CN100998614A - Method for extracting spore powder of glossy ganoderma and deep processing technique for the product - Google Patents
Method for extracting spore powder of glossy ganoderma and deep processing technique for the product Download PDFInfo
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Abstract
A process for preparing the ganoderma spore powder includes such steps as removing impurities, drying, sieving, breaking wall of spore, adding alcohol solution, extracting, filtering, sieving the filtrate, vacuum concentrating, and drying.
Description
Technical field
The present invention relates to contain the preparation method of raw-material preparation, especially belong to a kind of deep process technology of extracting process and goods thereof of Ganoderma spore powder.
Background technology
Ganoderma since ancient times among the people be exactly a kind of medicine-food two-purpose fungus, Ganoderma spore contains than the Ganoderma special compositions such as Ganoderma triterpenoids, ribosidoadenine, protein, enzyme and selenium element of horn of plenty more.Because the quantity of Ganoderma spore is few, seem precious, people also just seem careful to its processing, usually do not process and just be used for pharmacy, it is found that under study for action the Ganoderma spore epidermis is made of the hard chitin of one deck, water insoluble, digestive system by human body self can't destroy this epidermis, also just can't absorb active ingredient contained in the Ganoderma spore, therefore, in the recent period ganoderma lucidium spore powder wall breaking is become the main manufacturing process of Ganoderma spore powder, but Ganoderma spore powder viscosity behind breaking cellular wall increases, be unfavorable for the uniform mixing of it and other medical material, and influence the quality of patent medicine.
Simultaneously, human body is relevant with its content and concentration to the absorption of taking in substance in vivo, therefore works as the material of being taken in when not reaching certain amount, and the absorption by human body rate is very low, does not have therapeutic effect.Consumption according to pharmacopeia record Ganoderma is generally 6--12 gram/sky, a common capsular weight is the 250---500 milligram, will obey the 12---48 grain in just one day, and patient also will take other medicines in addition, give the people a kind of bad impression of taking medicine to eat, increased patient's psychological burden when meal.
Summary of the invention
The object of the present invention is to provide the extracting process of a kind of effective component content height, the measured Ganoderma spore powder of matter and the deep process technology of goods thereof.
The extracting process of a kind of Ganoderma spore powder of the present invention, choose big impurity after the Ganoderma spore powder collection, dry, sieve with the 200--400 mesh sieve, remove impurity, carry out broken wall treatment, its invention main points are Sporoderm-broken Ganoderma Lucidum Spore powder is extracted, and leaching process is: add the ethanol of 6--10 times of 40--95% concentration in Sporoderm-broken Ganoderma Lucidum Spore powder, 50--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, collect filtrate, filtrate is crossed the 200--400 mesh sieve again, 50～70 ℃ are evaporated to density is 1.15--1.2, carry out drying, get the Ganoderma spore powder extracts.
The extract of indication of the present invention be Chinese herbal medicine through extract, concentrate, the flour of dry back gained, the amount that adds solvent is that the weight with the extraction raw material is reference value.
Modern medicine study finds that three terpene components in the Ganoderma spore powder have stronger protective effect to chemical liver injury, is applicable to patients such as alcoholic liver, medicine liver, and the chemicotherapy patient is had repair preferably.The triterpene content of the Ganoderma spore powder extracts that obtains with said method is up to more than 17%, and the triterpene content of the Ganoderma spore powder behind the breaking cellular wall only is 1.5% to 4.0%, by relatively, can obviously find out the advantage of Ganoderma spore powder extracts.This high-load can not only make patient take medicine less, also helps the absorption of human body to the triterpene composition, has improved the Ganoderma spore powder medicinal effects.
For reducing cost, filtering residue after the Sporoderm-broken Ganoderma Lucidum Spore powder alcohol extraction is for the first time carried out alcohol extraction again, the ethanol that in filtering residue, adds 6--10 times of 40--95% concentration, 50--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, merge twice filtrate and cross the 200--400 mesh sieve, 50～70 ℃ are evaporated to density is 1.15--1.2, carry out drying, get the Ganoderma spore powder extracts.
