
Technical field
The object of the present invention is to provide a kind of extracting method of bolete extract, and application in cigarette.In literary composition, indication bolete is containing white, yellow, three kinds of Boletus aereus.
Background technology
Beef liver mushroom is the general designation of the fungi such as Boletaceae and pinecone Boletaceae, wherein except minority kind is poisonous or bitter and can not eating, and the equal edible of most of kind.Yunnan Province's beef liver mushroom aboundresources, has many good edible kinds, mainly contains white, yellow, Boletus aereus.Suillus albidipes (Peck) Sing, claims again cepe, grow in the loose oak mixed forest between 900 meters to 2,200 meters of height above sea level, or felling border area soon, growth period be at the bottom of annual May to October, while becoming a fine day after rain, grow more, be easy to gather.Suillus albidipes (Peck) Sing delicious flavour, nutritious.
8 seed amino acids that bolete contains needed by human, also contain the alkaloids such as gland fat purine, choline and putrescine.Pharmaceutically acceptable, treatment lumbocrural pain, numb in every limb, tic of limbs, also can be in order to control women's abnormal leucorrhea.It has heat-clearing solution be tired of, nourish blood and in, wind-evil dispelling and cold-evil expelling, relax the muscles and stimulate the blood circulation, the effect such as qi-restoratives is refreshed oneself.In addition, also have resisiting influenza virus, the anti-effect curing cold.
Have not yet to see bolete extract for increasing the fragrance dynamics of cigarette, the bright degree of flue gas and improve cigarette mouthfeel relevant report.
Summary of the invention
the object of the present invention is to provide a kind of bolete extract and preparation method thereof, and this bolete extract is used for increasing the bright degree of fragrance dynamics, flue gas of cigarette and improves cigarette mouthfeel.
In order to achieve the above object, the present invention has adopted following technical scheme: a kind of bolete extract, is prepared as follows:
(1) 40 mesh sieves are pulverized and crossed to commercially available bolete and obtain dry powder, then dry powder and solvent are added to extractor with the mass ratio of 1:6, carry out heating and refluxing extraction 3 hours, extract 80 ± 2 DEG C of temperature, obtain crude extract; Also the dry powder with 1:10 mass ratio and the solvent mixture that add extractor can be carried out to ultrasonic wave extraction, its ultrasonic frequency is 30KHZ, 30 minutes extraction times, obtains crude extract.
(2) crude extract is filtered to get filtrate through 150-200 eye mesh screen, then filtrate is carried out to reduced pressure concentration by falling liquid film concentrator and obtain bolete extract, in falling liquid film concentration technology, vacuum is-0.07 to-0.088MPa, maintain the temperature at 60-80 DEG C, cycles of concentration 5-10 doubly.
Described solvent is the ethanol of 50%-70% concentration, and optimum is 70% concentration ethanol solution.
Described bolete is Suillus albidipes (Peck) Sing, Boletus luridus, Boletus aereus.
By the bolete extract making for cigarette, can increase cigarette fragrance dynamics, increase flue gas bright degree and improve cigarette mouthfeel.
Beneficial effect of the present invention is: at the leaching process of bolete extract, adopt low temperature (extracting 80 ± 2 DEG C of temperature) to extract, to ensure as much as possible the fragrance component in bolete.Concentration process adopts vacuum-concentrcted, and realization is quick and low temperature is concentrated, can ensure that the aroma quality of extract has been saved again the energy.Creatively bolete extract is applied to cigarette, can increase cigarette fragrance dynamics, increase flue gas bright degree and improve cigarette mouthfeel, for cigarette blending provides a kind of new raw material.
Detailed description of the invention
Embodiment 1
(1) preparation of bolete extract
Commercially available Boletus aereus dry plate is pulverized, crossed 40 mesh sieves and obtain dry powder;
By dry powder: the mass ratio of 70% concentration ethanol solution=1:10 adds extractor, heating and refluxing extraction 3 hours, temperature is held in 80 ± 2 DEG C, obtains crude extract.Crude extract is filtered to get filtrate through 150-200 eye mesh screen, then filtrate is carried out to reduced pressure concentration by falling liquid film concentrator and obtain bolete extract, in falling liquid film concentration technology, vacuum is-0.07 to-0.088MPa, maintain the temperature at 60-80 DEG C, 5 times of cycles of concentration, obtain bolete extract.
(2) by the bolete extract making for cigarette, can increase cigarette fragrance dynamics, increase flue gas bright degree and improve cigarette mouthfeel, concrete grammar:
By 100 times of 70% ethanol dilutions for the bolete extract making, obtain bolete extract dilution, above bolete extract dilution is pressed to 0.1%, 0.3%, 0.5% and 1% amount (with respect to tobacco quality), spray equably respectively on the pure pipe tobacco that is balance 48h under 22 DEG C ± 1 DEG C and RH60% ± 2% condition with laryngeal spray, after spray, pipe tobacco is balance 48h under 22 DEG C ± 1 DEG C and RH60% ± 2% condition, and under this environment, aromatic tobacco is rolled into cigarette with cigarette-roller.Contrast experiment group is blank pipe tobacco, under the same conditions, sprays equably respectively distilled water with laryngeal spray.Smoked panel test by company's specialty personnel of group that smoke panel test, the situation of smokeing panel test is as follows:
Consumption smoking result
Blank pipe tobacco (control sample) cigarette flavor shows slightly flat, flue gas is muddy, pleasant impression has bitter taste.
