CN105132162A - Dendrobe glycerol triacetate extract and application thereof in cigarettes - Google Patents
Dendrobe glycerol triacetate extract and application thereof in cigarettes Download PDFInfo
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- CN105132162A CN105132162A CN201510336481.8A CN201510336481A CN105132162A CN 105132162 A CN105132162 A CN 105132162A CN 201510336481 A CN201510336481 A CN 201510336481A CN 105132162 A CN105132162 A CN 105132162A
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- glycerol triacetate
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Abstract
The invention discloses a dendrobe glycerol triacetate extract and an application thereof in cigarettes. The dendrobe glycerol triacetate extract is prepared by the steps: with a cleanly-washed and dried dendrobium officinale powder having the particle size of 20-40 mesh as a raw material, taking glycerol triacetate as an extraction agent, firstly, extracting by a heating reflux method, and extracting by ultrasonic waves to obtain the dendrobe glycerol triacetate extract. With glycerol triacetate as a solvent, the dendrobe glycerol triacetate extract is made into a solution with the concentration of 1-3%, the solution is evenly sprayed onto filter rod tows with the proportion of 7-8% of the weight of the acetate fiber tows, then cigarette filter rods are prepared, and the cigarettes having the filter rods containing dendrobe effective ingredients are prepared through a conventional cigarette rolling process. The extract can significantly enhance the smoke sweet feeling and fine and smooth properties, manifests fresh, sweet and fragrant style characteristics, and besides, removes miscellaneous odor and mitigates stimulation. The dendrobe glycerol triacetate extract has the advantages of simple production process, strong operability and normalization, easily available raw materials, low cost, easy realization of industrialized production, and good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of stem of noble dendrobium glycerine triacetate extract.Meanwhile, the invention still further relates to the described application of stem of noble dendrobium glycerine triacetate extract in cigarette.
Background technology
Herba Dendrobii is the orchid family Dendrobium Sw, and taste is sweet, and property is flat to be slightly cold.Contained by Herba Dendrobii, chemical composition structure is many, and pharmacological action is extensive.Experts and scholars have carried out large quantity research to its chemical composition, find in it containing abundant dendrobium polysaccharide, dendrobine, amino acid, trace element, luxuriant and rich with fragrance compounds, Bibenzyl compound, phenolic acid compound and volatile component.Therefore, there is reinforcing stomach reg fluid, the effect of nourishing Yin and clearing heat, moistening lung kidney-nourishing, simultaneously enhancing body immunizing power, antitumor, promoting digestion liquid secretion, hepatic cholagogic and hypoglycemic hypotensive etc. in have good curative effect.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in glycerine triacetate dissolve add in cigarette, or the additive some being insoluble in glycerine triacetate is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the dissolving power of glycerine triacetate to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in glycerine triacetate, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by glycerine triacetate, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable Technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco industry in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of Herba Dendrobii extract prepared using glycerine triacetate as extraction agent is provided, this extract be applied to cigarette can effectively strengthen the fresh and sweet fragrant breeze lattice of cigarette, the fine and smooth alcohol of flue gas and, suction comfort level promotes.
The present invention also aims to provide the described embody rule of stem of noble dendrobium glycerine triacetate extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
A kind of stem of noble dendrobium glycerine triacetate extract, is obtained by the method for following steps:
(1) dry after Herba Dendrobii being cleaned, obtain 20 ~ 40 object dendrobe powder through pulverizing, for subsequent use;
(2) get Dendrobium and be placed in round-bottomed flask, add glycerol triacetate for tobacco as extraction agent by solid-liquid ratio 1:10 ~ 20, soaking at room temperature, after 1 ~ 4 hour, carries out refluxing extraction under 80 ~ 120 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 800W, 40kHZ condition, extract 20 ~ 45 minutes, cross the settled solution obtained after filtering filter residue and be required stem of noble dendrobium glycerine triacetate extract.
The described application of stem of noble dendrobium glycerine triacetate extract in cigarette, it is characterized in that: take glycerine triacetate as solvent, described stem of noble dendrobium glycerine triacetate extract is mixed with the solution that concentration is 1 ~ 3%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the stem of noble dendrobium glycerine triacetate extract prepared by the present invention, can dissolve each other in any proportion with glycerine triacetate, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that the stem of noble dendrobium exists by prior art when filter stick additive is mixed and is fitted in softening agent.
2. adopt glycerine triacetate to be that extraction agent extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in glycerine triacetate in the stem of noble dendrobium fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to glycerine triacetate time, the loss of effective efficiency composition.