Can guarantee that through twice alcohol extraction the Ganoderma spore powder extraction rate reached is more than 20%.
Also can on the basis of above-mentioned alcohol extraction, carry out water extraction to residue.Concrete grammar is as follows:
Choose big impurity after the Ganoderma spore powder collection, dry, sieve with the 200--400 mesh sieve, remove impurity, carry out broken wall treatment, and Sporoderm-broken Ganoderma Lucidum Spore powder is extracted, leaching process is: the ethanol that adds 6--10 times of 40--95% concentration in Sporoderm-broken Ganoderma Lucidum Spore powder, 50--80 ℃ was extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate; The ethanol that adds 6--10 times of 40--95% concentration in the filtering residue, 50--80 ℃ was extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate; Add 6--10 water doubly in filtering residue, 60--100 ℃ was extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate; Three filtrates are merged, and cross the 200--400 mesh sieve, 50～70 ℃ are evaporated to density is 1.15--1.2, carries out drying, gets the Ganoderma spore powder extracts.
Said extracted can be under normal pressure, or carries out under 0.04 to 0.06Mpa pressure, and when normal pressure extracted, it was higher to extract temperature, and it is lower to extract temperature during low pressure.
In order to give full play to the therapeutic efficiency of Ganoderma spore powder, the present invention also can add Ganoderma extract and make ganoderma spore powder product, and specifically prescription and production method are as follows:
With Ganoderma spore powder extracts and Ganoderma extract mix homogeneously, Ganoderma spore powder extracts and Ganoderma extract mixing ratio are 1--9: 9-1, and described Ganoderma extract is meant with Ganoderma and carries out alcohol extraction and water extraction that extract concentrates, dry back gained.
When Ganoderma spore powder extracts and Ganoderma extract mixing ratio are 4--6: the 6-4 effect is better, and mixing ratio is that 4: 6 o'clock effects are best.
The preparation process of Ganoderma extract is: with sorting, after former Ganoderma Lucidum behind the decontamination carries out coarse pulverization, cross 20 mesh sieves, obtain REISH, in REISH, add the 6--10 times of alcoholic solution that concentration is 40--95%, 50--80 ℃ was extracted 2--3 hour, filter with the 60--80 mesh sieve, collect filtrate for the first time, add raw material weight 6--10 40--95% alcoholic solution doubly again in filtering residue, 50--80 ℃ was extracted 2--3 hour, filter with the 60--80 mesh sieve, collect filtrate for the second time, in the Ganoderma slag, add 6--8 water doubly again, under 40--100 ℃ of condition, extracted 1-3 hour, filter with the 60--80 mesh sieve, collect filtrate for the third time, the filtrate of extracting for three times is merged, filter the back with the 200--400 eye mesh screen and import concentration tank, carried out concentrating under reduced pressure 2--3 hour at 55--60 ℃, vacuum pressure is 0.04 to 0.06Mpa when concentrating, and is concentrated into density 1.1-1.2, collects concentrated solution, concentrated solution is carried out drying, get Ganoderma extract.
With this processing technique, the Ganoderma extract yield is about 5%, and active constituent content is also high especially, and wherein polyoses content is more than 20%, and the triterpene component content is up to more than 14%.
Because the mouthfeel of Ganoderma and spore powder thereof is very bitter, the raw material of un-extracted has bilgy odour, be unfavorable for taking, and the product mouthfeel of extracting is better.The present invention also has the following advantages, the finished product mix homogeneously, and the active constituent content height, consumption greatly reduces, and by original 6--12 gram/sky, reduces to 1--2 gram/sky, makes capsule, and just can as long as obey last four or five every day.The present invention puies forward two kinds of methods by alcohol extraction and water Ganoderma sporophore is extracted, and wherein water is carried and is suitable for extracting polysaccharide, and alcohol extraction is suitable for extracting triterpene, and water is carried with alcohol extraction and being used simultaneously, these two kinds of effective ingredient fully can be extracted.
