CN105802733A - Lemongrass glycerol triacetate extract and application thereof to cigarettes - Google Patents
Lemongrass glycerol triacetate extract and application thereof to cigarettes Download PDFInfo
- Publication number
- CN105802733A CN105802733A CN201610154584.7A CN201610154584A CN105802733A CN 105802733 A CN105802733 A CN 105802733A CN 201610154584 A CN201610154584 A CN 201610154584A CN 105802733 A CN105802733 A CN 105802733A
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- CN
- China
- Prior art keywords
- extract
- herba cymbopogonis
- cymbopogonis citrari
- lemongrass
- triacetyl glycerine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a lemongrass glycerol triacetate extract and application thereof to cigarettes.Lemongrass grass obtained after dried lemongrass leaves are smashed and screened serves as a raw material, glycerol triacetate serves as an extraction agent, extraction is conducted in a heating reflux mode, and then the lemongrass glycerol triacetate extract is prepared through ultrasonic extraction; glycerol triacetate serves as a solvent to prepare a lemongrass extract into a solution with the concentration being 1%o-5%o, the solution accounting for 7-8% of the weight of acetic acid fiber tows is evenly sprayed to filter stick tows, cigarette filter sticks are prepared, and the cigarettes with the lemongrass effective component filter sticks are prepared through conventional cigarette connection and assembly procedure.The extract makes cigarette flavor rich, harmonious, fresh and natural, miscellaneous qi is covered, and smoking comfort is obviously improved.Raw materials are easy to obtain, cost is low, operability and normalization are high, the production technology is simple, industrial production is convenient, and application prospects are good.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of Herba Cymbopogonis Citrari triacetyl glycerine extract.Meanwhile, the invention still further relates to the application in Medicated cigarette of the described Herba Cymbopogonis Citrari triacetyl glycerine extract.
Background technology
Herba Cymbopogonis Citrari, formal name used at school is Cymbopogoncitratus, English Lemongrass by name, belongs to grass family, has strong citris aromas.Herba Cymbopogonis Citrari is to be grown in semi-tropical a kind of Rhizoma Imperatae spice, natural in citrus scented, the effect having stomach function regulating ventilation, refreshment to promote the sexual maturity, and is the Tradition condiment preferred to use most of Dai people.Herba Cymbopogonis Citrari is containing acid saponins, tannin, saccharide and aldehydes matter, containing piperitone, carene, geraniol, Ethylgeranate, limonene etc. in leaf volatile oil, be used as medicine have relieving asthma, the effect of cough-relieving.Herba Cymbopogonis Citrari blade of grass is direct-edible, has become indispensable seasoning food materials, can play the effect of flavor and enhancing flavor aodorization in traditional cuisines of country in Southeast Asia.Herba Cymbopogonis Citrari dry product as the direct soaked use of Folium Camelliae sinensis, or can be taken after being infused in hot water or decoction as required together with other Folium Camelliae sinensis, makes Folium Camelliae sinensis effect and better tasting.
Along with smoking increasingly receives publicity with healthy problem, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also brings along Medicated cigarette gratification and natural cigarette perfume (or spice) is more or less lost, therefore, each tobacco productive corporation will promote Medicated cigarette gratification and Nicotiana tabacum L. nature fragrance gradually as researching and developing key task.Cigarette smoking quality can be effectively improved by cigarette tobacco leaf formulation flavoring and casing, but this mode finally needs that carrying out burns brings more complicated product, R&D worker will become a kind of simple and feasible application mode by adding some extracts with the effect such as flavouring, humectation in filter stick.R&D worker has carried out the work of some correlational studyes, and obtains certain achievement.The filtering material of such as a kind of cigarette filter rod and cigarette filter rod (200810219901.4), a kind of there are the application in cigarette filter rod of the Radix Et Rhizoma Fagopyri Tatarici cigarette filter rod (201410372333.7) of burnt odor, moringa seeds extract and cigarette filter rod (201310159094.2) thereof etc., but the filter stick additive described in above-mentioned patent mainly first passes through extraction or allotment additive dissolves in triacetyl glycerine and adds in Medicated cigarette, maybe by increase, interpolation granule is added operation and is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation, triacetyl glycerine in this interpolation application mode, the solvability of additive is limited, much Medicated cigarette is had flavouring, the extract of humectation effect is difficult to be dissolved in triacetyl glycerine, limits the application in cigarette filter rod of such extract.On the other hand, if being not that carrier carries out filter stick perfuming by triacetyl glycerine, but additive being applied directly in cigarette filter rod, can produce to filter stick and bring bigger difficulty, dramatically increasing production cost, being unfavorable for large-scale popularization and application.For meeting tobacco business demand in Medicated cigarette flavouring, humectation, how adopting suitable Technology, the additive of cigarette filter stick of the applicable Production requirement of preparation needs the technical barrier of solution badly by becoming this field.
