CN103263078A - Method for preparing low-temperature tobacco material used for non-combustion cigarette - Google Patents
Method for preparing low-temperature tobacco material used for non-combustion cigarette Download PDFInfo
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- CN103263078A CN103263078A CN2013101956639A CN201310195663A CN103263078A CN 103263078 A CN103263078 A CN 103263078A CN 2013101956639 A CN2013101956639 A CN 2013101956639A CN 201310195663 A CN201310195663 A CN 201310195663A CN 103263078 A CN103263078 A CN 103263078A
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Abstract
The invention discloses a method for preparing low-temperature tobacco material used for a non-combustion cigarette. Mashing is directly carried out on tobacco raw material to prepare a substrate, aroma components are extracted from natural fragrant plant flowers through a supercritical CO2 fluid extraction-molecule distillation method, and then the substrate is coated with the aroma components to obtain the needed low-temperature tobacco material. According to the method, the aroma components contained in the tobacco raw material self are kept to the maximum, and the selectivity of the supercritical CO2 fluid extraction-molecule distillation method is used for achieving directed extraction of low-boiling chemical constituents of the natural fragrant plants, so that regulating and controlling of the chemical constituents of the low-temperature tobacco material are achieved. The prepared low-temperature tobacco material is little in offensive odor and rich in aroma, and promotes a sense organ comfort level significantly.
Description
Technical field
The invention belongs to does not have the burning technical field of cigarettes, specifically relates to a kind of preparation method for the low temperature tobacco-containing material that does not have the burning cigarette.
Background technology
Tobacco industrial enterprise should pay close attention to the consumer health, reduce the burst size of cigarette harmful substance present stage, increased economic efficiency again, and development of new does not have the task of top priority that the burning type cigarette has become tobacco business.The low temperature cigarette is the novel tobacco product that a class is different from traditional cigarette, and it mainly is to rely on thermal source at a lower temperature the tobacco sheet base to be carried out destructive distillation, does not transmit flue gas to respiratory system thereby be implemented under the burning condition.At present, because destructive gasifying belongs to the physics category more, no matter its flue gas amount of being or matter all burn and suck the formula cigarette not as tradition.Therefore, exploitation can discharge the tobacco-containing material that similar tradition burns and sucks the formula cigarette smoke by destructive distillation at a lower temperature, and is significant for the development of cigarette.Do not see the relevant report of low temperature tobacco-containing material preparation in the prior art as yet.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of preparation method for the low temperature tobacco-containing material that does not have the burning cigarette is provided.This low temperature tobacco-containing material can enrich fragrance and the taste type of low temperature cigarette, caters to consumer's needs better.
Purpose of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight, and umber is weight portion.
A kind of preparation method for the low temperature tobacco-containing material that does not have the burning cigarette may further comprise the steps:
(1) gets 10～20 parts of tobaccos, soak after 0.5～2 hour that to discongest making beating with pulping equipment be fibre stuff;
(2) be 0.4～1.5% with deionized water diluted slurry to concentration expressed in percentage by weight, it is basic in flakes to manufacture paper with pulp with paper making equipment;
(3) get 1～5 part of natural perfume plant, place extraction equipment, at extracting pressure 20～30MPa, 35～45 ℃ of extraction temperature, parsing pressure 6.0～7.0MPa, 30～50 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours;
(4) get supercritical extract liquid, place molecular distillation equipment, under vacuum 50～100Pa, 100～200 ℃ of heating-up temperatures, rotor knifing rotating speed 260～280 commentaries on classics/min, flow velocity 1～2mL/min condition, must steam thing;
(5) get and steam 1～5 part of thing, 5～50 parts of ethanol, mixing jolting 10min is prepared into coating fluid;
(6) coating fluid evenly is applied on the sheet base by 30～50% coating weight, under 50～60 ℃ of temperature conditions, dries, namely get required low temperature tobacco-containing material.
Described natural perfume plant is selected from a kind of in rose, iris, lavender, the Pelargonium roseum or their mixture.