The specific embodiment
Embodiment 1, a kind of extracting process of Ganoderma spore powder, choose decontamination after the collection of log Ganoderma spore powder, dry, sieve with the 200--400 mesh sieve, remove impurity, carry out broken wall treatment, Sporoderm-broken Ganoderma Lucidum Spore powder is extracted: the ethanol that in Sporoderm-broken Ganoderma Lucidum Spore powder, adds 6--10 times of 40--95% concentration, under 0.04 to 0.06Mpa pressure, 40--65 ℃ was extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate, again filtrate is crossed the 200--400 mesh sieve, 50～70 ℃ are evaporated to density is 1.15--1.2, carries out vacuum drying, gets the Ganoderma spore powder extracts.Described vacuum drying be meant the Ganoderma spore powder concentrated solution is placed under temperature 70--80 ℃, pressure 0.01Mpa-0.04 Mpa condition 5--6 hour to its moisture less than 6%.
Embodiment 2, the log Ganoderma spore powder is after open-air bagging is gathered, naked eyes are chosen bulk impurity, no longer bondd to spore powder in dry 5--6 hour under the 70--80 ℃ of condition, sieve with the 200--400 mesh sieve, remove impurity, carry out broken wall treatment, can adopt mechanical breaking-wall method 30--50 minute, the sporoderm-broken rate of Ganoderma spore powder can reach more than 99%.Sporoderm-broken Ganoderma Lucidum Spore powder is extracted: the ethanol that in Sporoderm-broken Ganoderma Lucidum Spore powder, adds 6--10 times of 40--95% concentration of its weight, under normal pressure, 60--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, collect filtrate, the ethanol that in filtering residue, adds 6--10 times of 40--95% concentration, 60--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, merge twice filtrate and cross the 200--400 mesh sieve, under normal pressure, 50～70 ℃ are evaporated to density is 1.15--1.2, carry out drying, get the Ganoderma spore powder extracts.
Embodiment 3, and a kind of extracting process of Ganoderma spore powder is chosen big impurity after the Ganoderma spore powder collection, dry, sieve with the 200--400 mesh sieve, remove impurity, carry out broken wall treatment, it is characterized in that Sporoderm-broken Ganoderma Lucidum Spore powder is extracted, leaching process is: add the ethanol of 7 times of 75% concentration in Sporoderm-broken Ganoderma Lucidum Spore powder, under the 0.04Mpa pressure, 50 ℃ were extracted 2--3 hour, filter with 120 mesh sieves, collect filtrate; The ethanol that adds 9 times of 40% concentration in the filtering residue, under the 0.04 Mpa pressure, 50 ℃ were extracted 2--3 hour, with the filtration of 120 mesh sieves, collected filtrate; The water that adds 10 times in the filtering residue, 100 ℃ were extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate; Three filtrates are merged, and cross 300 mesh sieves, 50 ℃ are evaporated to density is 1.15--1.2, carries out drying, gets the Ganoderma spore powder extracts.It is identical with last example that all the other do not state part.
Embodiment 4, the log Ganoderma spore powder is after open-air bagging is gathered, naked eyes are chosen bulk impurity, no longer bondd to spore powder in dry 5 hours under 80 ℃ of conditions, sieve with 200 purposes sieve, remove impurity, carried out mechanical breaking-wall method 30--50 minute with the micronizing vibromill, the sporoderm-broken rate of Ganoderma spore powder reaches more than 99%.Get in 1 kilogram of Sporoderm-broken Ganoderma Lucidum Spore powder that to add 8 kilograms of concentration be 80% ethanol, under normal pressure, 75 ℃ were extracted 2.5 hours, filter with 100 mesh sieves, collect filtrate, in filtering residue, add 8 kilograms of concentration again and be 80% ethanol, under normal pressure, 75 ℃ were extracted 2.5 hours, filter with 100 mesh sieves, merge twice filtrate and cross 200 mesh sieves, 55--60 ℃ is evaporated to density is 1.15--1.2, carry out drying, get Ganoderma spore powder extracts 200---210 gram.