Summary of the invention
Present invention aims to the deficiencies in the prior art, a kind of Herba Cymbopogonis Citrari extract prepared as extractant using triacetyl glycerine is provided, this extract can be directly appended in triacetyl glycerine to be applied to cigarette filter tip shaping, cigarette sensory quality can be obviously improved, effectively strengthen that cigarette flavor is rich, the fragrant harmony of cigarette, alleviate flue gas residual and stimulate.
The present invention also aims to provide described Herba Cymbopogonis Citrari triacetyl glycerine extract specifically applying in production of cigarettes.
The purpose of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percent adopted in the present invention is mass percent.
A kind of Herba Cymbopogonis Citrari triacetyl glycerine extract, is prepared by the method for following steps:
(1) take fresh Herba Cymbopogonis Citrari blade to dry or dry, pulverize after shredding with shears, cross 20～40 mesh sieves and obtain Herba Cymbopogonis Citrari powder, standby；
(2) weigh 200～600g Herba Cymbopogonis Citrari powder and be placed in round-bottomed flask, glycerol triacetate for tobacco is added as extractant in the ratio of solid-liquid ratio 1:6～12, after soaking at room temperature 2～4 hours, reflux, extract, is carried out under 65～95 DEG C of conditions, 6～8 hours extraction times, standby after being cooled to room temperature；
(3) being placed in ultrasonic extractor by step (2) gains, when 400～600W, 40kHZ, extract 30～50 minutes, the settled solution obtained after being filtered to remove filtering residue is required Herba Cymbopogonis Citrari triacetyl glycerine extract.
The application in Medicated cigarette of the described Herba Cymbopogonis Citrari triacetyl glycerine extract, it is characterized in that: with triacetyl glycerine for solvent, described Herba Cymbopogonis Citrari triacetyl glycerine extract is configured to the solution that concentration is 1 ‰～5 ‰, it is sprayed onto on tow by the ratio uniform of acetate silk weight 7～8%, make cigarette filter rod, and this filter stick is applied to Medicated cigarette.
Compared with prior art, the invention have the advantages that
1. the present invention adopts triacetyl glycerine to be that extractant extracts Herba Cymbopogonis Citrari, the effective efficiency composition being dissolved in triacetyl glycerine in Herba Cymbopogonis Citrari fully can be extracted, avoid employing other solvent carry out extracting again redissolve to triacetyl glycerine time, lose part effective efficiency composition；The safety of production of cigarettes will not be had a negative impact simultaneously.
2. the Herba Cymbopogonis Citrari triacetyl glycerine extract prepared by, can dissolve each other with triacetyl glycerine arbitrary proportion, extract can be uniformly distributed in filter stick tow, solves and Herba Cymbopogonis Citrari is mixed directly as filter stick additive the limited or undissolvable problem of dissolving existed when being fitted in plasticizer.
3. gained Herba Cymbopogonis Citrari triacetyl glycerine extract can enrich coordination Medicated cigarette nature cigarette perfume, be effectively increased the pure and fresh note of Medicated cigarette, and covers miscellaneous QI, improves effect of suction quality.
4. raw material of the present invention be easy to get, with low cost, operability and standardization are strong, and production technology is simple, it is simple to realize industrialized production, have a good application prospect.
5. material used herein is food stage, has higher safety in utilization.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, is not limited to the technical solution.
Embodiment 1
Take fresh Herba Cymbopogonis Citrari blade to dry or dry, pulverize after shredding with shears, grind gained powder and cross 20 mesh sieves, weigh 200g Herba Cymbopogonis Citrari powder and be placed in round-bottomed flask, glycerol triacetate for tobacco is added in the ratio of solid-liquid ratio 1:6, after soaking at room temperature 2 hours, reflux, extract, is carried out under 65 DEG C of conditions, extraction time is 6 hours, naturally cool to room temperature, Herba Cymbopogonis Citrari after described reflux, extract, and triacetyl glycerine are placed in (400W in ultrasonic extraction equipment, 40kHZ), extract 30 minutes, settled solution is obtained after being filtered to remove filtering residue, it is required Herba Cymbopogonis Citrari triacetyl glycerine extract.
With triacetyl glycerine for solvent, Herba Cymbopogonis Citrari triacetyl glycerine extract is configured to the solution that concentration is 1 ‰, it is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make the Medicated cigarette containing Herba Cymbopogonis Citrari effective ingredient filter stick by conventional cigarette tipping program.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas note adding above-mentioned Herba Cymbopogonis Citrari triacetyl glycerine extract is pure and fresh substantially, and fragrance is rich to be increased to some extent, and miscellaneous QI is covered, and pleasant impression is comparatively clean.
Embodiment 2
Take fresh Herba Cymbopogonis Citrari blade to dry or dry, pulverize after shredding with shears, grind gained powder and cross 30 mesh sieves, weigh 400g Herba Cymbopogonis Citrari powder and be placed in round-bottomed flask, glycerol triacetate for tobacco is added as extractant in the ratio of solid-liquid ratio 1:9, after soaking at room temperature 3 hours, reflux, extract, is carried out under 80 DEG C of conditions, extraction time is 7 hours, naturally cool to room temperature, Herba Cymbopogonis Citrari after described reflux, extract, and triacetyl glycerine are placed in (500W in ultrasonic extraction equipment, 40kHZ), extract 40 minutes, settled solution is obtained after being filtered to remove filtering residue, required Herba Cymbopogonis Citrari triacetyl glycerine extract can be obtained.