3. gained stem of noble dendrobium glycerine triacetate extract effectively can be given prominence to the fresh and sweet note of cigarette, enrich cigarette nature fragrance, has the effect reducing flue gas pungency and assorted gas simultaneously.
4. material used herein is food grade, has higher safety in utilization.
5. production technique of the present invention is simple, operability and standardization strong, raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
It is dry after Herba Dendrobii is cleaned, 20-40 object dendrobe powder is obtained through pulverizing, Dendrobium is loaded in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:10 is as extraction agent, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, the stem of noble dendrobium after described refluxing extraction and glycerine triacetate are placed in ultrasonic extractor (400W, 40kHZ), extract 25 minutes, cross after filtering filter residue and obtain settled solution, be required stem of noble dendrobium glycerine triacetate extract.
Take glycerine triacetate as solvent, stem of noble dendrobium glycerine triacetate extract is mixed with the solution that concentration is 1%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains stem of noble dendrobium effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned stem of noble dendrobium glycerine triacetate extract increases, and flue gas pungency obviously reduces, and aroma quality promotes, and suction comfort level is obviously improved.
Embodiment 2
It is dry after Herba Dendrobii is cleaned, obtaining particle diameter through pulverizing is 40 object Dendrobiums, dendrobe powder raw material is loaded in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:20 is as extraction agent, soaking at room temperature is after 2 hours, refluxing extraction is carried out under 90 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, will, the stem of noble dendrobium after described refluxing extraction and glycerine triacetate are placed in ultrasonic extractor (600W, 40kHZ), extract 35 minutes, cross after filtering filter residue and obtain settled solution, required stem of noble dendrobium glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, stem of noble dendrobium glycerine triacetate extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains stem of noble dendrobium effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned stem of noble dendrobium glycerine triacetate extract has fresh and sweet note, the rich lifting of cigarette perfume (or spice), and flue gas pungency reduces, exquisiteness increase and decrease, and pleasant impression and pungency are improved.
Embodiment 3
It is dry after Herba Dendrobii is cleaned, 20 object dendrobe powder are obtained through pulverizing, Dendrobium raw material is loaded in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:15 is as extraction agent, soaking at room temperature is after 3 hours, refluxing extraction is carried out under 120 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, will, the stem of noble dendrobium after described refluxing extraction and glycerine triacetate are placed in ultrasonic extractor (400W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required stem of noble dendrobium glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, stem of noble dendrobium glycerine triacetate extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains stem of noble dendrobium effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the fresh and sweet sense of cigarette flue gas adding above-mentioned stem of noble dendrobium glycerine triacetate extract is obvious, the fine and smooth alcohol of flue gas and, assorted gas and pungency weaken, and the global comfort of suction promotes.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a stem of noble dendrobium glycerine triacetate extract, is obtained by the method for following steps:
(1) dry after Herba Dendrobii being cleaned, obtain 20 ~ 40 object dendrobe powder through pulverizing, for subsequent use;
(2) get Dendrobium and be placed in round-bottomed flask, add glycerol triacetate for tobacco as extraction agent by solid-liquid ratio 1:10 ~ 20, soaking at room temperature, after 1 ~ 4 hour, carries out refluxing extraction under 80 ~ 120 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 800W, 40kHZ condition, extract 20 ~ 45 minutes, cross the settled solution obtained after filtering filter residue and be required stem of noble dendrobium glycerine triacetate extract.
2. the application of stem of noble dendrobium glycerine triacetate extract according to claim 1 in cigarette, it is characterized in that: take glycerine triacetate as solvent, described stem of noble dendrobium glycerine triacetate extract is mixed with the solution that concentration is 1 ~ 3%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| CN201510336481.8A CN105132162A (en) | 2015-06-17 | 2015-06-17 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105733810A (en) * | 2016-03-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
| CN105779125A (en) * | 2016-03-18 | 2016-07-20 | 云南中烟工业有限责任公司 | Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes |
| CN105802733A (en) * | 2016-03-18 | 2016-07-27 | 云南中烟工业有限责任公司 | Lemongrass glycerol triacetate extract and application thereof to cigarettes |
-
2015
- 2015-06-17 CN CN201510336481.8A patent/CN105132162A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105733810A (en) * | 2016-03-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
| CN105779125A (en) * | 2016-03-18 | 2016-07-20 | 云南中烟工业有限责任公司 | Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes |
| CN105802733A (en) * | 2016-03-18 | 2016-07-27 | 云南中烟工业有限责任公司 | Lemongrass glycerol triacetate extract and application thereof to cigarettes |
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