With respect to prior art, the present invention has the following advantages:
(1) the present invention directly pulls an oar with tobacco material and prepares the sheet base, has kept the contained flavor matter of tobacco material itself to greatest extent;
(2) the present invention utilizes supercritical CO
2Fluid extraction-molecularly distilled selective realized that the orientation of natural perfume plant low boiling chemical constituent is extracted, thereby realized the regulation and control of low temperature tobacco-containing material chemical constituent;
(3) the assorted gas of the low temperature tobacco-containing material of the present invention's preparation is less, fragrance abundant, the sense organ comfort level significantly promotes.
The specific embodiment
The present invention is described in further detail below by embodiment, but embodiment is not limited to the technical solution.
Embodiment 1
Get 10 parts of tobacco materials, soak after 0.5 hour that to discongest making beating with pulping equipment be fibre stuff; Be 1.0% with deionized water diluted slurry to concentration expressed in percentage by weight, with the paper making equipment base in flakes of manufacturing paper with pulp; Get 5 parts of roses, place extraction equipment, at extracting pressure 30MPa, 35 ℃ of extraction temperature, parsing pressure 7.0MPa, 50 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours; Get supercritical extract liquid, place molecular distillation equipment, under vacuum 100Pa, 200 ℃ of heating-up temperatures, rotor knifing rotating speed 280 commentaries on classics/min, flow velocity 1mL/min condition, must steam thing; Get and steam 5 parts of things, 50 parts of ethanol, mixing jolting 10min is prepared into coating fluid; Coating fluid evenly is applied on the sheet base by 50% coating weight, under 50 ℃ of temperature conditions, dries, namely get low temperature tobacco-containing material 1.
After the low temperature tobacco-containing material 1 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, perfume quantity increases, assorted gas is few, delicate fragrance and fragrant and sweet obviously, comfortableness promotes to some extent.
Embodiment 2
Repeat embodiment 1, following difference is arranged: get 20 parts of tobacco materials, soaks after 2 hours and to discongest with pulping equipment that to pull an oar be fibre stuff; Be 0.4% with deionized water diluted slurry to concentration expressed in percentage by weight, with the paper making equipment base in flakes of manufacturing paper with pulp; Get 1 part of lavandulae flos, place extraction equipment, at extracting pressure 20MPa, 45 ℃ of extraction temperature, parsing pressure 6.0MPa, 30 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours; Get supercritical extract liquid, place molecular distillation equipment, under vacuum 50Pa, 100 ℃ of heating-up temperatures, rotor knifing rotating speed 260 commentaries on classics/min, flow velocity 2mL/min condition, must steam thing; Get and steam 1 part of thing, 5 parts of ethanol, mixing jolting 10min is prepared into coating fluid; Coating fluid evenly is applied on the sheet base by 30% coating weight, under 60 ℃ of temperature conditions, dries, namely get low temperature tobacco-containing material 2.
After the low temperature tobacco-containing material 2 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, assorted gas reduces to some extent, the residual reduction in oral cavity.
Embodiment 3
Repeat embodiment 1, following difference is arranged: the slurry weight percentage concentration is 1.5%, and natural perfume plant is flag flower, and extraction conditions is extracting pressure 25MPa, 40 ℃ of extraction temperature, parsing pressure 6.5MPa, 40 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours; Under molecular clock condition vacuum 60Pa, 150 ℃ of heating-up temperatures, rotor knifing rotating speed 270 commentaries on classics/min, the flow velocity 1.5mL/min condition, must steam thing; Coating fluid evenly is applied on the sheet base by 40% coating weight, under 55 ℃ of temperature conditions, dries, namely get low temperature tobacco-containing material 3.
After the low temperature tobacco-containing material 3 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, fragrance is full, fragrant and sweet obviously, moisture feeling is better, excitant reduces.
Embodiment 4
Repeat embodiment 1, following difference is arranged: the slurry weight percentage concentration is 1.2%, and natural perfume plant is Pelargonium roseum, and extraction conditions is extracting pressure 28MPa, 35 ℃ of extraction temperature, parsing pressure 6.3MPa, 45 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours; Under molecular clock condition vacuum 70Pa, 120 ℃ of heating-up temperatures, rotor knifing rotating speed 280 commentaries on classics/min, the flow velocity 1mL/min condition, must steam thing; Coating fluid evenly is applied on the sheet base by 45% coating weight, under 60 ℃ of temperature conditions, dries, namely get low temperature tobacco-containing material 4.