With triacetyl glycerine for solvent, Herba Cymbopogonis Citrari triacetyl glycerine extract is configured to the solution that concentration is 3 ‰, it is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make the Medicated cigarette containing Herba Cymbopogonis Citrari effective ingredient filter stick by conventional cigarette tipping program.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds the rich obvious increase of cigarette fragrance of above-mentioned Herba Cymbopogonis Citrari triacetyl glycerine extract, and perfume quantity is relatively big, and cigarette perfume (or spice) is coordinated naturally, and flue gas zest substantially reduces, and pleasant impression is clean, clear.
Embodiment 3
Take fresh Herba Cymbopogonis Citrari blade to dry or dry, pulverize after shredding with shears, grind gained powder and cross 40 mesh sieves, weigh 600g Herba Cymbopogonis Citrari lyophilized powder and be placed in round-bottomed flask, glycerol triacetate for tobacco is added as extractant in the ratio of solid-liquid ratio 1:12, after soaking at room temperature 4 hours, reflux, extract, is carried out under 95 DEG C of conditions, extraction time is 8 hours, naturally cool to room temperature, Herba Cymbopogonis Citrari after described reflux, extract, and triacetyl glycerine are placed in (600W in ultrasonic extraction equipment, 40kHZ), extract 50 minutes, settled solution is obtained after being filtered to remove filtering residue, required Herba Cymbopogonis Citrari triacetyl glycerine extract can be obtained.
With triacetyl glycerine for solvent, Herba Cymbopogonis Citrari triacetyl glycerine extract is configured to the solution that concentration is 5 ‰, it is sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8% and makes cigarette filter rod, make the Medicated cigarette containing Herba Cymbopogonis Citrari effective ingredient filter stick by conventional cigarette tipping program.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds the cigarette flue gas fragrance harmony of above-mentioned Herba Cymbopogonis Citrari triacetyl glycerine extract, pure and fresh, and rich better zest alleviates to some extent, and pleasant impression is clean.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all any amendment, equivalent replacement and improvement etc. made within the spirit and principles in the present invention, should be included within protection scope of the present invention.
Claims (2)
1. a Herba Cymbopogonis Citrari triacetyl glycerine extract, is prepared by the method for following steps:
(1) take fresh Herba Cymbopogonis Citrari blade to dry or dry, pulverize after shredding with shears, cross 20～40 mesh sieves and obtain Herba Cymbopogonis Citrari powder, standby；
(2) weigh 200～600g Herba Cymbopogonis Citrari powder and be placed in round-bottomed flask, glycerol triacetate for tobacco is added as extractant in the ratio of solid-liquid ratio 1:6～12, after soaking at room temperature 2～4 hours, reflux, extract, is carried out under 65～95 DEG C of conditions, 6～8 hours extraction times, standby after being cooled to room temperature；
(3) being placed in ultrasonic extractor by step (2) gains, when 400～600W, 40kHZ, extract 30～50 minutes, the settled solution obtained after being filtered to remove filtering residue is required Herba Cymbopogonis Citrari triacetyl glycerine extract.
2. the application in Medicated cigarette of the Herba Cymbopogonis Citrari triacetyl glycerine extract described in claim 1, it is characterized in that: with triacetyl glycerine for solvent, described Herba Cymbopogonis Citrari triacetyl glycerine extract is configured to the solution that concentration is 1 ‰～5 ‰, it is sprayed onto on tow by the ratio uniform of acetate silk weight 7～8%, make cigarette filter rod, and this filter stick is applied to Medicated cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610154584.7A CN105802733A (en) | 2016-03-18 | 2016-03-18 | Lemongrass glycerol triacetate extract and application thereof to cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610154584.7A CN105802733A (en) | 2016-03-18 | 2016-03-18 | Lemongrass glycerol triacetate extract and application thereof to cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105802733A true CN105802733A (en) | 2016-07-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610154584.7A Pending CN105802733A (en) | 2016-03-18 | 2016-03-18 | Lemongrass glycerol triacetate extract and application thereof to cigarettes |
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| Country | Link |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101342007A (en) * | 2008-08-19 | 2009-01-14 | 云南烟草科学研究院 | Citronella grass cigarette |
| CN105132162A (en) * | 2015-06-17 | 2015-12-09 | 云南中烟工业有限责任公司 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
-
2016
- 2016-03-18 CN CN201610154584.7A patent/CN105802733A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101342007A (en) * | 2008-08-19 | 2009-01-14 | 云南烟草科学研究院 | Citronella grass cigarette |
| CN105132162A (en) * | 2015-06-17 | 2015-12-09 | 云南中烟工业有限责任公司 | Dendrobe glycerol triacetate extract and application thereof in cigarettes |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20160727 |