Embodiment 5, and the preparation process of Ganoderma extract is: spray back approximately 20 days of spore powder at former Ganoderma Lucidum and Ganoderma sporophore autotomyed in the interior time on the wood under the saw, prevent to cause because of the spore powder injecting time is long the reduction of Ganoderma sporophore effective ingredient.With sorting, after former Ganoderma Lucidum behind the decontamination carries out coarse pulverization, cross 20 mesh sieves, obtain REISH, in REISH, add the 6--10 times of alcoholic solution that concentration is 40--95%, 50--80 ℃ was extracted 2--3 hour, filter with the 60--80 mesh sieve, collect filtrate for the first time, in filtering residue, add raw material weight 6--10 40--95% alcoholic solution doubly again, 50--80 ℃ was extracted 2--3 hour, filter with the 60--80 mesh sieve, collect filtrate for the second time, in the Ganoderma slag, add 6--8 water doubly again, under 40--100 ℃ of condition, extracted 1-3 hour, filter with the 60--80 mesh sieve, collect filtrate for the third time, the filtrate of three extractions is merged, filter the back with the 200--400 eye mesh screen and import concentration tank, carried out concentrating under reduced pressure 2--3 hour at 55--60 ℃, vacuum pressure is 0.04 to 0.06Mpa when concentrating, be concentrated into density 1.1-1.2, collect concentrated solution, adopt spray drying method to carry out drying concentrated solution, the spray drying tower inlet temperature is 280 ± 5 ℃, leaving air temp is 90 ± 1 ℃, and atomization temperature is 190 ± 5 ℃, gets Ganoderma extract.The Ganoderma extract that Ganoderma spore powder extracts that makes according to embodiment 3 and said method make stirred 20--35 minute with 20--35 rev/min speed, mix homogeneously, ganoderma spore powder product.
Embodiment 5,9 kilograms of concentration of adding are 80% ethanol in 1 kilogram of REISH, under 0.04 to 0.06Mpa pressure, 50--75 ℃ was extracted 2.5 hours, filtered with 60 mesh sieves, collected filtrate for the first time, adding 8 kilograms of concentration in the filtering residue again is 50% alcoholic solution, under 0.04 to 0.06Mpa pressure, 50--70 ℃ was extracted 3 hours, and filtered with 60 mesh sieves, collect filtrate for the second time, the water that adds 6 kilograms again in the Ganoderma slag extracts 2.5 hours after-filtration under 80--100 ℃ of condition, filter with 60 mesh sieves, collect filtrate for the third time, the filtrate of three extractions is merged, and the filtrate after the merging is filtered the back with 300 eye mesh screens and is imported concentration tank, carries out concentrating under reduced pressure 3 hours at 55--60 ℃, vacuum pressure is 0.04--0.05Mpa when concentrating, be concentrated into density 1.1-1.2, collect concentrated solution, adopt spray drying method to carry out drying concentrated solution, the spray drying tower inlet temperature is 280 ± 5 ℃, leaving air temp is 90 ± 1 ℃, and atomization temperature is 190 ± 5 ℃, gets Ganoderma extract.
With said method 600 kairine sesame extracts that make and Ganoderma spore powder extracts 400 grams that make according to embodiment 3, stirred 20--35 minute with 25 rev/mins speed, mix homogeneously gets ganoderma spore powder product.It is identical with last example that all the other do not state part.
Claims (9)
1, a kind of extracting process of Ganoderma spore powder, choose big impurity after the Ganoderma spore powder collection, dry, sieve with the 200--400 mesh sieve, remove impurity, carry out broken wall treatment, it is characterized in that Sporoderm-broken Ganoderma Lucidum Spore powder is extracted, leaching process is: add the ethanol of 6--10 times of 40--95% concentration in Sporoderm-broken Ganoderma Lucidum Spore powder, 50--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, collect filtrate, filtrate is crossed the 200--400 mesh sieve again, 50～70 ℃ are evaporated to density is 1.15--1.2, carry out drying, get the Ganoderma spore powder extracts.
2, the extracting process of a kind of Ganoderma spore powder according to claim 1, it is characterized in that the filtering residue after the Sporoderm-broken Ganoderma Lucidum Spore powder alcohol extraction is for the first time carried out alcohol extraction again, the ethanol that in filtering residue, adds 6--10 times of 40--95% concentration, 50--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, merge twice filtrate and cross the 200--400 mesh sieve, 50～70 ℃ are evaporated to density is 1.15--1.2, carry out drying, get the Ganoderma spore powder extracts.