Add the aroma of tobacco shreds dynamics of 0.1% extract to increase, flue gas is bright, mouthfeel is improved.
Add the aroma of tobacco shreds dynamics of 0.3% extract to increase, flue gas is bright, and pleasant impression is comfortable.
Add the fragrant richness of the increase of aroma of tobacco shreds dynamics, cigarette of 0.5% extract to increase, flue gas is bright, and pleasant impression is comfortable.
Add the aroma of tobacco shreds dynamics of 1% extract to increase, stimulate increase, mouthfeel is full.
Embodiment 2
(1) preparation of bolete extract:
Commercially available Boletus aereus dry plate is pulverized, crossed 40 mesh sieves and obtain dry powder;
By dry powder: the mass ratio of 70% concentration ethanol solution=1:10 adds extractor, carries out ultrasonic wave extraction, and its ultrasonic frequency is 30KHZ, 30 minutes extraction times, obtains crude extract.Crude extract is filtered to get filtrate through 150-200 eye mesh screen, then filtrate is carried out to reduced pressure concentration by falling liquid film concentrator and obtain bolete extract, in falling liquid film concentration technology, vacuum is-0.07 to-0.088MPa, maintain the temperature at 60-80 DEG C, 5 times of cycles of concentration, obtain bolete extract.
(2) by the bolete extract making for cigarette, can increase cigarette fragrance dynamics, increase flue gas bright degree and improve cigarette mouthfeel, concrete grammar leads to embodiment 1.
Same, the present invention has also done the preparation of the extraction bolete extract as described in embodiment 1 and 2 to Suillus albidipes (Peck) Sing, Boletus luridus, equally its bolete extract is also done to the evaluation method as described in embodiment 1 and 2 for cigarette, its increase cigarette fragrance dynamics, increase the bright degree of flue gas and improve cigarette mouthfeel texts with embodiment 1 and 2 without significant difference, therefore seldom do deposited stating at this.
Claims (2)
1. a bolete extract that improves cigarette mouthfeel, is characterized in that, this bolete extract is prepared as follows:
Commercially available Boletus aereus dry plate is pulverized, crossed 40 mesh sieves and obtain dry powder;
By dry powder: the mass ratio of 70% concentration ethanol solution=1:10 adds extractor, heating and refluxing extraction 3 hours, temperature remains on 80 ± 2 DEG C, obtains crude extract; Crude extract is filtered to get filtrate through 150-200 eye mesh screen, then filtrate is carried out to reduced pressure concentration by falling liquid film concentrator and obtain bolete extract, in falling liquid film concentration technology, vacuum is-0.07 to-0.088MPa, maintain the temperature at 60-80 DEG C, 5 times of cycles of concentration, obtain bolete extract.
2. bolete extract claimed in claim 1 is in the application improving in cigarette mouthfeel, its application process is: by 100 times of 70% ethanol dilutions for the bolete extract making, obtain bolete extract dilution, above bolete extract dilution is pressed to 0.1%, 0.3%, 0.5% and 1% amount with respect to tobacco quality, spray equably respectively on the pure pipe tobacco that is balance 48h under 22 DEG C ± 1 DEG C and RH60% ± 2% condition with laryngeal spray, after spray, pipe tobacco is balance 48h under 22 DEG C ± 1 DEG C and RH60% ± 2% condition.
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| CN201210444734.XA CN102920016B (en) | 2012-11-09 | 2012-11-09 | Porcini extract and preparation method and application thereof |
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| CN201210444734.XA CN102920016B (en) | 2012-11-09 | 2012-11-09 | Porcini extract and preparation method and application thereof |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104126868B (en) * | 2014-07-18 | 2016-08-24 | 云南中烟工业有限责任公司 | Come from the preparation method of the natural perfume material of bolete and to the purposes of fragrance-enhancing tobacco |
| CN106727736B (en) * | 2016-11-30 | 2020-05-19 | 中山大学 | Preparation method and application of active substance of boletus flavus |
| CN110122917A (en) * | 2018-02-08 | 2019-08-16 | 深圳波顿香料有限公司 | A kind of preparation method of preserved citron extract and its application and cigarette in cigarette |
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| CN100998614A (en) * | 2006-12-31 | 2007-07-18 | 李晔 | Method for extracting spore powder of glossy ganoderma and deep processing technique for the product |
| CN101194750A (en) * | 2007-11-02 | 2008-06-11 | 红云烟草(集团)有限责任公司 | Toadstool ferment produced perfume for tobacco and method for producing the same |
| CN101341888A (en) * | 2008-08-19 | 2009-01-14 | 北京市农林科学院 | Bolete extract, preparation and application thereof |
| CN101715948A (en) * | 2009-12-14 | 2010-06-02 | 楚雄宏桂绿色食品有限公司 | Bolete extracting solution and beverages as well as preparation methods thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2007111500A1 (en) * | 2006-03-27 | 2007-10-04 | Plant Research International B.V. | Immunization with transgenic mushrooms |
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| CN100998614A (en) * | 2006-12-31 | 2007-07-18 | 李晔 | Method for extracting spore powder of glossy ganoderma and deep processing technique for the product |
| CN101194750A (en) * | 2007-11-02 | 2008-06-11 | 红云烟草(集团)有限责任公司 | Toadstool ferment produced perfume for tobacco and method for producing the same |
| CN101341888A (en) * | 2008-08-19 | 2009-01-14 | 北京市农林科学院 | Bolete extract, preparation and application thereof |
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