After the low temperature tobacco-containing material 4 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, perfume quantity is abundant, fragrant and sweet obviously, comfortableness promotes to some extent.
Embodiment 5
Repeat embodiment 1, following difference is arranged: natural perfume plant is the mixture of rose and flag flower, and extraction conditions is extracting pressure 25MPa, 40 ℃ of extraction temperature, parsing pressure 6.8MPa, 45 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours; Under molecular clock condition vacuum 50Pa, 150 ℃ of heating-up temperatures, rotor knifing rotating speed 270 commentaries on classics/min, the flow velocity 1mL/min condition, must steam thing; Coating fluid evenly is applied on the sheet base by 40% coating weight, under 60 ℃ of temperature conditions, dries, namely get low temperature tobacco-containing material 5.
After the low temperature tobacco-containing material 5 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, delicate fragrance and fragrant and sweet obvious lifting, comfortableness promote to some extent, moisture feeling obviously strengthens, assorted gas decreases.
Embodiment 6
Repeat embodiment 5, following difference is arranged: natural perfume plant is the mixture of lavender and Pelargonium roseum.Get low temperature tobacco-containing material 6.
After the low temperature tobacco-containing material 6 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, comfortableness promotes to some extent, fragrance texture is better.
Embodiment 7
Repeat embodiment 5, following difference is arranged: natural perfume plant is the mixture of rose and Pelargonium roseum.Get low temperature tobacco-containing material 7.
After the low temperature tobacco-containing material 7 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, the fragrance quality and quantity all have in various degree promote, assorted gas obviously reduces, sweet enhancing, comfortableness promote to some extent.
Embodiment 8
Repeat embodiment 5, following difference is arranged: natural perfume plant is the mixture of rose, lavender, iris and Pelargonium roseum.Get low temperature tobacco-containing material 8.
After the low temperature tobacco-containing material 8 that this law makes adds in the low temperature cigarette, through the sensory evaluating smoking, compare with blank, fragrance comparatively coordinates, assorted gas is less, delicate fragrance and fragrant and sweet obviously, comfort is obvious.
Claims (2)
1. preparation method who be used for not to have the low temperature tobacco-containing material of burning cigarette may further comprise the steps:
(1) gets 10～20 parts of tobaccos, soak after 0.5～2 hour that to discongest making beating with pulping equipment be fibre stuff;
(2) be 0.4～1.5% with deionized water diluted slurry to concentration expressed in percentage by weight, it is basic in flakes to manufacture paper with pulp with paper making equipment;
(3) get 1～5 part of natural perfume plant, place extraction equipment, at extracting pressure 20～30MPa, 35～45 ℃ of extraction temperature, parsing pressure 6.0～7.0MPa, 30～50 ℃ of resolution temperatures, CO
2Flow velocity is under the 20kg/h condition, and the constant temperature and pressure extraction made supercritical extract liquid after 5 hours;
(4) get supercritical extract liquid, place molecular distillation equipment, under vacuum 50～100Pa, 100～200 ℃ of heating-up temperatures, rotor knifing rotating speed 260～280 commentaries on classics/min, flow velocity 1～2mL/min condition, must steam thing;
(5) get and steam 1～5 part of thing, 5～50 parts of ethanol, mixing jolting 10min is prepared into coating fluid;
(6) coating fluid evenly is applied on the sheet base by 30～50% coating weight, under 50～60 ℃ of temperature conditions, dries, namely get required low temperature tobacco-containing material.
2. the preparation method for the low temperature tobacco-containing material that does not have the burning cigarette according to claim 1 is characterized in that: described natural perfume plant is selected from a kind of in rose, iris, lavender, the Pelargonium roseum or their mixture.