3, a kind of extracting process of Ganoderma spore powder, choose big impurity after the Ganoderma spore powder collection, drying is sieved with the 200--400 mesh sieve, removes impurity, carry out broken wall treatment, it is characterized in that Sporoderm-broken Ganoderma Lucidum Spore powder is extracted, leaching process is: add the ethanol of 6--10 times of 40--95% concentration in Sporoderm-broken Ganoderma Lucidum Spore powder, 50--80 ℃ was extracted 2--3 hour, filter with the 100--120 mesh sieve, collect filtrate; The ethanol that adds 6--10 times of 40--95% concentration in the filtering residue, 50--80 ℃ was extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate; Add 6--10 water doubly in filtering residue, 60--100 ℃ was extracted 2--3 hour, filtered with the 100--120 mesh sieve, collected filtrate; Three filtrates are merged, and cross the 200--400 mesh sieve, 50～70 ℃ are evaporated to density is 1.15--1.2, carries out drying, gets the Ganoderma spore powder extracts.
4, a kind of deep process technology of ganoderma spore powder product, it is characterized in that Ganoderma spore powder extracts and Ganoderma extract mix homogeneously, Ganoderma spore powder extracts and Ganoderma extract mixing ratio are 1--9: 9-1, described Ganoderma extract is meant with Ganoderma and carries out alcohol extraction and water extraction that extracting solution concentrates, dry back gained.
5, the deep process technology of a kind of ganoderma spore powder product according to claim 4 is characterized in that Ganoderma spore powder extracts and Ganoderma extract mixing ratio are 4--6: 6--4.
6, the deep process technology of a kind of ganoderma spore powder product according to claim 4 is characterized in that Ganoderma spore powder extracts and Ganoderma extract mixing ratio are 4: 6.
7, the deep process technology of a kind of ganoderma spore powder product according to claim 4 is characterized in that the Ganoderma spore powder extracts mixes with Ganoderma extract, is to stir 20--35 minute with 20--35 rev/min speed.
8, the deep process technology of a kind of ganoderma spore powder product according to claim 4, the preparation process that it is characterized in that Ganoderma extract is: with sorting, after former Ganoderma Lucidum behind the decontamination carries out coarse pulverization, cross 20 mesh sieves, obtain REISH, in REISH, add the 6--10 times of alcoholic solution that concentration is 40--95%, 50--80 ℃ was extracted 2--3 hour, filter with the 60--80 mesh sieve, collect filtrate for the first time, in filtering residue, add raw material weight 6--10 40--95% alcoholic solution doubly again, 50--80 ℃ was extracted 2--3 hour, filter with the 60--80 mesh sieve, collect filtrate for the second time, in the Ganoderma slag, add 6--8 water doubly again, under 40--100 ℃ of condition, extracted 1-3 hour, filter with the 60--80 mesh sieve, collect filtrate for the third time, the filtrate of three extractions is merged, filter the back with the 200--400 eye mesh screen and import concentration tank, carried out concentrating under reduced pressure 2--3 hour at 55--60 ℃, vacuum pressure is 0.04 to 0.06Mpa when concentrating, be concentrated into density 1.1--1.2, collect concentrated solution, concentrated solution is carried out drying, get Ganoderma extract.
9, the deep process technology of a kind of ganoderma spore powder product according to claim 4 is characterized in that used former Ganoderma Lucidum plucked in the interior time in 20 days after spraying spore powder.
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| CN110393729A (en) * | 2019-09-04 | 2019-11-01 | 钟志强 | A kind of Reishi sporule preparation method of composition for treating senile dementia |
| CN114618689A (en) * | 2022-05-16 | 2022-06-14 | 广东华夏友美生物科技有限公司 | Ganoderma triterpene extraction and separation equipment and extraction and separation process thereof |
| CN114618689B (en) * | 2022-05-16 | 2022-08-12 | 广东华夏友美生物科技有限公司 | Ganoderma triterpene extraction and separation equipment and extraction and separation process thereof |
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