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| CN2013101956639A CN103263078A (en) | 2013-05-23 | 2013-05-23 | Method for preparing low-temperature tobacco material used for non-combustion cigarette |
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| CN2013101956639A CN103263078A (en) | 2013-05-23 | 2013-05-23 | Method for preparing low-temperature tobacco material used for non-combustion cigarette |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103919270A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Tobacco product |
| CN103919268A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Cigarette without generating secondhand smoke |
| CN104757703A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Tobacco distillate, and preparation and application thereof |
| CN105581374A (en) * | 2016-03-18 | 2016-05-18 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
| CN106433980A (en) * | 2016-08-28 | 2017-02-22 | 广西灏源盛世生物科技有限公司 | Extraction method of geranium essential oil |
| CN108165371A (en) * | 2018-01-10 | 2018-06-15 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of iris extract |
| CN108236127A (en) * | 2018-01-10 | 2018-07-03 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications for cigarette iris extract of fermenting |
| CN108315352A (en) * | 2018-01-31 | 2018-07-24 | 湖北中烟工业有限责任公司 | A kind of Enzyme treatment prepares the method and its application of lavender oil |
| CN108451008A (en) * | 2018-03-12 | 2018-08-28 | 湖北中烟工业有限责任公司 | A kind of biofermentation prepares the method and its application of lavender absolute oil |
| CN109423358A (en) * | 2017-09-04 | 2019-03-05 | 中国科学院西北高原生物研究所 | A kind of extracting method of Chinese small iris volatile oil |
| CN110537720A (en) * | 2019-10-16 | 2019-12-06 | 四川三联新材料有限公司 | Essence additive for temperature reduction section of heating non-combustible cigarette, preparation method and application thereof, and heating non-combustible cigarette |
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| US5435325A (en) * | 1988-04-21 | 1995-07-25 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts using a solvent in a supercritical state |
| WO2007052159A2 (en) * | 2005-07-29 | 2007-05-10 | Philip Morris Products S.A. | Extraction and storage of tobacco constituents |
| CN102018274A (en) * | 2010-12-31 | 2011-04-20 | 云南烟草科学研究院 | Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103919268A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Cigarette without generating secondhand smoke |
| CN103919268B (en) * | 2014-03-28 | 2016-03-30 | 广东中烟工业有限责任公司 | A kind of cigarette not producing second-hand-cigarette |
| CN103919270B (en) * | 2014-03-28 | 2016-08-17 | 广东中烟工业有限责任公司 | A kind of cigarette products |
| CN103919270A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Tobacco product |
| CN104757703B (en) * | 2014-12-31 | 2019-04-23 | 贵州中烟工业有限责任公司 | A kind of tobacco distillate and its preparation and application |
| CN104757703A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Tobacco distillate, and preparation and application thereof |
| CN105581374A (en) * | 2016-03-18 | 2016-05-18 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
| CN106433980A (en) * | 2016-08-28 | 2017-02-22 | 广西灏源盛世生物科技有限公司 | Extraction method of geranium essential oil |
| CN109423358A (en) * | 2017-09-04 | 2019-03-05 | 中国科学院西北高原生物研究所 | A kind of extracting method of Chinese small iris volatile oil |
| CN108236127A (en) * | 2018-01-10 | 2018-07-03 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications for cigarette iris extract of fermenting |
| CN108165371A (en) * | 2018-01-10 | 2018-06-15 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of iris extract |
| CN108236127B (en) * | 2018-01-10 | 2020-10-13 | 湖北中烟工业有限责任公司 | Preparation method and application of iris extract for fermented cigarettes |
| CN108315352A (en) * | 2018-01-31 | 2018-07-24 | 湖北中烟工业有限责任公司 | A kind of Enzyme treatment prepares the method and its application of lavender oil |
| CN108451008A (en) * | 2018-03-12 | 2018-08-28 | 湖北中烟工业有限责任公司 | A kind of biofermentation prepares the method and its application of lavender absolute oil |
| CN110537720A (en) * | 2019-10-16 | 2019-12-06 | 四川三联新材料有限公司 | Essence additive for temperature reduction section of heating non-combustible cigarette, preparation method and application thereof, and heating non-combustible cigarette |
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Application publication date: 20130828 |